#------------------------------------------------------------------------------
#$Date: 2016-04-02 22:00:57 +0300 (Sat, 02 Apr 2016) $
#$Revision: 180814 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/45/2014572.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2014572_Fobs
loop_
_publ_author_name
'Khera, Smriti'
'Carducci, Michael D.'
'Gu, Jian-Qiao'
'Timmermann, Barbara N.'
_publ_section_title
;
(4R,4aR,6S,7S,7aS)-6-Hydroxy-7-hydroxymethyl-4-methylperhydrocyclopenta[c]pyran-1-one
chloroform solvate from Valeriana laxiflora
;
_journal_issue 11
_journal_name_full 'Acta Crystallographica Section C'
_journal_page_first o773
_journal_page_last o775
_journal_volume 60
_journal_year 2004
_space_group_IT_number 4
_symmetry_space_group_name_Hall 'P 2yb'
_symmetry_space_group_name_H-M 'P 1 21 1'
_cell_angle_alpha 90.000
_cell_angle_beta 94.478
_cell_angle_gamma 90.000
_cell_length_a 10.5233
_cell_length_b 6.0404
_cell_length_c 11.2313
_exptl_crystal_F_000 332.00
_reflns_d_resolution_high 0.8400
_cod_data_source_file sx1145Isup2.hkl
_cod_data_source_block I
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' sk06s in P2(1)'
_shelx_refln_list_code 4
_shelx_f_calc_maximum 91.53
_shelx_f_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 -7 0 140.30 143.32 53.61 o
1 -6 0 26.22 41.13 29.43 o
2 -6 0 77.39 55.61 41.66 o
3 -6 0 102.06 114.60 32.43 o
4 -6 0 16.04 37.45 37.03 o
5 -6 0 18.64 45.18 56.41 o
6 -6 0 250.04 266.63 78.54 o
1 -5 0 129.74 151.36 28.32 o
2 -5 0 252.49 267.64 32.61 o
3 -5 0 112.83 128.21 46.83 o
6 -5 0 30.84 12.41 39.75 o
7 -5 0 54.59 47.48 43.14 o
8 -5 0 15.48 15.84 40.97 o
1 -4 0 80.89 109.35 31.93 o
3 -4 0 43.23 34.34 42.01 o
4 -4 0 107.04 134.27 30.65 o
5 -4 0 48.21 41.64 26.90 o
6 -4 0 934.15 987.03 79.50 o
7 -4 0 63.99 64.53 29.46 o
8 -4 0 16.55 31.23 29.18 o
9 -4 0 92.95 145.73 33.52 o
10 -4 0 45.48 204.93 72.02 o
2 -3 0 141.87 142.51 12.46 o
3 -3 0 295.52 319.84 14.83 o
4 -3 0 349.30 336.31 23.76 o
5 -3 0 221.07 196.88 52.07 o
6 -3 0 35.88 49.48 23.43 o
7 -3 0 270.84 265.88 38.71 o
8 -3 0 151.25 150.45 32.04 o
9 -3 0 33.94 -12.93 29.42 o
10 -3 0 38.52 59.82 40.19 o
11 -3 0 1.52 35.97 36.31 o
1 -2 0 357.26 429.41 30.15 o
2 -2 0 198.66 209.37 10.43 o
3 -2 0 2747.90 2903.23 49.64 o
4 -2 0 857.15 856.19 21.98 o
5 -2 0 68.50 75.43 10.23 o
6 -2 0 984.17 1008.24 57.72 o
7 -2 0 14.21 -1.87 23.70 o
