#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014695.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014695_Fobs loop_ _publ_author_name 'Comerlato, Nadia M.' 'Ferreira, Glaucio B.' 'Harrison, William T. A.' 'Howie, R. Alan' 'Wardell, James L.' _publ_section_title ; Bis(tetra-n-butylammonium) and bis(tetraphenylphosphonium) salts of tris(2-oxo-1,3-dithiole-4,5-dithiolato)stannate(IV), both at 120K ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m139 _journal_page_last m143 _journal_volume 61 _journal_year 2005 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.7732 _cell_length_b 18.3479 _cell_length_c 27.5862 _exptl_crystal_F_000 2392.00 _reflns_d_resolution_high 0.7706 _[local]_cod_data_source_file gg1230Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Bu4N]2 [Sn(dmio)3] P2(1)2(1)2(1) soton data' _shelx_refln_list_code 4 _shelx_f_calc_maximum 572.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 25168.32 23948.75 2055.80 o 4 0 0 1323.39 846.22 54.36 o 6 0 0 28363.28 28969.60 662.14 o 8 0 0 6575.06 6968.91 270.98 o 10 0 0 1486.18 1293.25 158.51 o 12 0 0 10641.12 11479.16 503.44 o 3 1 0 178.05 130.26 48.43 o 4 1 0 388.10 558.04 41.28 o 5 1 0 582.69 571.04 57.23 o 6 1 0 190.75 66.77 49.74 o 7 1 0 16084.12 16737.13 299.18 o 8 1 0 0.19 0.00 49.66 o 9 1 0 28.41 -62.07 62.07 o 10 1 0 70.23 222.87 98.97 o 11 1 0 1444.21 1794.26 160.76 o 12 1 0 357.75 864.78 227.44 o 13 1 0 6080.75 7120.10 547.04 o 2 2 0 7082.38 5720.60 67.46 o 3 2 0 9556.14 10634.07 151.79 o 4 2 0 23538.48 21009.67 388.27 o 5 2 0 4480.47 4224.87 106.81 o 6 2 0 5977.02 5952.05 213.21 o 7 2 0 5.68 12.22 53.23 o 8 2 0 19.59 -27.44 58.40 o 9 2 0 1.15 55.69 111.60 o 10 2 0 84.71 133.51 83.84 o 11 2 0 14.09 55.50 110.76 o 12 2 0 666.71 566.98 159.90 o 13 2 0 642.76 1013.14 562.75 o 1 3 0 15002.00 14239.32 214.95 o 2 3 0 5872.25 5746.40 82.82 o 3 3 0 35923.28 35656.59 904.11 o 4 3 0 827.46 988.44 43.86 o 5 3 0 1058.96 1074.11 47.44 o 6 3 0 9.06 36.20 44.31 o 7 3 0 3937.49 3791.84 147.48 o 8 3 0 1335.11 1402.80 97.80 o 9 3 0 2518.15 2502.04 120.43 o 10 3 0 428.65 220.84 110.41 o 11 3 0 2127.39 2171.12 189.63 o 12 3 0 10.34 165.16 140.73 o 13 3 0 1822.53 1992.55 474.67 o 0 4 0 327484.34 300593.38 13383.64 o 1 4 0 597.69 747.35 36.32 o 2 4 0 5.65 0.00 50.53 o 3 4 0 615.20 536.65 46.55 o 4 4 0 23392.34 23385.06 615.14 o 5 4 0 362.82 309.01 43.76 o 6 4 0 5543.66 5221.70 120.84 o 7 4 0 994.93 873.83 75.80 o 8 4 0 7281.35 7191.19 307.48 o 9 4 0 4546.83 4797.03 172.33 o 10 4 0 11036.51 10989.90 430.87 o 11 4 0 455.67 218.10 109.09 o 