#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014243.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014243_Fobs loop_ _publ_author_name 'Turkington, David E.' 'Ferguson, George' 'Lough, Alan J.' 'Glidewell, Christopher' _publ_section_title ; Supramolecular structures of three configurational isomers of 1-phenylethanaminium malate(1--) ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o617 _journal_page_last o622 _journal_volume 60 _journal_year 2004 _space_group_IT_number 9 _symmetry_space_group_name_Hall 'C -2yc' _symmetry_space_group_name_H-M 'C 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.811 _cell_angle_gamma 90.000 _cell_length_a 7.5373 _cell_length_b 15.0354 _cell_length_c 11.6624 _exptl_crystal_F_000 544.00 _reflns_d_resolution_high 0.8415 _[local]_cod_data_source_file sk1743Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title dt04 _shelx_refln_list_code 4 _shelx_f_calc_maximum 95.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3765.57 4173.52 245.44 o 4 0 0 335.93 371.67 10.38 o 6 0 0 816.77 887.50 32.11 o 8 0 0 7.51 9.49 6.04 o 1 1 0 2475.16 2735.05 294.76 o 3 1 0 2303.65 2370.49 148.29 o 5 1 0 108.52 115.40 3.85 o 7 1 0 1.29 3.45 3.26 o 0 2 0 8592.88 4542.92 3809.39 o 2 2 0 295.75 253.40 7.82 o 4 2 0 45.54 49.87 3.30 o 6 2 0 211.52 222.93 7.44 o 8 2 0 12.84 15.92 3.39 o 1 3 0 44.76 43.21 1.85 o 3 3 0 2377.52 2511.24 87.16 o 5 3 0 112.31 155.33 8.48 o 7 3 0 223.61 249.37 11.91 o 0 4 0 5034.86 4615.89 199.04 o 2 4 0 1112.18 1004.72 55.48 o 4 4 0 826.09 793.96 28.44 o 6 4 0 188.30 192.70 13.37 o 8 4 0 20.73 19.10 2.58 o 3 5 0 1254.84 1353.90 41.19 o 5 5 0 134.88 144.64 6.63 o 7 5 0 239.88 261.50 7.86 o 0 6 0 1632.15 1313.56 110.35 o 2 6 0 1525.75 1361.44 46.07 o 4 6 0 510.85 534.00 13.47 o 6 6 0 59.22 60.38 3.55 o 8 6 0 28.39 22.36 4.78 o 1 7 0 1122.27 1007.03 37.33 o 3 7 0 294.97 312.65 12.87 o 5 7 0 30.23 29.04 2.29 o 7 7 0 13.51 7.39 2.19 o 0 8 0 254.72 265.69 28.36 o 2 8 0 2636.19 2539.35 84.74 o 4 8 0 31.40 34.05 3.48 o 6 8 0 16.36 17.30 1.73 o 1 9 0 1516.99 1568.51 75.37 o 3 9 0 197.97 189.01 16.02 o 5 9 0 22.75 18.00 1.88 o 7 9 0 50.35 57.43 5.85 o 0 10 0 402.01 446.68 15.99 o 2 10 0 24.88 27.06 3.39 o 4 10 0 13.57 12.03 2.99 o 6 10 0 5.19 4.16 2.00 o 1 11 0 237.84 268.90 15.61 o 3 11 0 21.73 21.39 2.56 o 5 11 0 82.34 95.56 4.44 o 0 12 0 0.06 5.47 3.87 o 2 12 0 21.92 27.19 4.03 o 4 12 0 1.62 3.93 2.32 o 6 12 0 15.07 17.38 3.47 o 1 13 0 600.93 565.25 50.90 o 3 13 0 138.27 154.72 11.07 o 5 13 0 