#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/45/2014587.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2014587_Fobs
loop_
_publ_author_name
'Blewett, Gavin'
'Esterhuysen, Catharine'
'Bredenkamp, Martin W.'
'Koch, Klaus R.'
_publ_section_title
;
The first bipodal thiocarbamic acid ester, O,O'-diethyl
N,N'-(p-phenylenedicarbonyl)bis(thiocarbamate)
;
_journal_issue 12
_journal_name_full 'Acta Crystallographica Section C'
_journal_page_first o862
_journal_page_last o864
_journal_volume 60
_journal_year 2004
_space_group_IT_number 96
_symmetry_space_group_name_Hall 'P 4nw 2abw'
_symmetry_space_group_name_H-M 'P 43 21 2'
_cell_angle_alpha 90.000
_cell_angle_beta 90.000
_cell_angle_gamma 90.000
_cell_length_a 10.5794
_cell_length_b 10.5794
_cell_length_c 14.0773
_exptl_crystal_F_000 712.00
_reflns_d_resolution_high 0.8114
_[local]_cod_data_source_file ta1474Isup2.hkl
_[local]_cod_data_source_block I
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' c:\crystest2\w001m in P4(3)2(1)2'
_shelx_refln_list_code 4
_shelx_f_calc_maximum 264.18
_shelx_f_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y+1/2, x+1/2, z+3/4'
'-x, -y, z+1/2'
'y+1/2, -x+1/2, z+1/4'
'x+1/2, -y+1/2, -z+1/4'
'-x+1/2, y+1/2, -z+3/4'
'y, x, -z'
'-y, -x, -z+1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 1 0 1447.04 1508.90 19.22 o
0 2 0 270.39 233.67 4.66 o
1 2 0 1472.35 1756.95 15.22 o
2 2 0 69791.47 78396.94 907.46 o
1 3 0 1322.73 1344.05 12.75 o
2 3 0 2889.68 3581.62 30.23 o
3 3 0 6137.60 7021.70 80.44 o
0 4 0 534.44 387.57 7.91 o
1 4 0 7.24 4.90 2.59 o
2 4 0 985.96 920.86 10.42 o
3 4 0 743.54 942.39 11.04 o
4 4 0 7547.29 7761.19 89.97 o
1 5 0 1456.35 1470.81 16.15 o
2 5 0 15.31 7.59 2.29 o
3 5 0 62.90 45.89 3.28 o
4 5 0 1381.46 1461.56 16.04 o
5 5 0 5501.43 5776.39 70.31 o
0 6 0 4631.76 4481.64 54.42 o
1 6 0 720.39 779.50 10.42 o
2 6 0 151.68 191.11 5.45 o
3 6 0 54.45 66.67 4.16 o
4 6 0 259.10 253.38 6.83 o
5 6 0 79.89 92.40 5.22 o
6 6 0 1072.14 1084.18 22.39 o
1 7 0 648.59 590.96 10.55 o
2 7 0 2.36 3.40 3.08 o
3 7 0 1662.87 1642.31 19.81 o
4 7 0 204.81 208.99 7.13 o
5 7 0 88.15 97.38 6.19 o
6 7 0 1976.68 1924.24 26.90 o
7 7 0 1663.08 1550.86 35.58 o
0 8 0 681.94 665.73 17.74 o
1 8 0 178.16 193.14 7.49 o
2 8 0 1340.78 1280.85 19.58 o
3 8 0 14.65 12.40 5.03 o
4 8 0 35.80 34.65 5.92 o
