#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/45/2014504.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014504_Fobs loop_ _publ_author_name 'Feazell, Rodney P.' 'Carson, Cody E.' 'Klausmeyer, Kevin K.' _publ_section_title ; Self-assembly of a mixed-ligand silver-based coordination polymer ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m598 _journal_page_last m600 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 97.085 _cell_angle_beta 104.690 _cell_angle_gamma 101.691 _cell_length_a 13.2233 _cell_length_b 14.6535 _cell_length_c 16.7275 _exptl_crystal_F_000 1380.00 _reflns_d_resolution_high 0.7989 _[local]_cod_data_source_file hj1026Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ; ; _shelx_refln_list_code 4 _shelx_f_calc_maximum 350.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc 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14660.69 15431.99 395.39 o 5 1 0 15536.27 15736.04 404.27 o 6 1 0 93.81 103.40 15.60 o 7 1 0 162.75 56.90 18.92 o 8 1 0 10991.02 10719.78 278.28 o 9 1 0 1119.69 1141.26 67.96 o 10 1 0 370.86 343.79 43.06 o 11 1 0 8393.20 7805.37 298.79 o 12 1 0 4596.13 4863.86 186.85 o 13 1 0 140.50 204.45 83.27 o 14 1 0 272.83 166.82 106.98 o -15 2 0 375.83 365.78 110.09 o -14 2 0 261.40 338.34 84.06 o -13 2 0 399.81 391.25 66.49 o -12 2 0 1421.83 1201.37 109.01 o -11 2 0 5.13 14.84 49.63 o -10 2 0 1650.27 1598.77 193.90 o -9 2 0 10727.96 10522.82 614.45 o -8 2 0 2850.80 2962.85 204.10 o -7 2 0 1355.09 1270.78 94.82 o -6 2 0 333.30 451.28 52.14 o -5 2 0 37861.40 38332.65 1635.52 o -3 2 0 180.64 164.92 13.92 o -2 2 0 4556.89 4955.30 118.83 o -1 2 0 36267.15 36067.25 2009.63 o 0 2 0 1236.25 1347.24 68.71 o 1 2 0 10163.45 9575.82 273.21 o 2 2 0 349.63 288.54 16.99 o 3 2 0 411.62 348.76 15.66 o 4 2 0 1104.31 1112.09 38.37 o 5 2 0 7015.22 7308.31 191.61 o 6 2 0 5874.51 5917.98 145.84 o 7 2 0 1110.70 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1803.03 1889.21 83.27 o 11 3 0 1025.31 1086.76 131.02 o 12 3 0 2618.34 2612.04 196.84 o 13 3 0 405.89 275.01 115.35 o 14 3 0 641.91 996.98 148.31 o -15 4 0 6.65 -52.54 104.82 o -14 4 0 2172.15 1898.38 133.25 o -13 4 0 1122.39 986.76 110.18 o -12 4 0 6.14 -27.05 47.02 o -11 4 0 3330.54 3054.96 125.68 o -10 4 0 8215.37 8683.02 293.52 o -9 4 0 5574.40 5775.46 179.74 o -8 4 0 512.54 546.53 41.71 o -7 4 0 246.38 274.86 34.29 o -6 4 0 19754.87 19285.83 564.69 o -5 4 0 5.54 32.59 21.15 o -4 4 0 4078.37 4187.00 112.67 o -3 4 0 1937.29 1938.68 66.12 o -2 4 0 404.09 380.88 28.95 o -1 4 0 5834.49 5729.09 149.05 o 0 4 0 51606.47 52808.93 1205.65 o 1 4 0 4683.46 4546.87 111.33 o 2 4 0 3182.58 2942.37 89.02 o 3 4 0 2539.29 2573.95 95.76 o 4 4 0 32272.90 32671.15 