12 4 0 1259.54 1036.88 157.59 o 13 4 0 333.30 274.91 233.49 o 1 5 0 4265.80 4293.68 78.69 o 2 5 0 5172.30 5473.95 92.31 o 3 5 0 95985.34 97155.77 1455.40 o 4 5 0 4131.53 4970.23 101.51 o 5 5 0 5577.79 5422.60 97.49 o 6 5 0 1292.83 1017.94 50.75 o 7 5 0 3225.75 3079.69 115.80 o 8 5 0 3526.39 3351.67 108.38 o 9 5 0 3482.14 3240.13 167.66 o 10 5 0 1070.01 1240.18 167.91 o 11 5 0 1716.50 2135.90 162.40 o 12 5 0 95.88 92.25 168.50 o 13 5 0 360.23 109.45 231.79 o 0 6 0 7931.49 8155.44 181.68 o 1 6 0 4778.24 4904.26 85.24 o 2 6 0 6645.23 6799.58 113.54 o 3 6 0 22034.81 24026.45 357.51 o 4 6 0 23198.24 23496.54 353.14 o 5 6 0 245.45 189.61 53.22 o 6 6 0 518.40 470.51 43.37 o 7 6 0 77.87 26.89 46.00 o 8 6 0 649.61 644.63 71.73 o 9 6 0 3607.23 3537.09 143.40 o 10 6 0 5750.80 5733.72 240.47 o 11 6 0 945.35 1017.60 140.89 o 12 6 0 72.76 124.23 165.06 o 13 6 0 24.10 -163.23 493.24 o 1 7 0 816.81 872.99 62.93 o 2 7 0 576.14 812.28 46.06 o 3 7 0 47186.99 50062.28 754.76 o 4 7 0 12.97 180.62 51.50 o 5 7 0 1.63 -46.64 50.94 o 6 7 0 130.77 184.15 56.03 o 7 7 0 5128.67 5357.91 121.98 o 8 7 0 3.44 159.31 74.83 o 9 7 0 9765.79 9323.87 331.66 o 10 7 0 2041.30 2260.64 170.62 o 11 7 0 292.58 276.26 124.77 o 12 7 0 2.26 115.73 225.44 o 13 7 0 123.18 311.90 336.91 o 0 8 0 3493.66 4261.62 254.71 o 1 8 0 7067.59 7393.33 128.23 o 2 8 0 2804.05 2897.74 73.11 o 3 8 0 6716.89 6257.76 131.24 o 4 8 0 4426.15 4909.01 139.62 o 5 8 0 14840.81 15315.20 505.90 o 6 8 0 23451.98 22866.42 1259.16 o 7 8 0 7115.79 6728.91 334.80 o 8 8 0 1373.34 1345.39 125.71 o 9 8 0 3438.34 3669.25 149.40 o 10 8 0 2352.11 2190.21 180.18 o 11 8 0 186.84 35.43 133.88 o 12 8 0 294.65 246.76 220.74 o 13 8 0 30.95 -162.00 228.85 o 1 9 0 1041.85 922.12 82.88 o 2 9 0 8104.62 8191.40 163.43 o 3 9 0 590.98 594.56 68.31 o 4 9 0 4894.92 4482.56 116.35 o 5 9 0 918.37 787.57 147.44 o 6 9 0 3112.89 2622.42 176.18 o 7 9 0 15370.68 15181.35 352.75 o 8 9 0 33.73 42.59 80.22 o 9 9 0 512.15 354.45 116.15 o 10 9 0 2186.34 2518.51 143.26 o 11 9 0 192.29 80.65 137.89 o 12 9 0 1382.47 1162.50 221.65 o 0 10 0 4614.96 4054.59 151.91 o 1 10 0 1018.58 1075.59 56.65 o 2 10 0 11106.52 11144.11 245.34 o 3 10 0 506.24 465.63 64.67 o 4 10 0 3830.84 4203.37 125.38 o 5 10 0 5615.77 5594.25 249.82 o 6 10 0 14185.02 13411.01 385.76 o 7 10 0 655.27 815.41 145.02 o 8 10 0 324.55 242.00 107.44 o 9 10 0 203.71 295.27 107.69 o 10 10 0 1002.83 1101.15 117.68 o 11 10 0 1892.47 1749.12 245.55 o 12 10 0 49.98 -61.82 233.46 o 1 11 0 3.92 53.44 53.43 o 2 11 0 1040.00 776.92 127.27 o 3 11 0 8074.31 8259.08 173.58 