8 -2 0 29.41 -5.20 24.54 o
9 -2 0 129.63 87.41 32.16 o
10 -2 0 23.98 36.78 27.86 o
11 -2 0 16.68 33.85 28.47 o
1 -1 0 227.84 224.97 6.93 o
2 -1 0 3902.74 3904.35 64.43 o
3 -1 0 787.71 791.73 31.10 o
4 -1 0 859.24 813.05 19.78 o
5 -1 0 893.83 871.19 23.02 o
6 -1 0 78.01 69.17 11.99 o
7 -1 0 584.45 584.59 25.56 o
8 -1 0 688.16 724.32 40.06 o
9 -1 0 22.65 33.52 22.40 o
10 -1 0 2.24 -20.55 23.73 o
11 -1 0 28.33 51.08 26.80 o
12 -1 0 1.05 20.56 31.10 o
1 0 0 779.01 695.91 12.45 o
2 0 0 2829.56 2481.95 41.18 o
3 0 0 1159.62 1098.52 23.14 o
4 0 0 77.04 82.20 8.63 o
5 0 0 7.16 16.01 9.29 o
6 0 0 273.86 257.07 14.49 o
7 0 0 167.96 143.14 25.54 o
8 0 0 4.09 14.42 14.36 o
9 0 0 39.33 40.55 21.59 o
10 0 0 10.22 16.78 20.80 o
11 0 0 71.73 64.72 24.17 o
12 0 0 15.67 27.19 25.73 o
1 1 0 224.97 232.53 7.82 o
2 1 0 3923.10 3912.77 58.59 o
3 1 0 784.37 837.74 18.86 o
4 1 0 842.55 827.94 20.41 o
5 1 0 919.47 937.13 23.85 o
6 1 0 77.24 75.34 12.11 o
7 1 0 585.38 614.20 43.31 o
8 1 0 689.88 689.29 26.79 o
9 1 0 24.09 11.54 17.73 o
10 1 0 2.45 40.92 29.25 o
11 1 0 28.68 69.36 27.88 o
12 1 0 1.09 57.11 29.69 o
0 2 0 8013.50 8772.05 137.15 o
1 2 0 341.22 413.88 18.80 o
2 2 0 198.19 217.85 13.77 o
3 2 0 2777.80 3086.22 51.15 o
4 2 0 848.71 868.02 22.77 o
5 2 0 71.58 85.60 13.28 o
6 2 0 978.05 1008.60 28.30 o
7 2 0 15.77 23.41 14.57 o
8 2 0 28.36 35.07 19.56 o
9 2 0 132.25 121.29 21.10 o
10 2 0 24.25 27.28 22.65 o
11 2 0 15.74 30.32 29.40 o
1 3 0 785.79 799.65 32.97 o
2 3 0 136.66 137.27 15.35 o
3 3 0 291.73 297.42 24.61 o
4 3 0 354.38 349.35 46.48 o
5 3 0 215.74 247.39 33.61 o
6 3 0 35.09 62.73 19.79 o
7 3 0 266.19 289.65 25.76 o
8 3 0 149.53 189.45 23.78 o
9 3 0 33.95 56.36 33.01 o
10 3 0 38.98 29.76 42.86 o
11 3 0 1.63 46.25 51.24 o
0 4 0 1550.25 1589.46 36.93 o
1 4 0 78.78 58.48 10.27 o
2 4 0 347.56 363.29 30.56 o
3 4 0 43.71 29.41 17.47 o
4 4 0 105.21 110.36 23.31 o
5 4 0 46.51 33.59 22.24 o
6 4 0 936.73 832.85 40.60 o
7 4 0 67.22 73.15 38.88 o
8 4 0 17.11 66.97 42.09 o
9 4 0 95.81 66.39 46.04 o
1 5 0 134.11 138.78 14.82 o
2 5 0 250.91 223.83 19.08 o
3 5 0 111.92 148.10 28.86 o
4 5 0 19.81 -11.51 23.37 o
5 5 0 211.62 196.29 28.45 o
6 5 0 30.85 30.78 26.38 o
7 5 0 55.75 37.91 33.91 o
8 5 0 15.08 21.70 38.10 o
0 6 0 429.06 393.62 28.78 o
1 6 0 26.80 14.52 21.76 o
2 6 0 78.24 92.06 22.76 o
3 6 0 103.01 187.66 54.19 o
