#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014538.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014538_Fobs loop_ _publ_author_name 'Jones, Peter G.' 'Zerbe, Eva-Maria' 'W\"olper, Christoph' _publ_section_title ; Polysulfonylamines. CLXXI. [Di(methanesulfonyl)amido-\kN]bis(2-picoline-\kN)copper(I) ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m529 _journal_page_last m531 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.780 _cell_angle_gamma 90.000 _cell_length_a 10.2353 _cell_length_b 7.7684 _cell_length_c 23.0287 _exptl_crystal_F_000 872.00 _reflns_d_resolution_high 0.7100 _[local]_cod_data_source_file sk1763Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' dackel in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 256.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7.89 17.39 1.33 o 2 0 0 5515.90 5450.50 40.49 o 3 0 0 100.31 121.81 5.34 o 4 0 0 11975.58 13308.67 53.36 o 5 0 0 62.94 68.24 5.75 o 6 0 0 6713.91 6509.00 41.79 o 7 0 0 22.33 22.18 6.02 o 8 0 0 5559.88 5673.78 55.73 o 9 0 0 1806.10 1702.88 33.57 o 10 0 0 4527.58 4429.74 59.20 o 11 0 0 9.88 2.71 15.26 o 12 0 0 11.67 5.80 16.02 o 13 0 0 21.80 6.83 20.11 o 14 0 0 204.45 218.88 32.13 o 1 1 0 1068.40 1197.96 10.75 o 2 1 0 249.33 239.85 4.23 o 3 1 0 2245.59 2377.83 18.21 o 4 1 0 1543.95 1745.95 13.12 o 5 1 0 180.56 169.87 6.05 o 6 1 0 260.91 289.60 8.17 o 7 1 0 189.01 193.58 8.09 o 8 1 0 3.03 1.58 4.86 o 9 1 0 2667.99 2523.28 26.42 o 10 1 0 202.54 217.85 13.16 o 11 1 0 122.56 102.88 12.31 o 12 1 0 25.41 20.90 11.52 o 13 1 0 303.46 318.37 25.19 o 14 1 0 4.21 -7.63 48.64 o 0 2 0 6982.35 7442.46 49.47 o 1 2 0 11.68 14.61 2.53 o 2 2 0 22648.22 24218.98 94.48 o 3 2 0 31.50 39.27 3.34 o 4 2 0 1831.53 1624.94 13.05 o 5 2 0 139.29 150.55 5.88 o 6 2 0 4659.11 4439.10 29.95 o 7 2 0 734.85 733.98 12.75 o 8 2 0 987.79 1062.87 17.14 o 9 2 0 0.42 -3.78 5.88 o 10 2 0 1525.61 1479.72 25.07 o 11 2 0 145.79 114.47 14.73 o 12 2 0 826.39 849.82 29.28 o 13 2 0 99.93 82.05 19.99 o 1 3 0 306.15 440.44 7.63 o 2 3 0 2257.50 2399.02 21.18 o 3 3 0 491.01 520.34 10.50 o 4 3 0 387.53 430.84 8.56 o 5 3 0 1016.70 1082.99 14.71 o 6 3 0 3.57 -1.58 3.84 o 7 3 0 784.00 790.99 15.73 o 8 3 0 1.30 -3.48 5.80 o 9 3 0 909.17 920.34 21.14 o 10 3 0 180.77 186.49 13.25 o 11 3 0 0.45 6.59 9.98 o 12 3 