#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:58:04 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180811 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/42/2014211.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014211_Fobs loop_ _publ_author_name 'Curtis, Neil F.' 'Puschmann, Horst' _publ_section_title ; A compound of a novel tetraaza-macrocycle with trinuclear tetracyanonickelate-bridged cations ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m410 _journal_page_last m413 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 70.154 _cell_angle_beta 78.165 _cell_angle_gamma 81.290 _cell_length_a 11.7497 _cell_length_b 14.0540 _cell_length_c 17.9014 _exptl_crystal_F_000 1224.00 _reflns_d_resolution_high 0.7104 _cod_data_source_file na1674Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' X:\Horst\02srv199\raw\frm199_m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 265.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1346.35 1356.25 15.03 o 2 0 0 24403.88 34438.41 178.49 o 3 0 0 3614.33 4211.37 41.00 o 4 0 0 33622.13 39406.47 234.77 o 5 0 0 10428.34 11569.63 127.32 o 6 0 0 14997.94 15692.07 131.76 o 7 0 0 2359.52 2224.61 44.94 o 8 0 0 9550.06 10564.86 148.41 o 9 0 0 739.94 634.78 25.94 o 10 0 0 5404.11 5697.94 172.66 o 11 0 0 125.68 101.51 40.72 o 12 0 0 2532.54 2362.70 103.27 o 13 0 0 59.34 145.43 58.27 o 14 0 0 88.24 2.74 59.04 o 15 0 0 277.81 320.23 61.36 o -15 1 0 13.91 64.56 62.70 o -14 1 0 75.36 109.36 48.25 o -13 1 0 0.10 38.14 47.89 o -12 1 0 13.02 13.42 50.99 o -11 1 0 208.91 210.31 46.24 o -10 1 0 1299.91 1288.20 73.03 o -9 1 0 1113.58 975.38 57.70 o -8 1 0 3517.20 3573.98 45.44 o -7 1 0 5606.02 5680.54 167.08 o -6 1 0 1363.86 1390.37 80.87 o -5 1 0 257.40 306.91 32.85 o -4 1 0 1645.47 1972.73 64.54 o -3 1 0 61.00 71.68 9.88 o -2 1 0 2943.41 3190.68 30.68 o -1 1 0 1812.98 2081.79 32.26 o 0 1 0 3906.52 2158.16 257.25 o 1 1 0 8772.43 9197.44 84.69 o 2 1 0 663.01 525.02 19.20 o 3 1 0 48519.68 56462.68 478.83 o 4 1 0 4151.45 4734.06 88.69 o 5 1 0 4633.25 6266.66 86.34 o 6 1 0 799.15 692.68 46.47 o 7 1 0 4190.20 4687.77 65.56 o 8 1 0 1303.87 1227.52 31.17 o 9 1 0 1301.51 1353.44 48.22 o 10 1 0 766.77 828.50 32.60 o 11 1 0 2214.24 2282.82 110.49 o 12 1 0 27.51 88.04 38.71 o 13 1 0 2701.65 2873.00 114.98 o 14 1 0 14.78 78.08 50.42 