4 6 0 15.29 4.65 31.95 o
5 6 0 18.59 5.37 33.15 o
6 6 0 254.23 200.43 40.33 o
1 7 0 130.13 153.03 43.44 o
2 7 0 144.94 155.06 37.84 o
-2 -7 1 37.40 45.15 55.83 o
-1 -7 1 170.71 66.00 57.19 o
0 -7 1 290.97 276.23 61.91 o
2 -7 1 454.07 433.03 61.72 o
-5 -6 1 519.75 577.01 77.87 o
-4 -6 1 76.97 123.78 38.56 o
-3 -6 1 122.19 167.65 37.30 o
-2 -6 1 10.93 29.52 68.35 o
0 -6 1 17.41 15.57 28.20 o
1 -6 1 8.76 -10.38 29.33 o
2 -6 1 79.93 64.23 43.65 o
3 -6 1 2.94 39.70 29.21 o
4 -6 1 0.12 8.10 33.89 o
5 -6 1 13.79 52.33 39.68 o
6 -6 1 82.77 44.64 60.16 o
-9 -5 1 20.62 42.48 46.16 o
-8 -5 1 4.30 -39.68 40.67 o
-7 -5 1 32.51 5.91 52.46 o
-6 -5 1 75.78 73.59 46.09 o
-5 -5 1 7.31 65.09 40.18 o
-2 -5 1 105.12 77.60 24.31 o
-1 -5 1 286.41 298.36 43.80 o
0 -5 1 753.27 713.26 41.24 o
1 -5 1 38.50 22.14 16.58 o
2 -5 1 1105.90 1036.85 73.22 o
3 -5 1 169.67 186.52 31.05 o
4 -5 1 25.50 16.16 43.40 o
6 -5 1 31.47 92.48 44.30 o
7 -5 1 15.58 22.84 44.11 o
8 -5 1 9.63 46.10 36.63 o
-10 -4 1 4.81 53.71 36.51 o
-9 -4 1 11.80 36.49 76.60 o
-8 -4 1 130.41 168.71 34.29 o
-7 -4 1 19.46 -0.08 29.25 o
-6 -4 1 271.38 303.06 35.99 o
-5 -4 1 255.92 253.39 31.96 o
-4 -4 1 186.29 180.66 29.06 o
-3 -4 1 81.83 81.53 27.17 o
0 -4 1 195.42 193.44 31.31 o
2 -4 1 120.61 171.95 37.22 o
3 -4 1 48.78 66.28 47.19 o
4 -4 1 167.95 196.13 26.63 o
5 -4 1 13.56 40.91 30.11 o
6 -4 1 78.19 55.01 28.69 o
7 -4 1 165.82 108.56 30.15 o
8 -4 1 34.69 28.61 29.70 o
9 -4 1 47.94 83.02 65.02 o
10 -4 1 22.30 49.56 40.74 o
-11 -3 1 10.19 -30.84 30.84 o
-10 -3 1 136.15 139.60 34.57 o
-9 -3 1 6.94 -7.27 39.67 o
-8 -3 1 41.17 77.60 73.21 o
-7 -3 1 50.91 93.57 28.52 o
-6 -3 1 336.87 389.09 34.27 o
-5 -3 1 3.79 -10.38 21.48 o
-4 -3 1 1169.63 1146.55 34.87 o
-3 -3 1 56.11 54.96 10.63 o
-2 -3 1 229.99 233.17 18.47 o
-1 -3 1 454.43 444.14 38.88 o
1 -3 1 64.24 65.54 12.56 o
2 -3 1 2665.45 2824.91 73.76 o
3 -3 1 504.23 532.43 25.48 o
4 -3 1 76.30 80.31 14.43 o
5 -3 1 80.86 71.91 15.33 o
6 -3 1 214.54 208.62 28.00 o
7 -3 1 11.81 -5.05 31.87 o
8 -3 1 177.73 201.25 31.92 o
9 -3 1 35.09 86.02 42.97 o
10 -3 1 11.90 32.69 31.61 o
11 -3 1 9.15 73.32 36.42 o
-12 -2 1 17.70 31.50 56.04 o
-11 -2 1 120.04 179.09 76.79 o
-10 -2 1 17.99 44.05 25.10 o
-9 -2 1 79.80 102.58 63.45 o
-8 -2 1 25.13 0.25 32.85 o
-7 -2 1 36.14 31.75 23.08 o
-6 -2 1 584.76 597.75 35.57 o
-5 -2 1 421.41 335.25 25.18 o
