#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/46/2014696.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014696_Fobs loop_ _publ_author_name 'Comerlato, Nadia M.' 'Ferreira, Glaucio B.' 'Harrison, William T. A.' 'Howie, R. Alan' 'Wardell, James L.' _publ_section_title ; Bis(tetra-n-butylammonium) and bis(tetraphenylphosphonium) salts of tris(2-oxo-1,3-dithiole-4,5-dithiolato)stannate(IV), both at 120K ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m139 _journal_page_last m143 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.417 _cell_angle_gamma 90.000 _cell_length_a 14.2844 _cell_length_b 26.4828 _cell_length_c 15.4538 _exptl_crystal_F_000 2712.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file gg1230IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Ph4P]2 [Sn(dmio)3] (Z = 4, P21/n)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 458.47 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 6912.22 7207.26 161.88 o 6 0 0 35620.29 34333.75 650.75 o 8 0 0 1360.29 1528.89 58.53 o 10 0 0 739.33 858.92 49.57 o 12 0 0 429.98 539.76 53.07 o 14 0 0 24490.40 25894.17 693.59 o 16 0 0 1866.69 1571.41 160.17 o 18 0 0 3747.05 3776.61 386.66 o 3 1 0 9447.92 8663.50 143.75 o 4 1 0 5004.12 4990.52 73.40 o 5 1 0 2853.89 3016.25 50.94 o 6 1 0 1461.42 1666.95 34.04 o 7 1 0 12664.07 12139.20 188.49 o 8 1 0 5.09 24.39 23.06 o 9 1 0 50474.41 51181.46 685.69 o 10 1 0 6948.36 6796.10 148.04 o 11 1 0 2628.45 2725.34 64.62 o 12 1 0 2252.47 2314.45 58.74 o 13 1 0 882.06 832.21 48.72 o 14 1 0 1452.84 1627.64 71.16 o 15 1 0 8852.39 9026.72 319.98 o 16 1 0 822.98 746.19 83.89 o 17 1 0 29.17 89.32 72.07 o 18 1 0 79.36 97.04 69.71 o 2 2 0 24472.49 23783.28 515.66 o 3 2 0 14490.44 14145.21 216.76 o 4 2 0 20926.59 20379.07 309.30 o 5 2 0 4259.73 4617.44 64.80 o 6 2 0 5.83 12.36 13.52 o 7 2 0 169.25 265.73 22.10 o 8 2 0 2957.72 3050.06 53.86 o 9 2 0 3497.65 3433.90 63.24 o 10 2 0 7888.69 8326.16 151.65 o 11 2 0 4045.18 4098.13 99.96 o 12 2 0 3065.37 3146.62 74.51 o 13 2 0 6074.61 5950.51 146.99 o 14 2 0 1383.73 1432.57 125.05 o 15 2 0 919.81 844.65 73.28 o 16 2 0 345.26 377.33 62.88 o 17 2 0 3292.69 3205.83 170.63 o 18 2 0 985.03 761.67 167.37 o 2 3 0 6761.39 6793.90 108.00 o 3 3 0 9422.07 10404.23 152.97 o 4 3 0 3841.28 3895.70 54.87 o 5 3 0 2702.55 2816.64 42.81 o 6 3 0 169.13 115.65 12.24 o 7 3 0 1376.41 1285.85 26.45 o 8 3 0 22146.10 21298.91 290.81 o 9 3 0 3122.32 3017.83 54.17 o 10 3 0 8350.23 8263.28 