#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014519.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014519_Fobs loop_ _publ_author_name '\'Avila, Edward E.' 'Mora, Asilo\'e J.' 'Delgado, Gerzon E.' 'Ram\'irez, Belkis M.' 'Bahsas, Al\'i' 'Koteich, Sonia' _publ_section_title ; Hydrogen-bonding patterns in cis-4-ammoniocyclohexanecarboxylate hemihydrate ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o759 _journal_page_last o761 _journal_volume 60 _journal_year 2004 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.452 _cell_angle_gamma 90.000 _cell_length_a 19.8707 _cell_length_b 6.1614 _cell_length_c 13.4754 _exptl_crystal_F_000 664.00 _reflns_d_resolution_high 0.7499 _[local]_cod_data_source_file ob1197Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cc4am in C2/c (15) (acido cis-4 amino ciclohexano)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 215.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 433.51 523.16 10.24 o 4 0 0 46315.13 44166.12 200.27 o 6 0 0 5806.38 5878.97 69.41 o 8 0 0 69.08 82.68 6.28 o 10 0 0 1073.64 1217.69 16.21 o 12 0 0 601.43 628.39 16.21 o 14 0 0 20.21 13.98 9.84 o 16 0 0 1936.50 1987.07 77.19 o 18 0 0 134.19 132.08 17.78 o 20 0 0 0.36 -4.61 16.67 o 22 0 0 239.74 227.96 24.16 o 24 0 0 18.50 1.78 34.54 o 1 1 0 260.23 266.99 6.52 o 3 1 0 6745.83 6307.64 93.19 o 5 1 0 2278.00 2416.83 23.02 o 7 1 0 973.91 912.23 59.91 o 9 1 0 548.05 528.29 20.60 o 11 1 0 1722.33 1683.85 25.33 o 13 1 0 10.40 -2.68 7.33 o 15 1 0 111.34 112.67 9.00 o 17 1 0 44.64 27.94 9.59 o 19 1 0 22.80 22.78 12.65 o 21 1 0 11.31 37.79 16.38 o 23 1 0 7.18 20.73 18.43 o 25 1 0 4.77 -1.92 35.27 o 0 2 0 2571.71 2394.22 65.94 o 2 2 0 58.72 74.76 5.51 o 4 2 0 2333.37 2527.71 66.71 o 6 2 0 639.02 599.88 21.09 o 8 2 0 1104.86 1143.43 20.42 o 10 2 0 74.19 74.60 6.48 o 12 2 0 65.80 57.75 7.14 o 14 2 0 266.78 280.79 12.50 o 16 2 0 227.43 211.25 13.38 o 18 2 0 344.80 342.73 18.53 o 20 2 0 109.84 119.58 19.70 o 22 2 0 262.25 272.48 23.00 o 24 2 0 137.00 118.81 31.29 o 1 3 0 29.87 38.48 6.22 o 3 3 0 2672.84 2812.93 46.00 o 5 3 0 30.62 45.89 8.47 o 7 3 0 146.74 143.04 8.95 o 9 3 0 12.37 9.01 6.45 o 11 3 0 37.86 47.18 8.58 o 13 3 0 115.86 122.73 10.88 o 15 3 0 350.24 329.50 17.96 o 17 3 0 500.10 480.68 23.94 o 19 3 0 731.88 736.59 46.36 