#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/47/2014702.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2014702_Fobs
loop_
_publ_author_name
'Cornet, St\'ephanie M. M.'
'Dillon, Keith. B.'
'Goeta, Andr\'es E.'
'Thompson, Amber L.'
_publ_section_title
;
trans-Di-\m-bromo-bis[bromo(triethylphosphine-\kP)platinum(II)]
;
_journal_issue 2
_journal_name_full 'Acta Crystallographica Section C'
_journal_page_first m74
_journal_page_last m75
_journal_volume 61
_journal_year 2005
_space_group_IT_number 15
_symmetry_space_group_name_Hall '-C 2yc'
_symmetry_space_group_name_H-M 'C 1 2/c 1'
_cell_angle_alpha 90.000
_cell_angle_beta 120.930
_cell_angle_gamma 90.000
_cell_length_a 26.5224
_cell_length_b 6.8720
_cell_length_c 13.8115
_exptl_crystal_F_000 1712.00
_reflns_d_resolution_high 0.7829
_[local]_cod_data_source_file hj1034Isup2.hkl
_[local]_cod_data_source_block I
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' monoclinic in C2/c'
_shelx_refln_list_code 4
_shelx_f_calc_maximum 883.79
_shelx_f_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
4 0 0 65927.98 60192.79 1539.18 o
6 0 0 9263.26 10304.07 357.93 o
8 0 0 157706.69 160590.97 4056.99 o
12 0 0 284348.19 288142.84 6650.61 o
14 0 0 62782.57 67911.14 1857.30 o
16 0 0 12.82 252.75 154.23 o
18 0 0 40565.65 42924.25 1113.27 o
20 0 0 388570.72 393815.41 8333.51 o
22 0 0 95599.81 98765.13 2325.58 o
24 0 0 55010.00 56574.17 1506.20 o
26 0 0 11886.65 11265.95 769.32 o
28 0 0 535.63 275.33 772.16 o
1 1 0 46872.68 45029.26 748.41 o
3 1 0 94963.80 87413.14 3313.45 o
5 1 0 1328.86 1715.53 84.71 o
7 1 0 59240.18 58577.86 984.72 o
9 1 0 125994.38 126917.05 2077.27 o
11 1 0 106810.41 110030.75 1842.35 o
13 1 0 28420.71 29320.01 537.27 o
15 1 0 156.72 299.15 109.03 o
17 1 0 19850.11 20228.02 449.12 o
19 1 0 1794.78 2338.22 232.81 o
21 1 0 38876.26 40390.95 789.11 o
23 1 0 51920.54 53842.75 1126.10 o
25 1 0 3177.68 4134.46 327.93 o
27 1 0 10161.00 10806.17 555.72 o
0 2 0 231497.73 226987.75 9463.27 o
2 2 0 413.67 802.00 81.88 o
4 2 0 32320.17 32246.42 575.86 o
6 2 0 1933.93 2168.28 163.76 o
8 2 0 135731.58 133190.91 2317.62 o
10 2 0 4386.41 4772.70 197.50 o
12 2 0 161176.02 162127.38 2457.26 o
14 2 0 8455.08 8744.10 398.17 o
16 2 0 4407.80 4508.86 232.52 o
18 2 0 1357.87 1728.40 173.94 o
20 2 0 33499.21 35425.80 715.17 o
22 2 0 5899.88 6393.62 356.25 o
24 2 0 30439.46 31297.68 805.91 o
26 2 0 5509.77 5892.49 394.99 o
28 2 0 9129.80 9173.74 507.13 o
1 3 0 33557.48 36057.75 761.20 o
