#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014267.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014267_Fobs loop_ _publ_author_name 'Okabe, Nobuo' 'Muranishi, Yasunori' 'Odoko, Mamiko' _publ_section_title ; Cobalt(II), nickel(II) and copper(II) complexes of isoquinoline-3-carboxylate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m345 _journal_page_last m347 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _[local]_cod_data_source_file ta1443Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_calc _refln_observed_status 0 0 2 17880.56 908.44 18176.01 o 1 0 -2 5598.54 273.92 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871.54 o 1 2 -1 1562.60 79.60 1505.57 o 3 0 2 1334.76 70.92 1363.27 o 2 1 -4 1.31 5.54 1.54 o 2 1 3 367.82 22.32 379.02 o 1 1 4 751.75 39.48 702.07 o 1 2 1 7.56 5.05 2.50 o 3 1 1 5491.87 274.38 5387.53 o 0 2 2 2201.44 115.60 2269.35 o 1 2 -2 910.36 51.56 992.51 o 3 0 -4 153.13 11.80 155.79 o 3 1 -3 8.01 2.67 4.86 o 2 0 4 6308.65 319.69 6334.79 o 1 2 2 2329.32 122.16 2396.60 o 1 1 -5 13902.40 682.15 13404.22 o 2 2 -1 869.10 46.28 835.70 o 2 2 0 1146.20 56.35 998.61 o 3 1 2 70.82 6.51 80.63 o 0 1 5 271.80 18.22 293.98 o 4 0 -2 692.82 39.32 716.34 o 0 2 3 903.88 46.54 823.08 o 4 0 0 3245.28 163.65 3177.53 o 1 2 -3 26.11 3.09 28.80 o 2 2 -2 1514.19 81.73 1587.60 o 2 2 1 622.72 33.27 567.38 o 3 1 -4 1135.67 58.20 1058.01 o 2 1 -5 1332.86 71.50 1363.75 o 2 1 4 162.48 12.28 153.01 o 1 0 -6 388.94 22.93 364.45 o 1 2 3 489.25 26.94 431.47 o 1 1 5 4.38 2.63 4.03 o 2 2 -3 2004.56 100.45 1887.53 o 4 1 -1 571.99 34.12 617.52 o 0 0 6 561.07 33.59 601.49 o 2 2 2 1154.55 63.54 1213.49 o 4 1 -2 3.81 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561.32 o 3 6 6 295.27 26.62 258.59 o 9 4 -7 12.71 8.90 5.34 o 8 5 -4 244.92 25.80 242.65 o 0 6 8 142.17 13.67 151.95 o 7 1 11 344.69 33.23 364.17 o 9 2 7 16.08 10.79 0.20 o 2 6 7 17.77 12.90 6.79 o 10 1 -11 36.57 7.08 28.91 o 8 5 0 44.12 6.62 36.90 o 10 0 6 145.56 14.76 134.87 o 5 4 10 93.54 9.45 82.26 o 4 4 11 6.23 12.69 6.56 o 6 5 6 13.87 10.14 1.48 o 7 4 -11 5.81 11.34 0.07 o 6 4 -12 499.15 39.40 487.77 o 10 2 -10 83.05 9.29 83.61 o 4 6 -7 21.76 6.57 17.64 o 7 5 4 25.08 6.62 25.67 o 1 0 16 217.08 20.07 229.56 o 7 3 -13 74.30 8.43 73.36 o 2 3 -15 281.44 22.61 276.59 