#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014588.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014588_Fobs loop_ _publ_author_name 'Hu, Mao-Lin' 'Cai, Xiao-Qing' 'Shi, Qian' 'Cheng, Ya-Qian' _publ_section_title ; catena-Poly[[chloro(1,10-phenanthroline-\k^2^N,N')copper(II)]-\m-imidazolato-\k^2^N:N'] ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m575 _journal_page_last m577 _journal_volume 60 _journal_year 2004 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.5540 _cell_length_b 15.4561 _cell_length_c 18.4412 _exptl_crystal_F_000 1400.00 _reflns_d_resolution_high 0.8348 _[local]_cod_data_source_file ta1475Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' h in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 501.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10002.90 11167.06 240.48 o 4 0 0 30815.62 33337.36 709.29 o 6 0 0 3152.29 3373.41 87.92 o 8 0 0 3245.54 3362.84 118.69 o 10 0 0 7940.73 8321.92 334.81 o 2 1 0 3807.83 4097.97 59.56 o 4 1 0 30464.19 31720.46 477.43 o 6 1 0 16689.02 17176.72 266.54 o 8 1 0 8730.28 8992.34 187.25 o 10 1 0 2411.61 2602.72 111.01 o 0 2 0 738.67 755.70 26.41 o 2 2 0 14381.40 15920.01 240.43 o 4 2 0 5047.35 5539.86 90.31 o 6 2 0 1266.37 1312.91 31.70 o 8 2 0 15.13 17.75 15.36 o 10 2 0 280.54 271.63 40.36 o 2 3 0 1175.20 1205.25 25.75 o 4 3 0 607.82 759.85 17.73 o 6 3 0 1679.31 1670.46 40.49 o 8 3 0 1454.07 1370.55 69.99 o 10 3 0 1946.24 1780.52 88.56 o 0 4 0 251433.30 236059.14 6071.65 o 2 4 0 5854.61 5574.28 110.10 o 4 4 0 15399.58 16102.40 246.83 o 6 4 0 745.93 661.72 25.58 o 8 4 0 79.82 95.37 28.69 o 10 4 0 1148.10 1255.88 75.11 o 2 5 0 2119.14 2031.70 47.09 o 4 5 0 5354.34 5555.75 91.07 o 6 5 0 1649.63 1581.54 49.49 o 8 5 0 2679.23 2754.70 146.22 o 10 5 0 1008.53 1062.88 85.43 o 0 6 0 155.92 133.18 11.34 o 2 6 0 1457.10 1382.88 36.85 o 4 6 0 2817.08 3254.15 56.83 o 6 6 0 32.03 43.10 11.84 o 8 6 0 257.79 299.38 39.62 o 10 6 0 604.24 618.77 79.95 o 2 7 0 5166.02 5150.53 106.22 o 4 7 0 867.46 703.68 35.03 o 6 7 0 8444.64 8378.36 151.99 o 8 7 0 3205.19 3001.06 120.05 o 10 7 0 1444.23 1468.67 86.30 o 0 8 0 37634.02 40052.46 850.66 o 2 8 0 5847.23 5318.36 110.78 o 4 8 0 15500.76 16586.40 318.34 o 6 8 0 225.10 226.31 21.21 o 8 8 0 406.49 521.92 50.97 o 10 8 0 321.37 381.12 50.13 o 2 9 0 6072.60 6265.73 129.59 o 4 9 0 2266.78 2083.90 96.82 o 6 9 0 1689.88 1694.04 52.52 o 8 9 0 3227.54 3183.13 129.21 o 10 9 0 472.52 465.44 78.05 o 0 10 0 2453.03 2622.09 70.38 o 2 10 0 2431.74 2460.81 61.60 o 4 10 0 418.93 393.96 24.27 o 6 10 0 247.59 256.26 