o 15 1 0 648.51 756.64 89.64 o -15 2 0 75.58 26.06 68.28 o -14 2 0 1282.95 1207.75 85.26 o -13 2 0 113.43 146.52 45.67 o -12 2 0 2084.90 2133.19 98.47 o -11 2 0 943.28 1094.93 76.74 o -10 2 0 94.49 159.21 47.22 o -9 2 0 3115.62 3131.67 102.03 o -8 2 0 1332.75 1440.13 39.06 o -7 2 0 417.31 378.54 17.22 o -6 2 0 5440.51 5524.47 294.56 o -5 2 0 2574.28 2822.61 85.70 o -4 2 0 4557.54 4436.04 130.83 o -3 2 0 263.22 433.37 19.95 o -2 2 0 1174.81 1633.11 39.02 o -1 2 0 1003.88 838.85 65.41 o 0 2 0 293.80 179.67 10.35 o 1 2 0 198.85 247.19 33.01 o 2 2 0 135.45 128.97 16.05 o 3 2 0 6867.71 8665.41 96.35 o 4 2 0 17085.61 16928.58 157.46 o 5 2 0 7575.77 8240.99 104.17 o 6 2 0 7421.45 7534.75 154.13 o 7 2 0 10283.85 9780.26 232.21 o 8 2 0 3561.15 3650.14 134.72 o 9 2 0 2645.50 2511.47 59.37 o 10 2 0 1.25 -1.33 19.56 o 11 2 0 340.10 439.61 69.97 o 12 2 0 1.38 14.70 25.57 o 13 2 0 147.10 123.09 53.31 o 14 2 0 5.88 53.41 49.39 o 15 2 0 17.74 79.37 66.06 o -15 3 0 15.32 -61.05 61.05 o -14 3 0 37.94 17.50 51.14 o -13 3 0 1337.74 1417.79 89.13 o -12 3 0 24.42 73.08 43.92 o -11 3 0 1916.18 1970.57 91.40 o -10 3 0 13.14 77.15 33.24 o -9 3 0 3363.82 3705.61 108.69 o -8 3 0 155.60 214.85 35.25 o -7 3 0 3421.30 3357.49 76.56 o -6 3 0 36.68 59.25 12.28 o -5 3 0 8702.30 8866.74 208.11 o -4 3 0 5089.90 5388.46 93.46 o -3 3 0 11052.32 11063.15 128.09 o -2 3 0 58.98 142.49 18.01 o -1 3 0 68431.51 71090.39 247.45 o 0 3 0 326.53 301.14 10.12 o 1 3 0 41802.34 45742.20 362.91 o 2 3 0 1097.47 1268.18 35.35 o 3 3 0 4039.58 4604.27 71.07 o 4 3 0 2648.61 2687.57 60.85 o 5 3 0 2208.88 2434.85 60.95 o 6 3 0 4992.66 4850.11 64.92 o 7 3 0 12246.73 12261.13 168.45 o 8 3 0 453.67 352.02 21.68 o 9 3 0 2351.93 1899.67 655.14 o 10 3 0 93.48 93.03 16.38 o 11 3 0 5958.91 5987.37 86.38 o 12 3 0 0.24 -18.99 18.99 o 13 3 0 1123.32 1056.67 81.31 o 14 3 0 67.82 44.33 52.64 o 15 3 0 1.48 -13.78 54.81 o -14 4 0 15.80 30.45 68.64 o -13 4 0 101.34 150.13 65.49 o -12 4 0 2.48 49.23 47.07 o -11 4 0 309.06 359.66 60.23 o -10 4 0 515.08 490.70 56.10 o -9 4 0 709.10 806.70 60.07 o -8 4 0 2884.50 2573.83 90.11 o -7 4 0 1243.44 1221.47 65.13 o -6 4 0 178.02 214.02 31.95 o -5 4 0 3891.75 3728.88 87.12 o -4 4 0 556.94 627.20 40.10 o -3 4 0 0.17 24.88 16.21 o -2 4 0 1693.00 1371.50 44.51 o -1 4 0 12634.94 14244.85 127.63 o 0 4 0 4782.81 