-4 -2 1 580.29 598.76 29.21 o
-3 -2 1 216.38 229.30 13.69 o
-2 -2 1 265.74 286.13 16.98 o
-1 -2 1 62.68 51.50 15.82 o
1 -2 1 1775.23 1875.72 40.17 o
2 -2 1 1422.92 1460.74 34.52 o
3 -2 1 76.92 56.17 10.29 o
4 -2 1 445.26 476.11 18.56 o
5 -2 1 933.89 958.66 27.44 o
6 -2 1 62.21 57.30 14.00 o
7 -2 1 559.00 554.73 39.83 o
8 -2 1 124.09 116.41 35.17 o
9 -2 1 191.64 194.69 44.06 o
10 -2 1 25.09 46.46 52.90 o
11 -2 1 35.54 8.09 30.21 o
-12 -1 1 39.43 27.17 50.99 o
-11 -1 1 14.28 11.15 25.82 o
-10 -1 1 74.43 116.80 43.17 o
-9 -1 1 46.84 48.16 24.05 o
-8 -1 1 294.57 248.33 27.84 o
-7 -1 1 301.61 266.21 37.36 o
-6 -1 1 1456.87 1384.93 40.81 o
-5 -1 1 548.73 564.27 28.38 o
-4 -1 1 3000.90 3004.19 76.32 o
-3 -1 1 91.55 79.06 12.99 o
-2 -1 1 819.96 812.39 26.72 o
-1 -1 1 1053.68 1027.19 27.93 o
0 -1 1 2174.40 2230.76 36.58 o
1 -1 1 1290.49 1305.65 34.49 o
2 -1 1 6290.80 6430.35 103.44 o
3 -1 1 243.27 244.49 12.05 o
4 -1 1 64.19 57.08 10.12 o
5 -1 1 329.49 312.84 15.06 o
6 -1 1 489.29 486.82 19.63 o
7 -1 1 76.93 102.56 17.25 o
8 -1 1 410.76 438.82 33.53 o
9 -1 1 319.69 326.68 32.06 o
10 -1 1 94.15 104.87 26.27 o
11 -1 1 46.30 55.88 47.80 o
12 -1 1 20.29 52.25 32.69 o
-12 0 1 82.61 103.71 28.74 o
-11 0 1 130.64 112.90 32.94 o
-10 0 1 30.84 23.21 32.59 o
-9 0 1 153.16 111.59 22.24 o
-8 0 1 100.92 92.36 51.22 o
-7 0 1 0.12 15.65 16.16 o
-6 0 1 154.10 154.26 21.06 o
-5 0 1 251.72 254.11 15.26 o
-4 0 1 99.14 106.78 11.72 o
-3 0 1 8.66 -1.83 9.11 o
-2 0 1 1218.81 1129.65 24.29 o
-1 0 1 403.78 379.67 7.31 o
0 0 1 388.39 372.29 7.62 o
1 0 1 477.38 424.31 9.77 o
2 0 1 8337.00 8205.74 127.77 o
3 0 1 7067.25 6664.57 106.22 o
4 0 1 66.97 72.48 9.45 o
5 0 1 165.86 148.95 12.36 o
6 0 1 0.14 14.94 10.60 o
7 0 1 122.23 127.39 15.05 o
8 0 1 25.15 48.30 15.19 o
9 0 1 58.42 26.52 19.60 o
10 0 1 62.11 71.88 44.85 o
11 0 1 7.35 14.54 23.58 o
12 0 1 4.72 5.11 28.45 o
-12 1 1 38.26 50.16 54.94 o
-11 1 1 14.37 38.85 25.70 o
-10 1 1 74.16 135.04 26.15 o
-9 1 1 47.62 38.03 22.06 o
-8 1 1 293.35 278.46 30.66 o
-7 1 1 306.11 299.72 21.51 o
-6 1 1 1448.96 1414.33 39.58 o
-5 1 1 554.37 559.91 21.74 o
-4 1 1 2977.70 2895.24 62.26 o
-3 1 1 92.57 69.13 12.02 o
-2 1 1 824.24 799.73 23.46 o
-1 1 1 1038.89 1035.17 20.14 o
0 1 1 2177.82 2231.62 34.02 o
1 1 1 1296.23 1309.34 19.90 o
2 1 1 6257.36 6507.84 101.69 o
3 1 1 247.81 251.68 11.65 o
4 1 1 64.08 52.43 9.62 o