28.62 o 8 10 0 250.99 307.76 64.61 o 2 11 0 5761.24 5682.58 121.97 o 4 11 0 1990.02 1733.56 52.73 o 6 11 0 5839.73 5893.43 132.91 o 8 11 0 4255.93 4005.61 153.68 o 0 12 0 3513.32 3409.93 166.57 o 2 12 0 10031.73 9987.80 201.67 o 4 12 0 8690.27 8541.47 178.60 o 6 12 0 179.13 162.00 21.69 o 8 12 0 127.67 172.65 53.30 o 2 13 0 2688.39 2710.77 71.27 o 4 13 0 3031.70 2950.13 78.19 o 6 13 0 3276.20 3115.18 84.73 o 8 13 0 1949.40 1960.00 212.97 o 0 14 0 3102.26 3196.72 168.00 o 2 14 0 2645.85 2559.89 81.35 o 4 14 0 265.05 288.53 28.27 o 6 14 0 3.90 -14.70 14.70 o 2 15 0 88.58 137.23 30.50 o 4 15 0 6.33 -13.72 15.68 o 6 15 0 257.86 261.01 39.36 o 0 16 0 323.26 527.79 68.77 o 2 16 0 13.29 10.25 22.97 o 4 16 0 1152.32 1221.39 70.32 o 2 17 0 48.69 112.83 31.84 o 4 17 0 3.34 -1.25 24.07 o 0 18 0 176.51 269.13 63.06 o 2 18 0 0.39 -10.71 25.27 o 1 1 1 11618.69 12407.79 137.48 o 2 1 1 630.27 628.79 9.70 o 3 1 1 3120.83 3152.04 37.49 o 4 1 1 2568.80 2529.93 32.25 o 5 1 1 5295.34 5355.28 63.30 o 6 1 1 2618.38 2572.63 35.70 o 7 1 1 2039.93 2018.46 35.42 o 8 1 1 3348.93 3363.54 59.24 o 9 1 1 389.01 417.59 20.21 o 10 1 1 791.22 880.54 42.45 o 11 1 1 302.15 298.08 35.03 o 0 2 1 64992.07 64852.31 972.44 o 1 2 1 46185.21 49826.24 641.89 o 2 2 1 3494.78 3333.22 39.89 o 3 2 1 1450.23 1396.53 18.28 o 4 2 1 3817.39 3537.54 42.90 o 5 2 1 9457.96 10606.63 118.33 o 6 2 1 3717.05 3804.89 48.59 o 7 2 1 56.79 44.21 9.11 o 8 2 1 46.58 67.86 12.13 o 9 2 1 77.63 67.95 19.14 o 10 2 1 2036.86 2052.05 66.48 o 11 2 1 380.34 426.16 34.42 o 1 3 1 54.02 72.87 4.73 o 2 3 1 50.69 65.43 3.61 o 3 3 1 365.35 313.41 8.50 o 4 3 1 238.89 190.83 6.36 o 5 3 1 1680.72 1749.72 25.49 o 6 3 1 2339.60 2167.26 31.31 o 7 3 1 739.58 772.31 26.29 o 8 3 1 1126.98 1136.46 35.00 o 9 3 1 386.06 418.49 30.94 o 10 3 1 1429.05 1423.93 75.28 o 11 3 1 692.82 734.53 42.96 o 0 4 1 47090.38 51208.70 762.75 o 1 4 1 15652.98 16589.76 204.47 o 2 4 1 1405.41 1379.80 22.31 o 3 4 1 289.00 272.35 8.03 o 4 4 1 1074.85 1214.99 18.01 o 5 4 1 35.69 32.78 5.10 o 6 4 1 782.74 862.99 18.56 o 7 4 1 14.84 11.38 8.37 o 8 4 1 74.13 78.94 19.54 o 9 4 1 0.31 -14.45 14.45 o 10 4 1 862.45 828.53 77.68 o 11 4 1 2.93 -10.65 19.59 o 1 5 1 42993.70 46664.68 539.32 o 2 5 1 3733.63 3644.53 50.27 o 3 5 1 539.89 477.58 12.46 o 4 5 1 11502.22 11246.70 129.88 o 5 5 1 6952.66 6882.11 76.30 o 6 5 1 14753.00 14946.72 171.53 o 7 5 1 4069.77 4020.03 70.92 o 8 5 1 1839.17 1752.24 89.48 o 9 5 1 465.45 508.07 34.92 o 10 5 1 1942.24 1900.58 81.71 o 11 5 1 205.13 193.45 28.09 o 0 6 1 57337.27 61418.47 915.78 o 1 6 1 37637.15 