5694.50 136.40 o 1 4 0 4153.90 5040.88 58.60 o 2 4 0 1648.36 1897.47 135.60 o 3 4 0 507.30 697.65 32.36 o 4 4 0 9347.85 10091.97 127.47 o 5 4 0 2588.56 2553.44 66.58 o 6 4 0 1340.10 1525.04 54.76 o 7 4 0 198.68 132.15 14.96 o 8 4 0 892.27 952.71 46.43 o 9 4 0 365.29 403.36 33.44 o 10 4 0 1855.83 1687.56 45.21 o 11 4 0 103.26 137.98 23.87 o 12 4 0 2422.41 2126.23 172.38 o 13 4 0 70.42 90.59 27.46 o 14 4 0 1577.73 1489.68 88.97 o 15 4 0 11.86 122.26 56.82 o -14 5 0 13.40 -68.48 68.48 o -13 5 0 1228.30 1371.19 99.66 o -12 5 0 481.67 528.94 66.88 o -11 5 0 155.56 189.61 50.06 o -10 5 0 1163.96 1081.98 75.92 o -9 5 0 614.09 631.59 61.57 o -8 5 0 298.49 428.51 52.28 o -7 5 0 4614.80 4605.25 113.69 o -6 5 0 394.77 411.73 45.93 o -5 5 0 6070.89 5548.91 111.53 o -4 5 0 1106.31 1033.26 52.59 o -3 5 0 8551.92 7866.04 118.96 o -2 5 0 357.69 397.85 18.37 o -1 5 0 11831.82 13212.58 202.10 o 0 5 0 149.03 403.88 15.63 o 1 5 0 820.46 1309.04 31.74 o 2 5 0 1233.91 1748.82 45.71 o 3 5 0 5784.35 5043.25 85.93 o 4 5 0 2667.30 2462.30 65.44 o 5 5 0 7693.28 7310.22 118.18 o 6 5 0 3399.15 3488.24 83.71 o 7 5 0 4394.06 4413.63 142.98 o 8 5 0 2887.41 2968.04 89.38 o 9 5 0 21.69 13.85 13.75 o 10 5 0 62.76 68.30 25.43 o 11 5 0 26.19 -9.85 18.60 o 12 5 0 0.95 42.33 30.17 o 13 5 0 61.37 30.53 23.06 o 14 5 0 222.04 297.29 60.64 o 15 5 0 312.53 470.72 64.36 o -14 6 0 249.62 245.09 72.46 o -13 6 0 67.47 144.56 65.96 o -12 6 0 1331.01 1513.79 97.02 o -11 6 0 17.80 87.22 45.31 o -10 6 0 1471.84 1385.38 79.84 o -9 6 0 57.53 55.63 37.11 o -8 6 0 1994.55 1816.88 81.59 o -7 6 0 138.75 90.83 31.74 o -6 6 0 9016.61 8770.28 156.01 o -5 6 0 2857.02 2799.56 86.55 o -4 6 0 3428.63 3853.16 91.35 o -3 6 0 494.64 504.51 16.23 o -2 6 0 24022.41 24088.72 122.62 o -1 6 0 1122.17 1071.61 35.89 o 0 6 0 28446.48 29647.31 221.31 o 1 6 0 1248.01 1058.26 34.28 o 2 6 0 882.57 996.03 30.08 o 3 6 0 7590.50 7190.76 77.48 o 4 6 0 1951.05 2500.62 48.50 o 5 6 0 5856.40 5655.33 221.79 o 6 6 0 5499.06 5533.02 104.33 o 7 6 0 1666.55 1648.43 53.83 o 8 6 0 4884.82 4795.94 79.50 o 9 6 0 549.51 524.01 29.02 o 10 6 0 3175.16 2960.44 94.52 o 11 6 0 215.94 272.91 30.73 o 12 6 0 1118.37 1038.82 42.18 o 13 6 0 166.30 229.43 27.49 o 14 6 0 160.30 127.11 28.21 o 15 6 0 70.60 40.20 39.10 o -13 7 0 203.21 255.00 67.71 o -12 7 0 49.29 -53.52 53.52 o -11 7 0 