3 3 0 180278.09 177858.78 2705.02 o
5 3 0 74429.97 72224.70 1130.89 o
7 3 0 17876.69 18022.59 332.16 o
9 3 0 306565.09 300538.44 7589.39 o
11 3 0 260086.50 258164.02 3869.89 o
13 3 0 831.93 1278.13 151.65 o
15 3 0 66722.92 68091.48 1147.23 o
17 3 0 75729.49 75800.52 1280.36 o
19 3 0 2256.97 3483.76 550.85 o
21 3 0 50928.91 50179.97 1195.32 o
23 3 0 87844.39 86221.75 1850.05 o
25 3 0 34805.51 35043.55 905.94 o
27 3 0 6185.78 6338.86 524.07 o
0 4 0 54015.73 54188.51 2179.21 o
2 4 0 158344.22 157151.86 2909.09 o
4 4 0 41517.23 42005.27 811.60 o
6 4 0 78700.41 77675.63 1241.18 o
8 4 0 9904.84 10149.65 254.34 o
10 4 0 13902.91 13958.52 315.55 o
12 4 0 11304.02 11550.35 470.99 o
14 4 0 60795.79 60109.20 1048.92 o
16 4 0 167.33 59.88 172.41 o
18 4 0 95694.77 92965.39 1741.64 o
20 4 0 23706.66 23744.22 657.67 o
22 4 0 19048.85 19968.00 668.02 o
24 4 0 16620.38 16582.22 693.67 o
1 5 0 13753.20 13891.88 483.88 o
3 5 0 58607.68 59100.18 1258.92 o
5 5 0 26228.78 27456.29 960.96 o
7 5 0 1695.36 2396.40 232.24 o
9 5 0 100.50 583.59 354.35 o
11 5 0 833.65 1108.69 238.95 o
13 5 0 10676.58 11983.22 1057.05 o
15 5 0 31954.32 30942.06 994.32 o
17 5 0 62116.06 60195.64 1625.73 o
19 5 0 13086.72 12675.96 671.01 o
21 5 0 4925.49 5701.85 866.69 o
23 5 0 8509.06 8223.34 850.39 o
0 6 0 43135.46 44981.91 1519.69 o
2 6 0 42669.21 43564.02 1048.47 o
4 6 0 14398.67 15953.38 573.31 o
6 6 0 249968.28 250245.38 4315.02 o
8 6 0 52854.77 54891.08 1633.39 o
10 6 0 4920.21 5447.27 394.56 o
12 6 0 21205.29 21814.96 834.23 o
14 6 0 128443.23 124914.34 3058.62 o
16 6 0 16620.80 16964.06 904.46 o
18 6 0 65244.95 61165.21 1740.71 o
20 6 0 31300.81 30226.96 1133.70 o
1 7 0 7395.84 7987.02 658.64 o
3 7 0 38104.89 36581.25 889.58 o
5 7 0 13143.79 13720.09 519.57 o
7 7 0 4886.62 5549.34 370.88 o
9 7 0 33475.54 32559.06 1095.39 o
11 7 0 32727.96 33373.72 1120.20 o
13 7 0 1159.32 1580.18 400.83 o
15 7 0 15790.44 15742.85 812.56 o
17 7 0 22170.39 21862.78 2014.61 o
0 8 0 4169.74 3736.49 476.33 o
2 8 0 368.97 361.52 289.15 o
4 8 0 2418.19 2749.45 347.92 o
6 8 0 51681.58 54124.92 1603.78 o
8 8 0 5782.26 6180.64 825.86 o
10 8 0 1147.74 1319.82 437.63 o
-29 1 1 14623.96 14086.75 581.16 o
-27 1 1 10001.41 10027.29 474.86 o
-25 1 1 14105.89 14909.49 460.31 o
-23 1 1 50746.79 52405.35 980.06 o
-21 1 1 239700.00 247392.67 3768.45 o
-19 1 1 25990.36 28567.64 584.47 o
-17 1 1 183.81 481.91 122.20 o
-15 1 1 17189.46 18829.29 482.11 o
-13 1 1 195200.02 192084.98 3465.89 o