5 8 0 499.98 497.19 14.82 o
6 8 0 298.48 298.25 11.42 o
7 8 0 42.04 47.09 7.47 o
8 8 0 0.17 17.81 10.34 o
1 9 0 755.83 675.29 14.55 o
2 9 0 9.00 20.48 5.50 o
3 9 0 198.85 192.90 9.25 o
4 9 0 224.18 241.86 10.23 o
5 9 0 322.67 322.54 12.22 o
6 9 0 85.83 91.70 9.11 o
7 9 0 9.72 20.39 7.78 o
8 9 0 293.52 292.15 15.83 o
9 9 0 76.48 49.71 15.98 o
0 10 0 206.52 227.66 16.27 o
1 10 0 14.08 6.16 5.93 o
2 10 0 165.20 155.47 9.03 o
3 10 0 0.48 -2.77 5.35 o
4 10 0 1130.40 1108.02 21.91 o
5 10 0 22.60 29.93 7.43 o
6 10 0 207.15 208.18 14.73 o
7 10 0 4.93 20.82 8.51 o
8 10 0 61.37 53.45 10.71 o
1 11 0 65.79 60.42 7.97 o
2 11 0 74.19 68.93 8.93 o
3 11 0 40.75 43.24 7.77 o
4 11 0 135.30 136.06 10.85 o
5 11 0 122.40 142.13 11.30 o
6 11 0 6.17 30.35 8.68 o
7 11 0 18.95 32.41 9.20 o
0 12 0 17.31 15.13 12.31 o
1 12 0 21.93 26.81 9.00 o
2 12 0 399.85 422.01 18.17 o
3 12 0 3.93 -0.29 7.90 o
4 12 0 253.16 225.90 15.86 o
5 12 0 40.44 23.52 14.36 o
1 13 0 181.90 190.68 14.10 o
0 1 1 2355.62 2338.07 20.24 o
1 1 1 3274.13 4043.26 32.11 o
-1 2 1 3981.23 4234.12 31.67 o
0 2 1 158.09 215.46 3.76 o
1 2 1 3857.66 4103.68 36.14 o
2 2 1 4524.95 4930.13 39.92 o
-2 3 1 4171.73 4510.40 37.33 o
-1 3 1 6303.54 6801.41 56.00 o
0 3 1 39.48 52.02 2.81 o
1 3 1 6306.31 6804.85 58.10 o
2 3 1 4219.63 4532.90 37.51 o
3 3 1 4533.50 4879.28 40.63 o
-3 4 1 2388.56 2646.24 23.82 o
-2 4 1 2818.66 3087.09 26.03 o
-1 4 1 2698.17 2624.90 23.16 o
0 4 1 957.87 823.42 9.59 o
1 4 1 2686.22 2632.90 24.06 o
2 4 1 2820.51 3059.23 27.97 o
3 4 1 2304.96 2562.16 23.85 o
4 4 1 786.70 823.80 10.56 o
-4 5 1 1922.17 1924.02 19.57 o
-3 5 1 274.62 328.45 6.31 o
-2 5 1 19.57 20.13 2.59 o
-1 5 1 807.66 874.82 10.11 o
0 5 1 7.82 5.68 2.25 o
1 5 1 811.54 862.66 10.62 o
2 5 1 21.55 23.95 2.80 o
3 5 1 276.94 323.68 6.49 o
4 5 1 1951.13 1914.24 19.66 o
5 5 1 1809.82 1928.38 20.21 o
-5 6 1 428.21 397.21 9.28 o
-4 6 1 520.64 543.19 10.32 o
-3 6 1 991.89 956.64 12.49 o
-2 6 1 364.32 361.89 6.92 o
-1 6 1 1487.13 1338.00 14.27 o
0 6 1 449.13 464.07 7.44 o
1 6 1 1464.72 1317.38 14.94 o
2 6 1 359.28 346.42 6.96 o
3 6 1 959.64 909.97 11.94 o
4 6 1 522.00 542.19 9.18 o
5 6 1 412.59 382.12 8.64 o
6 6 1 207.12 227.17 8.11 o
-6 7 1 432.78 403.39 11.18 o
-5 7 1 11.83 11.81 4.35 o
-4 7 1 2145.98 1983.19 24.28 o
-3 7 1 60.78 70.83 5.30 o
-2 7 1 848.16 772.48 13.38 o
-1 7 1 325.28 330.41 9.59 o