40009.44 463.90 o 2 6 1 27541.40 28526.84 351.69 o 3 6 1 8763.10 8894.74 115.59 o 4 6 1 9675.14 9444.63 123.49 o 5 6 1 3181.91 3271.79 53.14 o 6 6 1 326.76 328.57 18.40 o 7 6 1 87.61 70.15 12.46 o 8 6 1 707.87 636.49 49.46 o 9 6 1 1542.62 1525.07 57.50 o 10 6 1 2418.94 2421.23 95.72 o 1 7 1 84.93 82.61 5.62 o 2 7 1 5192.49 5133.45 74.90 o 3 7 1 734.48 668.85 18.19 o 4 7 1 8673.82 8326.49 118.24 o 5 7 1 2469.77 2427.16 43.84 o 6 7 1 6067.06 5946.53 84.81 o 7 7 1 1023.95 1016.78 27.47 o 8 7 1 7908.54 7761.85 242.45 o 9 7 1 1669.70 1602.19 59.25 o 10 7 1 351.01 393.97 35.69 o 0 8 1 75.86 151.36 9.70 o 1 8 1 13841.22 14593.48 174.46 o 2 8 1 2907.29 2762.68 45.51 o 3 8 1 1035.59 1017.15 23.72 o 4 8 1 3050.70 3151.10 53.03 o 5 8 1 23.31 31.47 9.34 o 6 8 1 780.65 762.62 25.30 o 7 8 1 227.78 226.78 15.34 o 8 8 1 770.92 774.61 41.79 o 9 8 1 205.62 188.31 46.99 o 10 8 1 101.13 109.79 25.38 o 1 9 1 5771.56 6117.64 78.29 o 2 9 1 642.47 646.41 18.58 o 3 9 1 761.78 787.62 21.55 o 4 9 1 7.18 6.92 8.48 o 5 9 1 288.48 238.75 14.53 o 6 9 1 250.04 225.09 15.38 o 7 9 1 484.94 516.38 21.29 o 8 9 1 618.76 605.64 47.91 o 9 9 1 72.63 68.89 21.87 o 0 10 1 1800.23 1766.28 36.78 o 1 10 1 3844.76 3679.73 54.39 o 2 10 1 2344.61 2074.50 42.33 o 3 10 1 2246.85 2207.29 49.52 o 4 10 1 3144.81 3039.34 53.28 o 5 10 1 297.54 298.98 18.09 o 6 10 1 127.54 117.57 12.88 o 7 10 1 2.49 -0.60 9.26 o 8 10 1 92.86 91.67 21.84 o 9 10 1 519.38 481.86 38.72 o 1 11 1 425.79 402.29 15.68 o 2 11 1 96.06 126.39 11.69 o 3 11 1 201.00 181.12 14.88 o 4 11 1 116.60 116.02 12.64 o 5 11 1 47.15 45.87 12.30 o 6 11 1 213.26 227.67 16.44 o 7 11 1 113.62 132.48 16.71 o 8 11 1 319.98 315.41 32.86 o 9 11 1 786.87 838.01 48.77 o 0 12 1 1697.65 1507.47 133.73 o 1 12 1 87.01 106.30 11.26 o 2 12 1 228.30 212.66 14.40 o 3 12 1 267.30 248.50 18.76 o 4 12 1 0.76 5.43 9.82 o 5 12 1 29.74 28.11 10.86 o 6 12 1 43.51 55.68 12.59 o 7 12 1 10.74 40.19 12.95 o 8 12 1 111.88 137.61 25.94 o 1 13 1 658.22 647.57 28.47 o 2 13 1 2367.48 2194.87 43.41 o 3 13 1 7.22 11.49 9.73 o 4 13 1 1480.60 1482.63 42.95 o 5 13 1 597.50 624.38 27.52 o 6 13 1 2675.16 2608.91 52.96 o 7 13 1 873.68 905.44 33.13 o 8 13 1 696.53 670.51 44.59 o 0 14 1 2074.80 2261.52 92.96 o 1 14 1 1592.90 1509.85 53.37 o 2 14 1 5578.86 5321.55 108.94 o 3 14 1 813.10 839.50 26.64 o 4 14 1 2609.58 2546.52 51.00 o 5 14 1 21.66 18.32 11.50 o 6 14 1 57.53 27.55 12.09 o 7 14 1 5.51 13.55 13.92 o 1 15 1 70.52 47.92 16.56 o 2 15 1 63.17 63.33 18.46 o 3 15 1 190.17 193.01 21.00 o 4 15 1 897.30 858.25 28.78 o 5 15 1 242.96 283.42 19.51 