10.33 8.75 4.17 o 0 14 0 7.84 10.13 4.21 o 2 14 0 58.83 65.82 4.53 o 4 14 0 29.51 37.00 4.76 o 1 15 0 14.16 15.54 2.39 o 3 15 0 58.06 62.49 5.95 o 0 16 0 91.72 81.47 11.65 o 2 16 0 4.25 5.97 1.95 o 1 17 0 11.56 18.31 3.03 o -7 1 1 72.57 63.06 4.30 o -5 1 1 309.52 357.60 7.98 o -1 1 1 1205.45 853.05 129.14 o 1 1 1 567.16 592.16 33.13 o 3 1 1 4147.22 5041.33 139.06 o 5 1 1 26.45 29.85 1.99 o 7 1 1 20.07 17.22 2.15 o -8 2 1 43.73 35.31 4.56 o -6 2 1 31.09 34.18 1.86 o -4 2 1 628.42 728.86 18.24 o -2 2 1 4029.80 4300.58 223.85 o 0 2 1 1179.69 872.54 32.53 o 2 2 1 42.51 46.10 2.50 o 4 2 1 238.77 310.82 16.50 o 6 2 1 316.73 362.75 11.57 o 8 2 1 13.26 7.47 2.40 o -7 3 1 86.78 77.69 4.40 o -5 3 1 59.88 62.42 2.41 o -3 3 1 1490.43 1466.07 51.05 o 1 3 1 446.83 368.36 11.11 o 3 3 1 2120.55 2314.46 73.97 o 5 3 1 282.02 263.63 10.09 o 7 3 1 134.20 147.84 9.10 o -8 4 1 12.28 14.14 2.24 o -6 4 1 20.41 16.57 1.62 o -4 4 1 1362.18 1342.11 60.94 o -2 4 1 8277.15 10141.85 790.27 o 2 4 1 235.66 176.42 5.23 o 4 4 1 628.93 619.92 20.70 o 6 4 1 85.13 85.96 4.34 o 8 4 1 24.24 32.58 3.63 o -7 5 1 32.47 32.10 2.48 o -5 5 1 154.98 172.21 8.90 o -3 5 1 81.47 82.45 5.38 o -1 5 1 3844.15 3267.69 233.52 o 1 5 1 6148.45 5828.68 194.51 o 3 5 1 880.50 793.38 36.67 o 5 5 1 503.84 486.62 10.42 o 7 5 1 5.44 5.23 2.65 o -8 6 1 17.42 15.14 3.32 o -6 6 1 87.83 95.99 7.15 o -4 6 1 1291.77 1312.09 69.69 o -2 6 1 108.65 85.54 5.46 o 0 6 1 1005.91 819.20 35.00 o 2 6 1 31.62 33.68 2.31 o 4 6 1 288.78 316.21 7.19 o 6 6 1 53.28 54.74 4.78 o -7 7 1 25.14 27.99 4.36 o -5 7 1 168.20 175.72 6.89 o -3 7 1 1095.68 1032.88 58.77 o -1 7 1 22.15 27.13 2.06 o 1 7 1 61.71 49.19 3.17 o 3 7 1 314.10 290.33 9.07 o 5 7 1 56.01 70.57 2.86 o 7 7 1 73.06 74.87 7.00 o -6 8 1 170.31 152.99 9.52 o -4 8 1 168.23 148.61 6.98 o -2 8 1 493.76 470.35 24.04 o 0 8 1 3026.99 2661.45 135.45 o 2 8 1 1214.64 1099.71 35.11 o 4 8 1 238.20 255.81 12.51 o 6 8 1 74.87 77.30 3.26 o -7 9 1 0.08 -2.94 2.94 o -5 9 1 243.65 259.33 22.69 o -3 9 1 214.50 199.24 17.56 o -1 9 1 2400.17 2136.54 52.48 o 1 9 1 778.26 675.03 21.25 o 3 9 1 118.31 121.96 5.20 o 5 9 1 41.87 47.01 2.88 o 7 9 1 17.46 13.95 2.86 o -6 10 1 4.81 3.27 1.79 o -4 10 1 69.66 74.22 7.20 o -2 10 1 59.41 60.05 4.80 o 0 10 1 76.67 66.87 6.99 o 2 10 1 61.99 58.26 3.62 o 4 10 1 151.73 154.05 12.40 o 6 10 1 65.89 63.12 6.10 o -5 11 1 54.57 46.54 4.74 o -3 11 1 182.30 225.47 10.10 o -1 11 1 138.06 126.89 7.97 o 1 11 1 9.46 18.92 4.53 o 3 11 1 40.04 45.16 3.59 o 5 11 1 2.86 6.10 