5 1 1 322.35 357.12 15.44 o
6 1 1 489.15 473.92 19.11 o
7 1 1 76.22 120.44 27.32 o
8 1 1 416.95 443.96 31.25 o
9 1 1 316.79 308.74 24.65 o
10 1 1 94.31 61.20 33.34 o
11 1 1 46.72 27.63 27.49 o
12 1 1 20.76 31.45 31.08 o
-12 2 1 16.30 78.26 45.48 o
-11 2 1 120.12 180.05 43.63 o
-10 2 1 18.39 32.58 23.80 o
-9 2 1 79.13 74.23 47.18 o
-8 2 1 24.08 26.57 22.36 o
-7 2 1 36.10 26.30 39.81 o
-6 2 1 584.94 635.74 31.28 o
-5 2 1 421.03 391.39 22.98 o
-4 2 1 576.25 623.99 48.25 o
-3 2 1 219.31 262.20 18.41 o
-2 2 1 256.98 276.97 13.49 o
-1 2 1 66.21 62.30 9.70 o
0 2 1 1825.11 1784.01 42.17 o
1 2 1 1751.40 1929.11 52.61 o
2 2 1 1430.42 1478.09 27.55 o
3 2 1 81.26 75.62 10.51 o
4 2 1 435.38 474.98 17.26 o
5 2 1 939.05 993.71 40.47 o
6 2 1 63.53 58.71 17.68 o
7 2 1 558.52 575.71 24.44 o
8 2 1 125.54 135.77 19.30 o
9 2 1 192.44 222.28 21.57 o
10 2 1 24.18 19.72 27.11 o
11 2 1 36.20 55.63 45.33 o
-11 3 1 10.54 25.16 40.26 o
-10 3 1 133.63 142.13 26.82 o
-9 3 1 7.57 -9.27 27.67 o
-8 3 1 42.09 59.95 24.93 o
-7 3 1 51.42 71.03 25.14 o
-6 3 1 338.92 363.49 28.81 o
-5 3 1 4.27 14.46 18.53 o
-4 3 1 1170.17 1174.67 47.71 o
-3 3 1 51.81 71.97 12.98 o
-2 3 1 229.85 245.90 15.12 o
-1 3 1 453.92 434.38 16.42 o
0 3 1 1097.87 1166.53 46.10 o
1 3 1 62.65 87.36 14.32 o
2 3 1 2668.75 2821.90 57.49 o
3 3 1 522.35 565.88 19.20 o
4 3 1 75.36 105.63 15.61 o
5 3 1 76.82 84.55 14.93 o
6 3 1 216.08 237.70 19.30 o
7 3 1 12.04 60.78 29.14 o
8 3 1 179.39 219.86 27.03 o
9 3 1 35.00 53.35 31.13 o
10 3 1 11.99 74.77 54.97 o
11 3 1 8.91 106.78 61.37 o
-10 4 1 5.16 38.82 54.08 o
-9 4 1 12.35 38.28 29.46 o
-8 4 1 126.42 101.92 21.45 o
-7 4 1 20.00 31.80 18.17 o
-6 4 1 270.34 217.15 21.21 o
-5 4 1 256.96 255.92 21.61 o
-4 4 1 184.61 207.45 18.98 o
-3 4 1 82.84 95.01 16.29 o
-2 4 1 622.28 629.64 24.96 o
-1 4 1 58.28 52.16 12.71 o
0 4 1 192.05 176.97 12.02 o
1 4 1 494.16 492.94 23.48 o
2 4 1 122.49 156.76 22.76 o
3 4 1 51.72 65.50 35.98 o
4 4 1 164.92 151.35 22.15 o
5 4 1 13.73 22.09 26.69 o
6 4 1 79.08 27.83 30.33 o
7 4 1 161.45 140.38 33.09 o
8 4 1 35.40 1.19 48.48 o
-9 5 1 20.29 68.60 49.92 o
-8 5 1 4.30 23.89 29.21 o
-7 5 1 31.35 18.75 24.68 o
-6 5 1 77.80 56.86 27.04 o
-5 5 1 7.23 -0.24 19.32 o
-4 5 1 308.07 249.55 21.38 o
-3 5 1 308.06 255.21 29.48 o
-2 5 1 104.02 97.40 26.15 o
-1 5 1 283.43 276.42 15.49 o
0 5 1 744.27 750.44 24.93 o