181.27 o 11 3 0 5141.43 5041.02 101.34 o 12 3 0 994.15 946.96 43.64 o 13 3 0 958.26 1026.40 47.37 o 14 3 0 7257.77 7277.08 200.09 o 15 3 0 2553.85 2474.25 109.94 o 16 3 0 27.82 95.92 90.50 o 17 3 0 20.86 241.95 168.30 o 18 3 0 289.05 389.18 85.86 o 1 4 0 24186.86 23186.66 325.34 o 2 4 0 1663.59 1800.03 29.37 o 3 4 0 8258.83 8258.37 115.89 o 4 4 0 10324.22 10271.91 144.61 o 5 4 0 10788.17 11258.07 165.06 o 6 4 0 49830.89 49589.16 683.64 o 7 4 0 7188.33 7484.40 103.40 o 8 4 0 5780.92 5362.35 84.35 o 9 4 0 2107.94 2085.24 47.89 o 10 4 0 2314.50 2200.19 51.38 o 11 4 0 3446.89 3328.83 99.76 o 12 4 0 692.80 710.81 45.25 o 13 4 0 6907.61 7373.55 173.38 o 14 4 0 700.72 683.73 58.91 o 15 4 0 1446.66 1547.04 82.48 o 16 4 0 27.68 77.67 53.97 o 17 4 0 1751.39 1750.08 108.21 o 18 4 0 1298.86 1318.99 110.17 o 1 5 0 3722.55 3684.86 46.45 o 2 5 0 6746.01 6454.71 82.09 o 3 5 0 85403.30 83798.24 1292.39 o 4 5 0 297.69 313.62 36.59 o 5 5 0 9298.08 9213.47 121.25 o 6 5 0 1128.28 1412.87 35.43 o 7 5 0 19021.24 18509.48 328.05 o 8 5 0 128.25 117.90 14.02 o 9 5 0 52111.09 53231.00 752.87 o 10 5 0 166.34 211.28 28.54 o 11 5 0 272.54 267.53 24.05 o 12 5 0 1900.58 1920.29 62.16 o 13 5 0 1009.24 877.04 58.42 o 14 5 0 4218.39 4256.16 146.62 o 15 5 0 4075.75 4470.53 161.83 o 16 5 0 1154.04 1249.25 98.79 o 17 5 0 574.35 643.40 82.32 o 18 5 0 1146.45 1251.64 122.92 o 0 6 0 64345.05 62703.90 1191.33 o 1 6 0 16820.46 16028.66 212.83 o 2 6 0 41306.96 38719.06 577.36 o 3 6 0 2322.70 2436.51 34.01 o 4 6 0 19642.53 18923.79 213.85 o 5 6 0 10509.96 10777.61 157.74 o 6 6 0 59383.86 56819.47 849.37 o 7 6 0 40079.13 38023.68 460.81 o 8 6 0 11032.82 10848.84 159.82 o 9 6 0 0.23 3.62 22.30 o 10 6 0 3316.55 3349.41 75.16 o 11 6 0 375.19 365.53 42.54 o 12 6 0 8322.22 8504.10 166.87 o 13 6 0 1124.09 1241.93 74.25 o 14 6 0 8.97 -28.11 50.58 o 15 6 0 961.85 1025.01 73.26 o 16 6 0 377.01 329.46 64.10 o 17 6 0 81.20 43.48 74.48 o 18 6 0 3791.88 3829.89 219.60 o 1 7 0 13046.53 12574.35 168.67 o 2 7 0 1760.26 1850.86 25.46 o 3 7 0 10992.78 11324.45 127.51 o 4 7 0 84.61 57.64 12.03 o 5 7 0 4168.23 3792.48 56.62 o 6 7 0 5688.38 5507.48 94.00 o 7 7 0 14753.39 15026.86 204.90 o 8 7 0 35980.54 35155.28 478.12 o 9 7 0 3966.96 3783.72 77.11 o 10 7 0 2634.24 2773.49 77.56 o 11 7 0 157.59 247.68 37.75 o 12 7 0 2204.71 2150.65 82.16 o 13 7 0 11.98 64.19 37.17 o 14 7 0 15063.70 15388.40 425.96 o 15 7 0 124.50 169.15 56.35 o 16 7 0 1378.90 1392.01 85.21 o 17 7 0 120.78 