o 21 3 0 270.24 226.65 26.02 o 0 4 0 26.18 26.53 8.29 o 2 4 0 54.42 61.16 7.27 o 4 4 0 3.56 5.75 6.92 o 6 4 0 1165.91 1132.50 19.10 o 8 4 0 36.84 33.03 8.01 o 10 4 0 482.78 476.35 32.24 o 12 4 0 40.88 30.59 11.04 o 14 4 0 15.54 21.05 12.33 o 16 4 0 5.70 13.32 16.19 o 18 4 0 29.22 53.46 19.10 o 20 4 0 12.16 27.74 24.26 o 1 5 0 0.87 -7.82 10.59 o 3 5 0 902.45 896.21 23.06 o 5 5 0 1.15 2.56 8.90 o 7 5 0 60.96 61.60 9.63 o 9 5 0 28.85 39.31 10.57 o 11 5 0 46.72 54.17 12.38 o 13 5 0 40.73 40.65 14.82 o 15 5 0 72.97 107.05 18.01 o 17 5 0 5.89 23.38 22.94 o 19 5 0 24.22 20.43 45.36 o 0 6 0 164.10 203.79 27.26 o 2 6 0 0.06 17.37 14.06 o 4 6 0 12.03 9.12 12.54 o 6 6 0 3.18 10.96 12.38 o 8 6 0 129.66 155.61 16.95 o 10 6 0 6.45 16.22 15.71 o 12 6 0 110.92 126.46 20.28 o 14 6 0 2.02 -6.04 22.53 o 16 6 0 12.83 -55.37 65.21 o 1 7 0 97.88 63.24 26.20 o 3 7 0 30.72 29.64 20.99 o 5 7 0 13.39 28.44 21.68 o 7 7 0 12.54 18.38 26.30 o 9 7 0 28.07 33.58 25.60 o 11 7 0 0.38 -12.62 34.24 o 4 8 0 5.53 31.64 56.17 o -25 1 1 4.73 56.98 48.75 o -23 1 1 89.13 90.83 19.63 o -21 1 1 8.85 25.11 15.60 o -19 1 1 76.04 60.56 13.58 o -17 1 1 21.90 10.74 10.34 o -15 1 1 0.29 6.29 9.08 o -13 1 1 203.04 185.96 8.97 o -11 1 1 249.25 244.89 7.72 o -9 1 1 451.89 434.22 24.05 o -7 1 1 354.85 384.00 19.68 o -5 1 1 2857.52 2480.79 26.88 o -3 1 1 4134.42 3514.46 26.84 o -1 1 1 11321.84 11468.83 80.13 o 1 1 1 12720.90 12218.86 234.84 o 3 1 1 8932.54 9279.99 110.24 o 5 1 1 1350.07 1224.14 18.55 o 7 1 1 618.92 708.47 12.93 o 9 1 1 86.38 65.33 5.64 o 11 1 1 414.93 451.99 10.03 o 13 1 1 130.61 126.25 7.77 o 15 1 1 70.05 70.62 8.38 o 17 1 1 551.47 569.37 15.92 o 19 1 1 23.50 15.32 11.33 o 21 1 1 16.24 13.19 15.14 o 23 1 1 116.26 119.20 21.43 o -24 2 1 29.44 46.71 26.24 o -22 2 1 3.73 9.10 20.12 o -20 2 1 121.41 121.61 21.74 o -18 2 1 66.78 69.62 18.53 o -16 2 1 149.39 136.29 15.87 o -14 2 1 4.33 5.80 8.44 o -12 2 1 776.04 749.13 14.27 o -10 2 1 239.44 247.98 8.15 o -8 2 1 1675.64 1754.25 19.55 o -6 2 1 967.31 971.50 14.42 o -4 2 1 41.67 42.46 4.77 o -2 2 1 346.12 371.12 7.17 o 0 2 1 186.64 181.03 15.91 o 2 2 1 600.20 522.34 13.11 o 4 2 1 5742.97 5396.15 244.19 o 6 2 1 563.92 522.46 18.21 o 8 2 1 953.88 1027.68 13.62 o 10 2 1 2644.99 2651.30 37.38 o 12 2 1 198.18 202.40 11.03 o 14 2 1 456.93 450.90 