-11 1 1 2688.38 3843.23 200.28 o
-9 1 1 242492.39 232802.56 4139.25 o
-7 1 1 76161.05 75062.10 1371.02 o
-5 1 1 11650.17 12073.27 350.45 o
-3 1 1 56518.01 53251.49 974.03 o
1 1 1 150134.70 137412.70 1897.90 o
3 1 1 36771.60 35357.73 513.03 o
7 1 1 50732.41 50006.57 732.38 o
9 1 1 596.78 927.26 133.75 o
11 1 1 382754.19 370363.03 7111.06 o
13 1 1 101324.71 101514.08 1989.01 o
15 1 1 5732.79 6673.94 253.34 o
17 1 1 15777.33 16547.93 408.96 o
19 1 1 119735.95 121937.85 1954.94 o
21 1 1 55017.26 55718.64 1140.76 o
23 1 1 38484.98 39455.10 912.28 o
25 1 1 25305.31 26328.76 837.48 o
27 1 1 253.86 166.51 318.26 o
-28 2 1 19347.80 19697.20 671.54 o
-26 2 1 10457.85 10843.59 653.66 o
-24 2 1 52916.16 53318.58 1131.45 o
-22 2 1 15734.69 17285.32 473.50 o
-20 2 1 3859.02 4667.16 256.07 o
-18 2 1 66614.79 68093.89 1153.06 o
-16 2 1 36691.47 37287.17 685.47 o
-14 2 1 40253.10 41670.88 789.65 o
-12 2 1 280619.00 264858.78 5539.81 o
-10 2 1 291533.28 278972.00 5607.47 o
-8 2 1 44878.23 44577.18 876.82 o
-6 2 1 17696.94 17454.76 404.65 o
-4 2 1 75710.24 73667.96 1520.70 o
0 2 1 149422.16 144837.64 2982.10 o
2 2 1 241827.84 230448.97 3170.11 o
4 2 1 135280.31 133155.08 1999.68 o
6 2 1 32972.46 33283.62 681.05 o
8 2 1 282242.84 270779.81 3733.08 o
10 2 1 207226.83 207557.20 3122.32 o
12 2 1 16577.28 17802.66 344.44 o
14 2 1 21634.70 23037.12 478.88 o
16 2 1 18328.98 18730.07 438.23 o
18 2 1 2632.66 2786.80 208.90 o
20 2 1 85191.45 84611.94 1605.10 o
22 2 1 124575.77 128100.10 2693.28 o
24 2 1 30883.35 31402.84 824.65 o
26 2 1 4228.92 4319.88 429.98 o
-27 3 1 559.35 279.67 268.73 o
-25 3 1 31295.59 31439.88 827.01 o
-23 3 1 10638.61 11913.71 516.82 o
-21 3 1 154.93 167.49 174.22 o
-19 3 1 67049.65 67604.84 1300.03 o
-17 3 1 14467.58 15071.73 397.68 o
-15 3 1 12680.55 13609.48 399.32 o
-13 3 1 24170.47 24103.16 535.69 o
-11 3 1 9557.23 9418.98 349.59 o
-9 3 1 6932.15 7452.16 252.88 o
-7 3 1 12853.28 13661.78 386.82 o
-5 3 1 7837.78 8262.48 302.32 o
-3 3 1 69842.54 70023.71 1413.33 o
-1 3 1 291.80 671.03 131.95 o
1 3 1 54616.14 56056.00 1088.73 o
3 3 1 111904.02 109845.09 1626.06 o
5 3 1 5323.25 5412.39 165.68 o
7 3 1 13915.56 13931.53 280.44 o
9 3 1 88355.25 87731.53 1285.77 o
11 3 1 51.87 349.90 113.48 o
13 3 1 3289.52 3888.43 208.00 o
15 3 1 10966.85 11373.98 377.30 o
17 3 1 18063.60 18028.70 518.06 o
19 3 1 1248.76 1615.89 235.10 o
21 3 1 6.47 185.30 227.15 o
23 3 1 29621.18 30576.54 951.06 o
25 3 1 213.41 249.55 269.00 o
-26 4 1 23723.51 22788.06 830.66 o