129.83 76.36 o 18 7 0 2.02 -26.68 206.36 o 0 8 0 1661.22 1822.46 33.40 o 1 8 0 11841.29 11965.26 141.18 o 2 8 0 22990.56 23051.60 266.27 o 3 8 0 12729.39 13274.94 150.74 o 4 8 0 7609.85 7739.04 87.38 o 5 8 0 28583.22 28157.31 302.63 o 6 8 0 244.01 340.89 17.45 o 7 8 0 14657.65 15145.57 196.07 o 8 8 0 5022.06 4923.95 85.32 o 9 8 0 142.11 170.31 29.64 o 10 8 0 469.09 376.04 38.06 o 11 8 0 1045.68 997.24 42.59 o 12 8 0 80.60 109.84 46.27 o 13 8 0 4390.63 4555.90 148.88 o 14 8 0 3747.48 3809.01 135.09 o 15 8 0 4821.48 5006.46 192.65 o 16 8 0 211.91 205.13 71.48 o 17 8 0 2285.62 2391.34 153.35 o 18 8 0 1362.43 1213.70 172.06 o 1 9 0 11143.75 12151.21 128.09 o 2 9 0 22672.90 23978.00 280.38 o 3 9 0 9374.05 9293.35 101.55 o 4 9 0 68677.25 70362.10 699.15 o 5 9 0 329.76 369.06 20.56 o 6 9 0 1042.95 884.23 29.03 o 7 9 0 611.22 555.78 23.83 o 8 9 0 1859.43 1798.17 42.10 o 9 9 0 9440.84 9327.80 150.91 o 10 9 0 12491.41 12459.86 208.61 o 11 9 0 893.92 952.98 41.54 o 12 9 0 2723.75 2871.94 88.00 o 13 9 0 8.18 -34.20 39.01 o 14 9 0 2075.75 1996.57 100.35 o 15 9 0 4869.39 4949.96 170.71 o 16 9 0 52.87 127.18 62.92 o 17 9 0 173.25 237.94 90.94 o 0 10 0 17328.15 16744.97 390.06 o 1 10 0 691.10 612.32 11.79 o 2 10 0 895.38 1017.20 18.69 o 3 10 0 3236.30 3089.61 41.13 o 4 10 0 9981.63 9654.82 107.00 o 5 10 0 1.65 -1.05 11.64 o 6 10 0 54096.13 53247.70 621.49 o 7 10 0 12479.39 12848.54 160.78 o 8 10 0 538.68 512.80 28.08 o 9 10 0 7884.69 7912.76 144.19 o 10 10 0 177.44 176.88 25.53 o 11 10 0 1713.58 1714.87 73.26 o 12 10 0 2332.16 2285.54 89.40 o 13 10 0 2298.32 2269.83 102.69 o 14 10 0 1218.20 1099.28 69.84 o 15 10 0 1858.63 1849.78 103.87 o 16 10 0 2385.11 2164.02 194.37 o 17 10 0 431.57 367.69 92.48 o 1 11 0 9280.38 9166.34 98.31 o 2 11 0 5992.13 6031.76 65.67 o 3 11 0 17980.59 18168.99 200.38 o 4 11 0 415.00 370.30 10.32 o 5 11 0 37079.27 35588.18 449.33 o 6 11 0 5022.93 4931.62 70.99 o 7 11 0 12336.55 11951.95 150.31 o 8 11 0 6428.81 6131.39 102.67 o 9 11 0 4397.84 4367.92 86.24 o 10 11 0 3466.63 3413.71 82.77 o 11 11 0 15.72 -3.46 26.45 o 12 11 0 3575.58 3816.69 124.73 o 13 11 0 1591.67 1597.03 90.11 o 14 11 0 13534.81 13741.15 475.45 o 15 11 0 5140.94 5073.57 199.83 o 16 11 0 3603.38 3463.25 164.51 o 17 11 0 10.79 6.44 84.48 o 0 12 0 42105.50 42599.21 800.40 o 1 12 0 11854.85 11235.17 133.51 o 2 12 0 7305.20 7752.22 94.24 o 3 12 0 4749.38 5186.74 66.20 o 4 12 0 3282.09 2818.13 42.61 o 5 12 0 28702.45 29395.49 443.15 o 6 12 