14.58 o 16 2 1 503.26 505.19 16.63 o 18 2 1 17.60 26.28 11.25 o 20 2 1 642.04 669.18 25.22 o 22 2 1 0.61 10.35 19.22 o -23 3 1 1.03 15.05 30.47 o -21 3 1 16.17 -21.91 22.26 o -19 3 1 66.08 59.33 20.38 o -17 3 1 9.18 10.54 16.61 o -15 3 1 71.56 77.33 13.16 o -13 3 1 14.23 16.22 10.29 o -11 3 1 655.94 650.30 13.81 o -9 3 1 24.82 23.11 6.64 o -7 3 1 150.65 142.73 7.75 o -5 3 1 991.34 1035.93 23.13 o -3 3 1 275.08 324.16 8.53 o -1 3 1 439.23 479.35 8.82 o 1 3 1 394.23 370.56 26.42 o 3 3 1 148.17 163.10 9.67 o 5 3 1 745.45 770.42 16.54 o 7 3 1 2.62 -5.21 7.09 o 9 3 1 233.67 216.28 10.06 o 11 3 1 199.93 194.05 11.41 o 13 3 1 370.97 365.57 13.85 o 15 3 1 11.13 18.18 12.72 o 17 3 1 120.22 99.42 16.08 o 19 3 1 22.12 26.51 17.16 o 21 3 1 8.38 40.78 19.77 o -22 4 1 50.88 84.10 45.52 o -20 4 1 75.38 97.59 34.75 o -18 4 1 41.68 78.50 22.45 o -16 4 1 70.85 117.71 21.37 o -14 4 1 44.54 51.30 12.96 o -12 4 1 106.62 109.90 12.96 o -10 4 1 925.47 930.44 20.90 o -8 4 1 73.91 73.78 9.69 o -6 4 1 572.40 538.58 14.19 o -4 4 1 237.38 225.48 10.25 o -2 4 1 1115.59 1199.71 38.93 o 0 4 1 667.86 674.20 13.39 o 2 4 1 430.16 404.08 22.84 o 4 4 1 37.54 38.92 8.13 o 6 4 1 779.86 751.79 19.35 o 8 4 1 225.54 242.13 15.30 o 10 4 1 0.32 8.68 9.87 o 12 4 1 32.81 30.08 10.42 o 14 4 1 13.07 17.66 12.38 o 16 4 1 19.83 8.70 15.43 o 18 4 1 9.49 29.92 18.65 o 20 4 1 54.50 18.40 21.20 o -19 5 1 0.05 8.14 28.64 o -17 5 1 8.98 21.99 24.64 o -15 5 1 135.91 93.38 19.13 o -13 5 1 22.12 30.90 16.66 o -11 5 1 1907.31 2044.38 91.54 o -9 5 1 316.96 313.35 20.67 o -7 5 1 2143.80 2181.32 88.01 o -5 5 1 773.49 790.08 23.49 o -3 5 1 327.96 333.43 15.81 o -1 5 1 78.97 72.78 12.69 o 1 5 1 197.09 181.53 12.59 o 3 5 1 266.31 257.15 13.08 o 5 5 1 535.93 488.36 18.83 o 7 5 1 160.28 187.41 12.85 o 9 5 1 6.37 0.35 10.96 o 11 5 1 375.30 386.19 24.69 o 13 5 1 99.36 88.07 15.61 o 15 5 1 0.96 -4.78 16.23 o 17 5 1 6.64 5.91 19.51 o 19 5 1 2.29 -18.40 40.19 o -16 6 1 91.95 150.36 41.96 o -14 6 1 105.36 99.50 27.63 o -12 6 1 123.96 140.22 50.25 o -10 6 1 49.93 62.56 22.44 o -8 6 1 23.94 28.48 14.45 o -6 6 1 0.44 -5.83 12.11 o -4 6 1 141.00 136.68 15.17 o -2 6 1 7.24 24.50 13.27 o 0 6 1 644.00 554.96 23.26 o 2 6 1 280.83 263.07 19.25 o 4 6 1 524.52 513.73 21.52 o 6 6 1 6.69 21.25 13.93 o 8 6 1 0.60 12.90 15.02 o 10 6 