o 6 15 1 330.92 382.18 22.28 o 0 16 1 554.96 442.98 64.49 o 1 16 1 0.00 -0.73 13.99 o 2 16 1 43.48 65.34 19.08 o 3 16 1 245.46 227.85 25.78 o 4 16 1 30.77 18.40 15.69 o 5 16 1 15.06 17.57 11.91 o 1 17 1 1.43 -14.67 14.67 o 2 17 1 493.04 532.06 35.89 o 3 17 1 18.74 -1.68 21.74 o 4 17 1 315.93 331.05 38.16 o 0 18 1 1609.93 1618.02 152.77 o 1 18 1 278.69 332.58 39.50 o 2 18 1 1267.39 1360.13 56.60 o 0 0 2 438.25 259.14 14.52 o 1 0 2 54658.55 59952.73 1271.58 o 2 0 2 1861.98 1950.31 42.26 o 3 0 2 24090.56 24622.19 406.11 o 4 0 2 441.73 635.56 17.56 o 5 0 2 13436.47 14304.06 222.11 o 6 0 2 1476.45 1489.69 34.22 o 7 0 2 2041.56 2118.67 68.38 o 8 0 2 271.86 245.93 20.37 o 9 0 2 1922.24 1831.03 62.17 o 10 0 2 1681.68 1671.78 68.86 o 1 1 2 1381.56 1426.67 19.77 o 2 1 2 13766.21 14947.00 175.11 o 3 1 2 13890.67 14511.75 163.42 o 4 1 2 8910.94 9185.44 102.02 o 5 1 2 10270.26 9683.28 108.72 o 6 1 2 5263.94 5189.56 63.10 o 7 1 2 13310.03 13589.81 177.40 o 8 1 2 1423.23 1360.89 29.01 o 9 1 2 3816.72 3864.39 67.96 o 10 1 2 276.65 276.37 22.33 o 11 1 2 680.04 727.43 48.31 o 0 2 2 4101.33 4220.78 93.05 o 1 2 2 3312.12 3663.11 54.05 o 2 2 2 15741.35 16764.65 186.14 o 3 2 2 4826.26 5178.50 58.70 o 4 2 2 1215.24 1238.84 18.47 o 5 2 2 30.69 39.97 7.61 o 6 2 2 1768.55 1833.27 27.83 o 7 2 2 140.31 114.76 10.58 o 8 2 2 308.02 281.32 14.68 o 9 2 2 1365.97 1294.38 39.37 o 10 2 2 86.69 110.70 22.90 o 11 2 2 132.95 148.24 24.86 o 1 3 2 8.28 3.27 3.18 o 2 3 2 849.28 889.99 16.00 o 3 3 2 622.47 568.26 10.81 o 4 3 2 1584.06 1692.89 25.06 o 5 3 2 935.75 802.81 14.58 o 6 3 2 18.88 29.42 6.48 o 7 3 2 4043.15 3962.90 57.70 o 8 3 2 91.99 108.55 13.30 o 9 3 2 807.38 814.50 40.09 o 10 3 2 39.78 43.41 24.90 o 11 3 2 791.42 842.36 45.24 o 0 4 2 31075.42 35109.93 575.28 o 1 4 2 13797.83 14379.86 169.12 o 2 4 2 1054.00 1038.95 18.43 o 3 4 2 6308.81 5928.94 70.18 o 4 4 2 127.96 222.66 9.14 o 5 4 2 5611.85 5637.63 61.08 o 6 4 2 43.92 43.45 7.01 o 7 4 2 9.94 4.19 9.52 o 8 4 2 2460.00 2277.66 54.18 o 9 4 2 323.13 317.77 28.83 o 10 4 2 236.72 268.24 30.53 o 11 4 2 644.67 652.82 44.07 o 1 5 2 2362.08 2472.00 33.24 o 2 5 2 26.44 25.09 4.63 o 3 5 2 535.42 484.84 12.72 o 4 5 2 23.80 43.63 5.01 o 5 5 2 369.73 317.07 10.33 o 6 5 2 98.49 110.19 8.46 o 7 5 2 2205.93 2217.44 51.21 o 8 5 2 21.06 30.49 13.22 o 9 5 2 1559.14 1542.69 66.77 o 10 5 2 168.79 158.10 25.51 o 0 6 2 2253.59 2479.17 48.01 o 1 6 2 2902.40 3217.64 42.56 o 2 6 2 798.70 916.44 23.96 o 3 6 2 29.80 51.92 6.10 o 4 6 2 96.23 117.41 8.46 o 5 6 2 0.85 -5.24 7.40 o 6 6 2 750.88 830.72 28.02 o 7 6 2 27.54 