o 4 11 0 3.03 -34.49 81.52 o 5 11 0 2627.62 2683.33 188.07 o 6 11 0 4903.78 4974.90 256.60 o 7 11 0 7188.00 6511.07 262.11 o 8 11 0 152.18 347.57 206.71 o 9 11 0 3127.16 3133.59 150.42 o 10 11 0 99.08 80.53 107.50 o 11 11 0 1630.09 1618.98 291.15 o 12 11 0 1309.83 1058.94 266.33 o 0 12 0 649.80 529.48 83.48 o 1 12 0 2481.69 2274.12 94.78 o 2 12 0 27.71 157.79 52.65 o 3 12 0 1643.03 1445.67 134.00 o 4 12 0 6933.97 7347.80 382.14 o 5 12 0 8152.78 8395.23 368.96 o 6 12 0 6785.96 6838.02 257.84 o 7 12 0 465.90 462.64 123.19 o 8 12 0 1347.03 1825.89 187.71 o 9 12 0 89.83 279.17 126.16 o 10 12 0 63.77 9.83 115.88 o 11 12 0 227.10 196.06 224.50 o 12 12 0 5.30 398.61 394.64 o 1 13 0 1166.58 992.40 75.92 o 2 13 0 10624.67 10877.29 275.53 o 3 13 0 11.59 85.64 71.14 o 4 13 0 202.55 364.22 147.45 o 5 13 0 45.52 34.70 120.21 o 6 13 0 6000.42 5797.94 421.82 o 7 13 0 1313.92 1175.25 123.99 o 8 13 0 1384.86 1108.20 183.01 o 9 13 0 627.17 590.94 161.18 o 10 13 0 573.87 279.97 220.42 o 11 13 0 35.09 185.04 223.11 o 0 14 0 2994.45 2859.12 122.62 o 1 14 0 9949.38 10384.03 497.80 o 2 14 0 643.94 556.34 81.80 o 3 14 0 819.28 940.33 89.11 o 4 14 0 1074.78 1099.00 147.45 o 5 14 0 1666.72 1531.96 173.81 o 6 14 0 1082.71 847.02 147.11 o 7 14 0 313.46 471.21 154.55 o 8 14 0 183.63 9.65 115.42 o 9 14 0 7.37 -36.10 171.17 o 10 14 0 2193.80 2466.71 215.46 o 11 14 0 944.53 718.59 205.93 o 1 15 0 4089.27 3930.70 170.10 o 2 15 0 7239.52 7080.01 250.29 o 3 15 0 13372.55 13545.97 458.97 o 4 15 0 170.07 157.11 157.11 o 5 15 0 111.31 208.77 147.79 o 6 15 0 1406.67 1543.24 181.04 o 7 15 0 1461.72 1434.76 159.25 o 8 15 0 1617.26 2048.53 182.30 o 9 15 0 2221.03 2626.58 322.00 o 10 15 0 799.94 657.87 206.01 o 0 16 0 26.32 217.53 153.80 o 1 16 0 203.96 170.53 95.25 o 2 16 0 4109.56 4053.94 204.50 o 3 16 0 5971.63 5844.95 241.79 o 4 16 0 2131.63 2210.61 222.86 o 5 16 0 3568.90 3583.13 392.78 o 6 16 0 469.87 421.82 210.44 o 7 16 0 342.19 284.84 123.46 o 8 16 0 479.53 326.95 228.39 o 9 16 0 1000.74 914.89 407.76 o 10 16 0 166.18 8.49 215.46 o 1 17 0 4528.78 4356.39 315.75 o 2 17 0 3486.88 3602.54 338.92 o 3 17 0 15.58 63.83 177.14 o 4 17 0 40.04 0.00 210.44 o 5 17 0 4992.60 4459.18 296.93 o 6 17 0 44.26 32.12 165.47 o 7 17 0 1023.50 686.29 223.87 o 8 17 0 1076.90 1086.38 257.67 o 9 17 0 22.69 36.13 188.19 o 0 18 0 6535.53 6140.56 343.73 o 1 18 0 83.82 0.00 117.63 o 2 18 0 669.75 812.01 121.21 o 3 18 0 2335.56 2659.49 318.99 o 4 18 0 586.48 402.82 176.43 o 5 18 0 1939.30 2249.68 295.87 o 6 18 0 533.60 422.78 317.08 o 7 18 0 285.55 209.30 222.14 o 8 18 0 