1 0.87 -10.77 13.14 o 12 6 1 32.92 37.92 15.19 o 14 6 1 2.31 13.57 19.89 o 16 6 1 17.24 21.10 30.92 o -13 7 1 43.75 -18.40 61.66 o -11 7 1 0.97 -26.18 26.18 o -9 7 1 8.57 7.65 25.58 o -7 7 1 1.10 4.54 17.22 o -5 7 1 28.31 23.78 19.67 o -3 7 1 1.20 -5.12 18.28 o -1 7 1 0.20 0.13 22.39 o 1 7 1 0.64 22.90 18.76 o 3 7 1 0.00 -11.25 17.56 o 5 7 1 0.42 16.01 15.56 o 7 7 1 185.27 221.68 24.01 o 9 7 1 0.18 25.69 22.34 o 11 7 1 179.94 203.84 31.27 o 4 8 1 8.98 53.30 37.44 o -24 0 2 9.79 45.69 34.46 o -22 0 2 592.67 593.22 37.04 o -20 0 2 113.28 124.17 19.60 o -18 0 2 991.60 976.28 30.57 o -16 0 2 1723.86 1789.05 36.80 o -14 0 2 199.97 205.50 15.53 o -12 0 2 67.85 50.24 9.10 o -10 0 2 1442.63 1393.60 30.12 o -8 0 2 505.56 519.24 97.47 o -6 0 2 10867.86 11090.70 85.95 o -4 0 2 12552.33 12009.15 174.90 o -2 0 2 43.64 93.02 10.81 o 0 0 2 134.28 155.29 6.11 o 2 0 2 15791.36 16157.45 124.74 o 4 0 2 38.35 39.94 5.92 o 6 0 2 5591.69 5230.40 65.24 o 8 0 2 85.49 89.42 10.08 o 10 0 2 433.01 461.06 17.53 o 12 0 2 2.16 -11.07 11.07 o 14 0 2 481.45 508.80 31.93 o 16 0 2 9.14 12.14 11.31 o 18 0 2 454.68 492.59 20.24 o 20 0 2 108.10 104.95 17.66 o 22 0 2 71.20 52.70 21.67 o 24 0 2 23.30 -37.61 46.00 o -25 1 2 92.71 75.15 31.23 o -23 1 2 75.33 84.62 20.08 o -21 1 2 205.95 221.39 19.45 o -19 1 2 24.20 12.81 12.59 o -17 1 2 58.42 52.45 10.69 o -15 1 2 0.60 4.63 8.70 o -13 1 2 165.59 165.92 8.36 o -11 1 2 1219.02 1262.66 15.61 o -9 1 2 4334.64 4471.70 41.40 o -7 1 2 5515.14 5166.70 322.25 o -5 1 2 3732.33 3686.67 104.27 o -3 1 2 2315.81 2180.72 52.28 o -1 1 2 2325.56 2234.05 22.17 o 1 1 2 1080.84 1073.79 10.64 o 3 1 2 1066.90 1097.63 12.81 o 5 1 2 74.29 76.95 5.00 o 7 1 2 813.89 804.69 11.90 o 9 1 2 532.90 576.19 12.16 o 11 1 2 38.14 33.81 6.93 o 13 1 2 407.90 403.49 11.83 o 15 1 2 11.58 20.60 8.10 o 17 1 2 1.33 10.44 8.60 o 19 1 2 56.12 73.72 12.43 o 21 1 2 8.80 17.04 13.46 o 23 1 2 37.93 29.88 20.57 o -24 2 2 0.21 21.43 25.92 o -22 2 2 38.37 41.53 27.19 o -20 2 2 0.37 13.74 18.91 o -18 2 2 74.51 58.65 17.21 o -16 2 2 78.27 69.62 15.30 o -14 2 2 9.72 2.97 9.13 o -12 2 2 90.54 89.39 7.81 o -10 2 2 12.98 9.50 6.04 o -8 2 2 7.50 4.59 5.62 o -6 2 2 6912.46 7170.33 36.32 o -4 2 2 0.59 2.25 6.10 o -2 2 2 1435.08 1435.29 21.92 o 0 2 2 5359.43 5027.69 170.06 o 2 2 2 1990.03 1935.59 