46.84 13.52 o 8 6 2 278.45 313.32 21.36 o 9 6 2 198.45 171.13 24.32 o 10 6 2 481.43 475.13 37.12 o 1 7 2 623.42 563.59 18.39 o 2 7 2 66.33 60.56 7.28 o 3 7 2 3403.64 3300.51 48.95 o 4 7 2 4932.02 4981.86 75.56 o 5 7 2 5377.29 5329.29 86.55 o 6 7 2 384.28 345.15 16.08 o 7 7 2 5312.61 5131.21 88.28 o 8 7 2 272.37 255.74 20.99 o 9 7 2 579.27 558.09 37.95 o 10 7 2 263.31 288.43 34.00 o 0 8 2 4781.74 4800.77 87.82 o 1 8 2 25931.82 26604.17 312.10 o 2 8 2 410.76 316.15 12.79 o 3 8 2 5652.33 5464.44 81.46 o 4 8 2 1505.27 1486.94 31.30 o 5 8 2 3786.90 3591.97 59.83 o 6 8 2 1.83 5.30 8.23 o 7 8 2 67.49 54.40 12.69 o 8 8 2 12.85 17.18 15.36 o 9 8 2 382.28 411.58 34.61 o 10 8 2 158.96 185.83 29.06 o 1 9 2 1825.90 1833.33 29.02 o 2 9 2 153.85 178.93 11.95 o 3 9 2 1514.14 1392.15 29.80 o 4 9 2 30.46 32.46 9.10 o 5 9 2 869.81 807.79 23.98 o 6 9 2 64.68 57.31 11.20 o 7 9 2 1458.14 1511.77 38.95 o 8 9 2 244.88 235.56 23.31 o 9 9 2 732.36 710.60 55.09 o 0 10 2 2878.11 3032.19 61.38 o 1 10 2 1153.81 1093.83 26.97 o 2 10 2 942.85 913.05 23.88 o 3 10 2 2.05 6.97 8.43 o 4 10 2 5.88 -6.14 8.20 o 5 10 2 195.82 190.12 14.48 o 6 10 2 856.53 827.65 25.82 o 7 10 2 153.26 150.18 16.18 o 8 10 2 116.59 112.05 19.63 o 9 10 2 192.35 158.84 26.59 o 1 11 2 675.31 634.23 19.40 o 2 11 2 16.84 10.84 8.49 o 3 11 2 2795.36 2730.13 49.43 o 4 11 2 1410.61 1321.61 31.68 o 5 11 2 3274.87 3060.04 55.88 o 6 11 2 221.41 243.38 16.85 o 7 11 2 2686.53 2619.90 56.73 o 8 11 2 443.73 467.62 31.13 o 9 11 2 551.55 659.19 44.54 o 0 12 2 1733.26 1840.07 76.38 o 1 12 2 14259.75 14360.89 211.16 o 2 12 2 3861.89 3649.39 75.65 o 3 12 2 5934.90 5797.58 90.11 o 4 12 2 1912.07 1822.91 39.60 o 5 12 2 963.25 946.53 32.78 o 6 12 2 290.98 281.17 18.14 o 7 12 2 7.73 8.83 15.20 o 8 12 2 7.99 31.46 16.29 o 1 13 2 4.51 13.51 12.51 o 2 13 2 10.06 5.24 9.49 o 3 13 2 2603.50 2649.15 50.47 o 4 13 2 1341.74 1232.86 32.11 o 5 13 2 1864.29 1845.76 41.74 o 6 13 2 760.33 777.79 27.60 o 7 13 2 2216.89 2199.12 67.85 o 8 13 2 232.50 287.18 38.04 o 0 14 2 1720.34 1699.92 77.31 o 1 14 2 440.38 479.94 38.43 o 2 14 2 1049.04 966.73 36.30 o 3 14 2 393.88 436.44 20.27 o 4 14 2 112.39 108.09 14.23 o 5 14 2 20.74 21.89 11.85 o 6 14 2 0.04 5.20 11.41 o 7 14 2 1.58 -3.99 13.84 o 1 15 2 224.30 206.77 23.44 o 2 15 2 246.69 221.80 29.40 o 3 15 2 84.36 120.01 18.13 o 4 15 2 29.08 19.24 11.62 o 5 15 2 35.61 62.12 13.05 o 6 15 2 5.23 4.24 11.81 o 0 16 2 33.28 60.97 29.39 o 1 16 2 670.78 661.33 37.21 o 2 16 2 36.34 32.78 25.04 o 3 16 2 829.10 926.51 43.96 o 4 16 2 242.44 268.75 24.76 o 5 16 2 270.72 303.90 