2.27 o -6 12 1 6.80 8.21 3.12 o -4 12 1 42.76 55.22 6.24 o -2 12 1 437.91 438.28 27.07 o 0 12 1 204.85 187.83 13.47 o 2 12 1 6.25 5.36 2.23 o 4 12 1 101.25 105.35 4.84 o 6 12 1 61.80 56.82 4.93 o -5 13 1 23.65 23.82 3.73 o -3 13 1 59.51 66.44 8.27 o -1 13 1 183.91 186.46 12.60 o 1 13 1 85.98 96.02 7.60 o 3 13 1 23.36 25.14 3.04 o 5 13 1 9.53 6.97 2.81 o -4 14 1 15.15 14.67 2.21 o -2 14 1 138.86 149.95 11.22 o 0 14 1 20.68 22.79 4.90 o 2 14 1 18.56 18.82 4.61 o 4 14 1 5.73 2.64 2.73 o -3 15 1 27.65 26.93 3.08 o -1 15 1 91.57 82.04 7.72 o 1 15 1 1.25 -1.67 2.08 o 3 15 1 41.82 49.65 4.74 o -2 16 1 73.02 61.04 6.20 o 0 16 1 32.53 34.01 4.50 o 2 16 1 19.59 19.58 3.49 o -1 17 1 22.42 17.96 5.86 o 1 17 1 11.35 16.08 6.80 o -8 0 2 44.78 41.94 5.58 o -6 0 2 436.12 499.68 28.00 o -4 0 2 2013.30 2100.15 61.65 o -2 0 2 353.45 382.56 14.39 o 0 0 2 9071.43 10125.45 383.02 o 2 0 2 2381.82 2516.64 102.07 o 4 0 2 200.94 230.88 11.58 o 6 0 2 324.23 347.79 18.18 o 8 0 2 80.75 99.00 15.00 o -7 1 2 51.40 52.30 3.64 o -5 1 2 11.39 11.60 0.98 o -3 1 2 627.36 694.76 33.93 o -1 1 2 8238.51 8466.32 227.05 o 1 1 2 2894.15 2922.25 143.50 o 3 1 2 699.71 716.99 20.68 o 5 1 2 235.75 263.92 14.67 o 7 1 2 7.10 8.28 1.45 o -8 2 2 30.52 32.71 3.70 o -6 2 2 164.99 170.52 8.37 o -4 2 2 303.77 307.46 6.50 o -2 2 2 687.91 711.11 20.51 o 0 2 2 3482.00 3143.53 55.14 o 2 2 2 132.61 133.23 9.79 o 4 2 2 1091.71 1078.71 49.24 o 6 2 2 221.62 247.92 12.65 o 8 2 2 129.25 120.68 7.29 o -7 3 2 29.97 30.22 1.93 o -5 3 2 664.43 679.75 34.12 o -3 3 2 2557.59 2786.89 63.12 o -1 3 2 974.02 937.01 25.76 o 1 3 2 1090.16 1035.64 50.26 o 3 3 2 1979.06 2008.32 63.10 o 5 3 2 413.03 480.28 21.29 o 7 3 2 21.20 24.38 2.98 o -8 4 2 2.71 4.14 1.66 o -6 4 2 10.81 12.83 1.64 o -4 4 2 224.03 195.26 8.74 o -2 4 2 53.36 53.24 6.53 o 0 4 2 7818.55 7445.86 249.09 o 2 4 2 1141.54 1186.31 74.16 o 4 4 2 334.55 326.50 15.61 o 6 4 2 79.70 76.78 3.81 o -7 5 2 188.40 196.52 11.77 o -5 5 2 611.81 651.82 25.11 o -3 5 2 89.09 86.55 3.03 o -1 5 2 382.90 296.75 14.78 o 1 5 2 720.25 619.91 25.73 o 3 5 2 5.77 3.85 1.63 o 5 5 2 115.11 112.47 3.84 o 7 5 2 63.69 65.45 5.53 o -8 6 2 20.95 10.08 3.50 o -6 6 2 12.76 11.71 1.81 o -4 6 2 295.61 255.33 17.43 o -2 6 2 441.34 380.13 20.84 o 0 6 2 1139.87 1057.02 49.77 o 2 6 2 700.87 716.91 31.72 o 4 6 2 9.41 3.13 1.46 o 6 6 2 472.05 499.12 16.88 o -7 7 2 93.45 93.88 6.25 o -5 7 2 291.05 295.14 14.67 o -3 7 2 334.78 287.88 10.98 o -1 7 2 1480.44 1409.88 55.07 o 1 7 2 467.19 414.14 17.56 o 