36.88 o 4 2 2 0.01 -4.71 4.71 o 6 2 2 1083.20 1139.60 12.64 o 8 2 2 372.48 373.63 10.52 o 10 2 2 2079.21 1997.50 34.92 o 12 2 2 673.51 673.10 29.55 o 14 2 2 545.86 540.60 18.52 o 16 2 2 3.24 -10.15 10.15 o 18 2 2 54.00 38.92 12.56 o 20 2 2 2.12 -3.04 13.87 o 22 2 2 0.00 4.56 17.30 o -23 3 2 116.98 92.07 27.92 o -21 3 2 13.28 5.50 22.68 o -19 3 2 10.10 28.64 17.54 o -17 3 2 139.46 117.48 18.76 o -15 3 2 1.45 0.85 12.95 o -13 3 2 4.17 -6.75 11.02 o -11 3 2 119.58 86.03 16.53 o -9 3 2 1834.90 1881.30 25.22 o -7 3 2 14.51 15.47 6.25 o -5 3 2 56.93 56.54 6.44 o -3 3 2 3240.37 3340.45 39.39 o -1 3 2 3813.26 3732.62 60.24 o 1 3 2 10.47 14.56 5.73 o 3 3 2 2651.29 2740.82 28.99 o 5 3 2 9.83 9.60 8.24 o 7 3 2 298.49 307.72 11.40 o 9 3 2 257.93 225.15 12.54 o 11 3 2 1.18 0.99 9.16 o 13 3 2 1670.10 1668.18 38.97 o 15 3 2 6.92 0.04 11.93 o 17 3 2 281.25 275.49 18.50 o 19 3 2 33.31 20.89 16.52 o 21 3 2 4.92 13.72 19.99 o -22 4 2 25.05 14.53 67.96 o -20 4 2 8.56 39.80 23.68 o -18 4 2 12.34 -6.41 19.42 o -16 4 2 91.05 88.51 16.99 o -14 4 2 30.24 2.48 13.96 o -12 4 2 542.92 528.23 21.61 o -10 4 2 1624.08 1705.13 53.52 o -8 4 2 613.85 599.82 18.36 o -6 4 2 1831.32 1798.23 23.73 o -4 4 2 26.81 21.63 7.50 o -2 4 2 41.41 45.72 7.58 o 0 4 2 212.00 201.36 9.75 o 2 4 2 19.01 10.84 7.86 o 4 4 2 542.07 517.94 16.26 o 6 4 2 803.69 822.30 20.04 o 8 4 2 19.56 19.87 9.00 o 10 4 2 522.53 506.73 18.61 o 12 4 2 132.85 130.52 12.96 o 14 4 2 146.16 150.75 16.04 o 16 4 2 10.10 35.77 15.17 o 18 4 2 24.83 18.08 17.56 o 20 4 2 5.64 -0.15 29.71 o -19 5 2 38.31 44.96 32.70 o -17 5 2 5.53 23.30 26.69 o -15 5 2 116.77 144.48 23.75 o -13 5 2 0.23 4.44 16.54 o -11 5 2 5.09 12.80 14.27 o -9 5 2 219.27 237.96 16.34 o -7 5 2 395.86 385.15 18.03 o -5 5 2 166.89 160.84 12.62 o -3 5 2 59.48 54.30 11.40 o -1 5 2 596.28 552.10 19.16 o 1 5 2 169.78 152.18 11.66 o 3 5 2 90.69 90.57 10.25 o 5 5 2 143.01 116.98 11.04 o 7 5 2 108.11 130.68 11.88 o 9 5 2 4.49 12.44 12.51 o 11 5 2 12.66 10.79 11.74 o 13 5 2 100.80 116.57 15.06 o 15 5 2 0.07 13.38 17.53 o 17 5 2 3.68 20.25 18.64 o -16 6 2 1.10 -18.04 27.54 o -14 6 2 2.17 14.81 25.92 o -12 6 2 52.12 35.70 40.71 o -10 6 2 78.82 66.77 18.71 o -8 6 2 138.47 116.89 19.84 o -6 6 2 215.67 228.09 21.15 o -4 6 2 192.49 171.92 18.07 o -2 6 2 56.09 76.11 15.90 o 0 6 