#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014782.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014782_Fobs loop_ _publ_author_name 'Turgut, G\"unseli' 'Zora, Metin' 'Odaba\,so\(glu, Mustafa' 'Ersanl\?i, Cem C\"uneyt' 'B\"uy\"ukg\"ung\"or, Orhan' _publ_section_title ; (2-Hydroxyethyl)hydrazinium(2+) dichloride ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o321 _journal_page_last o323 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.208 _cell_angle_gamma 90.000 _cell_length_a 10.2367 _cell_length_b 8.4158 _cell_length_c 7.5111 _exptl_crystal_F_000 312.00 _reflns_d_resolution_high 0.7310 _[local]_cod_data_source_file dn1076Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TEST STRUCTURE D:\DATA\GUN1_DENE1\GUN1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 86.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 313.62 202.71 5.86 o 3 0 0 1967.91 2021.14 31.05 o 4 0 0 614.50 685.66 5.56 o 5 0 0 1314.63 1257.60 6.06 o 6 0 0 140.48 145.45 1.96 o 7 0 0 1150.55 1128.18 14.01 o 8 0 0 2458.49 2412.93 27.40 o 9 0 0 79.21 79.19 1.68 o 10 0 0 2.60 3.98 0.78 o 11 0 0 459.03 454.70 3.84 o 12 0 0 45.50 48.18 1.12 o 13 0 0 1871.29 1875.74 15.68 o 1 1 0 15.94 30.57 1.83 o 2 1 0 141.71 129.67 1.08 o 3 1 0 7432.30 7175.74 12.98 o 4 1 0 1348.73 1369.45 9.56 o 5 1 0 3902.39 3706.83 36.49 o 6 1 0 1192.37 1208.52 9.35 o 7 1 0 125.35 125.10 1.13 o 8 1 0 1685.30 1623.66 10.86 o 9 1 0 2.27 2.64 0.84 o 10 1 0 892.32 912.21 5.20 o 11 1 0 40.21 41.41 0.77 o 12 1 0 270.09 276.24 2.55 o 13 1 0 1.49 2.37 0.65 o 0 2 0 1027.20 1293.94 19.10 o 1 2 0 656.92 675.52 8.03 o 2 2 0 6564.55 5671.75 25.13 o 3 2 0 2278.70 2293.53 14.75 o 4 2 0 243.80 278.86 1.95 o 5 2 0 160.80 139.13 1.44 o 6 2 0 141.40 126.50 1.53 o 7 2 0 350.77 359.15 4.38 o 8 2 0 342.96 350.66 2.04 o 9 2 0 168.04 160.84 1.50 o 10 2 0 175.57 173.99 2.84 o 11 2 0 1085.08 1081.85 8.11 o 12 2 0 160.39 158.11 2.26 o 13 2 0 74.43 74.98 0.75 o 1 3 0 46.70 39.71 0.96 o 2 3 0 42.13 41.74 0.85 o 3 3 0 337.02 341.48 2.62 o 4 3 0 226.09 240.43 2.39 o 5 3 0 594.21 621.44 4.06 o 6 3 0 24.66 24.87 0.63 o 7 3 0 178.72 193.92 2.31 o 8 3 0 283.61 297.24 2.73 o 9 3 0 1.22 1.75 0.56 o 10 3 0 11.25 15.95 2.54 o 11 3 0 7.75 8.53 0.57 o 