0 7 1 52.44 78.08 4.84 o
1 7 1 321.39 332.35 7.95 o
2 7 1 857.45 786.74 11.53 o
3 7 1 62.75 71.24 4.64 o
4 7 1 2174.82 2056.64 22.71 o
5 7 1 12.22 17.85 4.06 o
6 7 1 430.57 415.96 10.69 o
7 7 1 1.20 10.53 5.32 o
-7 8 1 102.09 112.33 8.63 o
-6 8 1 434.83 418.56 13.37 o
-5 8 1 165.08 164.22 8.71 o
-4 8 1 89.35 92.87 7.10 o
-3 8 1 1365.42 1266.39 34.33 o
-2 8 1 72.49 84.56 6.37 o
-1 8 1 222.11 208.62 7.74 o
0 8 1 173.66 179.22 7.30 o
1 8 1 214.98 185.90 8.65 o
2 8 1 73.81 90.82 6.72 o
3 8 1 1368.18 1289.23 21.35 o
4 8 1 88.66 80.98 7.25 o
5 8 1 168.85 167.45 8.03 o
6 8 1 437.16 415.73 12.94 o
7 8 1 110.31 96.16 8.22 o
8 8 1 196.77 191.48 11.35 o
-8 9 1 97.84 120.02 11.11 o
-7 9 1 3.90 16.09 7.53 o
-6 9 1 352.83 399.44 14.59 o
-5 9 1 294.01 271.06 11.03 o
-4 9 1 568.87 532.94 13.95 o
-3 9 1 148.04 144.74 8.41 o
-2 9 1 1141.95 1064.37 19.22 o
-1 9 1 17.30 15.47 4.82 o
0 9 1 746.61 689.80 14.70 o
1 9 1 18.40 11.68 5.26 o
2 9 1 1181.87 1130.90 22.14 o
3 9 1 147.33 167.02 9.25 o
4 9 1 570.41 558.24 15.90 o
5 9 1 298.58 294.40 12.69 o
6 9 1 357.85 393.25 14.50 o
7 9 1 3.56 0.07 7.10 o
8 9 1 99.18 119.68 11.71 o
9 9 1 106.25 94.77 12.74 o
-8 10 1 7.97 23.34 8.51 o
-7 10 1 35.00 36.78 8.98 o
-6 10 1 5.82 3.42 7.00 o
-5 10 1 6.51 8.76 6.68 o
-4 10 1 49.75 46.25 7.10 o
-3 10 1 153.38 148.55 9.61 o
-2 10 1 0.87 3.15 5.61 o
-1 10 1 288.87 282.58 11.77 o
0 10 1 82.48 77.47 7.84 o
1 10 1 297.06 298.03 11.23 o
2 10 1 0.97 5.88 5.87 o
3 10 1 157.28 171.48 9.70 o
4 10 1 51.11 37.08 7.16 o
5 10 1 6.74 23.15 7.33 o
6 10 1 6.16 3.43 8.25 o
7 10 1 33.21 25.29 8.70 o
8 10 1 8.66 9.64 8.98 o
-6 11 1 230.95 250.87 15.87 o
-5 11 1 7.08 5.34 9.00 o
-4 11 1 177.17 220.30 16.32 o
-3 11 1 463.26 383.47 17.97 o
-2 11 1 450.64 432.34 15.93 o
-1 11 1 98.27 111.81 12.18 o
0 11 1 16.07 20.06 7.37 o
1 11 1 98.47 102.69 9.44 o
2 11 1 448.44 430.64 15.93 o
3 11 1 470.12 410.19 13.90 o
4 11 1 188.32 219.69 12.01 o
5 11 1 7.22 15.34 8.23 o
6 11 1 230.88 259.33 15.04 o
-5 12 1 100.75 109.81 13.84 o
-4 12 1 16.71 13.75 9.38 o
-3 12 1 19.04 34.24 9.45 o
-2 12 1 73.44 66.67 9.93 o
-1 12 1 222.56 211.80 13.02 o
0 12 1 15.70 30.97 8.14 o
1 12 1 219.91 234.46 13.45 o
2 12 1 72.42 77.41 9.80 o
3 12 1 18.15 32.02 8.41 o
4 12 1 16.76 13.34 8.14 o
5 12 1 101.78 124.92 12.30 o
0 13 1 202.47 169.30 13.51 o
0 1 2 5051.44 6387.70 51.77 o