20.58 o 1 17 2 24.75 26.36 18.81 o 2 17 2 43.95 48.97 19.74 o 3 17 2 130.57 106.72 21.72 o 4 17 2 0.36 42.93 18.81 o 0 18 2 53.08 104.93 59.37 o 1 18 2 137.14 154.45 25.97 o 2 18 2 848.77 889.42 46.09 o 1 1 3 2309.94 2619.14 42.68 o 2 1 3 2181.41 2244.08 31.33 o 3 1 3 2614.85 2409.09 32.54 o 4 1 3 238.77 307.00 8.79 o 5 1 3 5411.90 5156.75 61.35 o 6 1 3 1350.38 1347.06 27.84 o 7 1 3 2575.52 2453.96 48.26 o 8 1 3 753.04 710.90 21.01 o 9 1 3 2786.18 3010.89 58.88 o 10 1 3 709.06 668.76 30.71 o 11 1 3 792.39 868.59 51.73 o 0 2 3 2940.20 3223.55 73.31 o 1 2 3 26936.46 27826.35 455.87 o 2 2 3 9139.82 9592.88 119.96 o 3 2 3 10458.35 10341.89 123.95 o 4 2 3 503.19 467.33 10.13 o 5 2 3 472.64 346.08 10.31 o 6 2 3 161.83 145.47 10.28 o 7 2 3 124.27 98.80 10.61 o 8 2 3 4561.23 4454.49 65.55 o 9 2 3 7.97 11.76 13.09 o 10 2 3 0.37 -10.10 16.64 o 11 2 3 1228.69 1355.90 68.27 o 1 3 3 8729.47 8968.39 119.59 o 2 3 3 1029.11 1022.59 18.80 o 3 3 3 265.56 236.43 7.31 o 4 3 3 454.57 576.38 12.51 o 5 3 3 3278.35 3120.67 39.76 o 6 3 3 130.52 125.91 9.71 o 7 3 3 2041.43 2077.24 36.07 o 8 3 3 310.26 311.29 17.42 o 9 3 3 1037.43 1032.59 50.66 o 10 3 3 159.23 159.25 24.58 o 11 3 3 743.01 775.16 44.53 o 0 4 3 4071.23 4294.73 98.55 o 1 4 3 15316.51 16274.45 214.28 o 2 4 3 192.31 174.50 7.28 o 3 4 3 1596.56 1550.78 27.28 o 4 4 3 528.99 525.13 11.61 o 5 4 3 368.88 418.15 11.98 o 6 4 3 61.69 75.85 7.88 o 7 4 3 677.69 691.55 22.51 o 8 4 3 122.83 126.97 16.23 o 9 4 3 524.18 482.66 42.34 o 10 4 3 36.96 3.61 17.43 o 11 4 3 459.50 420.68 36.24 o 1 5 3 5.96 14.81 4.36 o 2 5 3 172.77 174.35 6.54 o 3 5 3 8715.15 8376.80 109.14 o 4 5 3 690.78 755.97 16.57 o 5 5 3 12087.99 11912.00 132.45 o 6 5 3 550.66 573.02 15.55 o 7 5 3 9238.46 8789.25 248.14 o 8 5 3 298.12 316.97 21.98 o 9 5 3 3300.20 3380.79 92.83 o 10 5 3 1.45 -7.01 18.65 o 0 6 3 16.97 19.38 7.56 o 1 6 3 39961.86 40467.34 469.59 o 2 6 3 439.24 437.52 15.04 o 3 6 3 19038.24 18668.36 234.23 o 4 6 3 98.15 131.82 8.82 o 5 6 3 2675.04 2416.93 61.00 o 6 6 3 704.67 733.46 22.40 o 7 6 3 115.25 127.21 17.47 o 8 6 3 536.18 477.17 25.25 o 9 6 3 493.86 589.72 61.93 o 10 6 3 24.71 43.67 20.67 o 1 7 3 1782.02 1643.07 25.42 o 2 7 3 223.33 217.76 10.54 o 3 7 3 18618.93 19079.44 240.06 o 4 7 3 156.22 195.38 10.58 o 5 7 3 12926.64 13108.48 181.13 o 6 7 3 17.84 23.53 9.71 o 7 7 3 6323.71 6046.06 101.44 o 8 7 3 13.68 -5.92 12.85 o 9 7 3 2333.74 2259.84 82.05 o 10 7 3 100.81 101.85 23.21 o 0 8 3 1869.13 1661.25 41.36 o 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3 11 618.97 607.76 37.95 o 3 3 11 2060.78 