0 99.94 117.79 16.88 o 13 3 0 599.13 701.27 35.58 o 0 4 0 452.56 483.56 18.08 o 1 4 0 460.72 520.60 13.31 o 2 4 0 3783.89 3838.22 42.87 o 3 4 0 342.73 321.66 9.86 o 4 4 0 13265.29 12913.32 87.47 o 5 4 0 183.85 163.00 10.07 o 6 4 0 6921.37 6900.39 42.44 o 7 4 0 210.52 175.06 8.66 o 8 4 0 22.23 18.85 7.10 o 9 4 0 2.80 3.48 7.59 o 10 4 0 166.40 170.59 13.10 o 11 4 0 3.39 -5.52 10.26 o 12 4 0 2736.40 2770.94 54.25 o 13 4 0 5.12 -6.58 16.52 o 1 5 0 341.00 350.22 14.91 o 2 5 0 1374.39 1412.37 22.28 o 3 5 0 435.90 404.35 12.72 o 4 5 0 44.58 20.13 5.44 o 5 5 0 5232.26 5183.64 43.33 o 6 5 0 72.53 64.43 9.05 o 7 5 0 10.49 10.74 8.70 o 8 5 0 39.90 55.29 11.58 o 9 5 0 108.82 109.07 12.45 o 10 5 0 25.15 17.73 11.59 o 11 5 0 470.99 445.69 19.94 o 12 5 0 17.52 17.44 12.89 o 0 6 0 1186.70 1218.97 40.50 o 1 6 0 1763.69 1744.51 27.91 o 2 6 0 1949.28 1999.25 40.22 o 3 6 0 887.06 844.67 16.43 o 4 6 0 1855.39 1825.98 24.99 o 5 6 0 101.46 112.42 10.27 o 6 6 0 1730.33 1718.49 37.12 o 7 6 0 108.38 121.30 13.32 o 8 6 0 1791.39 1729.67 35.64 o 9 6 0 23.88 14.08 13.36 o 10 6 0 232.83 253.26 22.88 o 11 6 0 96.85 101.76 16.58 o 1 7 0 5.29 5.86 10.85 o 2 7 0 101.50 100.80 13.21 o 3 7 0 498.68 522.36 25.22 o 4 7 0 72.22 68.91 13.19 o 5 7 0 1372.49 1385.77 34.26 o 6 7 0 407.13 400.55 19.41 o 7 7 0 20.00 10.97 11.77 o 8 7 0 0.09 -2.67 12.74 o 9 7 0 8.01 0.33 13.77 o 10 7 0 390.36 423.08 28.80 o 0 8 0 3722.45 3517.56 135.33 o 1 8 0 8.54 5.02 12.42 o 2 8 0 315.16 345.74 22.05 o 3 8 0 36.00 56.80 16.60 o 4 8 0 78.09 99.61 18.23 o 5 8 0 114.94 99.54 14.60 o 6 8 0 795.95 777.75 25.49 o 7 8 0 58.70 55.31 14.55 o 8 8 0 1049.73 1081.93 35.47 o 9 8 0 32.06 26.12 17.30 o 1 9 0 530.67 585.29 32.02 o 2 9 0 73.64 77.78 18.41 o 3 9 0 258.90 287.06 26.51 o 4 9 0 19.86 10.13 20.07 o 5 9 0 6.21 -13.75 18.96 o 6 9 0 37.59 28.04 17.52 o 7 9 0 92.35 68.76 20.00 o 0 10 0 147.47 164.85 35.95 o 1 10 0 379.10 444.04 33.11 o 2 10 0 264.49 290.20 33.78 o 3 10 0 472.70 452.20 49.07 o 4 10 0 186.72 181.55 38.47 o 5 10 0 2.06 16.98 32.18 o -14 1 1 1037.50 1073.24 44.57 o -13 1 1 1893.78 1939.06 47.23 o -12 1 1 403.02 420.55 22.90 o -11 1 1 1623.95 1586.48 29.23 o -10 1 1 467.97 410.83 15.74 o -9 1 1 179.55 168.63 9.57 o -8 1 1 269.86 278.34 10.08 o -7 1 1 1843.42 1783.53 18.68 o -6 1 1 22.36 6.81 3.58 o -5 1 1 7449.51 