1 1 2 149.89 198.72 3.26 o
-1 2 2 5349.06 5892.77 45.43 o
0 2 2 256.71 194.05 3.43 o
1 2 2 5359.33 5905.37 50.45 o
2 2 2 1775.00 2462.43 21.33 o
-2 3 2 425.55 482.07 6.24 o
-1 3 2 6032.62 6347.33 50.76 o
0 3 2 2084.46 2146.30 19.61 o
1 3 2 6000.08 6338.91 59.20 o
2 3 2 411.61 475.30 7.33 o
3 3 2 113.75 100.48 3.57 o
-3 4 2 1187.64 1273.60 13.62 o
-2 4 2 1690.45 1738.87 16.14 o
-1 4 2 978.70 1003.47 10.75 o
0 4 2 245.47 204.24 4.76 o
1 4 2 971.12 974.48 11.60 o
2 4 2 1641.01 1698.16 18.06 o
3 4 2 1183.94 1297.34 13.92 o
4 4 2 0.01 17.97 2.88 o
-4 5 2 622.28 683.05 9.78 o
-3 5 2 4403.71 4165.97 37.58 o
-2 5 2 205.07 255.56 5.74 o
-1 5 2 2599.60 2670.50 25.18 o
0 5 2 922.35 813.79 10.74 o
1 5 2 2639.47 2671.41 26.24 o
2 5 2 204.37 250.39 6.40 o
3 5 2 4378.04 4155.98 36.67 o
4 5 2 615.51 670.57 9.89 o
5 5 2 2817.00 2774.27 26.79 o
-5 6 2 70.34 81.43 5.27 o
-4 6 2 738.56 739.14 11.56 o
-3 6 2 226.59 248.04 6.28 o
-2 6 2 941.36 870.25 11.04 o
-1 6 2 1159.92 1219.26 14.06 o
0 6 2 740.30 736.96 10.59 o
1 6 2 1152.48 1217.88 16.29 o
2 6 2 926.32 840.54 12.02 o
3 6 2 223.27 222.75 9.20 o
4 6 2 734.14 682.59 10.62 o
5 6 2 71.18 83.88 4.97 o
6 6 2 773.58 775.96 13.13 o
-6 7 2 371.15 339.03 11.07 o
-5 7 2 1513.01 1400.27 21.42 o
-4 7 2 549.49 537.14 11.58 o
-3 7 2 161.21 144.26 7.18 o
-2 7 2 31.46 34.42 4.24 o
-1 7 2 1413.17 1338.66 17.57 o
0 7 2 688.95 627.17 11.22 o
1 7 2 1389.89 1326.25 16.55 o
2 7 2 31.61 29.70 4.03 o
3 7 2 159.49 161.14 6.14 o
4 7 2 545.30 535.33 10.31 o
5 7 2 1500.01 1370.81 21.19 o
6 7 2 367.37 352.39 10.15 o
7 7 2 274.11 292.28 10.88 o
-7 8 2 204.63 217.88 11.48 o
-6 8 2 144.85 149.71 9.34 o
-5 8 2 136.05 128.57 8.14 o
-4 8 2 504.07 507.13 12.97 o
-3 8 2 2.75 18.25 4.73 o
-2 8 2 153.16 171.44 7.50 o
-1 8 2 81.12 94.96 5.61 o
0 8 2 2093.50 1893.47 25.84 o
1 8 2 83.07 97.64 6.57 o
2 8 2 152.85 160.94 7.60 o
3 8 2 3.51 11.24 4.81 o
4 8 2 526.08 534.91 11.30 o
5 8 2 137.40 128.53 7.71 o
6 8 2 154.45 165.03 9.53 o
7 8 2 198.64 192.25 10.34 o
8 8 2 47.12 56.59 8.75 o
-8 9 2 262.51 206.84 13.15 o
-7 9 2 451.82 446.07 15.76 o
-6 9 2 59.05 90.14 8.57 o
-5 9 2 74.49 71.28 8.81 o
-4 9 2 10.68 9.21 5.37 o
-3 9 2 375.81 363.51 13.54 o
-2 9 2 917.33 814.96 22.65 o
-1 9 2 53.24 47.55 5.92 o
0 9 2 39.69 45.27 5.97 o
1 9 2 53.14 62.11 7.43 o
2 9 2 915.54 866.61 19.45 o
3 9 2 370.46 374.74 11.38 o