1889.54 56.20 o 4 3 11 3942.89 3734.21 127.46 o 5 3 11 107.68 111.49 27.85 o 6 3 11 1107.81 1206.23 46.75 o 7 3 11 25.19 18.12 18.21 o 8 3 11 2665.17 2712.13 71.75 o 9 3 11 140.11 140.35 22.80 o 0 4 11 11.20 17.08 13.42 o 1 4 11 1889.22 1821.12 40.36 o 2 4 11 1162.32 1211.25 28.48 o 3 4 11 171.38 156.50 18.74 o 4 4 11 1.65 0.25 13.95 o 5 4 11 361.91 365.43 27.25 o 6 4 11 29.84 37.14 17.71 o 7 4 11 1047.45 979.92 44.00 o 8 4 11 27.00 44.19 17.55 o 9 4 11 102.74 90.53 23.48 o 1 5 11 186.67 194.74 12.57 o 2 5 11 1081.03 910.00 31.48 o 3 5 11 271.70 272.91 23.18 o 4 5 11 2352.21 2327.06 64.77 o 5 5 11 1730.82 1615.50 52.97 o 6 5 11 1078.79 1099.18 44.70 o 7 5 11 82.22 57.29 16.59 o 8 5 11 3585.64 3566.20 98.29 o 9 5 11 2.67 -17.89 17.89 o 0 6 11 18705.08 18291.93 344.24 o 1 6 11 873.15 871.72 32.31 o 2 6 11 8670.85 8245.79 124.72 o 3 6 11 309.93 275.02 20.27 o 4 6 11 4382.03 4238.52 101.16 o 5 6 11 315.13 243.87 24.06 o 6 6 11 4.89 9.15 15.79 o 7 6 11 342.29 390.59 32.09 o 8 6 11 17.67 34.45 21.31 o 9 6 11 40.64 35.83 21.83 o 1 7 11 1224.29 1201.60 32.62 o 2 7 11 380.38 367.96 17.26 o 3 7 11 1279.83 1235.24 34.50 o 4 7 11 3032.70 3036.09 79.12 o 5 7 11 1664.95 1685.23 66.98 o 6 7 11 3568.25 3554.28 94.22 o 7 7 11 1669.59 1725.88 61.64 o 8 7 11 302.81 377.38 34.24 o 0 8 11 30.93 18.76 19.68 o 1 8 11 1322.10 1246.81 45.57 o 2 8 11 199.40 211.58 16.79 o 3 8 11 1449.19 1362.05 37.46 o 4 8 11 18.19 31.03 14.02 o 5 8 11 37.15 36.64 17.13 o 6 8 11 30.83 34.05 18.27 o 7 8 11 105.46 81.74 20.91 o 8 8 11 14.53 19.63 18.85 o 1 9 11 29.00 56.80 19.54 o 2 9 11 315.45 303.17 19.15 o 3 9 11 562.18 516.24 23.50 o 4 9 11 1307.87 1242.00 42.24 o 5 9 11 1646.23 1649.67 60.00 o 6 9 11 1877.60 1940.08 64.84 o 7 9 11 712.94 683.07 40.84 o 8 9 11 1168.72 1222.14 62.41 o 0 10 11 7341.81 7321.20 178.77 o 1 10 11 1488.59 1454.21 70.32 o 2 10 11 4190.02 4331.55 91.56 o 3 10 11 1490.77 1421.45 39.80 o 4 10 11 2187.57 2185.80 59.19 o 5 10 11 83.03 91.89 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98.42 o 4 0 12 3903.12 3999.91 137.04 o 5 0 12 42.15 137.99 40.93 o 6 0 12 1132.47 938.62 152.17 o 7 0 12 209.72 178.75 35.81 o 8 0 12 29.39 22.75 29.09 o 9 0 12 20.52 -21.61 30.50 o 1 1 12 428.04 408.79 18.95 o 2 1 12 3650.58 3533.23 66.66 o 3 1 12 194.45 168.75 20.13 o 4 1 12 2447.50 2470.08 68.55 o 5 1 12 66.69 56.93 18.50 o 6 1 12 8308.45 8012.79 174.13 o 7 1 12 62.83 98.64 22.60 o 8 1 12 2587.51 2523.55 77.67 o 9 1 12 167.04 179.75 27.56 o 0 2 12 610.22 586.14 34.84 o 1 2 12 525.33 527.41 20.98 o 2 2 12 691.28 692.46 23.96 o 3 2 12 