7544.95 31.53 o -4 1 1 12464.85 13330.27 78.06 o -3 1 1 14718.69 15293.65 85.80 o -2 1 1 546.17 542.49 5.69 o -1 1 1 2172.87 2348.51 14.93 o 0 1 1 487.04 537.08 4.62 o 1 1 1 11916.70 12655.29 84.42 o 2 1 1 14183.41 15532.79 83.59 o 3 1 1 25867.56 27749.85 127.75 o 4 1 1 13942.41 14715.99 66.15 o 5 1 1 4474.06 4716.20 27.15 o 6 1 1 1907.63 1829.15 16.85 o 7 1 1 1061.73 1026.30 14.77 o 8 1 1 79.08 90.85 7.07 o 9 1 1 558.95 583.64 15.48 o 10 1 1 976.32 972.74 22.72 o 11 1 1 634.01 654.41 20.88 o 12 1 1 1449.45 1481.73 32.77 o 13 1 1 863.29 895.36 44.01 o -13 2 1 504.48 536.30 32.57 o -12 2 1 248.48 280.66 20.45 o -11 2 1 110.91 99.49 14.11 o -10 2 1 983.91 943.48 19.74 o -9 2 1 119.99 120.80 8.91 o -8 2 1 427.42 404.62 11.90 o -7 2 1 48.81 41.26 5.46 o -6 2 1 1168.14 1207.00 13.48 o -5 2 1 3833.78 3983.08 21.23 o -4 2 1 36.77 11.65 2.79 o -3 2 1 29.44 11.20 2.62 o -2 2 1 3895.59 4487.57 41.93 o -1 2 1 6657.96 6978.17 54.20 o 0 2 1 36410.77 38004.77 136.69 o 1 2 1 10956.60 11567.47 40.41 o 2 2 1 1954.71 1927.91 11.30 o 3 2 1 151.42 104.79 3.99 o 4 2 1 2234.19 2138.31 15.53 o 5 2 1 505.31 470.11 8.50 o 6 2 1 3.68 2.99 3.55 o 7 2 1 405.06 376.76 10.20 o 8 2 1 92.68 102.77 7.69 o 9 2 1 783.48 763.77 17.18 o 10 2 1 57.89 52.97 9.53 o 11 2 1 152.28 185.41 17.12 o 12 2 1 535.23 558.67 27.33 o 13 2 1 536.84 553.36 30.95 o -13 3 1 74.97 53.66 18.22 o -12 3 1 7.86 -11.79 13.44 o -11 3 1 1192.38 1188.73 31.16 o -10 3 1 434.67 412.81 17.05 o -9 3 1 4218.73 4030.36 40.44 o -8 3 1 2644.39 2497.99 27.84 o -7 3 1 2920.26 2882.53 27.66 o -6 3 1 182.78 160.78 7.24 o -5 3 1 1535.72 1668.71 17.51 o -4 3 1 810.92 1035.09 12.00 o -3 3 1 13110.01 13942.48 83.64 o -2 3 1 8569.04 8966.47 47.73 o -1 3 1 19767.44 20448.14 129.58 o 0 3 1 1361.14 1235.58 16.20 o 1 3 1 6036.26 6125.32 37.77 o 2 3 1 7019.94 7574.08 62.16 o 3 3 1 2421.96 2513.03 21.63 o 4 3 1 422.79 471.61 9.09 o 5 3 1 102.52 80.69 5.79 o 6 3 1 1210.55 1158.21 15.08 o 7 3 1 2716.72 2729.53 29.23 o 8 3 1 2769.12 2687.08 31.42 o 9 3 1 1575.91 1512.98 25.98 o 10 3 1 684.73 689.57 20.30 o 11 3 1 66.68 68.99 12.91 o 12 3 1 12.76 10.03 12.87 o 13 3 1 72.58 81.83 21.63 o -13 4 1 32.89 26.92 17.64 o -12 4 1 166.85 158.56 18.21 o -11 4 1 113.78 102.63 13.23 o -10 4 1 34.47 21.00 9.12 o -9 4 1 36.29 13.48 7.70 o -8 4 1 373.70 332.01 