#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/42/2014292.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014292_Fobs loop_ _publ_author_name 'Peresypkina, Eugenia V.' 'Virovets, Alexander V.' 'Akhmerkina, Jeanne V.' 'Serezhkina, Larisa B.' _publ_section_title ; {[Ba~2~(C~2~O~4~)(H~2~O)~6~](NCS)~2~}~n~: a layered mixed-anion barium oxalate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m355 _journal_page_last m356 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 85.517 _cell_angle_beta 71.498 _cell_angle_gamma 67.037 _cell_length_a 6.8990 _cell_length_b 6.9441 _cell_length_c 9.6383 _exptl_crystal_F_000 274.00 _reflns_d_resolution_high 0.8417 _[local]_cod_data_source_file tr1090Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s2w in P-1 absc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 116.44 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l 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8264.96 58.49 o 4 2 0 1175.42 1169.97 25.73 o 5 2 0 1237.07 1267.19 31.26 o 6 2 0 2511.58 2432.67 48.31 o 7 2 0 2.80 5.13 10.26 o -5 3 0 1367.56 1446.35 43.64 o -4 3 0 169.38 181.69 16.01 o -3 3 0 4752.39 5816.96 69.46 o -2 3 0 1470.20 1526.13 32.74 o -1 3 0 2494.64 2939.83 40.99 o 0 3 0 4159.79 4589.91 101.60 o 1 3 0 40.09 32.86 6.01 o 2 3 0 7703.67 8766.15 58.63 o 3 3 0 80.78 55.90 7.02 o 4 3 0 2090.59 1893.49 33.73 o 5 3 0 2817.13 2698.42 45.13 o 6 3 0 40.50 36.40 9.28 o 7 3 0 1577.76 1605.07 43.75 o -4 4 0 618.46 755.65 32.01 o -3 4 0 212.34 37.68 10.98 o -2 4 0 2929.39 3037.84 52.19 o -1 4 0 1254.53 1533.60 35.59 o 0 4 0 1132.33 1323.25 26.17 o 1 4 0 6139.44 6273.95 58.83 o 2 4 0 3657.58 3971.99 45.60 o 3 4 0 1684.20 1686.39 31.44 o 4 4 0 5417.60 5298.30 59.62 o 5 4 0 149.06 135.57 12.49 o 6 4 0 1000.02 899.98 30.13 o 7 4 0 1057.93 970.50 34.85 o -3 5 0 1547.50 1679.34 47.02 o -2 5 0 2359.99 2685.05 55.20 o -1 5 0 97.13 153.46 16.58 o 0 5 0 4230.01 5133.05 56.34 o 1 5 0 1187.66 1286.43 32.18 o 2 5 0 726.06 794.18 24.43 o 3 5 0 2704.43 2712.72 44.05 o 4 5 0 5.94 1.92 3.83 o 5 5 0 4019.26 4035.17 60.03 o 6 5 0 341.47 324.08 19.80 o 7 5 0 701.34 633.11 29.11 o -2 6 0 9.16 2.75 5.51 o -1 6 0 1830.43 1873.35 50.57 o 0 6 0 281.15 296.95 17.91 o 1 6 0 1219.24 1324.64 37.59 o 2 6 0 2242.15 2455.99 46.55 o 3 6 0 54.56 57.74 10.59 o 4 6 0 2282.95 2429.47 47.52 o 5 6 0 612.98 638.89 26.45 o 6 6 0 285.16 260.52 19.20 o 7 6 0 1589.98 1553.02 46.50 o -1 7 0 876.55 552.91 33.40 o 0 7 0 612.53 705.12 31.88 o 1 7 0 1647.44 1942.40 52.17 o 2 7 0 34.64 29.15 12.03 o 3 7 0 1128.15 1141.28 35.80 o 4 7 0 1303.58 1343.68 39.40 o 5 7 0 363.00 357.66 22.03 o 6 7 0 1900.43 1728.36 47.62 o 2 8 0 2344.93 2520.46 59.43 o 3 8 0 646.96 677.68 31.21 o 4 8 0 502.92 541.92 27.65 o -4 -8 1 486.51 544.10 28.55 o -3 -8 1 650.65 793.21 33.18 o -2 -8 1 1339.75 1491.13 46.08 o -5 -7 1 391.96 398.37 23.97 o -4 -7 1 1016.33 1120.80 36.31 o -3 -7 1 1857.58 1915.82 46.05 o -2 -7 1 72.64 81.86 13.20 o 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1224.42 1477.15 35.37 o 3 -4 1 453.43 471.94 22.56 o 4 -4 1 1605.59 1947.96 48.37 o -7 -3 1 899.60 885.50 34.66 o -6 -3 1 1.34 1.56 3.11 o -5 -3 1 3153.64 2932.28 48.80 o -4 -3 1 3035.37 3011.07 44.42 o -3 -3 1 2010.33 2104.52 33.28 o -2 -3 1 10049.74 11507.70 70.25 o -1 -3 1 1217.25 1304.02 23.17 o 0 -3 1 3173.88 3857.13 32.28 o 1 -3 1 5402.55 6534.90 57.72 o 2 -3 1 111.57 163.70 12.26 o 3 -3 1 2782.35 3276.27 51.14 o 4 -3 1 186.70 142.89 14.56 o 5 -3 1 1377.45 1400.90 42.02 o -7 -2 1 26.39 28.15 11.35 o -6 -2 1 2087.14 1909.47 44.72 o -5 -2 1 2056.37 1939.88 39.77 o -4 -2 1 411.10 395.82 16.83 o -3 -2 1 3279.22 3136.07 38.60 o -2 -2 1 782.64 841.51 17.89 o -1 -2 1 3296.10 3409.17 31.10 o 0 -2 1 1707.96 1750.61 15.96 o 1 -2 1 6427.84 8106.56 53.29 o 2 -2 1 8659.65 10575.82 70.29 o 3 -2 1 329.13 331.65 15.68 o 4 -2 1 3591.02 3744.79 55.15 o 5 -2 1 1976.34 2179.35 48.04 o 6 -2 1 1.93 3.11 6.21 o -7 -1 1 1124.35 1178.74 40.12 o -6 -1 1 244.25 245.37 17.94 o -5 -1 1 373.01 375.13 18.86 o -4 -1 1 2157.15 2053.07 36.68 o -3 -1 1 329.34 333.18 13.24 o -2 -1 1 9635.92 9989.65 56.29 o -1 -1 1 7355.37 6918.19 37.95 o 0 -1 1 1040.57 956.26 15.91 o 1 -1 1 5461.23 6779.46 38.67 o 2 -1 1 6017.56 7299.50 50.08 o 3 -1 1 2493.13 2901.76 38.16 o 4 -1 1 1209.64 1218.93 29.53 o 5 -1 1 2.81 5.43 10.85 o 6 -1 1 1415.44 1423.79 40.78 o -6 0 1 263.16 251.63 19.23 o -5 0 1 4862.95 5001.70 67.24 o -4 0 1 285.90 278.64 15.30 o -3 0 1 2928.54 2912.05 38.64 o -2 0 1 11931.77 10729.32 60.52 o -1 0 1 162.59 172.07 6.94 o 0 0 1 12295.36 9755.99 47.15 o 1 0 1 38.61 48.22 3.62 o 2 0 1 1703.20 1792.03 21.98 o 3 0 1 4681.64 5043.10 45.69 o 4 0 1 373.08 331.65 15.06 o 5 0 1 5785.82 6314.54 69.94 o 6 0 1 206.17 182.69 15.35 o 7 0 1 822.03 779.08 32.83 o -6 1 1 1342.81 1326.17 41.93 o -5 1 1 24.44 26.02 9.42 o -4 1 1 2501.51 2354.68 43.17 o -3 1 1 2115.48 2238.40 36.85 o -2 1 1 2417.55 2458.92 33.14 o -1 1 1 11252.49 11136.96 58.23 o 0 1 1 1495.59 1749.56 16.83 o 1 1 1 4211.24 4503.04 26.52 o 2 1 1 10314.58 9918.60 49.06 o 3 1 1 109.58 126.69 7.91 o 4 1 1 2700.88 2665.50 37.75 o 5 1 1 845.67 831.85 25.28 o 6 1 1 730.20 761.28 27.66 o 7 1 1 1135.54 1123.68 37.76 o -6 2 1 200.33 260.64 21.58 o -5 2 1 1606.77 1684.11 45.13 o -4 2 1 2246.21 2353.38 47.51 o -3 2 1 49.39 42.15 9.12 o -2 2 1 2071.91 2152.25 35.70 o -1 2 1 2178.88 2424.86 33.66 o 0 2 1 3572.52 4129.63 44.11 o 1 2 1 3660.23 3971.63 32.61 o 2 2 1 4509.57 4818.55 37.64 o 3 2 1 6116.61 6330.18 49.67 o 4 2 1 2547.52 2456.74 36.15 o 5 2 1 3117.00 3150.52 47.05 