3 7 2 69.71 67.05 2.62 o 5 7 2 184.85 180.10 6.60 o 7 7 2 75.18 74.12 4.65 o -6 8 2 41.84 38.03 3.58 o -4 8 2 82.44 88.04 6.10 o -2 8 2 1018.77 842.40 46.79 o 0 8 2 462.01 371.99 20.31 o 2 8 2 218.15 195.74 11.06 o 4 8 2 211.49 217.55 9.38 o 6 8 2 83.92 85.78 3.88 o -7 9 2 7.05 10.45 2.52 o -5 9 2 459.37 479.02 22.48 o -3 9 2 68.35 56.22 3.66 o -1 9 2 968.80 981.88 30.36 o 1 9 2 228.26 209.73 13.94 o 3 9 2 37.40 50.79 4.04 o 5 9 2 100.13 88.22 4.67 o -6 10 2 6.54 8.33 1.71 o -4 10 2 245.61 224.83 12.57 o -2 10 2 142.60 125.11 10.46 o 0 10 2 196.60 159.05 10.97 o 2 10 2 239.46 246.94 21.41 o 4 10 2 414.55 472.12 22.03 o 6 10 2 23.66 21.04 2.65 o -7 11 2 66.64 62.26 6.51 o -5 11 2 127.37 128.89 8.16 o -3 11 2 113.72 124.98 7.44 o -1 11 2 41.80 39.59 6.60 o 1 11 2 965.26 1052.74 35.88 o 3 11 2 105.35 118.70 9.58 o 5 11 2 41.80 48.24 3.71 o -6 12 2 40.50 44.03 4.48 o -4 12 2 33.29 36.02 5.51 o -2 12 2 540.64 507.51 28.17 o 0 12 2 299.82 285.11 18.23 o 2 12 2 113.01 133.79 9.26 o 4 12 2 5.61 3.72 1.70 o -5 13 2 13.80 10.58 2.41 o -3 13 2 10.91 11.19 1.90 o -1 13 2 8.47 6.39 2.53 o 1 13 2 54.06 53.63 4.41 o 3 13 2 3.19 -0.18 2.78 o 5 13 2 9.61 8.95 3.02 o -4 14 2 10.21 7.98 2.39 o -2 14 2 55.40 54.55 3.72 o 0 14 2 158.40 180.46 10.12 o 2 14 2 12.89 8.53 4.09 o 4 14 2 75.21 81.45 5.12 o -3 15 2 28.25 40.57 7.87 o -1 15 2 44.07 43.57 5.07 o 1 15 2 7.47 12.38 4.16 o 3 15 2 20.61 22.00 3.23 o -2 16 2 5.21 2.92 1.69 o 0 16 2 31.09 38.37 6.58 o 2 16 2 37.15 37.68 3.96 o -1 17 2 47.05 42.87 10.83 o 1 17 2 15.51 17.15 4.00 o -7 1 3 67.15 59.67 4.69 o -5 1 3 220.09 217.67 9.29 o -3 1 3 889.58 862.04 23.09 o -1 1 3 5410.87 5681.72 225.87 o 1 1 3 1084.89 1139.48 42.17 o 3 1 3 50.00 50.90 2.57 o 5 1 3 427.64 492.63 21.45 o 7 1 3 40.75 30.04 2.89 o -8 2 3 34.42 29.87 3.35 o -6 2 3 35.76 38.45 1.92 o -4 2 3 5.66 8.33 1.04 o -2 2 3 623.48 656.59 23.23 o 0 2 3 5631.98 5312.03 103.49 o 2 2 3 2536.54 2621.60 127.92 o 4 2 3 1082.81 1068.23 54.91 o 6 2 3 191.64 197.65 11.10 o -7 3 3 8.10 13.07 1.51 o -5 3 3 55.20 57.35 2.96 o -3 3 3 1296.77 1247.45 32.79 o -1 3 3 879.40 789.94 28.17 o 1 3 3 2352.87 2087.71 108.75 o 3 3 3 171.81 158.75 10.38 o 5 3 3 2165.39 2342.65 92.08 o 7 3 3 4.54 5.09 2.41 o -8 4 3 33.84 30.88 4.85 o -6 4 3 76.45 79.32 7.03 o -4 4 3 364.08 400.77 22.39 o -2 4 3 27.78 19.94 1.29 o 0 4 3 324.74 268.70 7.63 o 2 4 3 2.96 10.20 1.30 o 4 4 3 387.61 357.61 9.93 o 6 4 3 56.15 59.61 3.63 o -7 5 3 84.30 87.77 5.81 o -5 5 3 552.61 502.40 14.63 o -3 5 3 476.42 