#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:00:14 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180813 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/44/2014404.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014404_Fobs loop_ _publ_author_name 'Cobo, Justo' 'S\'anchez Rodrigo, Adolfo' 'Nogueras Montiel, Manuel' 'Low, John N.' 'Glidewell, Christopher' _publ_section_title ; 4,5,6-Triamino-2-(methylsulfanyl)pyrimidine: \p-stacked hydrogen-bonded sheets of R~2~^2^(8), R~2~^2^(10) and R~6~^6^(32) rings ; _journal_coeditor_code SK1899 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o142 _journal_page_last o144 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.261 _cell_angle_gamma 90.000 _cell_length_a 7.7824 _cell_length_b 8.9623 _cell_length_c 10.5078 _exptl_crystal_F_000 360.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file sk1899Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 840' _shelx_refln_list_code 4 _shelx_f_calc_maximum 80.18 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 268.35 255.41 5.02 o 4 0 0 168.00 172.51 3.63 o 6 0 0 821.62 821.68 16.45 o 8 0 0 14.25 10.64 1.76 o 2 1 0 256.03 259.59 2.38 o 3 1 0 241.31 273.65 2.46 o 4 1 0 689.75 644.06 5.11 o 5 1 0 1876.51 1811.72 17.20 o 6 1 0 400.14 404.25 7.09 o 7 1 0 9.05 7.76 1.00 o 8 1 0 372.23 369.14 10.65 o 9 1 0 5.86 4.79 2.20 o 10 1 0 25.69 29.30 3.62 o 0 2 0 29.11 24.23 0.78 o 1 2 0 380.50 394.09 3.60 o 2 2 0 1500.80 1485.86 12.34 o 3 2 0 211.15 215.06 1.84 o 4 2 0 613.05 611.64 4.45 o 5 2 0 10.47 12.03 0.58 o 6 2 0 63.97 67.10 1.07 o 7 2 0 6.82 8.10 0.55 o 8 2 0 534.95 562.36 13.45 o 9 2 0 99.97 108.83 4.19 o 1 3 0 1515.27 1372.24 11.17 o 2 3 0 295.74 376.05 2.80 o 3 3 0 2059.69 2157.26 16.34 o 4 3 0 1261.99 1229.91 10.02 o 5 3 0 80.69 77.83 0.94 o 6 3 0 851.29 872.52 11.57 o 7 3 0 42.85 48.15 1.11 o 8 3 0 435.08 437.56 8.96 o 9 3 0 48.15 45.75 2.83 o 0 4 0 758.71 733.92 8.65 o 1 4 0 1440.64 1371.62 12.17 o 2 4 0 5.22 5.81 0.29 o 3 4 0 74.72 62.07 0.77 o 4 4 0 4.68 5.79 0.35 o 5 4 0 122.03 128.80 1.49 o 6 4 0 28.79 28.28 0.71 o 7 4 0 6.06 9.11 0.73 o 8 4 0 20.77 19.18 1.06 o 9 4 0 66.12 66.34 2.84 o 1 5 0 427.45 427.62 3.81 o 2 5 0 0.05 1.43 0.28 o 3 5 0 412.53 432.78 3.15 o 4 5 0 224.95 210.99 2.12 o 5 5 0 65.69 45.90 0.87 o 6 5 0 808.31 809.46 11.88 o 7 5 