#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014738.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014738_Fobs loop_ _publ_author_name 'Bomfim, Joao A. S.' 'Wardell, James L.' 'Low, John N.' 'Skakle, Janet M. S.' 'Glidewell, Christopher' _publ_section_title ; \p-Stacked hydrogen-bonded sheets in N,N'-bis(4-nitrobenzylidene)ethane-1,2-diamine and \p-stacked hydrogen-bonded chains in N,N'-bis(4-nitrobenzylidene)propane-1,3-diamine ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o53 _journal_page_last o56 _journal_volume 61 _journal_year 2005 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.559 _cell_angle_gamma 90.000 _cell_length_a 12.9412 _cell_length_b 7.3062 _cell_length_c 16.9061 _exptl_crystal_F_000 712.00 _reflns_d_resolution_high 0.7671 _[local]_cod_data_source_file sk1795IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 04src393' _shelx_refln_list_code 4 _shelx_f_calc_maximum 161.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9.90 5.85 4.81 o 6 0 0 2680.65 2725.07 81.10 o 8 0 0 24154.23 25309.46 603.87 o 10 0 0 130.06 250.75 20.22 o 12 0 0 1368.81 1959.05 289.88 o 14 0 0 69.84 485.59 80.22 o 16 0 0 91.41 39.33 29.39 o 1 1 0 2007.96 1764.27 44.71 o 3 1 0 13909.81 12667.61 244.21 o 5 1 0 794.14 822.39 20.27 o 7 1 0 9465.97 9598.56 164.34 o 9 1 0 1256.06 1353.63 30.06 o 11 1 0 3748.50 3818.57 86.17 o 13 1 0 702.83 716.25 32.30 o 15 1 0 1203.46 1353.22 65.43 o 0 2 0 46.16 46.67 3.19 o 2 2 0 483.93 478.19 9.84 o 4 2 0 1445.76 1425.53 24.95 o 6 2 0 0.52 4.03 2.45 o 8 2 0 18.49 12.97 3.31 o 10 2 0 762.77 721.28 23.34 o 12 2 0 25.00 24.25 4.45 o 14 2 0 455.25 396.81 29.90 o 16 2 0 67.20 30.68 22.72 o 1 3 0 2652.46 2554.07 85.56 o 3 3 0 3525.83 3711.46 80.32 o 5 3 0 224.10 220.93 6.81 o 7 3 0 1293.98 1345.76 32.73 o 9 3 0 0.29 92.53 12.74 o 11 3 0 179.58 187.08 18.05 o 13 3 0 30.25 10.30 11.24 o 15 3 0 26.29 15.86 20.86 o 0 4 0 3900.51 4592.49 188.37 o 2 4 0 5.35 4.17 6.60 o 4 4 0 1027.36 1223.22 30.62 o 6 4 0 511.68 496.09 17.38 o 8 4 0 534.15 546.00 20.08 o 10 4 0 36.85 18.82 7.24 o 12 4 0 52.76 37.60 11.92 o 14 4 0 30.82 38.29 17.40 o 1 5 0 152.56 136.88 7.07 o 3 5 0 194.01 169.30 11.09 o 5 5 0 27.65 19.53 8.26 o 7 5 0 90.90 102.36 5.16 o 9 5 0 57.73 68.36 9.26 o 11 5 0 13.31 5.33 7.98 o 13 5 0 80.94 81.52 