13.75 o -7 4 1 1826.02 1786.09 22.12 o -6 4 1 4.01 -4.63 6.07 o -5 4 1 1165.49 1213.52 20.93 o -4 4 1 601.35 637.36 13.53 o -3 4 1 881.18 899.97 16.13 o -2 4 1 838.81 841.47 12.24 o -1 4 1 407.50 490.14 15.19 o 0 4 1 200.69 172.60 9.11 o 1 4 1 3287.58 3458.75 33.20 o 2 4 1 825.38 832.83 12.45 o 3 4 1 644.28 648.78 12.04 o 4 4 1 177.85 178.62 8.99 o 5 4 1 16.04 13.79 5.88 o 6 4 1 1302.96 1340.33 17.71 o 7 4 1 211.53 183.56 9.34 o 8 4 1 138.95 128.09 9.95 o 9 4 1 224.55 217.99 13.20 o 10 4 1 179.99 157.31 12.90 o 11 4 1 147.28 141.71 13.95 o 12 4 1 9.82 2.85 14.34 o -12 5 1 73.39 69.26 13.91 o -11 5 1 87.89 87.47 12.49 o -10 5 1 432.73 452.90 22.00 o -9 5 1 1079.81 1078.86 28.86 o -8 5 1 1517.23 1527.83 32.46 o -7 5 1 1829.18 1834.61 29.84 o -6 5 1 121.57 104.63 10.15 o -5 5 1 161.66 158.79 10.59 o -4 5 1 750.96 727.78 15.05 o -3 5 1 1172.92 1208.40 20.39 o -2 5 1 3619.07 3476.29 34.07 o -1 5 1 2591.10 2352.16 28.78 o 0 5 1 1896.84 1771.85 29.26 o 1 5 1 2852.79 2912.28 31.84 o 2 5 1 232.51 230.67 9.43 o 3 5 1 2269.09 2266.97 25.74 o 4 5 1 204.62 215.23 10.94 o 5 5 1 9.07 17.94 9.16 o 6 5 1 984.95 956.97 21.06 o 7 5 1 758.71 788.09 23.41 o 8 5 1 1603.87 1621.69 33.75 o 9 5 1 2913.00 2923.04 39.73 o 10 5 1 8.68 -4.12 8.76 o 11 5 1 62.73 78.02 12.84 o 12 5 1 22.20 20.23 13.90 o -11 6 1 1.27 -8.00 13.56 o -10 6 1 172.28 167.22 19.64 o -9 6 1 941.30 900.60 31.47 o -8 6 1 1308.78 1242.71 33.43 o -7 6 1 20.28 13.06 9.93 o -6 6 1 3.38 -5.16 7.54 o -5 6 1 29.94 15.63 7.44 o -4 6 1 324.29 282.97 12.58 o -3 6 1 832.81 875.43 24.84 o -2 6 1 374.53 329.71 17.25 o -1 6 1 660.60 633.34 18.52 o 0 6 1 1733.42 1728.63 34.47 o 1 6 1 2936.42 3088.85 43.79 o 2 6 1 101.40 92.04 11.72 o 3 6 1 1179.98 1135.13 18.17 o 4 6 1 51.84 36.85 7.24 o 5 6 1 267.22 256.98 13.30 o 6 6 1 1.13 5.60 8.80 o 7 6 1 994.95 936.12 26.18 o 8 6 1 217.63 221.40 17.05 o 9 6 1 650.40 601.85 27.48 o 10 6 1 42.01 38.71 16.11 o 11 6 1 0.54 3.30 14.51 o -10 7 1 356.65 375.70 27.34 o -9 7 1 190.19 164.95 19.96 o -8 7 1 1.04 -8.36 12.62 o -7 7 1 844.60 869.49 28.60 o -6 7 1 1334.05 1366.84 29.68 o -5 7 1 3572.77 3516.67 40.68 o -4 7 1 1441.97 1471.11 35.18 o -3 7 1 421.13 425.62 21.20 o -2 7 1 1899.82 1880.93 36.97 o -1 7 1 322.21 331.03 21.37 o 0 7 1 3.75 2.05 7.99 o 1 7 1 1882.72 1836.16 35.90 o 2 7 1 140.20 