0 41.34 41.11 2.03 o 8 5 0 110.99 121.97 4.52 o 9 5 0 3.13 2.62 1.26 o 0 6 0 462.37 465.08 6.79 o 1 6 0 4.29 4.96 0.47 o 2 6 0 379.70 357.97 4.14 o 3 6 0 118.08 111.54 1.31 o 4 6 0 297.09 295.63 2.94 o 5 6 0 197.72 188.57 2.62 o 6 6 0 380.00 359.48 5.13 o 7 6 0 28.22 23.97 1.32 o 8 6 0 106.65 99.07 4.46 o 1 7 0 299.82 299.10 3.01 o 2 7 0 425.97 440.41 4.04 o 3 7 0 484.35 486.18 5.53 o 4 7 0 6.14 6.56 0.54 o 5 7 0 268.19 276.02 4.82 o 6 7 0 0.86 -0.03 0.52 o 7 7 0 83.17 84.72 2.81 o 8 7 0 15.94 13.45 2.59 o 0 8 0 1194.79 1233.94 22.93 o 1 8 0 129.05 131.48 1.94 o 2 8 0 1028.30 1103.65 12.74 o 3 8 0 32.90 33.12 0.96 o 4 8 0 32.42 31.58 1.04 o 5 8 0 24.73 20.61 1.03 o 6 8 0 21.54 22.99 1.53 o 7 8 0 5.94 5.19 0.92 o 1 9 0 10.46 11.49 0.78 o 2 9 0 566.02 574.14 10.40 o 3 9 0 36.05 36.92 1.60 o 4 9 0 103.18 98.74 3.50 o 5 9 0 184.73 181.95 5.57 o 6 9 0 31.05 29.91 2.51 o 0 10 0 1399.27 1439.23 60.96 o 1 10 0 0.21 3.06 1.17 o 2 10 0 9.29 7.33 0.88 o 3 10 0 99.75 96.27 3.52 o 4 10 0 25.71 24.51 1.69 o 5 10 0 47.91 43.14 3.17 o 1 11 0 197.02 192.01 6.86 o 2 11 0 18.86 18.21 2.05 o 3 11 0 59.29 42.53 2.74 o -9 0 1 384.47 366.02 18.81 o -7 0 1 4623.70 4698.80 113.47 o -5 0 1 5.27 3.57 0.28 o -3 0 1 3946.22 3661.78 37.69 o 5 0 1 311.71 300.95 5.19 o 7 0 1 33.08 32.20 1.93 o 9 0 1 73.77 69.34 6.22 o -10 1 1 70.43 61.03 4.92 o -9 1 1 20.62 17.70 2.41 o -8 1 1 273.91 278.89 7.98 o -7 1 1 63.80 65.11 1.29 o -6 1 1 400.69 411.73 5.13 o -5 1 1 336.16 350.00 3.39 o -4 1 1 183.97 189.81 1.44 o -3 1 1 156.42 166.85 1.52 o -2 1 1 1240.26 1090.57 8.68 o -1 1 1 1825.40 1665.01 19.64 o 1 1 1 1722.54 1623.69 54.73 o 3 1 1 1291.48 1331.96 12.48 o 4 1 1 1253.51 1248.52 11.63 o 5 1 1 7.61 9.99 0.38 o 6 1 1 453.66 454.67 4.98 o 7 1 1 6.06 4.86 0.85 o 8 1 1 1.58 -0.96 0.96 o 9 1 1 53.14 53.14 3.50 o -9 2 1 370.12 378.56 16.34 o -8 2 1 50.97 53.03 1.27 o -7 2 1 74.18 73.24 1.85 o -6 2 1 70.16 68.00 1.32 o -5 2 1 314.93 329.56 3.10 o -4 2 1 209.90 211.86 1.89 o -3 2 1 85.67 71.21 0.73 o -2 2 1 1043.50 985.28 7.75 o -1 2 1 375.14 366.43 3.40 o 0 2 1 281.44 269.06 2.28 o 2 2 1 281.22 297.21 2.32 o 3 2 1 118.64 126.65 1.23 o 4 2 1 221.61 160.13 2.20 o 5 2 1 115.87 103.57 1.51 o 6 2 1 1.42 1.52 0.41 o 7 2 1 452.57 456.41 6.07 o 8 2 1 954.54 1006.28 25.86 o 9 2 1 4.88 8.75 1.62 o -9 3 1 78.28 73.44 3.34 o -8 3 1 