15.79 -49.34 49.34 o -10 7 0 388.09 458.08 66.42 o -9 7 0 2492.26 2568.10 105.33 o -8 7 0 106.21 60.43 38.91 o -7 7 0 341.67 331.95 47.79 o -6 7 0 582.46 449.72 51.20 o -5 7 0 457.92 470.36 48.25 o -4 7 0 203.10 269.62 23.55 o -3 7 0 171.94 243.58 34.98 o -2 7 0 468.12 461.70 19.33 o -1 7 0 1317.68 1748.46 42.47 o 0 7 0 74.03 93.30 9.59 o 1 7 0 6382.50 6324.46 86.34 o 2 7 0 373.89 321.38 18.21 o 3 7 0 12683.48 12680.67 878.17 o 4 7 0 905.92 914.22 43.22 o 5 7 0 1066.76 1113.50 50.40 o 6 7 0 502.62 438.84 30.21 o 7 7 0 1571.59 1526.23 86.08 o 8 7 0 68.91 54.03 19.69 o 9 7 0 2127.32 2191.03 62.42 o 10 7 0 291.48 286.29 37.13 o 11 7 0 2941.08 2915.94 143.27 o 12 7 0 67.89 53.91 22.22 o 13 7 0 1302.83 1302.23 54.82 o 14 7 0 1.84 24.63 27.41 o 15 7 0 311.12 381.75 44.17 o -13 8 0 9.44 117.98 68.02 o -12 8 0 332.66 388.25 72.36 o -11 8 0 1360.87 1405.92 98.47 o -10 8 0 845.97 735.94 77.00 o -9 8 0 820.94 1018.70 76.33 o -8 8 0 1164.89 1236.08 76.43 o -7 8 0 4.58 -27.87 27.87 o -6 8 0 5676.67 5742.24 135.83 o -5 8 0 314.59 298.52 29.61 o -4 8 0 7842.12 7276.64 142.39 o -3 8 0 2.72 -2.78 23.71 o -2 8 0 7180.64 7103.46 88.96 o -1 8 0 42.28 42.05 12.40 o 0 8 0 3190.91 3015.28 36.48 o 1 8 0 1.81 11.98 8.14 o 2 8 0 51.31 68.14 10.73 o 3 8 0 122.35 182.88 16.98 o 4 8 0 7737.68 7244.26 128.45 o 5 8 0 1727.57 1552.26 123.60 o 6 8 0 2637.39 2282.29 56.16 o 7 8 0 766.19 734.69 37.39 o 8 8 0 3.23 -8.21 18.63 o 9 8 0 4.13 -16.63 21.98 o 10 8 0 10.82 -5.82 18.45 o 11 8 0 6.21 -9.15 19.90 o 12 8 0 33.69 -22.19 22.19 o 13 8 0 117.47 75.03 28.51 o 14 8 0 44.99 79.87 40.38 o 15 8 0 91.11 236.56 45.07 o -12 9 0 76.94 0.31 56.10 o -11 9 0 595.08 519.13 73.85 o -10 9 0 28.76 69.62 45.73 o -9 9 0 782.72 642.79 64.77 o -8 9 0 687.18 627.72 62.45 o -7 9 0 1330.33 1106.70 75.71 o -6 9 0 2495.40 2236.40 95.94 o -5 9 0 2903.07 2812.19 96.71 o -4 9 0 432.92 487.46 36.69 o -3 9 0 13066.67 13854.04 247.77 o -2 9 0 1549.25 1757.20 43.37 o -1 9 0 15438.65 15745.90 101.69 o 0 9 0 663.60 763.70 22.44 o 1 9 0 5566.83 5971.60 98.93 o 2 9 0 4378.08 4097.96 59.53 o 3 9 0 2856.68 2924.63 103.01 o 4 9 0 2097.12 2253.90 163.52 o 5 9 0 4897.18 4922.50 94.32 o 6 9 0 3294.36 3050.18 90.03 o 7 9 0 5752.89 5743.90 95.25 o 8 9 0 228.09 270.11 29.85 o 9 9 0 2179.30 1957.90 62.83 o 10 9 0 0.29 -22.95 29.96 o 11 9 0 2013.03 1812.52 