#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014268.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014268_Fobs loop_ _publ_author_name 'Okabe, Nobuo' 'Muranishi, Yasunori' 'Odoko, Mamiko' _publ_section_title ; Cobalt(II), nickel(II) and copper(II) complexes of isoquinoline-3-carboxylate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m345 _journal_page_last m347 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _[local]_cod_data_source_file ta1443IIsup3.hkl _[local]_cod_data_source_block II loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_calc _refln_observed_status 0 0 2 19431.32 960.52 18947.76 o 1 0 -2 5979.30 295.83 5839.27 o 0 1 1 11965.41 599.84 11960.32 o 1 0 2 8859.58 439.68 8703.92 o 1 1 0 1596.24 80.54 1558.46 o 1 1 -1 632.67 34.34 650.58 o 2 0 0 6586.47 331.04 6578.47 o 1 1 1 9.66 2.41 16.18 o 0 1 2 42.33 4.69 43.42 o 2 0 -2 561.93 29.54 525.25 o 1 1 -2 3.65 3.09 0.24 o 1 1 2 1844.95 93.78 1813.88 o 2 1 -1 6152.05 304.22 5973.40 o 2 1 0 175.68 12.41 164.49 o 2 0 2 544.78 31.75 592.14 o 0 1 3 119.87 10.03 104.80 o 1 1 -3 15092.74 741.38 14614.10 o 2 1 -2 129.78 10.85 140.71 o 2 1 1 900.98 47.45 881.45 o 1 0 -4 15217.31 750.73 14830.25 o 0 0 4 149.50 10.76 104.36 o 3 0 0 4320.09 217.38 4268.57 o 1 1 3 -2.09 6.81 6.53 o 3 0 -2 151.68 12.10 141.52 o 2 1 -3 1936.69 101.59 1986.05 o 2 0 -4 10772.33 505.11 9668.93 o 2 1 2 420.04 24.82 424.32 o 1 0 4 3071.02 153.57 2972.73 o 1 1 -4 19127.86 942.21 18606.22 o 0 1 4 178.52 12.84 172.22 o 0 2 0 33.82 3.78 30.06 o 3 1 -1 3752.62 191.19 3759.02 o 0 2 1 478.70 26.77 444.89 o 3 1 0 372.85 22.08 350.78 o 1 2 0 1308.54 67.12 1248.30 o 3 1 -2 339.40 20.82 335.87 o 1 2 -1 2021.26 101.46 1921.07 o 2 1 -4 1.32 6.53 0.68 o 3 0 2 1450.85 78.32 1515.94 o 1 1 4 740.54 38.95 673.61 o 1 2 1 21.51 3.43 19.26 o 2 1 3 314.34 20.12 319.29 o 0 2 2 2261.66 118.87 2325.03 o 3 1 1 5440.54 270.24 5277.69 o 1 2 -2 907.24 52.69 1017.36 o 3 0 -4 107.41 10.61 97.67 o 3 1 -3 8.73 3.08 5.37 o 2 0 4 6679.71 335.26 6602.37 o 1 2 2 2780.14 138.17 2636.88 o 1 1 -5 14269.58 714.25 14179.55 o 2 2 -1 1091.39 58.03 1070.62 o 2 2 0 869.15 43.37 725.90 o 0 1 5 488.00 30.32 536.38 o 3 1 2 63.06 6.92 55.96 o 0 2 3 844.19 44.56 783.03 o 1 2 -3 30.18 3.66 31.11 o 4 0 -2 716.99 41.46 760.63 o 2 2 -2 1439.05 80.74 1583.13 o 4 0 0 3065.06 157.59 3072.43 o 2 2 1 888.14 46.44 816.24 o 3 1 -4 1186.16 60.70 1095.93 o 2 1 -5 1475.68 79.54 1525.02 o 2 1 4 161.04 12.95 142.46 o 1 0 -6 469.74 27.83 461.35 o 1 2 3 404.42 23.39 351.26 o 1 1 5 27.35 3.75 34.19 o 2 2 -3 2000.18 99.75 1855.32 o 0 0 6 523.34 31.99 560.67 o 2 2 2 1541.69 81.54 1544.88 o 4 1 -1 786.12 46.83 884.14 o 4 1 -2 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