19.08 o 0 6 0 0.14 5.47 2.23 o 2 6 0 15.10 16.14 5.04 o 4 6 0 72.86 66.84 9.55 o 6 6 0 362.62 355.66 21.98 o 8 6 0 23.97 18.15 7.60 o 10 6 0 161.57 147.34 18.44 o 12 6 0 79.02 82.79 13.35 o 1 7 0 98.93 88.97 18.42 o 3 7 0 54.25 46.50 7.22 o 5 7 0 447.07 493.99 30.81 o 7 7 0 0.32 12.85 11.56 o 9 7 0 214.34 271.55 45.67 o 11 7 0 6.38 56.95 38.83 o 0 8 0 11.02 1.64 22.55 o 2 8 0 12.57 7.87 6.18 o 4 8 0 3.57 10.63 12.78 o 6 8 0 5.13 2.83 12.56 o 8 8 0 1.06 19.22 25.41 o 1 9 0 49.11 41.42 26.41 o 3 9 0 8.21 83.58 33.89 o 5 9 0 3.23 -5.48 40.41 o -15 1 1 632.73 648.38 40.41 o -13 1 1 4.14 1.95 8.95 o -11 1 1 516.77 541.06 19.89 o -9 1 1 392.01 383.67 13.41 o -7 1 1 1360.20 1426.09 28.72 o -5 1 1 31.78 54.10 3.27 o -3 1 1 333.07 272.48 7.05 o -1 1 1 1065.86 1041.66 17.81 o 1 1 1 1.11 1.54 1.37 o 3 1 1 21702.21 21416.43 574.85 o 5 1 1 1544.59 1493.02 34.68 o 7 1 1 8089.42 8140.97 173.32 o 9 1 1 9.60 11.46 4.35 o 11 1 1 4289.94 4421.34 107.85 o 13 1 1 15.56 22.01 10.21 o 15 1 1 882.85 992.51 85.46 o -16 2 1 69.76 98.32 33.82 o -14 2 1 13.81 29.31 12.15 o -12 2 1 94.26 69.11 11.08 o -10 2 1 73.63 70.30 7.65 o -8 2 1 0.84 4.64 4.14 o -6 2 1 495.84 462.26 15.74 o -4 2 1 774.18 745.66 15.00 o -2 2 1 1772.33 1468.46 25.81 o 0 2 1 3212.06 2946.38 69.66 o 2 2 1 1682.51 1496.66 54.98 o 4 2 1 1870.34 1813.52 40.51 o 6 2 1 281.35 292.46 13.23 o 8 2 1 333.84 338.04 14.28 o 10 2 1 0.22 1.04 9.59 o 12 2 1 9.08 18.58 11.85 o 14 2 1 85.75 58.42 16.70 o 16 2 1 5.10 27.10 24.17 o -15 3 1 329.63 374.76 31.99 o -13 3 1 253.61 305.51 22.46 o -11 3 1 715.80 757.06 32.12 o -9 3 1 338.29 367.82 14.28 o -7 3 1 2943.12 3084.36 63.05 o -5 3 1 2150.79 2313.29 38.81 o -3 3 1 1503.94 1541.21 35.92 o -1 3 1 1098.95 1217.23 38.03 o 1 3 1 1849.48 1741.28 43.95 o 3 3 1 1885.92 2133.05 47.77 o 5 3 1 9.18 7.07 3.41 o 7 3 1 12.03 19.42 3.43 o 9 3 1 121.06 105.58 9.12 o 11 3 1 3.33 -7.05 7.42 o 13 3 1 5.45 -5.15 10.07 o 15 3 1 61.46 86.93 22.65 o -14 4 1 7.27 66.66 35.81 o -12 4 1 63.23 59.65 14.33 o -10 4 1 18.68 10.36 5.98 o -8 4 1 1.50 2.94 2.63 o -6 4 1 184.32 205.73 13.54 o -4 4 1 1085.84 1216.99 40.45 o -2 4 1 751.33 779.69 31.35 o 0 4 1 4815.56 4853.60 104.18 o 2 4 1 317.30 335.44 15.41 o 4 4 1 5477.45 5692.48 121.40 o 6 4 1 23.77 31.08 7.32 o 8 4 1 1954.92 2106.93 67.69 o 10 4 1 15.18 