1843.32 1854.71 55.41 o 4 2 12 159.09 131.07 20.89 o 5 2 12 10.24 23.05 15.39 o 6 2 12 3.12 -8.28 16.40 o 7 2 12 33.74 37.24 23.97 o 8 2 12 19.99 16.76 20.41 o 9 2 12 182.88 160.90 24.18 o 1 3 12 546.74 533.47 21.37 o 2 3 12 3295.88 3178.02 61.58 o 3 3 12 5294.38 5143.84 116.22 o 4 3 12 30.73 30.11 19.85 o 5 3 12 4399.60 4476.79 107.49 o 6 3 12 1665.05 1629.69 55.88 o 7 3 12 1607.86 1528.94 55.77 o 8 3 12 1563.60 1597.40 59.33 o 9 3 12 1235.48 1323.70 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923.14 48.49 o 2 12 12 2111.40 2324.32 76.01 o 3 12 12 672.27 688.48 34.33 o 4 12 12 932.12 960.42 40.74 o 5 12 12 181.50 164.18 21.88 o 6 12 12 63.14 74.76 19.81 o 1 13 12 27.69 33.35 16.77 o 2 13 12 148.30 165.00 25.13 o 3 13 12 119.24 123.16 27.78 o 4 13 12 2283.79 2339.88 66.49 o 5 13 12 2.20 9.27 15.79 o 0 14 12 5.11 5.09 21.14 o 1 14 12 283.91 364.69 30.09 o 2 14 12 238.62 206.65 24.61 o 3 14 12 194.97 188.33 32.48 o 4 14 12 182.74 146.22 31.86 o 1 15 12 2.47 1.66 16.84 o 2 15 12 35.08 30.78 17.54 o 1 1 13 226.68 245.06 16.91 o 2 1 13 3568.41 3433.98 66.83 o 3 1 13 3297.81 3337.88 89.42 o 4 1 13 38.61 14.28 17.89 o 5 1 13 2606.41 2737.02 78.86 o 6 1 13 666.68 573.03 34.92 o 7 1 13 4413.12 4245.97 108.95 o 8 1 13 70.35 106.18 25.62 o 9 1 13 1058.23 1009.34 57.10 o 0 2 13 651.96 642.56 33.30 o 1 2 13 19636.04 20131.04 341.27 o 2 2 13 90.00 103.18 13.98 o 3 2 13 10032.87 10043.94 207.54 o 4 2 13 63.41 67.30 18.59 o 5 2 13 3552.25 3304.42 87.35 o 6 2 13 1506.17 1467.08 54.06 o 7 2 13 57.60 23.80 20.88 o 8 2 13 99.61 90.42 24.42 o 9 2 13 297.82 320.44 29.89 o 1 3 13 39.71 34.94 11.93 o 2 3 13 800.28 718.78 25.35 o 3 3 13 4557.42 4576.82 107.37 o 4 3 13 4.36 25.02 16.91 o 5 3 13 2597.54 2486.80 72.48 o 6 3 13 36.61 37.08 19.35 o 7 3 13 6999.29 6473.66 172.81 o 8 3 13 20.10 5.87 21.18 o 9 3 13 1009.38 1041.58 59.65 o 0 4 13 1590.29 1603.75 55.86 o 1 4 13 636.81 638.43 35.63 o 2 4 13 40.69 58.42 11.26 o 3 4 13 722.36 645.56 33.00 o 4 4 13 72.35 77.80 19.38 o 5 4 13 0.78 0.20 17.14 o 6 4 13 26.32 11.99 18.06 o 7 4 13 201.55 176.06 26.43 o 8 4 13 35.81 60.55 23.30 o 1 5 13 58.97 65.63 12.69 o 2 5 13 2644.97 2627.30 51.01 o 3 5 13 3007.66 2949.59 77.88 o 4 5 13 1287.72 1252.46 77.32 o 5 5 13 16.60 42.65 17.73 o 6 5 13 1865.36 1679.21 57.80 o 7 5 13 2114.21 2068.64 74.74 o 8 5 13 521.52 554.84 39.58 o 0 6 13 6577.35 6645.03 139.32 o 1 6 13 6736.21 6387.68 101.96 o 2 6 13 1085.09 1135.14 28.00 o 3 6 13 3372.64 3321.90 74.94 o 4 6 13 602.26 525.44 31.96 o 5 6 13 2259.83 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