4 9 2 10.98 4.40 5.74 o
5 9 2 72.10 71.24 8.43 o
6 9 2 62.02 82.08 9.68 o
7 9 2 449.03 455.29 17.09 o
8 9 2 260.21 220.23 14.70 o
9 9 2 322.40 305.46 22.94 o
-8 10 2 112.11 129.21 13.67 o
-7 10 2 9.35 10.61 8.40 o
-6 10 2 137.38 148.40 12.41 o
-5 10 2 103.68 104.03 9.62 o
-4 10 2 8.82 2.89 7.06 o
-3 10 2 57.39 58.27 8.89 o
-2 10 2 697.78 634.78 17.84 o
-1 10 2 14.63 11.84 6.35 o
0 10 2 645.78 570.87 17.76 o
1 10 2 15.16 11.23 5.96 o
2 10 2 704.91 660.47 16.70 o
3 10 2 57.58 62.54 7.34 o
4 10 2 10.86 10.03 6.41 o
5 10 2 100.37 91.07 10.98 o
6 10 2 140.03 159.47 12.24 o
7 10 2 9.73 9.60 8.14 o
8 10 2 113.24 131.31 12.98 o
-6 11 2 8.70 23.50 9.64 o
-5 11 2 110.16 111.66 13.66 o
-4 11 2 19.08 29.30 8.69 o
-3 11 2 127.77 149.09 12.11 o
-2 11 2 63.90 73.21 8.92 o
-1 11 2 5.37 8.61 6.97 o
0 11 2 254.31 264.80 14.97 o
1 11 2 5.30 18.29 7.44 o
2 11 2 63.27 57.55 8.08 o
3 11 2 124.11 143.03 10.36 o
4 11 2 20.27 34.23 7.86 o
5 11 2 111.89 128.38 11.19 o
6 11 2 8.89 4.45 8.69 o
-4 12 2 406.56 419.86 18.48 o
-3 12 2 71.46 78.90 12.67 o
-2 12 2 13.50 20.27 8.09 o
-1 12 2 56.13 60.35 9.31 o
0 12 2 60.76 86.82 9.95 o
1 12 2 54.55 55.09 9.10 o
2 12 2 13.99 15.43 8.52 o
3 12 2 69.69 56.21 9.29 o
4 12 2 402.34 399.36 16.85 o
0 1 3 2094.02 2542.40 22.95 o
1 1 3 1821.65 2153.41 19.02 o
-1 2 3 4101.97 4474.59 36.40 o
0 2 3 191.34 140.64 3.52 o
1 2 3 4112.71 4478.53 39.28 o
2 2 3 2130.37 2405.98 21.95 o
-2 3 3 661.09 725.22 8.47 o
-1 3 3 415.81 459.14 5.72 o
0 3 3 2903.45 3009.99 26.68 o
1 3 3 408.27 441.83 7.46 o
2 3 3 674.78 738.58 9.52 o
3 3 3 3715.54 4190.09 35.67 o
-3 4 3 1753.63 1700.96 16.94 o
-2 4 3 1918.99 1991.04 18.88 o
-1 4 3 1724.42 1699.72 16.46 o
0 4 3 730.74 732.32 9.07 o
1 4 3 1708.20 1688.13 19.44 o
2 4 3 1926.48 1975.37 20.50 o
3 4 3 1737.60 1704.84 17.29 o
4 4 3 127.64 121.70 4.37 o
-4 5 3 244.48 223.36 6.00 o
-3 5 3 44.48 57.93 3.25 o
-2 5 3 1198.51 1214.10 13.76 o
-1 5 3 2300.70 2499.83 24.16 o
0 5 3 47.90 84.74 3.80 o
1 5 3 2312.04 2512.56 26.18 o
2 5 3 1197.23 1197.96 14.73 o
3 5 3 42.98 54.31 3.69 o
4 5 3 247.53 212.36 5.89 o
5 5 3 3.60 9.74 3.31 o
-5 6 3 1685.29 1667.14 26.87 o
-4 6 3 133.67 141.95 6.20 o
-3 6 3 407.93 365.04 8.29 o
-2 6 3 417.19 421.77 8.26 o
-1 6 3 577.80 554.17 8.62 o
0 6 3 305.55 307.17 6.81 o
1 6 3 565.05 527.13 9.68 o
2 6 3 424.81 418.31 9.37 o