o 11 2 1 4.40 15.38 19.56 o 4 6 5 2.69 14.14 12.55 o 9 1 8 6.23 8.98 8.41 o 8 1 -14 1.75 13.94 3.05 o 8 2 9 12.32 8.35 7.37 o 1 5 11 169.82 16.81 172.62 o 9 2 -12 18.81 17.29 42.67 o 4 5 -11 117.04 11.76 105.84 o 10 3 -8 198.24 18.84 199.49 o 11 2 -7 14.06 12.74 5.75 o 5 1 -16 17.93 15.11 22.49 o 6 6 -2 154.75 16.32 155.36 o 8 5 -5 268.22 28.84 272.51 o 6 6 -1 0.84 11.13 2.20 o 8 3 -12 26.17 6.32 10.80 o 3 3 -15 154.11 16.19 130.45 o 8 0 10 426.21 34.44 402.83 o 3 6 -8 268.50 30.61 311.48 o 2 3 14 23.54 6.47 23.28 o 5 6 -6 485.02 39.43 502.36 o 2 2 -16 20.84 6.09 9.96 o 6 4 9 11.04 13.46 0.90 o 3 4 12 80.70 9.01 80.45 o 8 5 1 392.15 33.12 376.58 o 11 1 3 268.56 26.21 246.37 o 1 6 8 221.66 24.04 208.75 o 10 1 6 9.03 12.45 1.53 o 3 2 -16 11.79 8.16 9.63 o 4 5 9 320.28 30.83 329.93 o 6 6 0 390.55 32.61 373.69 o 7 1 -15 96.55 10.74 104.27 o 2 2 15 12.41 13.65 4.93 o 9 1 -13 364.61 37.01 439.90 o 11 1 -9 73.71 8.65 67.65 o 9 4 3 11.31 6.06 11.00 o 10 3 3 147.83 16.34 156.56 o 8 4 -10 273.51 28.39 290.01 o 5 4 -13 11.72 12.89 10.83 o 3 1 15 86.06 9.19 94.34 o 3 5 10 40.59 7.94 47.10 o 0 7 1 237.08 25.05 189.28 o 5 5 8 82.47 8.92 85.00 o 12 0 -4 248.47 26.03 239.47 o 9 4 -8 566.65 44.73 558.68 o 6 6 -4 151.23 14.57 156.01 o 9 3 6 9.46 10.41 13.08 o 12 0 -2 68.90 7.88 61.07 o 4 3 -15 317.26 33.01 353.27 o 1 7 -1 227.66 20.43 229.69 o 8 5 -6 15.82 16.36 22.46 o 0 3 15 28.12 6.46 22.07 o 5 2 13 19.34 13.32 12.13 o 5 3 12 4.57 8.21 3.91 o 4 2 -16 157.87 17.30 182.08 o 6 0 -16 15.57 13.17 1.94 o 1 7 1 184.61 18.50 208.11 o 6 2 12 257.43 24.92 195.18 o 5 6 4 60.56 7.43 56.58 o 11 2 2 149.73 14.43 154.79 o 0 7 2 56.76 7.23 58.54 o 8 4 6 402.68 35.77 425.63 o 10 0 -12 83.70 9.59 87.37 o 1 7 -2 9.41 6.63 16.45 o 11 2 -8 139.87 13.26 123.57 o 6 3 11 11.54 15.06 25.54 o 9 3 -11 266.87 26.60 245.02 o 11 0 4 365.24 32.75 381.26 o 6 5 -10 135.77 14.33 166.87 o 2 4 -14 214.59 23.65 212.05 o 3 6 7 16.82 13.23 16.46 o 2 5 -12 21.53 14.47 11.46 o 4 6 -8 118.31 11.52 110.48 o 0 2 16 9.23 16.67 43.20 o 4 3 13 42.99 7.24 30.86 o 10 4 -3 18.14 16.89 38.65 o 12 1 -3 234.25 25.33 225.98 o 1 5 -12 15.46 13.76 14.78 o 10 4 -2 395.25 34.29 332.98 o 7 5 5 48.69 7.17 49.68 o 11 0 -10 184.49 17.30 164.45 o 1 7 2 10.07 11.62 17.19 o 7 4 8 373.63 34.95 380.57 o 11 3 -3 313.83 30.15 265.63 