611.95 425.82 194.89 o 9 18 0 923.15 898.12 195.92 o 1 19 0 1334.19 851.60 197.78 o 2 19 0 4773.72 4626.10 307.30 o 3 19 0 1501.80 1654.66 181.46 o 4 19 0 619.16 850.31 424.68 o 5 19 0 113.87 53.01 224.21 o 6 19 0 553.14 684.36 223.18 o 7 19 0 338.96 424.68 530.37 o 8 19 0 939.52 440.93 232.03 o 0 20 0 617.62 821.84 166.10 o 1 20 0 3585.01 3344.58 309.86 o 2 20 0 374.55 626.35 221.58 o 3 20 0 413.87 372.26 196.62 o 4 20 0 300.58 553.24 196.16 o 5 20 0 1819.31 1276.90 318.99 o 6 20 0 56.50 -105.21 223.51 o 7 20 0 556.64 599.41 216.36 o 1 21 0 36.24 81.86 169.26 o 2 21 0 158.89 105.80 183.38 o 3 21 0 72.60 -68.59 181.98 o 4 21 0 6.47 -136.15 136.15 o 5 21 0 24.80 -151.71 151.71 o 6 21 0 139.13 37.77 259.52 o 0 22 0 1117.97 1165.49 423.73 o 1 22 0 548.50 881.54 293.17 o 2 22 0 1826.07 1796.18 219.32 o 3 22 0 0.39 -48.96 166.39 o 4 22 0 95.69 -59.30 306.52 o 5 22 0 1789.98 1952.79 347.03 o 1 23 0 719.82 1377.51 633.21 o 2 23 0 1027.90 1078.01 362.04 o 3 23 0 632.25 839.65 262.57 o 2 0 1 68534.94 66193.08 2468.38 o 3 0 1 466.15 860.47 43.56 o 4 0 1 360.04 482.14 36.40 o 5 0 1 3873.37 4310.41 129.99 o 6 0 1 17103.56 16993.34 318.56 o 7 0 1 575.45 518.56 49.83 o 8 0 1 141.52 156.30 49.85 o 9 0 1 104.91 -45.05 85.74 o 10 0 1 1139.61 1386.38 112.21 o 11 0 1 6855.94 6891.92 223.22 o 12 0 1 3999.09 4656.04 257.02 o 13 0 1 224.57 55.94 236.67 o -13 1 1 389.01 224.72 449.44 o -12 1 1 3907.17 4080.12 293.67 o -11 1 1 1042.75 1035.55 119.43 o -10 1 1 1675.79 2133.06 120.53 o -9 1 1 17.23 22.39 84.30 o -8 1 1 988.61 1005.01 71.02 o -7 1 1 778.71 821.78 71.22 o -6 1 1 1326.06 1587.44 56.89 o -5 1 1 18307.78 17458.85 276.30 o -4 1 1 11818.43 11861.31 156.33 o -3 1 1 223.31 389.93 44.23 o -2 1 1 31739.47 31147.74 1097.73 o 2 1 1 33377.18 34146.97 1028.47 o 3 1 1 254.31 384.71 49.13 o 4 1 1 11081.54 10934.37 207.49 o 5 1 1 18164.52 17638.49 298.66 o 6 1 1 1312.92 1623.12 126.32 o 7 1 1 808.12 873.13 53.70 o 8 1 1 1246.57 1254.33 80.81 o 9 1 1 4.36 18.71 70.78 o 10 1 1 1643.95 1806.36 145.69 o 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138.15 248.07 110.29 o -9 3 1 1296.50 1437.97 136.25 o -8 3 1 2045.66 2219.68 103.32 o -7 3 1 363.03 345.73 64.07 o -6 3 1 2903.12 2628.71 129.47 o -5 3 1 2455.07 2729.92 87.95 o -4 3 1 2942.64 3285.93 81.08 o -3 3 1 6837.41 7914.16 193.73 o -2 3 1 29391.96 31538.06 364.07 o -1 3 1 1183.39 1126.79 34.21 o 1 3 1 908.66 811.45 41.84 o 2 3 1 28209.53 30837.56 385.04 o 3 3 1 6842.86 7819.25 133.15 o 4 3 1 3148.84 3625.04 103.83 o 5 3 1 2722.05 3152.18 88.55 o 6 3 1 2623.81 2207.93 88.81 o 7 