0 549.91 532.50 24.84 o 7 12 0 4596.15 4441.44 68.86 o 8 12 0 9721.22 9691.70 180.44 o 9 12 0 3317.65 3273.83 86.87 o 10 12 0 7144.92 7271.68 184.79 o 11 12 0 970.30 984.77 58.72 o 12 12 0 3581.31 3387.26 118.52 o 13 12 0 12003.25 12393.80 386.09 o 14 12 0 3879.07 4096.29 170.25 o 15 12 0 89.97 295.17 92.63 o 16 12 0 91.90 244.07 88.60 o 17 12 0 3697.52 3659.51 202.12 o 1 13 0 28906.71 31881.01 360.51 o 2 13 0 1578.00 1517.60 23.91 o 3 13 0 2002.09 1897.25 36.36 o 4 13 0 379.13 306.72 18.74 o 5 13 0 8695.76 9046.31 153.98 o 6 13 0 2182.72 2255.97 58.64 o 7 13 0 5398.94 5387.80 94.72 o 8 13 0 1907.02 1871.16 57.04 o 9 13 0 2931.39 2718.85 89.27 o 10 13 0 130.39 156.82 24.83 o 11 13 0 1429.31 1443.61 61.44 o 12 13 0 569.35 505.53 43.83 o 13 13 0 5924.59 6401.23 217.58 o 14 13 0 16381.42 16926.70 557.63 o 15 13 0 1049.58 921.34 102.30 o 16 13 0 1574.24 1321.50 113.51 o 17 13 0 1040.11 802.49 132.44 o 0 14 0 16576.78 15622.92 334.08 o 1 14 0 1096.29 884.41 34.83 o 2 14 0 2308.99 2263.19 33.54 o 3 14 0 13766.68 13831.98 165.02 o 4 14 0 11837.23 12051.33 152.60 o 5 14 0 51.37 16.72 28.75 o 6 14 0 1705.08 1685.46 49.20 o 7 14 0 370.53 375.90 25.11 o 8 14 0 7024.67 6849.91 155.89 o 9 14 0 5530.47 5637.36 187.46 o 10 14 0 5941.04 5845.30 245.27 o 11 14 0 6293.28 6442.21 232.35 o 12 14 0 3475.48 3448.83 134.00 o 13 14 0 684.94 643.66 68.93 o 14 14 0 1099.99 1083.20 110.93 o 15 14 0 404.06 423.83 87.53 o 16 14 0 1019.77 790.13 183.91 o 1 15 0 10075.79 10147.72 157.47 o 2 15 0 351.72 327.46 12.76 o 3 15 0 26407.94 26240.86 324.38 o 4 15 0 2116.13 2251.91 40.48 o 5 15 0 5014.75 5175.65 110.81 o 6 15 0 2350.55 2552.64 59.87 o 7 15 0 792.52 766.48 35.96 o 8 15 0 58.40 53.24 34.58 o 9 15 0 1910.57 1876.88 81.62 o 10 15 0 51.84 50.81 44.48 o 11 15 0 6122.99 6261.55 205.03 o 12 15 0 190.76 189.60 58.45 o 13 15 0 579.42 577.28 80.30 o 14 15 0 376.67 180.62 103.74 o 15 15 0 1515.52 1321.32 117.59 o 16 15 0 1955.84 1930.47 152.78 o 0 16 0 10092.99 9909.60 201.32 o 1 16 0 33088.03 32527.59 497.41 o 2 16 0 3308.35 3539.59 52.52 o 3 16 0 4718.70 4384.55 84.11 o 4 16 0 18801.00 18550.76 216.68 o 5 16 0 314.70 287.97 26.68 o 6 16 0 22.81 52.37 21.48 o 7 16 0 34982.10 35353.87 790.41 o 8 16 0 2.29 31.56 20.47 o 9 16 0 487.94 523.28 46.42 o 10 16 0 7572.69 7505.00 209.27 o 11 16 0 623.52 615.76 64.05 o 12 16 0 4409.16 4537.25 165.97 o 13 16 0 8653.35 8821.85 255.39 o 14 16 0 1313.40 1194.34 95.11 o 15 16 0 150.66 81.87 78.28 o 16 16 0 