12 3 0 75.99 77.82 0.89 o 13 3 0 23.08 20.76 0.64 o 0 4 0 54.11 62.61 1.44 o 1 4 0 649.65 667.45 6.87 o 2 4 0 701.89 716.43 8.15 o 3 4 0 2.28 4.22 0.62 o 4 4 0 73.13 75.50 0.74 o 5 4 0 88.69 90.04 0.93 o 6 4 0 40.10 40.56 1.23 o 7 4 0 11.74 11.39 0.65 o 8 4 0 17.77 17.52 0.64 o 9 4 0 82.69 89.06 1.09 o 10 4 0 87.09 88.26 1.10 o 11 4 0 26.58 26.02 0.72 o 12 4 0 72.51 71.49 1.23 o 1 5 0 294.05 301.29 2.84 o 2 5 0 55.53 65.90 1.28 o 3 5 0 987.96 986.86 7.66 o 4 5 0 364.89 363.21 4.27 o 5 5 0 375.47 371.61 2.27 o 6 5 0 351.71 354.50 2.98 o 7 5 0 559.81 552.97 5.56 o 8 5 0 280.41 280.03 3.21 o 9 5 0 19.66 20.96 0.62 o 10 5 0 530.86 539.33 7.32 o 11 5 0 0.35 -0.29 0.69 o 12 5 0 0.08 2.69 1.02 o 0 6 0 1453.72 1406.12 22.96 o 1 6 0 193.71 196.59 3.08 o 2 6 0 1874.70 1854.87 18.59 o 3 6 0 335.94 326.35 2.55 o 4 6 0 196.51 200.22 2.63 o 5 6 0 346.51 344.05 3.07 o 6 6 0 505.22 504.82 3.08 o 7 6 0 376.13 382.97 3.93 o 8 6 0 58.87 61.20 0.66 o 9 6 0 171.15 174.27 2.92 o 10 6 0 204.46 206.29 2.81 o 11 6 0 251.52 246.63 2.04 o 1 7 0 680.36 692.11 6.01 o 2 7 0 281.58 290.11 3.32 o 3 7 0 1105.13 1096.86 10.29 o 4 7 0 143.42 139.31 1.07 o 5 7 0 1179.62 1162.72 6.54 o 6 7 0 29.54 33.98 0.65 o 7 7 0 240.81 237.37 1.76 o 8 7 0 1153.90 1152.21 7.44 o 9 7 0 0.02 1.04 0.66 o 10 7 0 640.43 639.77 7.61 o 0 8 0 1052.56 1082.43 13.87 o 1 8 0 4.47 5.71 0.64 o 2 8 0 1087.12 1088.10 7.09 o 3 8 0 36.10 35.34 0.74 o 4 8 0 9.23 11.42 0.98 o 5 8 0 1527.85 1499.78 6.20 o 6 8 0 103.98 107.93 1.76 o 7 8 0 33.43 35.18 0.66 o 8 8 0 366.25 367.97 2.37 o 9 8 0 32.81 35.27 0.99 o 1 9 0 323.83 322.37 2.74 o 2 9 0 128.81 128.05 1.30 o 3 9 0 308.08 313.93 3.10 o 4 9 0 333.05 334.68 2.46 o 5 9 0 139.40 137.67 2.62 o 6 9 0 34.23 36.99 1.35 o 7 9 0 47.16 47.37 0.83 o 8 9 0 88.51 88.88 0.98 o 0 10 0 80.25 82.41 1.54 o 1 10 0 357.50 360.54 2.92 o 2 10 0 3.11 3.78 0.67 o 3 10 0 8.80 10.50 0.74 o 4 10 0 0.39 1.51 0.69 o 5 10 0 2.01 4.74 0.81 o 6 10 0 291.86 288.38 3.69 o 1 11 0 47.37 44.72 1.21 o 2 11 0 225.34 217.01 5.71 o 3 11 0 15.33 17.02 0.98 o 4 11 0 104.89 109.81 2.02 o -13 1 1 1.93 2.36 0.63 o -12 1 1 8.64 9.99 0.90 o -11 1 1 302.93 307.66 1.93 o -10 1 1 243.82 240.84 2.09 o -9 1 1 60.92 60.68 0.86 o -8 1 1 32.74 30.16 0.61 o -7 1 1 14.91 15.44 0.62 o -6 1 1 127.01 133.39 2.16 o -5 1 1 1132.61 1044.90 4.35 o -4 1 1 41.27 46.53 1.59 o -3 1 1 3716.36 3671.72 36.03 o -2 1 1 139.50 162.56 1.44 o -1 1 1 640.65 554.31 6.31 o 0 1 1 146.86 147.44 1.51 o 1 1 1 1796.81 1582.15 10.14 o 2 1 1 1595.24 1650.58 7.87 o 3 1 1 1759.73 1701.52 8.73 o 4 1 1 8.99 13.84 0.67 o 5 1 1 108.76 101.39 1.18 o 6 1 1 142.52 131.26 1.07 o 7 1 1 14.56 16.33 0.65 o 8 1 1 316.23 324.40 2.91 o 9 1 1 22.63 23.53 0.59 o 10 1 1 646.12 639.50 2.54 o 11 1 1 2.17 2.67 0.59 o 12 1 1 13.98 14.44 0.79 o 13 1 1 70.47 71.13 1.10 o -13 2 1 244.24 242.42 1.41 o -12 2 1 135.19 134.08 2.15 o -11 2 1 817.59 817.87 4.99 o -10 2 1 295.83 298.66 3.42 o -9 2 1 1.58 2.16 0.60 o -8 2 1 1408.87 1380.00 9.54 o -7 2 1 19.09 22.34 0.75 o -6 2 1 1320.76 1300.06 10.48 o -5 2 1 29.56 35.14 0.69 o -4 2 1 50.61 54.71 1.49 o -3 2 1 277.51 280.64 2.51 o -2 2 1 2717.68 2786.46 28.80 o -1 2 1 1759.69 1664.94 14.02 o 0 2 1 2981.11 3108.95 37.91 o 1 2 1 2397.02 2285.05 18.94 o 2 2 1 5193.25 4719.14 47.46 o 3 2 1 976.69 939.52 3.63 o 4 2 1 0.04 1.84 0.61 o 5 2 1 2592.56 2546.70 15.37 o 6 2 1 9.67 9.04 0.69 o 7 2 1 833.24 813.99 5.18 o 8 2 1 12.91 14.77 0.55 o 9 2 1 10.86 11.45 0.91 o 10 2 1 20.59 20.99 0.58 o 11 2 1 205.57 209.66 1.49 o 12 2 1 134.85 134.40 1.07 o 13 2 1 490.46 492.83 5.92 o -13 3 1 258.10 259.10 1.41 o -12 3 1 216.68 215.70 2.36 o -11 3 1 303.00 308.42 4.05 o -10 3 1 297.18 304.04 3.43 o -9 3 1 36.02 31.14 0.62 o -8 3 1 633.56 632.36 6.68 o -7 3 1 406.67 384.95 4.41 o -6 3 1 191.74 190.88 2.03 o -5 3 1 5533.99 5248.30 9.04 o -4 3 1 7.78 8.84 0.65 o -3 3 1 3087.96 2997.18 26.79 o -2 3 1 166.68 172.31 1.78 o -1 3 1 4466.14 4323.72 34.36 o 0 3 1 2443.48 2486.60 22.90 o 1 3 1 2060.05 2072.50 30.90 o 2 3 1 2092.62 2004.67 22.66 o 3 3 1 417.12 371.21 3.19 o 4 3 1 15.46 25.10 4.11 o 5 3 1 930.95 962.17 6.33 o 6 3 1 191.28 196.87 1.72 o 7 3 1 199.35 196.63 2.25 o 8 3 1 3034.19 2980.40 24.84 o 9 3 1 55.21 58.63 1.63 o 10 3 1 820.92 827.39 6.38 o 11 3 1 197.93 204.42 2.70 o 12 3 1 331.91 337.82 4.06 o -13 4 1 795.21 791.62 11.33 o -12 4 1 0.91 0.71 0.68 o -11 4 1 171.73 181.04 2.56 o -10 4 1 506.11 500.18 8.01 o -9 4 1 247.28 235.07 2.40 o -8 4 1 2179.32 2150.27 17.50 