o 1 4 -14 31.04 7.46 34.54 o 5 6 -7 4.05 12.70 0.02 o 2 5 11 296.71 28.12 264.86 o 10 3 -9 302.97 31.79 320.45 o 5 5 -11 127.84 12.55 112.64 o 6 6 -5 11.81 8.81 26.00 o 2 4 13 7.11 7.04 4.62 o 4 2 14 78.58 8.42 69.19 o 12 1 -2 11.02 7.76 3.44 o 2 7 0 4.02 12.64 0.00 o 2 7 -1 410.31 36.79 399.60 o 10 4 -4 262.01 27.09 276.37 o 11 3 -2 6.32 13.21 1.38 o 3 4 -14 25.45 7.16 27.77 o 4 6 6 95.96 10.62 97.11 o 2 6 8 365.50 33.72 364.77 o 12 0 -6 735.19 55.24 831.08 o 7 2 11 2.17 13.46 9.99 o 10 2 -11 65.07 7.72 58.56 o 6 1 -16 0.31 14.39 4.99 o 6 5 7 166.05 17.65 192.77 o 0 7 3 110.98 10.53 108.02 o 2 0 16 178.90 18.04 194.20 o 6 6 2 379.60 31.36 385.97 o 3 5 -12 65.02 8.24 67.93 o 1 7 -3 200.91 19.75 207.54 o 12 1 -5 310.12 31.90 363.34 o 2 7 -2 31.39 7.32 33.78 o 10 1 -12 268.26 27.92 260.05 o 2 7 1 270.39 29.85 246.92 o 7 5 -9 32.56 6.82 26.63 o 0 5 12 0.09 12.70 0.08 o 11 1 4 38.51 7.24 40.38 o 11 3 -1 311.77 29.77 309.41 o 12 0 0 45.40 7.01 42.02 o 12 1 -1 269.82 22.18 265.81 o 9 4 4 118.22 12.27 107.04 o 11 3 -5 240.85 21.31 248.51 o 8 5 -7 250.16 25.46 224.02 o 10 4 -5 46.84 7.42 42.78 o 7 3 10 35.48 7.40 39.25 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7.59 o 10 1 7 183.72 17.88 166.48 o 12 1 0 6.16 13.91 8.65 o 1 2 16 81.56 9.58 89.47 o 3 2 15 22.58 7.14 29.00 o 9 1 9 22.63 15.54 33.03 o 3 7 -1 226.68 20.63 235.78 o 8 3 -13 196.63 19.36 218.17 o 6 6 3 59.86 7.33 43.85 o 10 4 -6 3.88 15.15 7.81 o 3 7 0 67.21 8.44 72.89 o 4 1 -17 48.39 8.03 50.49 o 4 4 12 24.95 6.38 16.41 o 7 3 -14 35.07 7.32 38.60 o 3 7 -2 11.25 14.79 24.75 o 8 2 10 400.89 35.28 430.04 o 1 5 12 3.15 16.20 12.08 o 2 7 -4 121.62 13.07 126.78 o 4 5 10 12.36 14.80 2.12 o 5 6 -8 249.38 27.01 227.49 o 6 4 10 28.85 7.04 25.68 o 10 4 1 12.11 9.96 11.57 o 9 3 7 453.29 38.25 479.42 o 2 7 3 175.69 16.86 166.55 o 1 7 4 42.38 7.36 47.99 o 8 1 -15 219.99 18.92 201.13 o 3 7 1 652.71 48.36 645.55 o 9 5 -2 9.65 12.89 0.02 o 7 0 -16 61.21 7.88 51.28 o 9 5 -3 133.70 13.08 115.41 o 7 6 -2 96.79 10.17 98.60 o 12 1 -7 313.08 31.04 323.07 o 5 5 9 108.62 11.26 80.88 o 10 3 -10 2.48 15.37 0.46 o 7 6 -1 94.72 10.54 101.18 o 9 1 -14 104.22 11.74 112.20 o 3 7 -3 11.51 14.57 20.94 o 4 1 15 12.76 14.49 1.52 o 9 5 -1 212.52 19.89 208.29 o 1 4 14 352.52 32.15 363.59 o 3 6 8 434.26 34.92 387.88 o 0 