113.57 15.35 o 3 7 1 1400.46 1453.15 37.51 o 4 7 1 2111.84 2038.44 39.94 o 5 7 1 809.33 837.44 22.44 o 6 7 1 621.39 641.89 22.04 o 7 7 1 30.50 25.72 11.34 o 8 7 1 276.87 261.57 21.15 o 9 7 1 82.84 80.86 17.39 o 10 7 1 277.79 263.61 25.14 o -9 8 1 1.42 3.74 16.46 o -8 8 1 278.46 339.58 24.33 o -7 8 1 77.74 53.07 14.37 o -6 8 1 868.90 861.38 26.56 o -5 8 1 70.72 65.19 14.62 o -4 8 1 124.68 119.08 16.77 o -3 8 1 808.17 824.63 32.87 o -2 8 1 20.60 17.21 15.53 o -1 8 1 1375.25 1399.56 39.83 o 0 8 1 523.28 547.68 27.65 o 1 8 1 27.75 29.51 12.06 o 2 8 1 1292.11 1345.81 34.77 o 3 8 1 34.11 24.45 12.66 o 4 8 1 505.21 514.35 28.43 o 5 8 1 166.46 210.03 19.21 o 6 8 1 8.47 -1.40 10.88 o 7 8 1 995.60 1079.32 33.53 o 8 8 1 10.33 15.67 14.87 o 9 8 1 2.42 -5.98 16.29 o -8 9 1 46.29 40.35 16.05 o -7 9 1 3.63 -2.68 18.25 o -6 9 1 504.15 479.90 31.10 o -5 9 1 178.05 147.57 27.40 o -4 9 1 770.23 739.47 51.17 o -3 9 1 686.95 740.40 40.53 o -2 9 1 41.82 55.12 17.57 o -1 9 1 135.64 164.67 22.33 o 0 9 1 457.14 466.54 30.67 o 1 9 1 7.98 4.81 15.72 o 2 9 1 531.96 542.95 30.83 o 3 9 1 168.76 179.65 22.92 o 4 9 1 103.65 85.42 20.63 o 5 9 1 888.78 911.75 46.41 o 6 9 1 34.32 17.41 16.79 o 7 9 1 205.51 224.90 26.23 o -5 10 1 63.22 65.76 32.46 o -4 10 1 18.75 35.47 30.67 o -3 10 1 52.40 32.31 44.65 o -2 10 1 274.10 289.75 41.79 o -1 10 1 71.31 78.60 21.73 o 0 10 1 78.35 64.11 21.55 o 1 10 1 37.53 49.24 23.60 o 2 10 1 11.12 14.07 23.42 o 3 10 1 163.95 202.23 40.23 o 4 10 1 498.70 455.09 52.84 o 5 10 1 31.41 49.39 34.85 o -14 0 2 315.75 319.60 46.75 o -13 0 2 14.61 11.14 19.71 o -12 0 2 108.16 106.07 21.20 o -11 0 2 4252.80 4141.72 65.12 o -10 0 2 1305.48 1229.30 30.97 o -9 0 2 7509.00 7239.70 76.89 o -8 0 2 244.40 227.25 14.41 o -7 0 2 2419.65 2242.49 26.40 o -6 0 2 218.42 215.96 9.74 o -5 0 2 115.45 117.73 6.89 o -4 0 2 602.04 618.33 11.05 o -3 0 2 7994.10 8108.50 39.14 o -2 0 2 127.84 116.15 4.43 o -1 0 2 60338.00 62293.45 260.84 o 0 0 2 396.16 447.63 8.35 o 1 0 2 65644.35 66670.98 313.96 o 2 0 2 1003.02 1109.19 11.41 o 3 0 2 243.69 229.92 6.99 o 4 0 2 32.80 25.32 4.18 o 5 0 2 6914.28 7654.87 42.83 o 6 0 2 291.96 324.78 11.48 o 7 0 2 7820.97 7644.13 49.70 o 8 0 2 379.16 358.31 17.33 o 9 0 2 3517.55 3519.14 48.67 o 10 0 2 2.51 -9.26 11.25 o 11 0 2 103.30 81.30 18.81 o 12 0 2 77.49 55.78 22.50 