118.37 24.65 85.54 o 1 17 0 2181.87 2162.17 54.15 o 2 17 0 5643.43 6165.31 84.51 o 3 17 0 6060.71 6382.13 107.07 o 4 17 0 12690.84 12466.40 187.05 o 5 17 0 5223.12 4848.37 121.78 o 6 17 0 3702.12 3770.60 98.13 o 7 17 0 244.36 242.50 25.15 o 8 17 0 13921.38 13831.86 309.56 o 9 17 0 1946.14 1749.07 80.56 o 10 17 0 1019.15 1044.70 67.94 o 11 17 0 4703.73 4613.93 175.69 o 12 17 0 942.47 979.60 83.27 o 13 17 0 1383.91 1244.21 91.89 o 14 17 0 12282.18 12522.47 443.45 o 15 17 0 104.98 71.94 75.87 o 16 17 0 282.37 318.29 106.48 o 0 18 0 226.01 237.10 32.15 o 1 18 0 7955.75 7508.37 136.64 o 2 18 0 6.60 8.98 13.57 o 3 18 0 3.43 8.69 12.57 o 4 18 0 2480.23 2384.50 44.77 o 5 18 0 4084.33 4119.47 91.37 o 6 18 0 0.52 18.48 20.52 o 7 18 0 7969.13 7862.56 226.75 o 8 18 0 2432.12 2313.14 176.26 o 9 18 0 127.23 87.84 43.95 o 10 18 0 319.59 369.97 50.65 o 11 18 0 12555.83 13024.88 374.78 o 12 18 0 231.32 244.02 57.92 o 13 18 0 5476.87 5522.22 230.95 o 14 18 0 668.67 827.15 93.86 o 15 18 0 4.63 71.74 75.55 o 1 19 0 207.23 223.90 21.36 o 2 19 0 1457.29 1520.10 45.19 o 3 19 0 4870.34 4843.21 88.17 o 4 19 0 465.17 514.28 22.25 o 5 19 0 7.72 24.33 13.89 o 6 19 0 527.07 485.09 39.43 o 7 19 0 3162.40 3256.99 113.59 o 8 19 0 4888.87 4933.39 142.01 o 9 19 0 56.93 39.62 56.88 o 10 19 0 5964.70 5792.20 200.84 o 11 19 0 9.60 14.07 69.60 o 12 19 0 2076.38 2275.47 120.32 o 13 19 0 400.60 448.39 92.28 o 14 19 0 208.61 105.09 77.69 o 15 19 0 28.49 46.76 78.40 o 0 20 0 288.10 239.95 37.27 o 1 20 0 895.02 859.24 40.58 o 2 20 0 34.41 26.09 19.86 o 3 20 0 717.74 737.93 25.44 o 4 20 0 15681.86 15339.77 320.73 o 5 20 0 3281.49 3253.81 76.21 o 6 20 0 2447.78 2325.86 80.01 o 7 20 0 5186.00 5120.58 168.04 o 8 20 0 1008.04 1007.83 62.01 o 9 20 0 228.72 180.51 52.92 o 10 20 0 5294.00 5485.09 215.49 o 11 20 0 2669.44 2658.87 138.68 o 12 20 0 654.69 589.89 73.17 o 13 20 0 635.47 574.76 111.60 o 14 20 0 29.63 52.26 95.87 o 15 20 0 967.96 1053.90 259.39 o 1 21 0 7650.80 7894.46 190.00 o 2 21 0 5633.19 5814.81 154.27 o 3 21 0 252.86 332.70 47.10 o 4 21 0 8643.53 8183.19 224.13 o 5 21 0 15264.35 14940.07 383.14 o 6 21 0 6165.25 6162.76 229.33 o 7 21 0 161.50 190.94 52.10 o 8 21 0 403.93 327.67 58.99 o 9 21 0 8413.89 8207.65 298.14 o 10 21 0 1223.71 1277.04 109.42 o 11 21 0 55.99 136.74 61.68 o 12 21 0 2417.21 2164.22 350.84 o 13 21 0 748.89 794.96 137.45 o 14 21 0 2060.75 1826.75 223.77 o 0 22 0 4433.26 4209.65 191.02 o 1 22 0 1717.94 1566.62 61.62 o 2 22 0 616.53 