-24 4 1 73854.80 70869.98 1478.78 o
-22 4 1 18087.85 18111.82 592.68 o
-20 4 1 10961.11 11673.83 456.24 o
-18 4 1 75095.74 74610.59 1296.19 o
-16 4 1 35704.55 37087.44 793.03 o
-14 4 1 168.28 298.77 132.73 o
-12 4 1 22408.58 23558.08 497.13 o
-10 4 1 62132.16 61794.07 953.63 o
-8 4 1 870.63 1379.54 221.00 o
-6 4 1 104013.99 103380.81 1745.15 o
-4 4 1 178403.55 180696.81 3322.50 o
-2 4 1 28446.04 28299.79 676.79 o
0 4 1 42867.10 44182.80 946.04 o
2 4 1 121314.46 122805.77 2728.53 o
4 4 1 38409.78 40019.14 656.22 o
6 4 1 8786.10 8744.02 235.78 o
8 4 1 47422.37 46220.64 739.84 o
10 4 1 46581.42 44811.50 732.80 o
12 4 1 321.36 761.24 149.29 o
14 4 1 89003.41 84232.54 1559.55 o
16 4 1 95383.00 92417.59 1835.87 o
18 4 1 9172.14 9221.46 414.70 o
20 4 1 24196.38 24086.74 930.41 o
22 4 1 44743.28 41766.28 1490.71 o
24 4 1 3048.48 3139.67 412.97 o
-23 5 1 37763.62 36043.33 1581.25 o
-21 5 1 60039.05 58679.83 2375.14 o
-19 5 1 75556.66 70689.02 1861.68 o
-17 5 1 6150.14 7020.00 744.63 o
-15 5 1 130651.18 130143.65 2975.77 o
-13 5 1 13658.94 14667.48 540.93 o
-11 5 1 16.64 329.01 202.62 o
-9 5 1 16671.46 18430.44 576.94 o
-7 5 1 231785.22 235973.14 4347.14 o
-5 5 1 8292.63 8115.96 395.09 o
-3 5 1 168084.56 170839.94 3205.21 o
-1 5 1 87951.69 88147.50 1765.79 o
1 5 1 55285.53 54839.52 1185.61 o
3 5 1 1114.18 2416.35 634.58 o
5 5 1 148980.23 145340.70 2488.35 o
7 5 1 15097.61 14994.12 443.66 o
9 5 1 34753.14 34698.28 755.06 o
11 5 1 35676.82 34306.97 1009.37 o
13 5 1 102368.69 102201.00 2425.89 o
15 5 1 22803.38 22542.74 843.92 o
17 5 1 113752.30 107194.24 4224.17 o
19 5 1 75979.23 74343.48 4329.93 o
21 5 1 806.94 16.07 372.10 o
-22 6 1 3.96 136.42 381.61 o
-20 6 1 2095.32 3086.68 492.14 o
-18 6 1 14.10 -225.77 399.02 o
-16 6 1 3608.59 4909.59 485.36 o
-14 6 1 9737.22 10293.66 698.10 o
-12 6 1 16761.43 17873.58 637.43 o
-10 6 1 16652.19 18108.83 634.29 o
-8 6 1 19015.89 20468.44 675.45 o
-6 6 1 5038.15 5641.87 382.98 o
-4 6 1 420.74 477.98 228.31 o
-2 6 1 3236.90 3264.85 306.82 o
0 6 1 24055.99 24081.50 634.69 o
2 6 1 7118.33 8080.84 375.08 o
4 6 1 272.88 1441.57 628.90 o
6 6 1 1910.26 2587.08 282.66 o
8 6 1 6826.16 6924.39 385.16 o
10 6 1 11599.97 11419.84 599.66 o
12 6 1 12127.77 12636.48 681.20 o
14 6 1 4743.81 5427.85 497.41 o
16 6 1 56.36 411.51 344.48 o
18 6 1 3112.97 2862.24 551.28 o
20 6 1 17645.32 17703.55 892.31 o
-17 7 1 12018.19 10923.45 918.48 o
-15 7 1 131306.98 130004.45 4856.96 o
-13 7 1 31332.51 32256.90 1126.32 o
