#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/43/2014348.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014348_Fobs loop_ _publ_author_name 'Agostinho, Magno' 'Banu, Andrei' 'Braunstein, Pierre' 'Welter, Richard' 'Morise, Xavier' _publ_section_title ; New palladium complexes with phosphino- and phosphinitopyridine ligands ; _journal_coeditor_code GG1299 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m81 _journal_page_last m86 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.924 _cell_angle_gamma 90.000 _cell_length_a 11.5070 _cell_length_b 12.0110 _cell_length_c 17.4900 _exptl_crystal_F_000 1096.00 _reflns_d_resolution_high 0.7100 _[local]_cod_data_source_file gg1299Vsup4.hkl _[local]_cod_data_source_block V #BEGIN Tags that were not found in dictionaries: _shelx_title ' Andrei P 21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 279.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7263.60 7423.93 461.25 o 4 0 0 15771.63 15595.60 843.20 o 6 0 0 836.35 963.48 59.83 o 8 0 0 2617.44 2712.60 175.07 o 10 0 0 1193.29 1337.40 105.45 o 12 0 0 4044.71 3947.84 435.09 o 1 1 0 5.47 10.09 6.38 o 2 1 0 24789.95 24035.22 1288.18 o 3 1 0 17449.53 18179.06 932.18 o 4 1 0 482.55 585.96 324.08 o 5 1 0 1961.40 2173.39 109.78 o 6 1 0 21469.91 22070.47 1138.03 o 7 1 0 62.84 124.71 56.95 o 8 1 0 2415.79 2524.76 147.36 o 9 1 0 103.11 82.18 35.73 o 10 1 0 5418.54 5341.26 275.78 o 11 1 0 2.40 9.37 40.68 o 12 1 0 1411.37 1350.48 102.26 o 13 1 0 278.04 263.73 77.54 o 14 1 0 121.48 87.84 78.99 o 15 1 0 50.67 83.52 82.38 o 0 2 0 14261.62 14547.06 823.94 o 1 2 0 9584.97 9531.11 499.66 o 2 2 0 12236.25 12981.97 640.64 o 3 2 0 1652.48 1651.80 79.09 o 4 2 0 8016.70 7705.69 354.35 o 5 2 0 184.16 189.07 34.29 o 6 2 0 1704.45 1654.68 108.44 o 7 2 0 106.53 95.46 21.93 o 8 2 0 793.21 826.21 55.51 o 9 2 0 110.03 112.66 43.05 o 10 2 0 2724.63 2666.36 175.89 o 11 2 0 3.16 38.41 44.80 o 12 2 0 3002.38 3046.87 203.59 o 13 2 0 36.44 26.47 105.66 o 14 2 0 875.61 875.23 168.06 o 15 2 0 22.53 94.54 125.43 o 1 3 0 1940.89 1918.11 94.84 o 2 3 0 15241.29 15007.07 728.89 o 3 3 0 3961.62 4075.02 199.78 o 4 3 0 1505.31 1604.74 79.81 o 5 3 0 78.84 110.39 27.08 o 6 3 0 30391.89 30550.98 1464.17 o 7 3 0 1179.96 1167.79 199.58 o 8 3 0 638.16 686.98 57.36 o 9 3 0 357.26 324.49 50.05 o 10 3 0 3169.65 3070.66 192.88 o 11 3 0 1.66 -32.95 46.96 