820.02 o 5 4 0 3202.38 3160.74 100.70 o 6 4 0 558.15 575.03 53.22 o 7 4 0 4110.77 4533.42 145.32 o 8 4 0 7143.04 7286.51 279.22 o 9 4 0 885.07 836.40 93.27 o 10 4 0 2812.97 3028.22 118.01 o 11 4 0 821.83 892.67 84.87 o 12 4 0 647.07 609.01 102.82 o 13 4 0 2452.27 2726.88 286.09 o 14 4 0 911.89 946.33 158.85 o -15 5 0 96.48 126.56 109.68 o -14 5 0 11.80 0.02 85.71 o -13 5 0 283.46 248.35 78.76 o -12 5 0 3625.23 3602.54 213.02 o -11 5 0 725.54 823.13 79.70 o -10 5 0 2.36 16.36 34.37 o -9 5 0 3924.91 4005.38 166.62 o -8 5 0 9019.58 8755.91 304.48 o -7 5 0 673.13 615.38 55.93 o -6 5 0 252.63 203.47 29.56 o -5 5 0 8718.78 8589.91 260.67 o -4 5 0 2579.71 2738.57 113.23 o -3 5 0 8796.97 8925.64 305.27 o -2 5 0 11366.29 11620.36 381.06 o -1 5 0 1201.66 1166.52 47.26 o 0 5 0 12116.34 12646.58 293.91 o 1 5 0 25117.96 24529.06 621.90 o 2 5 0 1766.32 1631.56 116.96 o 3 5 0 769.48 922.51 79.49 o 4 5 0 783.24 960.15 62.24 o 5 5 0 3450.79 3308.36 139.29 o 6 5 0 5914.06 5703.67 176.98 o 7 5 0 104.64 105.13 43.08 o 8 5 0 1454.55 1364.82 69.20 o 9 5 0 149.03 85.71 45.75 o 10 5 0 308.87 221.81 60.62 o 11 5 0 2558.85 2569.68 114.43 o 12 5 0 2263.00 2391.57 197.82 o 13 5 0 315.94 293.10 116.49 o -15 6 0 2699.65 2970.42 224.76 o -14 6 0 308.40 406.43 167.15 o -13 6 0 1.52 91.65 82.39 o -12 6 0 325.27 297.94 50.80 o -11 6 0 4170.75 4454.81 152.06 o -10 6 0 899.97 956.35 59.88 o -9 6 0 928.78 958.69 60.44 o -8 6 0 1042.13 1120.32 62.07 o -7 6 0 3578.61 3380.81 117.13 o -6 6 0 5501.41 5610.00 178.52 o -5 6 0 8128.22 7780.30 229.96 o -4 6 0 1564.27 1514.35 113.44 o -3 6 0 1995.42 2236.67 117.60 o -2 6 0 5107.11 5236.54 188.67 o -1 6 0 23004.52 22689.69 641.69 o 0 6 0 4871.70 4409.38 158.16 o 1 6 0 3791.53 4144.75 130.74 o 2 6 0 2675.23 2515.89 103.68 o 3 6 0 1064.61 984.01 48.90 o 4 6 0 2491.43 2733.93 96.50 o 5 6 0 33.52 3.84 32.07 o 6 6 0 11.19 24.73 40.56 o 7 6 0 1528.72 1599.74 75.01 o 8 6 0 3239.19 3185.58 137.96 o 9 6 0 11530.41 11399.12 346.19 o 10 6 0 1.63 -66.70 66.70 o 11 6 0 33.06 85.04 71.85 o 12 6 0 2267.40 2205.46 166.86 o 13 6 0 1494.56 1539.10 209.03 o -15 7 0 51.39 92.53 122.51 o -14 7 0 209.07 268.10 102.52 o -13 7 0 959.52 1222.33 105.49 o -12 7 0 328.85 254.76 72.21 o -11 7 0 1332.90 1320.39 72.76 o 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78.79 o 2 9 0 14114.43 13263.11 449.63 o 3 9 0 2132.37 2020.03 97.90 o 4 9 0 967.29 947.45 83.16 o 5 9 0 6382.02 6292.54 236.68 o 6 9 0 457.06 441.92 71.18 o 7 9 0 496.35 500.02 121.64 o 8 9 0 120.92 85.70 78.32 o 9 9 0 678.87 1023.92 154.30 o 10 9 0 1.38 83.11 93.46 o 11 9 0 1109.08 943.96 199.41 o -15 10 0 610.79 453.24 123.39 o -14 10 0 2485.10 2801.19 174.73 o -13 10 0 29.21 148.07 95.86 o -12 10 0 