0.03 0.78 0.47 o -7 3 1 133.08 130.71 2.28 o -6 3 1 296.13 298.19 4.51 o -5 3 1 897.20 902.84 8.55 o -4 3 1 2070.04 2147.38 15.05 o -3 3 1 1232.24 1196.95 7.71 o -2 3 1 1562.05 1584.82 11.72 o -1 3 1 2164.69 2005.42 15.65 o 0 3 1 123.75 139.91 1.72 o 1 3 1 35.73 41.10 1.06 o 2 3 1 0.02 0.16 0.21 o 3 3 1 65.81 41.64 0.82 o 4 3 1 55.05 68.45 0.96 o 5 3 1 766.92 754.73 8.12 o 6 3 1 0.79 1.53 0.59 o 7 3 1 970.29 975.38 13.65 o 8 3 1 0.12 0.33 0.52 o 9 3 1 410.40 423.61 12.48 o -9 4 1 17.90 16.28 1.55 o -8 4 1 119.15 118.40 2.92 o -7 4 1 75.06 77.80 1.90 o -6 4 1 83.46 74.99 1.55 o -5 4 1 0.19 0.75 0.28 o -4 4 1 846.13 822.12 5.73 o -3 4 1 2.77 -0.25 0.25 o -2 4 1 60.79 48.24 0.66 o -1 4 1 65.87 74.91 0.96 o 0 4 1 1055.39 995.72 7.91 o 1 4 1 60.27 55.65 0.58 o 2 4 1 110.51 99.33 0.98 o 3 4 1 145.27 151.13 2.20 o 4 4 1 189.10 190.55 1.88 o 5 4 1 41.79 50.28 0.78 o 6 4 1 46.28 55.03 1.09 o 7 4 1 61.34 53.44 1.42 o 8 4 1 17.81 17.38 1.07 o 9 4 1 41.81 38.76 1.92 o -9 5 1 210.35 222.02 6.11 o -8 5 1 8.47 10.86 1.80 o -7 5 1 86.59 82.85 1.68 o -6 5 1 393.76 378.49 5.67 o -5 5 1 155.71 163.06 1.63 o -4 5 1 473.91 477.11 4.50 o -3 5 1 91.02 81.83 1.29 o -2 5 1 4.38 6.40 0.41 o -1 5 1 953.99 1022.78 7.46 o 0 5 1 35.41 38.40 0.68 o 1 5 1 52.06 56.92 0.70 o 2 5 1 171.38 181.25 3.16 o 3 5 1 4.91 3.99 0.40 o 4 5 1 61.20 52.85 0.88 o 5 5 1 2005.81 2028.50 20.19 o 6 5 1 19.88 22.90 0.59 o 7 5 1 594.71 561.03 11.76 o 8 5 1 1.52 0.50 1.07 o -8 6 1 18.16 14.46 1.86 o -7 6 1 19.42 16.17 0.90 o -6 6 1 16.33 12.15 0.60 o -5 6 1 17.83 18.49 0.88 o -4 6 1 19.86 16.71 0.51 o -3 6 1 56.54 54.40 0.85 o -2 6 1 50.24 57.25 0.99 o -1 6 1 1703.10 1831.49 18.63 o 0 6 1 707.53 696.39 5.28 o 1 6 1 1027.16 997.53 7.81 o 2 6 1 26.85 25.45 0.69 o 3 6 1 189.58 180.59 2.11 o 4 6 1 206.61 221.82 2.72 o 5 6 1 12.11 13.29 0.59 o 6 6 1 66.64 53.23 1.22 o 7 6 1 39.92 36.67 1.49 o 8 6 1 1.72 -1.39 1.62 o -8 7 1 84.98 79.49 3.86 o -7 7 1 0.52 1.35 0.80 o -6 7 1 468.46 469.36 9.15 o -5 7 1 403.01 395.93 5.90 o -4 7 1 1000.32 999.79 13.84 o -3 7 1 0.36 0.39 0.37 o -2 7 1 8.99 9.99 0.66 o -1 7 1 7.58 7.80 0.68 o 0 7 1 1.12 1.34 0.37 o 1 7 1 1.29 1.37 0.31 o 2 7 1 138.90 138.93 1.88 o 3 7 1 185.36 184.61 2.78 o 4 7 1 373.23 379.21 5.40 o 5 7 1 4.84 2.55 0.54 o 6 7 1 198.28 206.88 4.99 o 7 7 1 1.55 0.75 0.87 o -7 8 1 115.57 