16.84 6.89 o 12 4 1 514.68 540.69 36.35 o 14 4 1 0.67 18.38 19.58 o -13 5 1 4.72 18.49 15.04 o -11 5 1 40.34 60.12 16.21 o -9 5 1 98.22 111.95 12.46 o -7 5 1 49.92 45.50 3.89 o -5 5 1 40.36 32.07 6.99 o -3 5 1 728.99 742.36 39.01 o -1 5 1 59.82 54.33 6.47 o 1 5 1 268.22 319.43 12.78 o 3 5 1 273.22 307.75 12.76 o 5 5 1 111.42 112.09 9.45 o 7 5 1 108.47 107.76 5.96 o 9 5 1 107.71 102.89 10.77 o 11 5 1 140.45 121.04 15.75 o 13 5 1 78.98 36.30 21.19 o -12 6 1 157.90 126.94 17.59 o -10 6 1 178.42 150.34 15.71 o -8 6 1 355.60 344.46 24.34 o -6 6 1 342.11 333.91 20.92 o -4 6 1 114.76 95.20 10.67 o -2 6 1 1009.79 931.71 34.92 o 0 6 1 35.90 29.31 2.30 o 2 6 1 619.44 605.72 26.87 o 4 6 1 27.17 9.11 5.49 o 6 6 1 397.64 455.21 46.29 o 8 6 1 0.51 5.02 5.99 o 10 6 1 59.99 111.98 26.30 o 12 6 1 0.22 25.07 21.48 o -11 7 1 10.58 14.07 33.83 o -9 7 1 111.23 70.63 21.79 o -7 7 1 11.34 23.30 9.59 o -5 7 1 125.43 124.61 16.63 o -3 7 1 171.77 140.79 10.61 o -1 7 1 249.37 254.21 15.54 o 1 7 1 118.36 84.98 5.63 o 3 7 1 26.85 29.37 8.15 o 5 7 1 215.38 243.22 19.20 o 7 7 1 20.32 15.08 25.10 o 9 7 1 55.90 27.54 22.31 o 11 7 1 3.63 27.31 27.31 o -8 8 1 5.53 11.47 30.97 o -6 8 1 3.72 25.75 18.36 o -4 8 1 28.07 36.86 11.21 o -2 8 1 26.76 37.56 12.54 o 0 8 1 22.13 19.60 18.96 o 2 8 1 24.27 19.43 8.66 o 4 8 1 77.37 82.09 14.89 o 6 8 1 17.27 47.88 22.82 o 8 8 1 2.26 -3.03 17.78 o -5 9 1 11.58 -7.45 82.85 o -3 9 1 101.42 124.96 23.83 o -1 9 1 0.28 17.47 19.95 o 1 9 1 0.00 -2.58 20.68 o 3 9 1 2.91 -11.77 19.16 o 5 9 1 14.30 16.85 12.82 o -16 0 2 703.45 648.27 63.48 o -14 0 2 491.40 596.66 63.39 o -12 0 2 3929.90 4467.88 249.25 o -10 0 2 2234.26 2277.28 56.17 o -8 0 2 8522.93 8802.43 195.22 o -6 0 2 1010.46 1029.58 28.68 o -4 0 2 26189.88 25229.53 449.58 o -2 0 2 2754.14 2620.04 46.65 o 2 0 2 2092.29 1728.09 38.63 o 4 0 2 28.57 48.19 8.06 o 6 0 2 74.11 47.26 9.98 o 8 0 2 1351.24 1489.63 78.21 o 10 0 2 155.62 159.38 12.75 o 12 0 2 71.06 88.13 13.77 o 14 0 2 3.24 -6.30 22.89 o 16 0 2 50.91 21.59 37.01 o -15 1 2 1.08 -9.92 13.76 o -13 1 2 0.13 -3.42 6.61 o -11 1 2 19.75 15.18 5.70 o -9 1 2 788.06 875.92 19.54 o -7 1 2 185.85 183.77 7.55 o -5 1 2 7342.58 7158.42 123.08 o -3 1 2 190.62 185.54 5.40 o -1 1 2 24599.52 22034.94 299.81 o 1 1 2 24.13 28.93 2.04 o 3 1 2 15382.74 15460.98 