124.53 o 12 9 0 6.02 -18.42 26.56 o 13 9 0 227.82 239.92 35.92 o 14 9 0 110.88 102.66 35.55 o -12 10 0 120.78 62.09 61.16 o -11 10 0 347.91 395.84 66.78 o -10 10 0 274.02 301.55 60.33 o -9 10 0 417.04 375.42 64.43 o -8 10 0 370.30 366.85 72.95 o -7 10 0 55.38 100.83 32.17 o -6 10 0 222.08 259.52 34.32 o -5 10 0 89.57 91.47 26.80 o -4 10 0 616.48 582.97 126.60 o -3 10 0 2.19 14.39 22.33 o -2 10 0 1409.67 1229.06 92.95 o -1 10 0 425.99 343.73 17.97 o 0 10 0 2056.17 2044.40 39.52 o 1 10 0 3019.67 3009.42 41.80 o 2 10 0 4594.58 4539.03 61.05 o 3 10 0 1491.21 1360.32 75.08 o 4 10 0 1753.78 1850.00 51.57 o 5 10 0 0.22 22.73 37.65 o 6 10 0 281.38 383.55 37.70 o 7 10 0 38.65 51.42 20.85 o 8 10 0 478.23 607.22 39.45 o 9 10 0 14.18 -1.77 22.10 o 10 10 0 633.52 640.22 45.79 o 11 10 0 199.02 288.85 53.15 o 12 10 0 800.84 809.30 49.07 o 13 10 0 1.82 -8.36 40.07 o -11 11 0 119.50 189.09 77.15 o -10 11 0 384.37 369.41 47.45 o -9 11 0 1832.54 1675.22 115.11 o -8 11 0 14.59 46.71 76.69 o -7 11 0 2101.24 2176.46 169.61 o -6 11 0 13.49 72.50 29.57 o -5 11 0 2269.54 2194.46 65.85 o -4 11 0 89.02 119.80 29.71 o -3 11 0 1249.27 1277.50 133.18 o -2 11 0 428.28 408.16 45.05 o -1 11 0 568.69 570.32 73.16 o 0 11 0 265.73 263.61 18.45 o 1 11 0 471.38 498.69 23.55 o 2 11 0 0.39 28.22 14.54 o 3 11 0 1326.82 1248.20 37.20 o 4 11 0 1242.89 1216.19 100.22 o 5 11 0 1179.75 1289.54 47.62 o 6 11 0 899.88 692.53 38.41 o 7 11 0 496.56 433.63 36.01 o 8 11 0 106.38 29.70 27.71 o 9 11 0 31.10 -19.60 33.24 o 10 11 0 129.70 105.00 30.47 o 11 11 0 2.83 18.26 41.39 o 12 11 0 131.22 160.33 46.32 o 13 11 0 43.31 32.02 69.23 o -10 12 0 201.23 130.98 62.86 o -9 12 0 80.16 130.93 66.94 o -8 12 0 21.74 40.28 37.30 o -7 12 0 108.54 165.87 35.11 o -6 12 0 1375.79 1255.50 58.89 o -5 12 0 18.38 14.30 31.39 o -4 12 0 1100.29 1048.85 114.16 o -3 12 0 90.52 45.79 29.20 o -2 12 0 3319.85 3279.65 75.21 o -1 12 0 9.75 22.86 37.83 o 0 12 0 1036.50 1066.05 36.63 o 1 12 0 761.63 804.91 37.13 o 2 12 0 743.31 760.10 27.55 o 3 12 0 2714.34 2477.50 51.38 o 4 12 0 3281.01 3266.74 72.30 o 5 12 0 345.34 358.45 30.38 o 6 12 0 2918.75 2669.51 139.58 o 7 12 0 451.11 456.76 38.33 o 8 12 0 3104.77 2682.94 75.68 o 9 12 0 5.92 -19.70 24.53 o 10 12 0 1732.72 1504.48 109.23 o 11 12 0 93.60 105.35 33.92 o 12 12 0 312.81 289.54 37.70 o -9 13 0 225.40 247.31 