463.41 24.13 o -1 5 3 122.91 102.77 4.81 o 1 5 3 174.50 155.24 12.05 o 3 5 3 1055.50 1068.48 33.02 o 5 5 3 162.62 179.61 6.45 o 7 5 3 128.16 122.26 6.60 o -8 6 3 29.79 33.06 2.97 o -6 6 3 263.93 246.67 15.20 o -4 6 3 525.60 511.19 18.66 o -2 6 3 1144.27 1053.36 58.23 o 0 6 3 278.50 301.95 7.79 o 2 6 3 219.50 204.14 10.72 o 4 6 3 1151.94 1175.98 28.48 o 6 6 3 96.57 96.62 3.93 o -7 7 3 41.99 59.17 6.05 o -5 7 3 106.27 104.73 4.54 o -3 7 3 100.07 88.97 3.93 o -1 7 3 1086.39 967.58 27.07 o 1 7 3 855.45 727.39 21.41 o 3 7 3 340.18 365.59 13.76 o 5 7 3 74.70 88.13 3.83 o 7 7 3 27.40 28.15 2.60 o -8 8 3 50.23 45.53 6.93 o -6 8 3 169.45 186.19 10.27 o -4 8 3 73.21 67.49 4.29 o -2 8 3 2007.56 1932.76 63.83 o 0 8 3 41.15 27.58 2.00 o 2 8 3 6.18 3.96 2.03 o 4 8 3 228.55 233.18 12.00 o 6 8 3 204.23 202.67 7.69 o -7 9 3 43.41 41.46 4.20 o -5 9 3 24.80 24.06 2.39 o -3 9 3 382.10 377.59 15.13 o -1 9 3 540.70 575.61 28.43 o 1 9 3 396.74 374.05 12.95 o 3 9 3 185.90 205.12 12.90 o 5 9 3 101.54 94.82 6.02 o -6 10 3 13.81 14.58 3.19 o -4 10 3 143.61 136.11 8.44 o -2 10 3 646.60 695.96 26.96 o 0 10 3 195.86 182.14 7.22 o 2 10 3 249.03 265.83 16.79 o 4 10 3 251.78 284.99 13.80 o 6 10 3 24.00 21.24 2.67 o -7 11 3 10.55 7.46 2.05 o -5 11 3 25.19 25.32 2.38 o -3 11 3 108.62 103.89 6.39 o -1 11 3 304.77 347.82 22.60 o 1 11 3 70.92 64.16 5.62 o 3 11 3 233.98 244.58 24.14 o 5 11 3 21.74 23.31 4.52 o -6 12 3 10.11 6.17 2.58 o -4 12 3 51.84 44.61 2.73 o -2 12 3 218.25 214.04 15.04 o 0 12 3 22.44 26.02 3.54 o 2 12 3 155.99 163.87 10.93 o 4 12 3 25.35 29.63 4.40 o -5 13 3 99.55 94.40 6.30 o -3 13 3 187.64 201.59 14.70 o -1 13 3 61.63 57.80 3.48 o 1 13 3 32.51 35.33 3.38 o 3 13 3 37.57 30.12 3.94 o 5 13 3 86.31 90.14 7.39 o -4 14 3 82.60 89.45 10.56 o -2 14 3 7.58 6.94 1.93 o 0 14 3 156.87 177.29 12.06 o 2 14 3 49.81 59.48 7.61 o 4 14 3 25.98 27.63 3.90 o -3 15 3 4.98 8.84 1.99 o -1 15 3 27.57 25.15 7.32 o 1 15 3 95.05 102.97 8.28 o 3 15 3 50.77 56.06 6.31 o -2 16 3 33.88 33.91 5.97 o 0 16 3 11.24 16.16 3.51 o 2 16 3 25.91 26.85 4.47 o -1 17 3 17.77 18.46 7.43 o 1 17 3 1.69 2.77 2.64 o -8 0 4 42.51 36.72 5.33 o -6 0 4 278.50 240.89 15.01 o -4 0 4 100.22 96.54 3.44 o -2 0 4 1024.92 1027.55 22.41 o 0 0 4 1283.00 946.35 33.21 o 2 0 4 1916.48 2424.94 133.92 o 4 0 4 360.63 326.71 29.91 o 6 0 4 2.50 2.13 2.54 o -7 1 4 97.65 79.09 5.66 o -5 1 4 457.51 471.90 22.43 o -3 1 4 88.76 109.06 3.70 o -1 1 4 1315.65 1242.05 27.22 o 1 1 4 3521.83 3786.56 143.81 o 3 1 4 178.72 157.81 6.42 o 5 1 