o 6 2 1 4217.49 4003.33 59.80 o 7 2 1 21.61 17.94 10.60 o -5 3 1 739.68 793.53 34.47 o -4 3 1 108.68 114.39 14.25 o -3 3 1 3182.01 3549.94 56.99 o -2 3 1 12.65 20.96 9.56 o -1 3 1 3804.20 3957.92 50.81 o 0 3 1 7320.55 8251.14 55.80 o 1 3 1 958.90 1028.14 21.18 o 2 3 1 8454.61 9607.15 61.38 o 3 3 1 2243.97 2201.78 31.89 o 4 3 1 1006.90 973.42 23.89 o 5 3 1 2878.14 2799.12 44.95 o 6 3 1 26.76 37.70 8.85 o 7 3 1 1405.38 1321.66 39.22 o -4 4 1 2213.28 2214.61 54.90 o -3 4 1 414.38 520.97 25.67 o -2 4 1 1516.53 1632.18 40.80 o -1 4 1 3172.60 3377.92 54.71 o 0 4 1 205.13 207.75 113.32 o 1 4 1 2195.31 2208.69 37.51 o 2 4 1 3252.84 3471.43 42.97 o 3 4 1 1877.68 1821.33 32.10 o 4 4 1 1523.45 1484.65 31.12 o 5 4 1 1.83 5.73 11.46 o 6 4 1 1594.43 1486.05 37.39 o 7 4 1 1272.70 1118.18 36.14 o -3 5 1 670.22 794.02 34.27 o -2 5 1 1529.67 1519.43 43.69 o -1 5 1 68.19 62.43 14.03 o 0 5 1 5300.82 6168.74 133.24 o 1 5 1 980.34 952.98 29.71 o 2 5 1 2187.58 2442.66 41.33 o 3 5 1 4728.05 4974.86 58.85 o 4 5 1 49.26 53.26 9.56 o 5 5 1 3355.39 3212.65 53.03 o 6 5 1 1165.70 1242.23 35.13 o 7 5 1 472.11 430.42 23.88 o -2 6 1 2.32 24.40 14.08 o -1 6 1 1917.56 2.89 5.79 o 0 6 1 221.59 255.06 17.30 o 1 6 1 198.40 216.54 18.29 o 2 6 1 2088.75 2348.66 46.63 o 3 6 1 109.43 98.77 11.75 o 4 6 1 2584.15 2660.28 49.24 o 5 6 1 580.05 544.10 24.27 o 6 6 1 575.13 572.52 26.45 o 7 6 1 1853.82 1789.21 48.46 o -1 7 1 257.70 88.69 19.94 o 0 7 1 713.85 893.26 31.10 o 1 7 1 2038.32 2254.68 57.93 o 2 7 1 0.03 10.53 12.06 o 3 7 1 1936.16 1932.15 45.99 o 4 7 1 1978.50 2144.11 48.53 o 5 7 1 492.44 451.63 25.16 o 6 7 1 1465.81 1395.76 42.65 o 2 8 1 1264.78 1400.11 46.08 o 3 8 1 639.99 685.31 31.09 o 4 8 1 201.88 202.32 18.90 o -5 -7 2 475.80 461.59 26.38 o -4 -7 2 753.30 802.97 32.14 o -3 -7 2 1118.84 1106.02 36.45 o -2 -7 2 54.09 57.42 12.60 o -1 -7 2 1943.23 2354.31 52.62 o 0 -7 2 455.45 646.91 24.84 o 1 -7 2 428.21 213.55 21.93 o -6 -6 2 159.27 154.81 16.58 o -5 -6 2 701.12 630.91 28.15 o -4 -6 2 2021.55 2056.10 46.92 o -3 -6 2 110.04 97.36 12.51 o -2 -6 2 3052.53 3212.22 54.54 o -1 -6 2 1050.32 991.01 31.67 o 0 -6 2 46.35 59.30 10.57 o 1 -6 2 1912.27 2402.07 52.68 o 2 -6 2 81.22 15.68 13.35 o -6 -5 2 558.45 532.72 26.97 o -5 -5 2 1720.18 1581.67 40.70 o -4 -5 2 67.84 72.15 10.38 o -3 -5 2 2092.02 2152.34 42.25 o -2 -5 2 1471.06 1591.02 35.49 o -1 -5 2 1887.82 2235.69 41.53 o 0 -5 2 5100.60 6448.75 52.53 o 1 -5 2 19.39 7.88 15.76 o 2 -5 2 1847.26 2241.83 47.64 o 3 -5 2 1436.26 1847.09 46.69 o 4 -5 2 98.28 19.74 13.33 o -7 -4 2 722.93 602.27 30.32 o -6 -4 2 1474.69 1370.34 40.50 o -5 -4 2 0.91 3.79 7.58 o -4 -4 2 2851.68 2884.20 48.09 o -3 -4 2 2566.35 2606.29 42.40 o -2 -4 2 505.31 507.60 18.75 o -1 -4 2 2382.10 2602.49 39.93 o 0 -4 2 367.27 356.46 11.73 