436.59 476.83 102.05 o -11 10 0 3347.41 3338.36 243.00 o -10 10 0 709.86 881.22 117.51 o -9 10 0 301.50 148.72 95.36 o -8 10 0 2049.90 1961.38 120.82 o -7 10 0 1410.75 1585.74 106.12 o -6 10 0 2234.47 2466.98 122.51 o -5 10 0 43.09 -25.72 54.30 o -4 10 0 114.28 10.24 39.14 o -3 10 0 96.91 199.03 75.25 o -2 10 0 54.90 -19.54 44.46 o -1 10 0 3443.42 3388.01 135.88 o 0 10 0 3028.72 3019.98 126.90 o 1 10 0 2011.87 1923.76 95.55 o 2 10 0 350.92 422.39 85.42 o 3 10 0 11634.16 10970.27 380.57 o 4 10 0 560.98 548.77 58.87 o 5 10 0 259.89 278.76 88.95 o 6 10 0 2475.76 2293.66 121.85 o 7 10 0 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13 0 2326.43 1984.87 112.43 o 0 13 0 1652.14 1575.41 160.53 o 1 13 0 61.27 -58.57 72.25 o 2 13 0 255.23 449.29 101.96 o 3 13 0 455.10 355.39 101.66 o 4 13 0 511.20 462.48 97.02 o 5 13 0 1973.25 2158.01 158.69 o 6 13 0 2202.74 2522.79 151.33 o 7 13 0 127.16 247.63 114.04 o 8 13 0 22.66 216.74 123.17 o -12 14 0 46.26 -67.67 141.42 o -11 14 0 670.12 541.24 158.44 o -10 14 0 1184.19 1045.62 121.41 o -9 14 0 311.90 228.16 85.66 o -8 14 0 665.95 682.65 154.06 o -7 14 0 3540.98 3348.69 215.04 o -6 14 0 4459.36 4269.51 227.16 o -5 14 0 50.32 74.98 98.70 o -4 14 0 1147.34 1215.85 134.67 o -3 14 0 1342.16 1532.99 106.70 o -2 14 0 726.05 818.29 91.04 o -1 14 0 772.72 952.42 94.11 o 0 14 0 13.52 1.02 79.42 o 1 14 0 650.15 747.25 115.86 o 2 14 0 35.80 -16.07 106.58 o 3 14 0 1534.27 1554.41 155.00 o 4 14 0 2947.33 2963.75 201.94 o 5 14 0 90.29 244.88 105.91 o 6 14 0 441.16 560.44 121.46 o -11 15 0 40.70 -20.69 97.09 o -10 15 0 232.28 293.66 96.15 o -9 15 0 922.77 930.82 103.61 o -8 15 0 1443.48 1667.95 206.93 o -7 15 0 122.48 151.98 110.83 o -6 15 0 283.32 283.75 107.87 o -5 15 0 1290.10 1374.84 140.13 o -4 15 0 319.19 267.45 110.23 o -3 15 0 562.94 674.83 116.50 o -2 15 0 0.66 -24.44 82.57 o -1 15 0 746.17 941.79 105.10 o 0 15 0 499.45 482.59 123.59 o 1 15 0 1141.39 1044.30 195.38 o 2 15 0 258.83 339.47 127.27 o 3 15 0 85.79 21.79 104.78 o 4 15 0 1631.93 1614.45 142.41 o 5 15 0 1209.08 1868.34 377.72 o -10 16 0 465.36 318.21 135.81 o -9 16 0 3.52 -123.81 123.81 o -8 16 0 506.13 449.23 130.08 o -7 16 0 1607.08 1757.71 161.58 o -6 16 0 1429.16 1485.11 253.80 o -5 16 0 2245.99 2647.48 378.41 o -4 16 0 432.04 382.93 123.75 o -3 16 0 124.99 85.64 112.93 o -2 16 0 4265.08 5094.07 278.46 o -1 16 0 2306.67 2728.96 322.08 o 0 16 0 29.58 32.47 149.73 o 1 16 0 355.42 416.77 146.15 o 2 16 0 553.61 791.54 155.73 o 3 16 0 246.20 283.13 142.66 o -9 17 0 859.18 908.54 158.24 o -8 17 0 121.95 339.51 144.83 o -7 17 0 174.89 -15.55 132.12 o -6 17 0 154.78 227.92 140.02 o -5 17 0 232.75 139.71 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