105.30 3.46 o -6 8 1 21.84 20.79 1.43 o -5 8 1 203.79 185.55 3.45 o -4 8 1 1.53 1.53 0.54 o -3 8 1 497.54 521.12 6.85 o -2 8 1 1.26 2.02 0.63 o -1 8 1 172.44 169.56 2.94 o 0 8 1 86.55 79.16 1.65 o 1 8 1 1894.14 1947.00 22.91 o 2 8 1 64.47 66.74 1.62 o 3 8 1 92.77 96.77 2.33 o 4 8 1 0.02 -0.39 0.58 o 5 8 1 11.61 9.22 0.97 o 6 8 1 4.67 2.16 0.89 o 7 8 1 23.52 21.36 1.75 o -6 9 1 2.08 4.76 1.50 o -5 9 1 573.11 594.09 13.00 o -4 9 1 210.77 219.71 5.45 o -3 9 1 102.53 97.77 2.20 o -2 9 1 4.48 5.00 0.90 o -1 9 1 3.30 3.03 0.90 o 0 9 1 17.04 16.82 1.13 o 1 9 1 82.34 83.55 2.28 o 2 9 1 891.56 918.83 19.45 o 3 9 1 44.87 45.60 1.72 o 4 9 1 95.68 82.37 3.33 o 5 9 1 206.52 214.13 7.51 o 6 9 1 275.03 259.92 10.59 o -5 10 1 2.64 4.83 1.70 o -4 10 1 26.70 21.19 1.66 o -3 10 1 43.05 41.45 2.25 o -2 10 1 33.30 34.07 2.33 o -1 10 1 139.43 140.60 5.26 o 0 10 1 510.62 497.88 13.60 o 1 10 1 0.26 3.20 1.37 o 2 10 1 38.66 36.65 2.03 o 3 10 1 113.55 108.39 4.36 o 4 10 1 115.62 105.97 4.19 o 5 10 1 69.10 63.20 6.21 o -3 11 1 121.56 116.46 6.97 o -2 11 1 39.81 42.02 3.54 o -1 11 1 577.72 574.73 21.35 o 0 11 1 34.86 32.76 2.33 o 1 11 1 102.71 99.87 4.66 o 2 11 1 0.04 -0.93 1.54 o 3 11 1 80.25 75.82 5.09 o -8 0 2 632.71 623.89 29.71 o -6 0 2 117.62 117.97 2.09 o -4 0 2 105.73 109.73 1.39 o -2 0 2 68.41 79.74 1.33 o 2 0 2 367.05 377.31 4.63 o 4 0 2 815.59 792.87 11.10 o 6 0 2 17.81 20.89 1.44 o 8 0 2 141.09 139.06 4.53 o -10 1 2 0.44 0.83 2.31 o -9 1 2 27.34 26.39 3.13 o -8 1 2 1.03 0.88 0.47 o -7 1 2 870.58 874.32 17.95 o -6 1 2 173.50 172.88 1.82 o -5 1 2 2528.88 2527.10 22.00 o -4 1 2 1224.12 1209.99 8.44 o -3 1 2 2220.33 2195.78 18.64 o -2 1 2 526.87 527.65 3.96 o -1 1 2 46.95 61.43 0.70 o 0 1 2 74.64 55.92 0.68 o 1 1 2 2798.38 2784.92 27.41 o 2 1 2 26.44 16.11 0.58 o 3 1 2 1328.21 1406.60 10.94 o 4 1 2 997.27 1028.16 9.06 o 5 1 2 855.91 833.29 8.54 o 6 1 2 752.02 749.75 9.07 o 7 1 2 211.65 220.12 4.02 o 8 1 2 26.14 24.43 1.52 o 9 1 2 230.22 238.07 6.54 o -9 2 2 336.50 352.97 11.44 o -8 2 2 43.11 44.74 1.62 o -7 2 2 0.05 0.82 0.76 o -6 2 2 779.59 764.46 7.82 o -5 2 2 18.54 18.04 0.41 o -4 2 2 143.84 158.66 1.49 o -3 2 2 745.23 853.82 6.63 o -2 2 2 203.67 189.06 1.52 o -1 2 2 60.51 67.87 0.70 o 0 2 2 6429.49 6041.74 52.89 o 2 2 2 55.49 44.33 0.66 o 3 2 2 170.80 143.65 1.39 o 4 2 2 19.47 13.93 0.36 o 5 2 