2 248.72 191.19 20.71 o 2 6 2 108.40 108.55 14.74 o 4 6 2 12.48 4.25 12.57 o 6 6 2 442.20 483.91 21.73 o 8 6 2 301.09 303.48 20.92 o 10 6 2 267.17 315.10 19.73 o 12 6 2 244.16 265.00 19.18 o 14 6 2 1.77 0.76 19.15 o -13 7 2 6.71 -19.05 66.34 o -11 7 2 4.13 -10.52 26.76 o -9 7 2 22.44 56.24 21.84 o -7 7 2 4.65 14.90 24.63 o -5 7 2 21.28 42.92 22.98 o -3 7 2 45.56 48.60 19.33 o -1 7 2 115.91 93.02 19.06 o 1 7 2 9.41 -7.12 18.19 o 3 7 2 3.48 12.78 18.11 o 5 7 2 100.77 114.62 18.28 o 7 7 2 40.64 48.67 20.62 o 9 7 2 439.50 506.58 34.55 o 11 7 2 84.93 91.60 25.89 o 4 8 2 6.20 -54.25 101.29 o -25 1 3 0.77 22.41 23.99 o -23 1 3 71.96 50.19 28.54 o -21 1 3 646.69 691.89 36.28 o -19 1 3 439.91 402.76 18.76 o -17 1 3 696.87 707.24 20.75 o -15 1 3 12.72 3.17 7.86 o -13 1 3 421.97 430.65 10.71 o -11 1 3 592.87 618.90 39.79 o -9 1 3 440.76 417.07 9.51 o -7 1 3 3628.94 3640.84 28.64 o -5 1 3 21039.29 21203.19 76.77 o -3 1 3 1976.74 2081.73 16.14 o -1 1 3 4727.35 4857.83 155.53 o 1 1 3 20697.11 19811.17 186.44 o 3 1 3 1560.98 1585.90 93.73 o 5 1 3 40.80 41.46 4.97 o 7 1 3 362.28 378.35 9.58 o 9 1 3 757.68 695.65 39.26 o 11 1 3 1849.98 1761.27 23.19 o 13 1 3 26.03 16.81 8.97 o 15 1 3 0.45 10.22 8.64 o 17 1 3 551.74 544.62 17.60 o 19 1 3 166.29 172.82 14.31 o 21 1 3 15.33 13.05 13.91 o 23 1 3 74.59 64.50 23.32 o -24 2 3 12.54 38.73 25.47 o -22 2 3 87.99 84.93 22.05 o -20 2 3 37.02 40.17 20.58 o -18 2 3 28.36 25.59 16.39 o -16 2 3 163.98 144.32 14.67 o -14 2 3 5.81 1.41 9.02 o -12 2 3 186.83 147.99 16.63 o -10 2 3 2395.47 2616.62 71.51 o -8 2 3 257.64 265.12 8.13 o -6 2 3 2651.64 2740.68 29.18 o -4 2 3 384.78 413.58 40.93 o -2 2 3 6555.48 6733.11 38.67 o 0 2 3 25.55 15.13 4.85 o 2 2 3 2491.39 2663.98 29.23 o 4 2 3 631.35 591.21 10.50 o 6 2 3 5.32 19.45 5.78 o 8 2 3 362.60 371.41 9.42 o 10 2 3 43.11 37.25 8.46 o 12 2 3 554.94 571.92 35.45 o 14 2 3 536.67 497.91 18.65 o 16 2 3 90.85 93.17 13.57 o 18 2 3 1.28 7.18 11.76 o 20 2 3 10.32 15.64 13.94 o 22 2 3 36.07 63.49 17.80 o -23 3 3 51.71 27.47 26.54 o -21 3 3 0.18 20.41 24.01 o -19 3 3 10.44 20.27 21.52 o -17 3 3 249.47 232.15 21.69 o -15 3 3 8.05 19.18 13.45 o -13 3 3 357.91 290.08 41.69 o -11 3 3 152.22 127.22 14.82 o -9 3 3 226.25 189.72 10.00 o -7 3 3 3.14 5.40 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