1 17 130.10 12.41 112.06 o 11 3 1 2.96 10.37 15.26 o 12 2 -3 22.09 6.92 27.07 o 3 5 11 505.62 41.99 523.44 o 6 5 -11 25.86 17.72 41.78 o 8 3 9 260.86 27.10 261.25 o 4 6 7 38.65 7.93 46.51 o 9 3 -12 18.32 14.93 11.11 o 12 2 -4 12.21 16.94 37.16 o 11 3 -7 739.69 54.38 777.10 o 12 0 -8 574.86 45.91 605.01 o 12 1 1 104.66 10.78 106.70 o 7 6 0 189.44 18.03 172.40 o 1 7 -5 305.98 29.37 281.38 o 12 2 -2 98.07 10.59 91.27 o 1 6 -10 53.35 7.59 56.79 o 5 4 -14 105.89 11.33 107.72 o 3 7 2 36.27 7.27 31.28 o 10 4 -7 98.64 10.79 103.66 o 0 7 5 20.40 14.18 13.50 o 2 6 -10 287.19 31.64 306.12 o 9 4 5 42.12 6.68 23.34 o 6 6 -7 14.84 6.59 15.12 o 7 6 -4 293.18 28.58 264.27 o 6 2 -16 16.38 6.79 20.38 o 6 3 -15 9.30 15.85 4.08 o 7 5 -10 11.55 14.61 12.11 o 11 1 5 151.66 13.61 146.89 o 3 3 -16 210.79 21.61 241.05 o 10 3 5 218.29 20.32 223.30 o 5 1 -17 115.37 11.72 118.84 o 2 6 9 3.15 14.73 1.37 o 10 2 -12 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16.31 0.94 o 2 2 -18 40.00 8.18 47.27 o 3 2 -18 202.19 20.12 187.74 o 7 3 12 11.69 11.92 0.06 o 2 7 -8 34.33 7.71 25.24 o 3 7 6 31.32 6.91 18.26 o 8 2 -16 29.18 7.73 33.64 o 1 0 18 81.87 10.26 86.70 o 2 4 -16 29.29 7.70 22.79 o 9 5 -9 171.40 15.79 164.02 o 11 1 -13 63.05 9.10 70.19 o 8 6 -6 170.97 17.24 195.15 o 2 7 7 84.84 9.64 85.32 o 4 5 -14 19.39 14.91 14.11 o 8 3 -15 106.43 11.57 102.83 o 6 5 -13 50.94 8.10 38.76 o 3 4 -16 14.66 7.31 13.16 o 6 0 -18 54.60 8.33 48.90 o 10 4 5 9.84 14.72 17.83 o 12 3 -7 284.77 23.58 261.91 o 4 7 -7 12.35 14.00 3.15 o 13 1 0 56.19 7.96 40.72 o 2 4 15 75.52 9.05 63.51 o 9 3 -14 11.62 15.08 3.62 o 5 7 3 345.77 34.62 338.29 o 8 6 2 144.96 14.16 125.71 o 9 0 -16 63.00 8.92 58.83 o 1 4 -16 46.62 9.36 63.32 o 5 5 11 169.33 15.63 162.01 o 4 3 15 154.37 16.75 154.63 o 6 6 -10 16.56 7.41 31.36 o 8 5 -11 60.58 8.14 56.73 o 1 2 -18 27.99 7.70 31.62 o 9 1 11 69.15 8.88 71.71 o 2 6 -12 17.50 17.42 29.39 o 0 3 17 33.15 8.51 39.00 o 12 1 -11 23.48 6.78 13.90 o 4 2 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6.91 20.92 o 4 2 16 28.72 8.27 36.63 o 7 2 -17 10.18 12.75 0.01 o 11 3 -11 54.85 8.56 44.70 o 13 2 -2 4.58 16.34 34.74 o 13 2 -5 9.37 15.95 0.27 o 7 0 14 81.12 10.19 73.93 o 8 6 -7 13.64 14.81 2.24 o 0 4 16 112.22 11.66 119.56 o 12 1 5 81.20 9.49 89.74 o 13 1 1 119.09 12.42 124.28 o 