-11 7 1 76.36 -158.15 309.81 o
-9 7 1 15930.44 17642.38 915.14 o
-7 7 1 95937.21 96765.59 2354.75 o
-5 7 1 3664.04 4295.73 434.66 o
-3 7 1 13131.47 14022.15 531.83 o
-1 7 1 371.36 466.86 230.28 o
1 7 1 7854.51 9067.95 437.57 o
3 7 1 12840.85 11970.55 480.26 o
5 7 1 208179.36 197810.19 3921.77 o
7 7 1 61373.88 62076.89 1686.83 o
9 7 1 3080.40 3625.47 451.95 o
11 7 1 7168.44 6495.11 671.47 o
13 7 1 20791.99 20867.04 1062.03 o
15 7 1 1001.15 1264.11 434.53 o
-12 8 1 44822.18 47013.33 1326.71 o
-10 8 1 27565.83 28762.77 1043.93 o
-8 8 1 7779.50 8295.25 525.46 o
-6 8 1 64491.65 63362.08 1694.92 o
-4 8 1 70320.33 69660.58 1516.67 o
-2 8 1 18844.30 18924.01 906.61 o
0 8 1 9769.88 9717.10 703.17 o
2 8 1 73004.25 69273.26 1464.96 o
4 8 1 44998.64 43091.21 1931.83 o
6 8 1 5140.56 5782.00 552.46 o
8 8 1 62570.23 62706.61 1798.77 o
10 8 1 25657.92 26389.76 1084.57 o
-30 0 2 74004.38 72043.61 2411.04 o
-28 0 2 34327.91 33789.52 1098.04 o
-26 0 2 7883.82 8576.70 523.38 o
-24 0 2 92601.88 93836.37 2230.02 o
-22 0 2 351378.69 359934.72 7636.14 o
-20 0 2 38471.54 40664.84 1286.13 o
-18 0 2 2576.96 3402.41 308.69 o
-16 0 2 719.39 1408.84 126.56 o
-14 0 2 81541.55 82967.87 1822.19 o
-12 0 2 13167.06 13650.86 632.78 o
-10 0 2 657403.94 599864.88 20131.64 o
-8 0 2 129266.99 125987.07 2667.00 o
0 0 2 37447.12 36701.07 1006.52 o
2 0 2 78176.65 72859.76 1359.23 o
4 0 2 25445.61 26044.12 528.50 o
6 0 2 3649.31 3954.09 184.32 o
8 0 2 14386.04 16255.28 548.59 o
10 0 2 571119.63 528362.06 9635.29 o
12 0 2 317198.16 312602.28 5758.09 o
14 0 2 2533.82 3160.51 314.21 o
16 0 2 32533.83 33557.12 1095.61 o
18 0 2 78301.89 83322.18 1971.91 o
20 0 2 13533.25 13498.19 1145.37 o
22 0 2 62870.34 67860.63 2211.84 o
24 0 2 34049.79 35011.07 1417.11 o
26 0 2 559.94 518.21 409.47 o
-29 1 2 13532.42 14674.98 571.89 o
-27 1 2 4641.74 5300.38 321.46 o
-25 1 2 11615.77 11965.56 440.17 o
-23 1 2 1329.25 1402.19 193.45 o
-21 1 2 35381.38 37425.93 874.88 o
-19 1 2 33970.35 35472.59 811.46 o
-17 1 2 7361.57 7815.81 266.03 o
-15 1 2 6901.93 7500.69 245.41 o
-13 1 2 70132.50 72496.44 1242.94 o
-11 1 2 128771.56 128455.98 2111.68 o
-9 1 2 54275.03 55079.46 937.41 o
-7 1 2 20235.61 20316.11 349.39 o
-5 1 2 28323.92 27175.89 408.46 o
-3 1 2 34191.82 32448.20 447.58 o
1 1 2 106247.81 101629.00 1524.88 o
3 1 2 26685.24 26768.65 384.62 o
7 1 2 41891.83 41600.84 630.85 o
9 1 2 43453.63 42203.45 649.75 o
11 1 2 3901.22 4216.28 196.86 o
13 1 2 19661.39 19216.22 477.69 o