3 1 450.16 357.69 77.19 o 8 3 1 1997.23 2077.38 97.61 o 9 3 1 1382.66 1520.69 103.16 o 10 3 1 123.82 132.29 103.14 o 11 3 1 238.18 179.45 125.48 o 12 3 1 2577.21 2901.79 225.44 o 13 3 1 192.11 561.80 337.08 o -13 4 1 34.19 266.14 262.18 o -12 4 1 837.87 806.61 166.47 o -11 4 1 3378.80 3457.22 184.41 o -10 4 1 600.01 456.83 117.90 o -9 4 1 5717.11 5891.33 298.51 o -8 4 1 596.04 584.09 127.16 o -7 4 1 1334.26 1197.25 77.07 o -6 4 1 3187.77 3196.59 115.32 o -5 4 1 10165.69 10132.97 174.15 o -4 4 1 1779.19 1793.33 55.39 o -3 4 1 3935.83 4087.72 91.63 o -2 4 1 28599.60 30595.15 712.14 o -1 4 1 5136.89 5889.94 95.47 o 0 4 1 10439.94 10880.14 140.10 o 1 4 1 4486.44 5217.42 65.99 o 2 4 1 29680.05 31863.31 387.63 o 3 4 1 3923.02 4148.92 107.95 o 4 4 1 1781.26 1714.70 54.83 o 5 4 1 10595.11 10853.57 213.91 o 6 4 1 2987.20 3155.41 160.54 o 7 4 1 1449.27 1516.23 96.79 o 8 4 1 685.80 871.58 96.88 o 9 4 1 5778.30 6211.37 346.11 o 10 4 1 584.97 543.39 78.55 o 11 4 1 3489.52 3730.33 199.15 o 12 4 1 779.73 515.01 203.74 o 13 4 1 40.55 0.00 336.13 o -13 5 1 78.83 163.46 231.79 o -12 5 1 115.49 108.70 203.48 o -11 5 1 2924.65 2941.11 182.92 o -10 5 1 365.06 406.42 108.27 o -9 5 1 8290.35 8606.28 590.85 o -8 5 1 5126.22 5038.93 141.93 o -7 5 1 648.42 591.13 57.38 o -6 5 1 1188.27 1057.90 57.26 o -5 5 1 7983.86 8180.95 171.01 o -4 5 1 23409.03 23434.58 433.50 o -3 5 1 6892.40 8231.12 182.32 o -2 5 1 13211.18 14620.11 246.57 o -1 5 1 6495.00 5997.07 86.79 o 0 5 1 4020.45 3403.35 63.65 o 1 5 1 6562.74 6048.25 100.33 o 2 5 1 12768.07 14140.64 220.42 o 3 5 1 6899.40 7923.04 163.42 o 4 5 1 22643.40 23091.23 366.55 o 5 5 1 7604.58 7935.76 157.37 o 6 5 1 1006.04 941.31 61.76 o 7 5 1 648.46 533.11 50.48 o 8 5 1 5533.45 5687.14 151.68 o 9 5 1 8264.04 8863.22 322.72 o 10 5 1 352.26 434.50 117.09 o 11 5 1 2878.86 2952.55 170.26 o 12 5 1 175.10 149.00 211.30 o 13 5 1 74.82 51.57 168.59 o -13 6 1 9.37 216.32 386.59 o -12 6 1 27.09 184.34 156.17 o -11 6 1 573.03 496.24 130.19 o -10 6 1 1585.30 1468.98 116.91 o -9 6 1 5836.18 5999.42 319.50 o -8 6 1 6461.38 6371.98 237.90 o -7 6 1 643.01 599.98 71.55 o -6 6 1 5499.43 5166.78 171.73 o -5 6 1 3354.40 3604.84 88.53 o -4 6 1 8661.80 9257.15 231.11 o -3 6 1 1992.59 2667.47 73.86 o -2 6 1 51771.89 56040.07 842.21 o -1 6 1 1819.71 2073.12 55.86 o 0 6 1 1009.65 881.38 39.35 o 1 6 1 1472.86 1726.03 45.90 o 2 6 1 52667.08 55858.93 849.99 o 3 6 1 1914.43 2411.60 72.97 o 4 6 1 8590.45 9132.88 186.27 o 5 6 1 2755.88 3021.71 105.98 o 6 6 1 5184.42 5145.39 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