6 7 -4 0.91 16.94 3.06 o 10 3 -13 72.37 9.67 78.47 o 13 1 -8 14.90 10.50 3.76 o 0 2 18 72.04 10.08 78.24 o 4 4 14 99.82 10.29 96.89 o 3 5 13 159.03 16.15 159.50 o 5 5 -14 12.42 10.91 11.01 o 10 1 -15 8.60 17.35 23.03 o 10 5 -7 8.13 19.47 29.36 o 12 2 4 96.66 10.08 91.98 o 6 7 1 200.62 18.18 160.53 o 9 5 5 106.78 11.30 93.19 o 5 2 -18 50.34 8.25 41.87 o 7 4 11 20.87 17.19 15.35 o 8 6 3 11.12 13.42 3.08 o 8 1 -17 18.37 18.62 29.45 o 5 7 4 47.52 8.69 53.64 o 5 0 16 216.19 22.20 227.47 o 13 2 -1 8.57 15.12 3.55 o 13 2 -6 17.46 21.06 58.01 o 3 3 16 15.35 16.58 30.22 o 6 1 15 79.75 9.68 76.30 o 4 6 -12 11.37 13.73 2.31 o 7 5 9 149.91 15.44 154.83 o 12 3 2 42.17 8.03 42.52 o 3 7 7 13.53 12.41 4.09 o 12 0 -12 203.66 21.02 201.63 o 1 3 17 25.34 7.47 22.70 o 10 0 10 35.85 7.60 27.56 o 10 5 2 6.66 15.55 13.06 o 13 0 2 196.12 18.97 166.79 o 1 7 -9 20.45 6.88 16.07 o 11 2 7 8.16 15.61 9.79 o 7 1 14 27.63 7.85 25.30 o 4 7 -8 38.61 8.13 43.84 o 9 4 8 149.16 15.34 157.12 o 8 4 -14 33.00 7.64 19.90 o 2 0 18 66.39 9.67 70.78 o 2 7 -9 220.46 23.74 171.62 o 5 4 -16 72.52 9.17 59.82 o 11 0 -14 146.57 15.50 139.27 o 5 7 -7 12.87 16.09 15.78 o 6 7 -5 173.16 17.94 155.61 o 1 6 12 25.91 17.81 32.65 o 4 7 6 11.66 12.99 2.24 o 2 7 8 6.82 13.51 0.49 o 11 2 -13 21.69 14.91 15.04 o 4 6 10 87.12 10.37 71.63 o 7 0 -18 12.89 8.85 0.82 o 0 7 9 54.93 8.19 51.75 o 6 7 2 18.50 7.03 14.39 o 11 4 3 141.22 14.51 105.50 o 10 3 8 16.12 19.42 18.53 o 5 1 16 5.61 17.29 7.67 o 9 6 -2 59.79 8.54 50.38 o 10 4 6 199.79 19.07 175.07 o 3 1 -19 44.64 7.68 30.04 o 7 4 -15 30.95 8.16 40.61 o 5 6 9 73.20 9.13 61.22 o 2 1 -19 6.04 16.91 14.26 o 13 2 0 49.65 8.30 44.78 o 9 4 -13 3.78 13.40 0.79 o 7 6 6 131.08 13.08 107.05 o 11 4 -9 12.91 16.14 11.76 o 13 2 -7 18.58 14.68 0.97 o 0 8 0 353.33 34.37 338.22 o 9 6 -1 2.92 18.63 25.61 o 1 4 16 200.66 20.51 188.91 o 7 5 -13 2.93 18.71 4.86 o 8 6 -8 135.24 14.72 140.17 o 9 2 11 35.50 7.99 18.82 o 13 1 2 39.48 6.88 13.36 o 2 5 -15 38.12 7.33 32.22 o 9 6 -4 53.90 8.53 47.17 o 8 1 13 93.06 11.41 99.59 o 12 3 -9 177.99 17.09 163.92 o 13 1 -9 88.22 10.54 81.96 o 0 8 1 14.49 7.42 12.44 o 3 2 17 32.02 7.45 25.49 o 3 7 -9 26.92 20.79 49.94 o 6 6 -11 18.81 14.87 3.97 o 10 5 -8 32.49 7.68 22.92 o 2 1 18 0.28 16.12 5.77 o 11 1 -14 20.73 16.62 2.44 o 1 8 0 9.24 15.09 20.44 