67.14 o -8 13 0 147.95 141.05 64.92 o -7 13 0 3.56 -5.06 64.98 o -6 13 0 320.54 405.85 65.13 o -5 13 0 43.97 92.17 44.44 o -4 13 0 50.89 21.63 39.45 o -3 13 0 116.84 179.51 35.10 o -2 13 0 399.33 461.56 38.91 o -1 13 0 115.58 166.56 31.90 o 0 13 0 1391.97 1286.88 128.04 o 1 13 0 823.69 833.39 36.35 o 2 13 0 3147.99 3028.90 50.28 o 3 13 0 16.81 31.93 20.12 o 4 13 0 0.37 -10.72 22.48 o 5 13 0 2.32 -20.03 20.03 o 6 13 0 9.81 -30.66 38.24 o 7 13 0 51.29 26.39 26.75 o 8 13 0 94.02 100.35 41.75 o 9 13 0 277.30 268.60 40.57 o 10 13 0 3.94 7.04 33.80 o 11 13 0 616.64 703.78 52.48 o -9 14 0 422.75 406.16 84.84 o -8 14 0 1532.26 1494.38 112.61 o -7 14 0 5.65 -65.34 65.34 o -6 14 0 2534.14 2698.98 121.02 o -5 14 0 156.78 19.61 53.57 o -4 14 0 1901.07 1810.79 108.22 o -3 14 0 635.72 565.84 67.19 o -2 14 0 2522.96 2637.05 108.07 o -1 14 0 843.29 1049.72 78.65 o 0 14 0 307.56 204.27 50.94 o 1 14 0 74.29 75.65 30.94 o 2 14 0 2164.35 2002.23 45.11 o 3 14 0 62.33 116.56 41.31 o 4 14 0 2758.36 2672.22 73.88 o 5 14 0 56.96 38.77 28.72 o 6 14 0 774.90 812.01 143.89 o 7 14 0 200.02 200.94 33.98 o 8 14 0 57.65 27.09 28.55 o 9 14 0 88.87 134.57 35.63 o 10 14 0 66.07 82.84 35.46 o -8 15 0 79.98 199.88 78.29 o -7 15 0 195.28 68.90 77.41 o -6 15 0 8.56 45.67 71.27 o -5 15 0 770.95 864.76 97.95 o -4 15 0 0.63 67.87 61.52 o -3 15 0 2223.29 2426.85 111.53 o -2 15 0 26.41 111.53 59.66 o -1 15 0 1391.85 1550.22 89.02 o 0 15 0 600.98 749.82 75.86 o 1 15 0 1116.84 1155.62 78.29 o 2 15 0 750.10 588.03 65.54 o 3 15 0 985.47 899.93 50.09 o 4 15 0 208.41 188.76 55.84 o 5 15 0 1957.20 2037.46 72.71 o 6 15 0 64.39 106.71 35.15 o 7 15 0 2948.34 2816.99 99.97 o 8 15 0 3.16 -0.30 39.43 o 9 15 0 929.34 884.05 151.57 o -6 16 0 10.90 80.20 81.95 o -5 16 0 0.36 66.88 72.97 o -4 16 0 96.68 86.13 67.25 o -3 16 0 29.31 211.75 69.57 o -2 16 0 117.20 157.82 63.22 o -1 16 0 447.19 573.73 71.37 o 0 16 0 618.18 604.39 76.23 o 1 16 0 198.08 345.88 55.58 o 4 16 0 9.09 40.56 44.90 o 5 16 0 0.14 55.51 35.76 o 6 16 0 23.69 -36.10 36.10 o 7 16 0 68.93 -21.62 37.69 o 8 16 0 96.02 97.33 40.16 o -5 17 0 500.09 693.05 90.73 o -4 17 0 58.84 63.58 81.28 o -3 17 0 427.09 590.09 84.38 o 5 17 0 688.29 599.49 72.67 o 6 17 0 62.19 55.78 70.42 o 7 17 0 46.03 83.40 41.47 o -7 -17 1 236.45 285.60 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