o 12 3 0 445.06 486.68 80.53 o 13 3 0 209.10 244.89 62.61 o 14 3 0 29.23 86.50 89.70 o 15 3 0 2.07 140.26 87.43 o 0 4 0 40009.42 38412.27 2003.27 o 1 4 0 25.15 28.94 15.34 o 2 4 0 1310.54 1451.09 94.64 o 3 4 0 3456.16 3674.84 164.36 o 4 4 0 5071.97 4384.79 214.30 o 5 4 0 2326.88 2442.38 137.07 o 6 4 0 718.54 715.81 77.85 o 7 4 0 1870.51 1940.25 144.89 o 8 4 0 2114.30 2139.00 160.24 o 9 4 0 363.13 293.80 53.76 o 10 4 0 624.08 649.08 124.81 o 11 4 0 36.62 43.97 61.48 o 12 4 0 2122.66 2077.83 148.81 o 13 4 0 179.59 154.98 69.72 o 14 4 0 139.00 155.60 72.70 o 15 4 0 0.69 94.23 87.53 o 1 5 0 340.56 365.68 31.31 o 2 5 0 1240.72 1051.12 54.79 o 3 5 0 906.09 970.90 57.36 o 4 5 0 163.46 122.44 67.86 o 5 5 0 283.64 309.04 35.01 o 6 5 0 8355.18 8064.06 481.84 o 7 5 0 497.17 589.15 57.05 o 8 5 0 1840.86 1733.46 138.61 o 9 5 0 71.54 83.93 29.35 o 10 5 0 2640.05 2541.96 183.10 o 11 5 0 127.08 208.43 85.99 o 12 5 0 963.40 801.80 52.93 o 13 5 0 97.58 180.32 68.38 o 14 5 0 111.15 442.81 459.91 o 15 5 0 23.49 -37.28 120.59 o 0 6 0 30868.20 30004.15 1499.39 o 1 6 0 370.48 344.16 30.59 o 2 6 0 4.18 11.22 26.36 o 3 6 0 1.10 11.53 36.76 o 4 6 0 6683.63 6672.59 349.41 o 5 6 0 1402.04 1377.05 106.89 o 6 6 0 974.82 923.22 73.42 o 7 6 0 577.18 590.08 49.95 o 8 6 0 1255.27 1266.45 102.16 o 9 6 0 5.64 19.67 45.21 o 10 6 0 221.87 197.62 44.69 o 11 6 0 12.08 84.03 54.89 o 12 6 0 2056.59 2072.27 189.38 o 13 6 0 170.90 214.20 148.60 o 14 6 0 212.93 212.04 72.91 o 1 7 0 384.49 384.12 44.08 o 2 7 0 5407.24 5293.58 283.20 o 3 7 0 742.56 725.80 57.57 o 4 7 0 456.24 456.10 66.73 o 5 7 0 237.51 269.91 66.83 o 6 7 0 10045.81 10331.06 669.06 o 7 7 0 927.24 905.81 83.31 o 8 7 0 674.43 698.00 67.97 o 9 7 0 61.12 39.54 37.18 o 10 7 0 1122.82 1069.65 88.87 o 11 7 0 17.54 59.93 43.87 o 12 7 0 352.28 541.88 107.20 o 13 7 0 395.78 383.81 68.58 o 14 7 0 157.40 37.48 101.23 o 0 8 0 2337.53 1975.77 152.51 o 1 8 0 334.73 421.19 54.48 o 2 8 0 889.90 1155.74 398.84 o 3 8 0 53.15 79.29 37.69 o 4 8 0 3969.32 3862.57 245.30 o 5 8 0 297.61 285.05 127.28 o 6 8 0 1735.63 1653.76 148.70 o 7 8 0 1274.05 1345.23 167.86 o 8 8 0 2845.51 2860.27 222.54 o 9 8 0 317.72 302.86 62.61 o 10 8 0 260.25 315.43 70.34 o 11 8 0 56.17 108.64 52.83 o 12 8 0 1085.11 987.27 120.49 o 13 8 0 11.30 137.89 71.16 o 14 8 0 241.36 79.91 82.08 o 1 9 0 2128.93 1971.35 118.43 o 2 9 0 4900.31 4752.94 