345.70 o 5 1 2 77.98 99.10 4.88 o 7 1 2 3018.09 3146.44 75.64 o 9 1 2 67.44 64.12 4.69 o 11 1 2 531.62 496.69 17.98 o 13 1 2 16.05 15.80 13.12 o 15 1 2 108.08 47.82 32.13 o -16 2 2 3.03 -0.32 19.34 o -14 2 2 169.19 168.05 22.25 o -12 2 2 57.59 35.08 7.63 o -10 2 2 34.69 43.36 5.57 o -8 2 2 95.48 98.96 5.41 o -6 2 2 1142.69 1164.77 22.24 o -4 2 2 3451.10 3414.52 52.71 o -2 2 2 542.94 551.51 10.04 o 0 2 2 1035.81 1004.32 17.59 o 2 2 2 1529.39 1478.32 33.26 o 4 2 2 1578.35 1545.23 38.76 o 6 2 2 447.21 591.02 20.69 o 8 2 2 1.34 5.38 6.12 o 10 2 2 413.57 438.04 21.11 o 12 2 2 53.29 56.94 12.18 o 14 2 2 806.46 698.17 49.82 o -15 3 2 67.32 31.55 21.95 o -13 3 2 26.75 15.40 10.85 o -11 3 2 240.80 213.25 14.72 o -9 3 2 16.28 10.53 4.06 o -7 3 2 195.46 206.66 7.00 o -5 3 2 22.40 22.94 3.37 o -3 3 2 48.39 71.26 3.22 o -1 3 2 6.41 14.72 1.73 o 1 3 2 36.91 35.13 2.40 o 3 3 2 2.04 -2.91 2.91 o 5 3 2 7.38 5.59 3.28 o 7 3 2 20.37 18.06 6.10 o 9 3 2 0.39 -2.50 6.42 o 11 3 2 0.02 4.67 7.84 o 13 3 2 5.48 0.05 11.55 o 15 3 2 0.00 18.75 20.31 o -14 4 2 2.00 6.02 15.57 o -12 4 2 173.89 225.00 21.55 o -10 4 2 28.73 29.15 5.20 o -8 4 2 375.86 337.81 13.30 o -6 4 2 29.47 26.97 3.21 o -4 4 2 2003.25 2119.86 52.13 o -2 4 2 68.42 77.26 6.69 o 0 4 2 661.59 775.34 17.65 o 2 4 2 1.82 3.23 1.43 o 4 4 2 533.52 642.10 17.77 o 6 4 2 512.35 510.75 15.23 o 8 4 2 11.29 5.66 5.70 o 10 4 2 136.65 151.68 13.15 o 12 4 2 75.95 89.51 16.61 o 14 4 2 100.70 109.33 23.31 o -13 5 2 0.00 26.83 18.42 o -11 5 2 40.03 47.28 12.52 o -9 5 2 16.20 10.72 4.64 o -7 5 2 90.07 89.30 5.47 o -5 5 2 287.61 280.06 21.97 o -3 5 2 113.28 120.44 10.66 o -1 5 2 103.27 100.75 8.27 o 1 5 2 42.60 51.16 4.87 o 3 5 2 6.82 5.05 4.81 o 5 5 2 77.32 81.85 6.19 o 7 5 2 419.02 410.08 16.30 o 9 5 2 113.24 104.41 10.32 o 11 5 2 373.57 408.42 29.72 o 13 5 2 23.45 62.40 24.54 o -12 6 2 45.15 18.54 12.80 o -10 6 2 122.13 115.28 25.04 o -8 6 2 62.30 63.29 9.93 o -6 6 2 0.30 8.66 6.72 o -4 6 2 16.64 25.75 6.06 o -2 6 2 4.21 2.20 6.66 o 0 6 2 1.03 4.32 3.67 o 2 6 2 162.82 179.72 9.85 o 4 6 2 18.46 7.64 4.50 o 6 6 2 0.55 5.26 6.82 o 8 6 2 4.21 14.51 5.79 o 10 6 2 0.03 -6.65 6.65 o 12 6 2 11.42 29.05 14.64 o -11 7 2 22.45 30.22 33.99 o -9 7 2 381.95 364.73 46.81 o -7 7 2 148.41 140.46 19.06 o -5 7 2 1316.83 1309.35 61.15 o -3 7 2 146.34 