3 6 3 393.37 348.06 7.68 o
4 6 3 130.27 138.12 5.44 o
5 6 3 1689.85 1667.62 20.39 o
6 6 3 10.95 21.98 4.71 o
-6 7 3 592.54 546.73 13.87 o
-5 7 3 598.66 589.40 14.30 o
-4 7 3 1373.70 1337.51 19.45 o
-3 7 3 76.18 88.70 7.64 o
-2 7 3 431.02 416.97 9.27 o
-1 7 3 1408.41 1329.43 18.22 o
0 7 3 473.77 415.04 9.89 o
1 7 3 1398.02 1301.51 17.50 o
2 7 3 422.87 386.09 9.21 o
3 7 3 78.57 86.12 5.33 o
4 7 3 1362.26 1343.76 18.08 o
5 7 3 606.31 573.98 12.09 o
6 7 3 595.32 555.24 16.55 o
7 7 3 61.96 69.77 7.08 o
-7 8 3 70.18 76.80 8.15 o
-6 8 3 270.78 253.47 11.30 o
-5 8 3 123.94 122.29 8.40 o
-4 8 3 439.11 424.17 11.90 o
-3 8 3 1373.98 1354.52 29.12 o
-2 8 3 101.22 119.75 6.23 o
-1 8 3 358.27 321.24 9.28 o
0 8 3 16.69 18.37 4.43 o
1 8 3 341.61 301.03 9.11 o
2 8 3 97.07 98.55 6.58 o
3 8 3 1359.53 1364.53 19.47 o
4 8 3 434.68 422.47 10.28 o
5 8 3 128.08 132.04 7.42 o
6 8 3 269.31 248.61 10.48 o
7 8 3 69.72 88.55 8.68 o
8 8 3 482.00 456.52 17.04 o
-8 9 3 279.87 305.66 17.67 o
-7 9 3 0.58 3.46 7.41 o
-6 9 3 434.20 439.41 22.40 o
-5 9 3 26.44 25.52 6.78 o
-4 9 3 661.39 662.06 17.53 o
-3 9 3 427.63 416.91 15.51 o
-2 9 3 805.52 767.88 18.42 o
-1 9 3 202.56 203.48 10.84 o
0 9 3 1631.03 1546.22 28.99 o
1 9 3 199.63 196.34 10.40 o
2 9 3 813.87 768.53 16.46 o
3 9 3 430.25 431.30 12.78 o
4 9 3 661.21 664.42 15.65 o
5 9 3 26.21 25.71 7.13 o
6 9 3 435.19 422.06 21.44 o
7 9 3 0.66 11.32 8.37 o
8 9 3 283.77 340.53 18.80 o
9 9 3 25.22 27.66 12.74 o
-8 10 3 39.87 50.24 10.87 o
-7 10 3 89.76 125.95 12.20 o
-6 10 3 70.07 91.75 12.65 o
-5 10 3 9.14 9.49 7.52 o
-4 10 3 55.48 56.78 8.80 o
-3 10 3 30.40 38.35 8.36 o
-2 10 3 317.47 329.51 14.97 o
-1 10 3 833.13 780.91 19.41 o
0 10 3 5.38 22.29 6.61 o
1 10 3 822.74 795.90 17.35 o
2 10 3 312.51 300.65 12.15 o
3 10 3 28.32 24.53 7.22 o
4 10 3 54.48 63.47 8.11 o
5 10 3 8.51 2.29 6.98 o
6 10 3 71.64 88.16 10.94 o
7 10 3 90.11 122.01 12.83 o
8 10 3 41.25 48.54 17.64 o
-6 11 3 287.31 285.13 18.06 o
-5 11 3 209.17 226.68 14.19 o
-4 11 3 396.85 328.81 16.92 o
-3 11 3 70.44 79.53 10.25 o
-2 11 3 853.24 817.40 22.73 o
-1 11 3 287.41 269.53 13.65 o
0 11 3 894.48 843.55 27.38 o
1 11 3 295.23 296.70 14.91 o
2 11 3 854.81 848.69 26.72 o
3 11 3 71.12 96.17 9.33 o
4 11 3 410.76 406.28 21.85 o
5 11 3 205.05 204.99 13.04 o
6 11 3 283.74 320.61 16.53 o
-4 12 3 9.56 12.23 8.59 o
-3 12 3 157.90 163.21 13.15 o