1 5 1 37.95 52.38 20.75 o
2 5 1 1090.82 1142.32 50.26 o
3 5 1 174.77 221.35 41.49 o
-6 6 1 25.92 23.01 29.06 o
-5 6 1 517.09 435.87 44.05 o
-4 6 1 78.97 81.87 40.89 o
-3 6 1 121.19 113.14 27.09 o
-2 6 1 12.42 28.00 18.28 o
-1 6 1 150.36 131.91 17.17 o
0 6 1 17.92 56.32 20.98 o
1 6 1 9.66 11.84 30.35 o
2 6 1 79.21 59.41 25.32 o
3 6 1 3.13 14.99 31.39 o
4 6 1 0.18 42.51 32.24 o
5 6 1 13.46 -13.19 36.87 o
6 6 1 84.11 107.92 40.58 o
-2 7 1 37.39 134.88 41.58 o
-1 7 1 165.57 111.30 64.39 o
0 7 1 297.89 272.69 45.69 o
1 7 1 28.16 65.84 40.00 o
2 7 1 453.15 527.91 123.47 o
-2 -7 2 21.15 62.53 28.69 o
-1 -7 2 5.97 -27.31 51.51 o
0 -7 2 165.57 167.80 54.88 o
1 -7 2 99.41 87.39 52.79 o
-4 -6 2 202.13 234.99 67.93 o
-3 -6 2 34.86 -25.22 50.36 o
-2 -6 2 239.33 220.88 59.89 o
-1 -6 2 81.09 53.25 22.64 o
0 -6 2 23.76 12.81 31.38 o
1 -6 2 71.22 76.57 35.47 o
2 -6 2 17.25 65.14 67.68 o
3 -6 2 15.58 -30.41 43.39 o
4 -6 2 79.47 49.51 31.46 o
5 -6 2 88.81 61.83 52.26 o
6 -6 2 4.92 65.38 67.37 o
-8 -5 2 13.54 3.43 38.85 o
-7 -5 2 2.10 -12.04 34.97 o
-6 -5 2 4.27 -32.54 32.54 o
-5 -5 2 37.67 87.99 32.76 o
-4 -5 2 48.24 43.04 38.39 o
-1 -5 2 69.32 65.64 23.99 o
0 -5 2 396.02 361.69 25.81 o
1 -5 2 51.99 119.54 35.45 o
2 -5 2 21.67 91.36 37.54 o
3 -5 2 696.74 701.57 83.83 o
4 -5 2 153.18 149.06 46.90 o
5 -5 2 13.68 43.03 55.04 o
7 -5 2 87.45 125.91 42.85 o
8 -5 2 14.95 72.30 45.56 o
-10 -4 2 106.55 155.96 38.65 o
-9 -4 2 14.20 14.06 38.93 o
-8 -4 2 67.97 56.24 34.13 o
-7 -4 2 53.35 54.93 43.20 o
-6 -4 2 5.18 -16.29 27.30 o
-5 -4 2 114.23 156.13 46.58 o
-4 -4 2 1644.09 1753.98 61.67 o
-3 -4 2 20.60 28.31 21.56 o
-2 -4 2 306.10 362.84 26.66 o
-1 -4 2 216.69 261.06 46.53 o
1 -4 2 213.90 234.48 31.35 o
2 -4 2 178.32 187.87 21.17 o
3 -4 2 170.89 174.48 22.62 o
4 -4 2 429.00 455.65 43.47 o
5 -4 2 49.04 54.17 39.61 o
6 -4 2 21.29 67.63 46.49 o
7 -4 2 13.10 19.59 25.40 o
8 -4 2 89.00 129.20 34.27 o
9 -4 2 39.25 79.94 33.71 o
10 -4 2 13.15 -6.75 34.71 o
-11 -3 2 18.30 42.52 65.88 o
-10 -3 2 30.09 41.27 47.49 o
-9 -3 2 172.03 125.47 30.83 o
-8 -3 2 64.33 100.38 35.63 o
-7 -3 2 37.24 45.57 28.01 o
-6 -3 2 740.50 769.11 47.70 o
-5 -3 2 334.88 357.31 29.97 o
-4 -3 2 64.96 58.64 22.36 o
-3 -3 2 883.26 916.89 32.96 o
-2 -3 2 908.47 940.28 35.78 o
-1 -3 2 257.17 298.74 21.16 o
0 -3 2 321.11 346.14 15.60 o
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