102.53 10.89 o -1 7 2 1082.44 1026.90 42.53 o 1 7 2 369.70 339.33 19.23 o 3 7 2 637.73 563.00 33.94 o 5 7 2 82.29 78.75 12.29 o 7 7 2 22.76 -12.40 12.40 o 9 7 2 33.43 8.62 20.42 o -8 8 2 12.53 23.93 28.92 o -6 8 2 38.01 35.24 13.85 o -4 8 2 16.00 0.70 8.22 o -2 8 2 13.60 13.75 6.67 o 0 8 2 387.91 369.86 39.06 o 2 8 2 42.69 51.23 16.70 o 4 8 2 451.20 485.62 48.91 o 6 8 2 30.98 10.89 15.43 o 8 8 2 445.72 579.95 75.52 o -5 9 2 28.33 -1.46 33.61 o -3 9 2 0.93 20.40 20.28 o -1 9 2 48.57 73.46 25.46 o 1 9 2 48.46 35.95 23.65 o 3 9 2 0.02 5.83 16.68 o -15 1 3 1.72 -18.89 18.89 o -13 1 3 82.54 81.57 12.40 o -11 1 3 9.96 13.26 4.47 o -9 1 3 133.77 137.35 7.42 o -7 1 3 993.45 1049.87 20.27 o -5 1 3 1143.46 1101.53 17.39 o -3 1 3 522.73 448.11 8.35 o -1 1 3 19202.91 18062.50 220.65 o 1 1 3 2292.31 2181.52 34.07 o 3 1 3 6352.13 6229.11 108.95 o 5 1 3 307.10 305.19 9.03 o 7 1 3 2036.65 2093.59 56.58 o 9 1 3 0.00 0.46 2.94 o 11 1 3 2.48 -1.79 6.64 o 13 1 3 17.86 32.27 11.92 o 15 1 3 1.92 9.90 17.43 o -16 2 3 12.61 39.87 20.12 o -14 2 3 23.89 12.91 11.42 o -12 2 3 66.32 68.99 7.64 o -10 2 3 63.82 58.07 7.37 o -8 2 3 18.50 18.04 3.74 o -6 2 3 17.48 29.18 2.84 o -4 2 3 190.87 208.13 6.89 o -2 2 3 3.63 4.14 1.81 o 0 2 3 1611.00 1614.74 28.21 o 2 2 3 452.48 391.51 9.38 o 4 2 3 727.75 765.85 19.37 o 6 2 3 670.90 721.42 26.29 o 8 2 3 96.59 97.96 10.77 o 10 2 3 556.11 547.44 49.01 o 12 2 3 0.34 13.67 11.14 o 14 2 3 252.43 288.74 27.44 o -15 3 3 0.07 18.58 22.30 o -13 3 3 6.78 23.70 10.58 o -11 3 3 3.05 6.86 6.80 o -9 3 3 7.26 11.83 4.38 o -7 3 3 470.25 445.62 12.77 o -5 3 3 485.00 461.52 11.30 o -3 3 3 112.86 126.77 4.86 o -1 3 3 61.96 87.17 3.80 o 1 3 3 192.76 179.38 5.89 o 3 3 3 11.40 17.72 2.81 o 5 3 3 443.32 477.39 14.65 o 7 3 3 147.78 141.54 13.15 o 9 3 3 19.31 135.29 27.11 o 11 3 3 0.73 1.75 10.33 o 13 3 3 11.50 10.82 13.46 o 15 3 3 13.07 41.09 26.14 o -14 4 3 11.44 26.08 15.66 o -12 4 3 38.27 73.41 15.57 o -10 4 3 49.89 69.86 6.23 o -8 4 3 493.21 505.18 20.21 o -6 4 3 222.51 222.33 9.06 o -4 4 3 1196.80 1262.11 31.18 o -2 4 3 13.04 11.37 2.02 o 0 4 3 1363.68 1416.43 34.27 o 2 4 3 21.60 18.13 2.54 o 4 4 3 139.34 158.89 7.33 o 6 4 3 58.09 45.35 3.68 o 8 4 3 10.40 2.84 5.46 o 10 4 3 3.39 2.14 7.94 o 12 4 3 0.03 16.34 18.12 o 14 4 3 3.78 25.89 18.24 o -13 5 3 