o 13 0 2 67.99 69.06 23.19 o -14 1 2 518.98 540.18 35.70 o -13 1 2 19.85 26.70 16.37 o -12 1 2 9.44 -10.06 10.06 o -11 1 2 405.53 382.12 16.84 o -10 1 2 580.19 601.09 17.64 o -9 1 2 12.61 21.26 6.13 o -8 1 2 817.76 778.78 14.16 o -7 1 2 1.25 -3.21 3.96 o -6 1 2 1413.40 1683.45 16.06 o -5 1 2 1555.85 1702.70 14.52 o -4 1 2 2455.40 2541.01 18.71 o -3 1 2 1.53 0.99 1.90 o -2 1 2 23983.81 25638.87 107.06 o -1 1 2 976.82 1139.96 7.02 o 0 1 2 6505.56 7121.98 34.62 o 1 1 2 542.17 508.43 6.07 o 2 1 2 4497.08 4988.78 22.63 o 3 1 2 61.57 75.68 3.83 o 4 1 2 50.16 21.23 3.12 o 5 1 2 11.97 11.61 3.29 o 6 1 2 10.48 7.32 3.79 o 7 1 2 95.77 97.85 6.50 o 8 1 2 2019.42 1949.36 24.88 o 9 1 2 465.98 428.43 14.05 o 10 1 2 3.89 -7.76 7.76 o 11 1 2 258.13 224.38 16.19 o 12 1 2 325.33 352.38 20.77 o 13 1 2 0.54 -8.76 15.59 o -13 2 2 716.16 726.61 32.25 o -12 2 2 5.67 -1.93 12.09 o -11 2 2 747.67 751.79 25.52 o -10 2 2 8.97 2.42 6.98 o -9 2 2 1061.51 1021.37 18.05 o -8 2 2 943.47 926.27 16.13 o -7 2 2 2853.87 2760.38 29.27 o -6 2 2 12.53 15.39 3.93 o -5 2 2 2034.58 2010.25 16.71 o -4 2 2 1447.22 1544.91 12.62 o -3 2 2 2243.41 2043.20 14.84 o -2 2 2 2119.28 2346.75 22.24 o -1 2 2 13672.78 14156.13 81.25 o 0 2 2 12825.15 13502.93 56.69 o 1 2 2 8105.86 8510.94 58.27 o 2 2 2 4845.48 5216.44 32.39 o 3 2 2 3111.96 2817.90 17.74 o 4 2 2 2472.27 2797.97 21.00 o 5 2 2 3202.31 3076.73 21.54 o 6 2 2 0.04 -0.30 3.57 o 7 2 2 2080.54 2062.22 20.13 o 8 2 2 14.73 10.41 5.56 o 9 2 2 101.89 104.14 9.08 o 10 2 2 199.95 192.48 15.74 o 11 2 2 1323.23 1293.05 32.50 o 12 2 2 0.03 -12.83 13.19 o 13 2 2 264.07 294.45 28.99 o -13 3 2 16.43 26.12 16.91 o -12 3 2 3.05 -4.34 13.71 o -11 3 2 147.65 159.15 14.69 o -10 3 2 383.40 405.60 17.13 o -9 3 2 245.36 225.88 12.12 o -8 3 2 902.57 902.80 18.09 o -7 3 2 528.07 539.26 13.60 o -6 3 2 196.31 163.24 6.69 o -5 3 2 12.91 16.31 4.09 o -4 3 2 71.49 77.60 4.58 o -3 3 2 71.46 86.23 5.45 o -2 3 2 2847.58 2821.35 22.18 o -1 3 2 3006.32 3359.06 20.24 o 1 3 2 139.67 147.03 5.77 o 2 3 2 110.00 114.08 6.04 o 3 3 2 41.01 38.92 3.89 o 4 3 2 3255.69 3619.98 22.03 o 5 3 2 709.20 744.74 12.13 o 6 3 2 992.06 1013.21 14.37 o 7 3 2 129.77 138.09 8.82 o 8 3 2 3049.82 3005.63 33.68 o 9 3 2 874.24 810.12 20.33 o 10 3 2 0.58 -3.29 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