-2 12 3 30.32 23.69 8.54 o
-1 12 3 330.41 325.68 15.46 o
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1 8 13 12.33 15.61 7.01 o
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1 1 14 134.95 139.35 8.68 o
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1 2 14 404.92 350.00 13.98 o
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1 3 14 127.22 139.62 9.17 o
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0 6 14 42.48 34.19 7.71 o
1 6 14 160.09 157.53 10.66 o
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3 6 14 90.15 99.49 10.98 o
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1 7 14 139.45 154.79 10.95 o
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1 1 15 1026.46 1087.99 22.37 o
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1 2 15 69.02 61.60 7.87 o
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-1 3 15 324.26 360.91 15.32 o
0 3 15 154.92 167.46 10.72 o
1 3 15 320.50 343.14 14.05 o
2 3 15 1.06 10.32 6.52 o
3 3 15 411.70 474.50 17.48 o
-3 4 15 43.59 56.51 10.12 o
-2 4 15 176.33 187.91 13.67 o
-1 4 15 154.58 140.38 11.06 o
0 4 15 230.98 232.39 13.75 o
1 4 15 153.38 135.23 10.92 o
2 4 15 173.76 189.82 13.20 o
3 4 15 42.99 44.24 8.61 o
4 4 15 894.95 920.00 36.35 o
-4 5 15 1.21 2.93 8.64 o
-3 5 15 154.13 170.94 14.80 o
-2 5 15 20.18 26.40 9.08 o
-1 5 15 226.20 262.16 17.16 o
0 5 15 4.62 4.12 7.39 o
1 5 15 226.04 228.77 13.20 o
2 5 15 20.51 17.30 7.83 o
3 5 15 149.15 168.24 14.43 o
4 5 15 1.43 1.35 7.93 o
-2 6 15 202.92 241.10 15.99 o
-1 6 15 27.14 31.00 8.75 o
0 6 15 158.73 167.25 12.85 o
1 6 15 26.60 25.27 7.79 o
2 6 15 207.37 227.62 14.94 o
0 0 16 418.84 453.23 34.14 o
0 1 16 203.05 226.32 12.77 o
1 1 16 44.50 33.10 7.86 o
-1 2 16 435.52 467.51 20.12 o
0 2 16 9.37 7.17 6.47 o
1 2 16 440.46 490.50 16.68 o
2 2 16 61.80 78.30 9.64 o
-2 3 16 39.69 40.56 8.66 o
-1 3 16 1.89 7.24 7.13 o
0 3 16 508.05 583.74 20.55 o
1 3 16 1.80 7.90 5.93 o
2 3 16 39.79 55.52 8.56 o
3 3 16 132.34 132.69 13.02 o
-3 4 16 200.94 225.22 15.35 o
-2 4 16 58.04 70.78 11.29 o
-1 4 16 5.25 9.21 8.44 o
0 4 16 4.83 12.53 7.97 o
1 4 16 5.18 12.17 7.08 o
2 4 16 58.97 58.76 9.26 o
3 4 16 203.29 251.14 17.23 o
0 5 16 13.08 16.95 8.40 o
0 1 17 4.04 8.18 8.00 o
1 1 17 0.26 6.88 8.67 o
-1 2 17 9.41 11.88 8.23 o
0 2 17 134.52 167.69 12.97 o
1 2 17 10.67 17.24 7.34 o