15 1 2 17414.99 17959.76 418.10 o
17 1 2 17377.81 18396.19 449.78 o
19 1 2 77713.76 79918.00 2088.34 o
21 1 2 44894.80 45926.91 1010.57 o
23 1 2 9835.35 10649.54 543.51 o
25 1 2 75.78 183.83 311.88 o
-30 2 2 19249.68 19375.55 722.97 o
-28 2 2 725.87 863.07 271.09 o
-26 2 2 11667.61 12069.48 442.96 o
-24 2 2 118.10 340.15 183.17 o
-22 2 2 67921.30 68506.87 1201.75 o
-20 2 2 440.55 600.02 150.27 o
-18 2 2 19146.96 20005.25 563.45 o
-16 2 2 8167.72 8310.59 323.28 o
-14 2 2 92496.63 93085.50 1769.74 o
-12 2 2 812.65 1895.48 303.40 o
-10 2 2 166676.25 162301.05 2999.67 o
-8 2 2 13023.12 14319.58 417.60 o
-6 2 2 4370.63 5203.75 194.21 o
-4 2 2 14253.52 14761.31 289.29 o
-2 2 2 121138.52 118504.91 1658.78 o
0 2 2 23987.59 22740.97 374.73 o
2 2 2 106517.42 103515.55 1456.57 o
4 2 2 31174.40 30874.86 503.20 o
6 2 2 22103.80 22051.91 371.15 o
8 2 2 4393.28 4576.56 178.84 o
10 2 2 101098.23 100258.96 1449.41 o
12 2 2 5665.46 6238.95 238.14 o
14 2 2 31497.91 31724.95 614.44 o
16 2 2 1029.98 1412.75 201.34 o
18 2 2 13421.49 14023.25 480.89 o
20 2 2 26832.61 27792.04 804.21 o
22 2 2 31735.97 33187.24 931.60 o
24 2 2 30592.79 31436.35 1017.93 o
26 2 2 95.87 204.00 315.97 o
-29 3 2 1967.88 2374.80 348.99 o
-27 3 2 17958.98 18196.01 637.49 o
-25 3 2 40432.14 38593.82 1124.21 o
-23 3 2 12861.44 13454.23 442.21 o
-21 3 2 35810.70 37424.45 699.77 o
-19 3 2 148291.73 149430.83 2566.57 o
-17 3 2 63371.07 63152.59 1183.54 o
-15 3 2 36750.80 37014.84 963.91 o
-13 3 2 255403.39 249500.34 4082.52 o
-11 3 2 138345.67 135865.77 2521.51 o
-9 3 2 1560.53 2196.20 169.97 o
-7 3 2 71601.19 70729.14 1745.83 o
-5 3 2 87723.37 89856.52 1695.42 o
-3 3 2 4518.33 5770.82 268.58 o
-1 3 2 121492.20 121783.19 1725.61 o
1 3 2 306391.53 290554.22 4593.00 o
3 3 2 95811.80 92620.32 1403.82 o
5 3 2 29690.69 28695.79 515.21 o
7 3 2 235939.84 230022.53 3445.50 o
9 3 2 49720.85 49477.73 772.47 o
11 3 2 11472.62 11946.91 314.78 o
13 3 2 60568.47 59285.73 1135.21 o
15 3 2 50350.73 50461.87 1021.24 o
17 3 2 965.20 1097.63 207.66 o
19 3 2 79416.09 76314.27 1930.71 o
21 3 2 125731.88 120326.68 2495.38 o
23 3 2 27906.24 27264.75 777.15 o
25 3 2 15853.95 16731.18 744.25 o
-26 4 2 4197.65 3979.68 432.37 o
-24 4 2 35883.80 35164.27 1125.98 o
-22 4 2 26433.46 26952.01 608.33 o
-20 4 2 113396.90 112839.23 1868.13 o
-18 4 2 5643.97 6515.45 330.36 o
-16 4 2 61439.19 63138.44 1307.39 o
-14 4 2 6774.20 7129.69 312.88 o
-12 4 2 49226.53 50445.50 1502.90 o
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