290.61 o 3 9 0 230.16 173.62 43.66 o 4 9 0 24.00 54.06 92.06 o 5 9 0 125.28 161.99 71.26 o 6 9 0 4151.31 4112.61 293.08 o 7 9 0 382.54 460.84 98.65 o 8 9 0 616.87 726.83 86.71 o 9 9 0 6.78 86.09 77.96 o 10 9 0 1840.54 1697.42 151.90 o 11 9 0 87.62 82.59 60.24 o 12 9 0 395.70 423.45 97.93 o 13 9 0 164.03 205.75 72.60 o 0 10 0 7497.90 7610.22 432.52 o 1 10 0 670.99 617.88 74.15 o 2 10 0 402.37 471.34 62.41 o 3 10 0 251.16 273.82 59.52 o 4 10 0 4277.92 4230.83 247.36 o 5 10 0 519.66 544.04 93.81 o 6 10 0 0.94 49.22 62.41 o 7 10 0 1251.73 1175.83 129.03 o 8 10 0 1276.50 1232.57 121.83 o 9 10 0 211.91 160.13 61.17 o 10 10 0 72.79 226.35 119.46 o 11 10 0 90.61 219.76 70.03 o 12 10 0 492.71 580.60 119.46 o 1 11 0 956.37 937.74 118.43 o 2 11 0 3066.09 2855.94 184.03 o 3 11 0 90.33 332.42 99.68 o 4 11 0 1.65 11.84 58.08 o 5 11 0 45.13 40.06 40.99 o 6 11 0 2235.15 2222.72 197.00 o 7 11 0 91.17 95.36 75.90 o 8 11 0 316.46 852.16 1078.72 o 9 11 0 5.97 7.72 123.58 o 10 11 0 602.20 632.81 93.09 o 11 11 0 107.25 141.80 109.26 o 12 11 0 450.11 476.28 89.59 o 0 12 0 2443.14 2364.52 193.29 o 1 12 0 92.14 55.20 41.60 o 2 12 0 290.75 368.15 101.44 o 3 12 0 15.58 89.08 111.01 o 4 12 0 1948.61 2049.10 191.54 o 5 12 0 550.28 530.45 78.37 o 6 12 0 147.90 340.86 117.50 o 7 12 0 358.22 451.16 120.49 o 8 12 0 974.52 922.80 184.54 o 9 12 0 44.41 533.85 245.61 o 10 12 0 4.75 230.26 135.32 o 11 12 0 88.27 237.78 147.26 o 1 13 0 615.86 580.70 112.25 o 2 13 0 1662.94 1813.79 171.05 o 3 13 0 76.70 117.19 86.30 o 4 13 0 7.19 35.12 95.26 o 5 13 0 11.27 96.80 139.74 o 6 13 0 1034.21 1039.89 155.50 o 7 13 0 57.93 161.88 82.80 o 8 13 0 74.65 396.58 387.82 o 9 13 0 1.50 116.88 72.09 o 10 13 0 321.38 672.36 241.28 o 0 14 0 1523.93 1504.64 136.86 o 1 14 0 21.49 45.72 69.31 o 2 14 0 210.02 458.98 136.04 o 3 14 0 19.07 64.16 82.59 o 4 14 0 934.82 900.15 152.82 o 5 14 0 74.26 41.60 47.06 o 6 14 0 51.06 137.27 67.35 o 7 14 0 216.18 294.83 100.20 o 8 14 0 912.41 1268.92 374.95 o 1 15 0 232.52 171.46 69.10 o 2 15 0 873.44 1199.41 303.38 o 3 15 0 38.90 1.65 40.06 o 4 15 0 97.46 133.67 89.59 o 5 15 0 389.09 543.43 132.23 o 6 15 0 223.33 251.17 98.04 o 7 15 0 11.05 289.89 134.59 o 0 16 0 271.82 481.74 136.86 o 1 16 0 48.10 287.62 202.77 o 2 16 0 48.30 174.76 83.62 o 3 16 0 4.00 53.03 181.97 o 4 16 0 565.98 836.51 215.33 o 5 16 0 235.33 201.33 83.10 o -15 0 1 716.41 