2 5.13 5.31 0.39 o 6 2 2 2.97 1.82 0.40 o 7 2 2 151.83 159.48 2.60 o 8 2 2 167.73 163.90 4.15 o 9 2 2 6.06 5.62 1.93 o -9 3 2 213.23 220.66 8.94 o -8 3 2 67.68 68.76 1.95 o -7 3 2 0.03 0.47 0.40 o -6 3 2 88.64 87.62 1.21 o -5 3 2 39.82 45.57 0.68 o -4 3 2 817.48 750.83 5.50 o -3 3 2 211.41 202.94 1.77 o -2 3 2 76.18 72.44 0.86 o -1 3 2 18.07 25.31 0.69 o 0 3 2 2295.34 2442.01 17.31 o 1 3 2 150.85 136.41 1.17 o 2 3 2 11.92 15.92 0.48 o 3 3 2 17.90 19.33 0.40 o 4 3 2 249.91 243.48 2.16 o 5 3 2 90.12 93.29 1.40 o 6 3 2 1194.64 1185.05 16.26 o 7 3 2 41.23 39.46 0.95 o 8 3 2 210.60 205.63 4.93 o 9 3 2 51.34 42.98 2.54 o -9 4 2 182.66 170.07 6.31 o -8 4 2 8.51 8.59 0.98 o -7 4 2 8.33 8.85 0.58 o -6 4 2 3.11 3.26 0.38 o -5 4 2 10.00 12.95 0.45 o -4 4 2 50.94 55.43 0.71 o -3 4 2 759.21 748.40 4.96 o -2 4 2 18.62 19.47 0.57 o -1 4 2 714.18 660.54 4.79 o 0 4 2 362.24 410.98 3.90 o 1 4 2 149.29 133.87 1.49 o 2 4 2 194.49 220.09 1.42 o 3 4 2 818.97 804.73 5.60 o 4 4 2 5.91 4.91 0.37 o 5 4 2 383.39 386.25 4.69 o 6 4 2 154.13 148.40 2.03 o 7 4 2 507.83 490.07 9.63 o 8 4 2 80.89 78.05 2.17 o 9 4 2 683.72 708.68 21.22 o -9 5 2 58.70 71.49 3.39 o -8 5 2 30.23 37.33 1.76 o -7 5 2 121.88 109.83 2.37 o -6 5 2 115.48 119.56 1.70 o -5 5 2 269.84 287.28 3.12 o -4 5 2 259.11 263.40 2.42 o -3 5 2 52.01 39.67 0.67 o -2 5 2 2066.51 2135.04 16.05 o -1 5 2 7.44 10.71 0.48 o 0 5 2 1233.95 1230.41 9.64 o 1 5 2 165.22 167.38 1.52 o 2 5 2 250.14 242.47 2.27 o 3 5 2 14.63 14.03 0.67 o 4 5 2 451.04 453.40 4.33 o 5 5 2 464.32 470.25 5.71 o 6 5 2 117.58 129.56 2.32 o 7 5 2 98.16 101.98 3.02 o 8 5 2 214.30 204.28 6.87 o -8 6 2 440.93 443.46 27.09 o -7 6 2 48.85 47.18 1.52 o -6 6 2 78.06 82.92 1.74 o -5 6 2 1.19 0.75 0.36 o -4 6 2 48.78 46.72 0.80 o -3 6 2 71.90 60.24 1.00 o -2 6 2 325.74 324.21 2.99 o -1 6 2 506.18 524.85 4.82 o 0 6 2 509.53 482.11 4.76 o 1 6 2 222.81 232.30 2.20 o 2 6 2 1224.16 1246.02 13.67 o 3 6 2 197.95 187.77 2.04 o 4 6 2 53.04 58.12 1.14 o 5 6 2 11.35 12.69 0.57 o 6 6 2 99.20 89.53 1.94 o 7 6 2 58.11 63.42 2.24 o 8 6 2 11.97 14.29 2.16 o -8 7 2 16.66 18.34 3.10 o -7 7 2 235.57 250.67 7.41 o -6 7 2 8.33 8.63 0.70 o -5 7 2 574.38 569.35 8.20 o -4 7 2 28.42 23.56 0.74 o -3 7 2 350.08 353.70 4.24 o -2 7 2 85.68 89.60 1.76 o -1 7 2 31.61 26.62 0.87 o 0 7 2 0.01 -0.55 0.57 o 1 7 2 242.35 241.36 