4 747.27 869.07 46.14 o 7 1 4 53.04 54.99 3.64 o -8 2 4 5.47 4.75 3.08 o -6 2 4 492.01 493.51 18.63 o -4 2 4 126.31 139.57 4.11 o -2 2 4 328.75 362.11 7.27 o 0 2 4 79.90 109.96 4.82 o 2 2 4 1583.20 1849.99 91.52 o 4 2 4 126.65 123.08 6.89 o 6 2 4 24.48 21.29 2.45 o -7 3 4 175.10 163.91 6.17 o -5 3 4 858.45 880.22 38.56 o -3 3 4 672.78 591.16 22.18 o -1 3 4 698.37 685.55 19.69 o 1 3 4 2267.99 2029.62 117.58 o 3 3 4 380.77 345.39 16.47 o 5 3 4 475.88 510.01 22.67 o 7 3 4 55.42 60.03 4.85 o -8 4 4 15.93 14.20 2.37 o -6 4 4 466.30 481.64 36.97 o -4 4 4 73.56 69.63 3.75 o -2 4 4 41.10 61.87 2.22 o 0 4 4 1292.62 1236.95 44.72 o 2 4 4 463.79 385.28 17.36 o 4 4 4 80.67 77.67 6.67 o 6 4 4 91.79 96.42 4.40 o -7 5 4 26.87 29.76 3.57 o -5 5 4 440.13 418.11 17.97 o -3 5 4 79.64 80.70 3.98 o -1 5 4 1034.70 1147.06 33.71 o 1 5 4 384.02 389.95 15.37 o 3 5 4 207.83 231.36 8.76 o 5 5 4 226.25 208.54 12.36 o 7 5 4 222.96 212.75 7.88 o -8 6 4 44.33 42.20 3.44 o -6 6 4 17.94 14.55 2.51 o -4 6 4 411.07 375.17 23.28 o -2 6 4 1069.76 1074.89 45.94 o 0 6 4 824.96 810.53 28.04 o 2 6 4 1127.17 1174.80 54.01 o 4 6 4 984.20 1059.76 23.66 o 6 6 4 18.46 18.15 2.60 o -7 7 4 50.90 51.18 4.12 o -5 7 4 378.76 360.07 23.99 o -3 7 4 338.48 314.80 17.91 o -1 7 4 180.42 165.35 4.25 o 1 7 4 1587.67 1537.74 49.37 o 3 7 4 312.40 327.84 23.17 o 5 7 4 193.23 183.41 6.42 o -8 8 4 65.73 69.37 8.94 o -6 8 4 87.93 80.23 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1 12 5.78 -1.61 3.01 o -1 1 12 28.71 26.45 3.62 o 1 1 12 60.10 61.20 4.89 o -6 2 12 5.10 -1.38 4.09 o -4 2 12 39.66 36.61 3.99 o -2 2 12 245.53 226.09 7.19 o 0 2 12 8.92 6.34 3.92 o -5 3 12 43.04 39.04 4.03 o -3 3 12 27.05 26.97 2.98 o -1 3 12 88.12 76.23 5.46 o 1 3 12 119.78 110.52 6.68 o -6 4 12 17.21 11.88 4.14 o -4 4 12 0.90 4.59 2.98 o -2 4 12 55.64 53.66 3.99 o 0 4 12 8.39 7.01 3.19 o -5 5 12 50.08 43.68 4.56 o -3 5 12 64.50 80.49 6.68 o -1 5 12 90.49 90.78 4.75 o 1 5 12 57.02 51.90 7.07 o -4 6 12 13.69 13.07 3.11 o -2 6 12 85.63 83.39 6.56 o 0 6 12 27.00 18.60 3.77 o -3 7 12 157.52 154.95 15.59 o -1 7 12 62.43 59.28 8.09 o -4 8 12 12.15 14.08 4.35 o -2 8 12 23.89 24.79 4.57 o -5 1 13 35.07 36.01 5.92 o -3 1 13 11.32 13.87 2.72 o -1 1 13 21.77 20.39 3.58 o -4 2 13 37.62 26.17 4.12 o -2 2 13 66.90 64.29 6.25 o 0 2 13 23.19 24.48 5.30 o -3 3 13 57.25 53.86 3.85 o -1 3 13 41.19 31.35 5.24 o -4 4 13 27.65 22.96 3.49 o -2 4 13 110.32 126.12 8.38 o -3 5 13 0.75 -3.42 3.42 o -1 5 13 5.55 1.26 6.19 o -2 6 13 10.64 8.74 3.82 o