5.01 -5.55 12.18 o -11 5 3 18.66 50.21 18.21 o -9 5 3 16.80 13.63 3.65 o -7 5 3 4.85 6.85 2.87 o -5 5 3 20.44 14.95 5.53 o -3 5 3 132.82 131.05 10.12 o -1 5 3 741.19 755.60 19.42 o 1 5 3 52.94 56.53 3.90 o 3 5 3 391.88 436.66 15.39 o 5 5 3 186.28 170.80 9.31 o 7 5 3 479.60 524.98 18.96 o 9 5 3 15.66 15.50 8.84 o 11 5 3 105.97 86.85 16.48 o 13 5 3 35.30 2.03 14.45 o -12 6 3 88.07 107.93 21.12 o -10 6 3 58.56 39.00 20.83 o -8 6 3 3.90 4.55 9.00 o -6 6 3 68.12 68.03 10.78 o -4 6 3 9.06 5.82 6.04 o -2 6 3 193.47 196.32 16.49 o 0 6 3 236.62 289.79 11.45 o 2 6 3 759.38 703.85 28.39 o 4 6 3 53.44 30.36 8.63 o 6 6 3 1179.04 1134.35 51.79 o 8 6 3 43.40 45.22 8.64 o 10 6 3 346.50 348.80 38.46 o 12 6 3 2.01 -7.21 10.67 o -11 7 3 77.83 68.21 29.46 o -9 7 3 52.07 54.92 22.55 o -7 7 3 497.26 532.46 38.09 o -5 7 3 21.04 19.85 11.56 o -3 7 3 614.61 529.14 38.10 o -1 7 3 97.41 107.86 13.08 o 1 7 3 813.14 799.64 39.54 o 3 7 3 0.05 -5.65 6.69 o 5 7 3 202.09 189.23 18.40 o 7 7 3 5.50 -12.70 12.70 o 9 7 3 85.38 109.68 38.83 o -8 8 3 27.91 10.30 29.00 o -6 8 3 0.03 -12.02 12.02 o -4 8 3 29.63 44.10 30.28 o -2 8 3 94.99 78.86 12.13 o 0 8 3 83.31 106.10 20.80 o 2 8 3 76.78 60.03 10.70 o 4 8 3 5.84 7.40 12.29 o 6 8 3 140.23 137.25 54.05 o 8 8 3 10.95 -19.11 25.43 o -5 9 3 63.22 59.06 20.09 o -3 9 3 55.65 126.10 30.97 o -1 9 3 103.44 146.12 28.39 o 1 9 3 59.16 47.43 24.47 o 3 9 3 10.76 15.04 16.87 o -16 0 4 117.13 45.01 28.50 o -14 0 4 52.03 32.60 23.57 o -12 0 4 853.92 892.03 47.21 o -10 0 4 1384.63 1341.25 83.08 o -8 0 4 1474.56 1477.90 45.17 o -6 0 4 2781.23 2486.99 55.50 o -4 0 4 8810.02 8302.12 136.28 o -2 0 4 8323.46 7350.95 138.46 o 0 0 4 2404.76 2184.31 40.87 o 2 0 4 54.69 65.98 4.48 o 4 0 4 1424.17 1399.99 38.34 o 6 0 4 206.45 223.05 20.85 o 8 0 4 195.87 187.79 13.58 o 10 0 4 571.04 598.82 36.98 o 12 0 4 68.64 99.53 50.54 o 14 0 4 18.72 27.44 19.78 o -15 1 4 11.10 -4.17 14.74 o -13 1 4 33.25 36.02 8.34 o -11 1 4 0.33 -4.95 4.95 o -9 1 4 141.56 115.84 6.56 o -7 1 4 116.53 116.76 5.01 o -5 1 4 2553.64 2324.06 37.40 o -3 1 4 1414.51 1441.88 19.54 o -1 1 4 8056.75 7416.03 90.26 o 1 1 4 2283.13 2399.87 37.14 o 3 1 4 3763.69 3605.65 55.66 o 5 1 4 1056.16 1000.28 22.99 o 7 1 4 523.75 495.76 12.86 o 9 1 4 158.91 154.81 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