2.92 o 2 7 2 402.36 414.64 4.92 o 3 7 2 1003.60 1040.62 13.23 o 4 7 2 0.17 0.08 0.59 o 5 7 2 191.22 184.44 3.52 o 6 7 2 227.14 223.45 5.55 o 7 7 2 154.52 145.31 5.43 o -7 8 2 30.72 28.05 2.29 o -6 8 2 382.03 377.74 9.81 o -5 8 2 4.71 2.84 0.80 o -4 8 2 92.17 89.51 2.03 o -3 8 2 36.26 34.15 1.10 o -2 8 2 181.44 171.41 2.76 o -1 8 2 89.92 84.62 1.64 o 0 8 2 408.76 424.99 6.19 o 1 8 2 163.84 165.77 2.73 o 2 8 2 0.10 -0.08 0.60 o 3 8 2 4.37 4.44 0.75 o 4 8 2 204.37 214.83 4.32 o 5 8 2 3.97 4.08 1.00 o 6 8 2 48.12 51.53 2.79 o 7 8 2 63.63 56.64 2.98 o -6 9 2 158.04 143.99 6.83 o -5 9 2 954.72 979.12 28.84 o -4 9 2 11.39 10.22 1.17 o -3 9 2 118.98 115.90 2.83 o -2 9 2 147.41 150.54 4.14 o -1 9 2 156.51 151.26 3.58 o 0 9 2 59.57 58.01 1.90 o 1 9 2 233.90 229.60 5.53 o 2 9 2 123.80 126.96 3.21 o 3 9 2 192.13 181.70 4.14 o 4 9 2 367.54 348.12 13.77 o 5 9 2 202.39 226.30 9.77 o 6 9 2 133.09 108.34 9.82 o -5 10 2 7.32 3.41 2.02 o -4 10 2 1.99 2.73 1.74 o -3 10 2 38.98 37.78 2.16 o -2 10 2 0.06 -0.69 1.01 o -1 10 2 582.80 574.64 17.77 o 0 10 2 8.17 8.46 1.38 o 1 10 2 591.57 621.00 17.01 o 2 10 2 36.64 34.58 1.76 o 3 10 2 266.18 271.53 8.35 o 4 10 2 0.01 -0.29 1.18 o -3 11 2 18.46 16.81 2.63 o -2 11 2 92.96 93.81 4.51 o -1 11 2 143.34 137.93 5.88 o 0 11 2 8.48 7.73 1.66 o 1 11 2 0.02 0.52 1.43 o 2 11 2 11.79 11.92 1.67 o -7 0 3 275.97 280.72 5.92 o -5 0 3 34.02 25.72 0.66 o -3 0 3 444.73 420.71 4.39 o -1 0 3 838.38 792.93 16.08 o 1 0 3 5315.05 5126.35 158.24 o 3 0 3 30.08 41.06 0.88 o 5 0 3 15.02 4.50 0.29 o 7 0 3 0.30 0.55 1.47 o 9 0 3 64.52 79.99 4.35 o -9 1 3 77.10 71.53 4.30 o -8 1 3 384.77 401.03 9.96 o -7 1 3 89.55 90.39 1.48 o -6 1 3 875.52 892.62 10.28 o -5 1 3 42.14 34.53 0.53 o -4 1 3 2857.19 3058.57 22.70 o -3 1 3 984.18 994.85 7.90 o -2 1 3 173.54 188.82 2.09 o -1 1 3 3204.59 2913.26 33.54 o 0 1 3 518.92 475.52 4.30 o 1 1 3 35.84 53.02 0.64 o 2 1 3 20.72 19.06 0.37 o 3 1 3 391.67 380.07 2.83 o 4 1 3 513.59 483.57 4.87 o 5 1 3 692.67 699.42 6.78 o 6 1 3 561.78 552.47 7.42 o 7 1 3 116.42 104.62 2.76 o 8 1 3 210.14 204.12 5.74 o 9 1 3 12.48 12.80 1.88 o -9 2 3 171.64 182.75 6.40 o -8 2 3 158.21 161.11 3.62 o -7 2 3 356.12 348.95 5.45 o -6 2 3 1880.61 1844.83 17.65 o -5 2 3 6.11 9.37 0.35 o -4 2 3 3.76 7.49 0.29 o -3 2 3 1134.07 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