532.84 49.97 o 3 22 0 616.68 540.08 42.30 o 4 22 0 1340.03 1446.94 85.00 o 5 22 0 19382.59 20210.96 1459.66 o 6 22 0 345.66 236.15 64.61 o 7 22 0 10327.67 10818.70 540.39 o 8 22 0 599.68 625.77 152.15 o 9 22 0 5523.45 5242.31 405.71 o 10 22 0 433.60 551.29 122.47 o 11 22 0 4853.11 4846.30 445.01 o 12 22 0 476.27 559.37 118.31 o 13 22 0 1196.82 1274.90 176.84 o 14 22 0 185.69 283.99 113.37 o 1 23 0 5583.62 5727.93 188.69 o 2 23 0 12532.93 13146.30 338.94 o 3 23 0 997.26 1061.23 58.89 o 4 23 0 7967.80 8144.38 226.10 o 5 23 0 4978.80 4626.67 255.83 o 6 23 0 1325.80 1271.74 182.96 o 7 23 0 144.50 187.91 97.50 o 8 23 0 3806.83 3726.88 284.46 o 9 23 0 18.33 69.35 77.63 o 10 23 0 6371.42 6896.10 334.13 o 11 23 0 529.50 347.40 140.24 o 12 23 0 690.65 853.62 221.57 o 13 23 0 134.35 209.78 135.94 o 0 24 0 1257.73 1230.66 133.69 o 1 24 0 8766.53 8902.26 285.55 o 2 24 0 1996.27 2167.20 102.19 o 3 24 0 184.23 144.84 34.99 o 4 24 0 2473.25 2607.41 109.08 o 5 24 0 10873.87 10877.62 465.89 o 6 24 0 5612.92 6114.64 433.16 o 7 24 0 4276.31 4182.21 230.65 o 8 24 0 864.44 803.31 147.81 o 9 24 0 306.06 343.97 86.71 o 10 24 0 434.77 477.74 218.80 o 11 24 0 509.62 528.37 113.19 o 12 24 0 180.26 327.08 212.48 o 13 24 0 1650.19 1444.57 167.36 o 1 25 0 4347.48 4678.35 203.17 o 2 25 0 269.63 245.89 87.92 o 3 25 0 5600.19 5878.57 196.87 o 4 25 0 463.98 362.31 72.76 o 5 25 0 417.38 331.68 91.73 o 6 25 0 10.87 -63.21 112.56 o 7 25 0 41.16 84.83 96.20 o 8 25 0 1035.07 1121.69 201.52 o 9 25 0 246.07 331.58 86.86 o 10 25 0 365.30 269.72 132.51 o 11 25 0 115.47 109.06 141.69 o 12 25 0 370.32 414.72 159.81 o 0 26 0 10.07 128.75 78.79 o 1 26 0 280.67 231.09 55.89 o 2 26 0 1086.83 1074.74 99.53 o 3 26 0 464.99 442.58 63.91 o 4 26 0 5013.89 4887.60 215.30 o 5 26 0 169.52 282.51 108.51 o 6 26 0 62.90 -19.56 116.21 o 7 26 0 2053.06 2101.70 196.59 o 8 26 0 93.79 -66.82 101.90 o 9 26 0 528.07 516.34 154.05 o 10 26 0 746.45 633.53 108.60 o 11 26 0 2969.43 2924.70 269.95 o 12 26 0 1637.14 1332.96 277.25 o 1 27 0 1081.89 1041.82 93.50 o 2 27 0 10974.38 11978.54 585.89 o 3 27 0 7906.58 8507.06 511.95 o 4 27 0 5409.10 5902.72 405.42 o 5 27 0 534.44 544.83 167.85 o 6 27 0 5313.15 4880.44 306.38 o 7 27 0 912.75 778.06 240.13 o 8 27 0 4184.49 3865.35 232.15 o 9 27 0 7.81 66.59 96.92 o 10 27 0 714.65 567.91 124.61 o 11 27 0 553.19 481.55 208.34 o 0 28 0 141.93 249.61 97.36 o 1 28 0 4977.24 5265.19 250.51 o 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