o 8 5 -12 15.34 15.26 0.02 o 4 1 -19 18.06 18.10 25.48 o 8 4 10 87.12 9.85 91.88 o 9 3 10 59.12 9.09 50.29 o 3 5 -15 92.61 9.57 83.39 o 12 0 6 405.27 38.37 394.49 o 1 5 -15 18.79 19.09 38.08 o 2 5 14 23.79 7.54 14.67 o 1 2 18 71.79 9.25 67.79 o 1 1 -19 16.53 15.93 7.42 o 7 1 -18 16.95 12.91 7.34 o 7 6 -10 90.15 10.19 74.74 o 8 6 4 206.01 20.68 214.12 o 1 8 1 8.09 10.19 1.60 o 9 6 0 186.32 19.65 175.67 o 6 2 -18 23.18 17.93 34.14 o 0 8 2 160.08 15.35 167.50 o 5 7 5 266.97 24.24 274.85 o 6 7 -6 16.96 12.93 4.88 o 1 7 9 108.87 11.85 111.41 o 9 6 -5 41.55 8.83 42.85 o 1 8 -2 92.69 10.38 95.38 o 6 6 8 47.54 8.28 42.85 o 9 2 -16 84.43 9.57 76.26 o 10 5 3 100.18 10.55 106.85 o 5 6 -12 23.43 7.66 25.20 o 9 0 12 184.02 16.43 177.72 o 11 3 -12 7.30 15.55 2.05 o 12 3 3 15.33 5.95 1.15 o 6 7 3 203.79 19.68 188.02 o 6 3 14 36.85 7.27 21.59 o 9 3 -15 71.39 9.21 60.28 o 1 8 2 37.47 7.06 32.39 o 13 0 -10 264.16 23.77 274.46 o 8 5 8 4.14 15.22 0.01 o 13 2 -8 69.16 9.03 63.51 o 2 6 -13 53.68 9.06 57.43 o 3 3 -18 45.82 9.74 66.54 o 9 5 6 54.33 8.19 51.21 o 12 4 -2 2.62 15.24 1.07 o 2 8 -1 14.80 14.25 2.46 o 2 8 0 25.44 8.07 39.79 o 4 5 -15 43.08 8.42 43.84 o 8 3 -16 6.14 14.94 7.71 o 10 2 -15 20.11 7.25 13.30 o 0 5 15 13.18 18.60 31.00 o 1 6 -13 19.92 13.93 16.09 o 7 3 13 9.57 18.91 71.83 o 5 5 12 55.73 8.06 43.42 o 5 3 15 85.44 9.27 63.54 o 8 2 -17 5.50 17.74 10.98 o 2 6 12 35.17 7.44 24.51 o 1 8 -3 4.13 13.08 0.03 o 9 6 1 38.32 7.79 32.68 o 5 1 -19 34.78 7.58 17.67 o 2 3 17 44.84 8.35 47.04 o 2 8 -2 31.64 7.63 27.58 o 4 7 -9 59.14 8.98 52.91 o 10 4 -12 178.08 16.18 175.30 o 7 7 -1 34.92 8.01 40.53 o 3 6 -13 13.10 16.68 14.68 o 6 5 11 151.21 15.53 145.93 o 7 7 -3 75.09 9.41 72.60 o 9 5 -11 69.70 9.66 75.92 o 6 2 15 7.53 6.61 2.26 o 9 6 -6 46.22 8.34 40.04 o 11 4 4 247.23 21.67 208.50 o 1 3 -18 1.49 11.13 3.08 o 12 4 -1 32.45 7.04 20.14 o 0 1 19 70.48 9.67 70.86 o 3 7 8 36.96 8.88 46.32 o 9 1 12 14.51 14.23 15.65 o 4 3 -18 18.66 15.82 14.41 o 7 2 14 75.89 9.41 64.13 o 10 0 -16 359.55 38.03 375.66 o 4 5 13 40.91 7.95 29.95 o 4 7 7 151.97 15.31 135.08 o 13 1 3 197.60 20.13 185.00 o 10 3 -14 9.57 17.10 11.18 o 11 4 -10 6.29 18.89 10.44 o 1 8 3 13.69 13.74 0.23 o 11 5 -3 271.74 28.71 205.09 o 13 1 -10 36.57 7.74 32.33 o 3 4 -17 5.58 17.97 11.05 o 7 7 0 42.12 8.05 39.59 o