o 1 -4 2 1168.27 1180.38 29.26 o 2 -4 2 636.14 701.04 25.33 o 3 -4 2 280.91 78.45 12.85 o 4 -4 2 1716.79 1920.50 47.36 o 5 -4 2 28.79 39.14 13.15 o -7 -3 2 1534.38 1524.79 45.92 o -6 -3 2 274.19 236.98 17.78 o -5 -3 2 2234.53 1990.57 42.85 o -4 -3 2 1801.34 1734.16 35.70 o -3 -3 2 319.77 304.38 14.42 o -2 -3 2 2043.99 2014.84 32.05 o -1 -3 2 574.81 589.13 17.52 o 0 -3 2 6485.29 6084.54 266.33 o 1 -3 2 2974.66 3299.70 41.13 o 2 -3 2 978.76 1134.78 27.14 o 3 -3 2 6047.81 6901.36 72.01 o 4 -3 2 482.53 505.53 23.35 o 5 -3 2 847.95 1070.62 36.05 o -7 -2 2 7.39 10.25 13.49 o -6 -2 2 1336.65 1201.66 37.46 o -5 -2 2 888.90 884.02 28.95 o -4 -2 2 2951.15 2764.18 44.57 o -3 -2 2 5446.60 5206.84 53.45 o -2 -2 2 84.30 107.50 7.96 o -1 -2 2 10150.72 11100.92 64.77 o 0 -2 2 10567.09 10235.69 227.14 o 1 -2 2 550.29 1.47 2.95 o 2 -2 2 4387.82 4811.80 47.41 o 3 -2 2 298.61 338.01 15.58 o 4 -2 2 549.36 677.68 23.96 o 5 -2 2 1201.21 1440.48 38.12 o 6 -2 2 211.37 276.76 20.36 o -6 -1 2 706.83 690.37 29.20 o -5 -1 2 68.22 73.16 10.86 o -4 -1 2 2445.74 2277.68 40.64 o -3 -1 2 580.51 574.12 18.44 o -2 -1 2 5930.12 6080.98 49.88 o -1 -1 2 133.72 116.36 7.54 o 0 -1 2 188.47 213.34 9.51 o 1 -1 2 8087.99 7820.51 45.08 o 2 -1 2 1961.81 1957.07 26.61 o 3 -1 2 6493.95 7095.42 58.86 o 4 -1 2 3112.19 3213.41 46.11 o 5 -1 2 0.39 1.88 3.76 o 6 -1 2 2406.04 2561.36 52.95 o 7 -1 2 575.21 654.53 31.21 o -6 0 2 318.13 297.33 21.17 o -5 0 2 2967.52 2923.19 55.02 o -4 0 2 45.78 43.89 8.73 o -3 0 2 4725.98 4607.02 52.48 o -2 0 2 6861.27 6860.50 55.03 o -1 0 2 19.62 41.93 5.91 o 0 0 2 10416.37 10212.65 614.66 o 1 0 2 2720.25 2655.85 23.22 o 2 0 2 3121.46 3060.62 29.57 o 3 0 2 2796.78 2849.55 34.35 o 4 0 2 485.17 494.35 17.53 o 5 0 2 3573.80 3707.96 53.13 o 6 0 2 52.85 45.08 10.47 o 7 0 2 811.10 906.24 34.14 o -6 1 2 1771.62 1700.92 49.45 o -5 1 2 128.58 109.91 13.69 o -4 1 2 740.51 732.84 26.67 o -3 1 2 4723.08 4909.90 58.19 o -2 1 2 264.88 274.51 12.97 o -1 1 2 2375.99 2112.49 30.19 o 0 1 2 2.21 13.97 5.43 o 1 1 2 3329.76 3138.63 26.74 o 2 1 2 3236.96 3027.85 28.58 o 3 1 2 732.07 704.69 16.78 o 4 1 2 6107.69 6137.68 56.69 o 5 1 2 1038.35 1033.90 27.38 o 6 1 2 526.36 535.50 22.93 o 7 1 2 2197.02 2141.82 49.83 o -5 2 2 632.62 695.04 31.01 o -4 2 2 830.98 801.84 29.95 o -3 2 2 768.03 712.97 25.49 o -2 2 2 4762.50 4796.58 56.73 o -1 2 2 1450.22 1637.74 31.29 o 0 2 2 13558.71 14657.36 317.68 o 1 2 2 9527.46 9346.95 55.74 o 2 2 2 1150.50 1195.05 19.80 o 3 2 2 8752.41 9323.89 60.65 o 4 2 2 4803.65 4707.87 49.65 o 5 2 2 1259.47 1212.20 29.18 o 6 2 2 2027.61 1831.12 40.20 o 7 2 2 5.43 1.83 3.65 o 8 2 2 1174.98 1110.92 39.71 o -5 3 2 1244.25 1204.57 42.81 o -4 3 2 237.51 199.56 18.18 o -3 3 2 2215.71 2638.66 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