707.06 103.19 o -11 0 1 449.11 388.54 52.73 o -9 0 1 424.79 569.38 74.56 o -7 0 1 328.17 299.98 34.40 o -5 0 1 26034.11 25550.37 1272.01 o -3 0 1 592.96 581.22 42.12 o 1 0 1 52.61 62.20 7.62 o 3 0 1 6224.36 5940.50 279.69 o 5 0 1 4032.41 4452.86 242.72 o 7 0 1 9743.17 9840.77 629.00 o 9 0 1 460.51 472.27 113.18 o 11 0 1 3527.92 3628.81 256.01 o 15 0 1 23.57 182.38 105.45 o -16 1 1 5.44 51.49 96.49 o -14 1 1 16.54 92.89 67.04 o -13 1 1 800.04 823.02 66.01 o -12 1 1 132.19 98.76 39.13 o -11 1 1 5246.86 5123.87 269.19 o -10 1 1 106.07 155.19 64.47 o -9 1 1 851.12 910.65 108.64 o -8 1 1 0.41 4.33 47.89 o -7 1 1 8636.07 9046.48 588.53 o -6 1 1 18.12 28.22 32.13 o -5 1 1 5887.89 6222.67 308.84 o -4 1 1 93.67 102.57 191.65 o -3 1 1 4935.62 4833.57 240.05 o -2 1 1 1182.19 1232.88 109.88 o -1 1 1 5565.25 3456.63 253.54 o 2 1 1 8398.98 8767.72 456.20 o 3 1 1 50.10 68.17 21.01 o 4 1 1 789.41 834.76 52.42 o 5 1 1 22624.88 22694.22 1127.22 o 6 1 1 1578.12 1743.86 126.67 o 7 1 1 184.60 203.59 43.05 o 8 1 1 73.36 103.08 38.72 o 9 1 1 353.74 398.43 43.25 o 10 1 1 132.41 136.55 37.69 o 11 1 1 1516.51 1615.14 124.40 o 12 1 1 56.92 69.82 36.35 o 13 1 1 781.39 890.57 161.06 o 14 1 1 33.75 183.51 117.40 o 15 1 1 604.25 556.30 102.88 o -15 2 1 530.20 574.42 123.27 o -14 2 1 62.52 30.79 97.93 o -13 2 1 316.60 316.56 72.29 o -12 2 1 20.69 29.66 46.65 o -11 2 1 528.41 535.60 59.01 o -10 2 1 65.88 69.82 41.19 o -9 2 1 1861.12 1899.26 118.02 o -8 2 1 516.22 476.90 45.83 o -7 2 1 1245.06 1211.56 78.88 o -6 2 1 2528.17 2968.09 150.87 o -5 2 1 41971.57 41985.26 2044.57 o -4 2 1 2927.49 3078.48 137.27 o -3 2 1 12202.34 12892.79 627.05 o -2 2 1 3652.93 3955.87 202.15 o -1 2 1 42086.91 40627.26 2186.68 o 0 2 1 3501.27 3426.87 194.84 o 1 2 1 2716.16 2757.50 142.11 o 2 2 1 909.02 964.82 49.95 o 3 2 1 2417.36 2361.95 128.21 o 4 2 1 3176.87 3403.80 157.97 o 5 2 1 22.56 38.00 24.82 o 6 2 1 21.24 27.39 33.78 o 7 2 1 13214.26 13454.85 813.85 o 8 2 1 270.55 270.32 40.37 o 9 2 1 352.95 358.58 46.75 o 10 2 1 280.10 275.68 72.29 o 11 2 1 4984.47 4875.69 286.80 o 12 2 1 30.46 125.33 68.17 o 13 2 1 1053.24 1146.37 192.68 o 14 2 1 4.32 22.45 59.83 o 15 2 1 56.46 194.12 128.00 o -15 3 1 220.13 329.02 129.14 o -13 3 1 374.61 369.60 58.49 o -12 3 1 274.53 332.63 96.39 o -11 3 1 4869.95 5041.18 352.40 o -10 3 1 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