o -7 4 1 425.30 406.25 4.05 o -6 4 1 775.31 738.29 5.85 o -5 4 1 69.21 73.41 0.73 o -4 4 1 0.92 3.29 0.66 o -3 4 1 638.14 676.62 4.94 o -2 4 1 1954.54 1914.38 23.92 o -1 4 1 236.95 274.21 1.51 o 0 4 1 5524.24 31004.71 22015.92 o 1 4 1 356.96 411.85 3.98 o 2 4 1 1266.61 1255.75 14.33 o 3 4 1 2558.17 2570.14 17.07 o 4 4 1 183.46 189.05 1.24 o 5 4 1 3488.76 3283.63 29.03 o 6 4 1 241.09 243.70 1.69 o 7 4 1 470.98 483.72 3.97 o 8 4 1 3.01 4.19 0.57 o 9 4 1 92.44 95.34 1.86 o 10 4 1 100.51 100.27 0.92 o 11 4 1 568.35 582.19 7.24 o 12 4 1 8.96 11.37 0.73 o -12 5 1 42.94 44.04 0.71 o -11 5 1 360.78 343.66 4.69 o -10 5 1 697.35 670.52 10.08 o -9 5 1 122.27 130.78 1.29 o -8 5 1 64.63 70.54 0.74 o -7 5 1 880.16 888.76 8.92 o -6 5 1 112.70 112.13 1.10 o -5 5 1 308.99 306.36 2.51 o -4 5 1 262.41 256.80 1.61 o -3 5 1 5004.10 4878.91 77.85 o -2 5 1 5.39 9.88 0.68 o -1 5 1 13.06 9.98 0.65 o 0 5 1 1346.38 1393.77 12.41 o 1 5 1 187.27 181.33 2.31 o 2 5 1 530.16 484.09 3.20 o 3 5 1 562.34 573.35 5.46 o 4 5 1 539.58 549.24 4.22 o 5 5 1 555.88 532.66 3.70 o 6 5 1 479.63 482.23 3.25 o 7 5 1 28.25 26.48 0.63 o 8 5 1 566.87 558.12 4.84 o 9 5 1 48.45 49.92 0.83 o 10 5 1 1058.97 1089.02 9.93 o 11 5 1 1.71 1.03 0.64 o -11 6 1 66.26 63.29 1.07 o -10 6 1 15.71 17.90 1.17 o -9 6 1 114.79 112.15 1.79 o -8 6 1 123.37 122.75 1.40 o -7 6 1 189.40 192.07 1.42 o -6 6 1 907.07 901.63 7.21 o -5 6 1 81.25 80.06 1.13 o -4 6 1 452.63 457.13 2.29 o -3 6 1 118.99 119.89 1.13 o -2 6 1 65.25 66.44 1.43 o -1 6 1 178.47 183.31 2.18 o 0 6 1 535.02 534.01 6.13 o 1 6 1 195.75 185.98 1.75 o 2 6 1 482.34 484.38 5.38 o 3 6 1 118.39 112.37 1.27 o 4 6 1 690.64 679.18 7.11 o 5 6 1 497.15 499.63 4.79 o 6 6 1 0.32 2.79 1.04 o 7 6 1 323.91 330.35 2.32 o 8 6 1 61.97 64.73 1.63 o 9 6 1 1.32 2.49 0.60 o 10 6 1 25.82 30.49 0.80 o 11 6 1 34.87 34.00 0.73 o -11 7 1 45.12 40.76 5.96 o -10 7 1 78.17 76.65 1.08 o -9 7 1 0.06 0.42 0.71 o -8 7 1 0.70 1.68 0.68 o -7 7 1 81.29 86.60 1.67 o -6 7 1 252.59 247.93 1.70 o -5 7 1 23.91 26.59 0.88 o -4 7 1 74.56 75.26 0.70 o -3 7 1 4.37 5.98 0.63 o -2 7 1 797.80 789.89 7.13 o -1 7 1 35.07 36.19 0.78 o 0 7 1 150.67 144.53 2.08 o 1 7 1 261.61 264.43 2.32 o 2 7 1 63.46 69.46 0.79 o 3 7 1 3.29 4.38 0.66 o 4 7 1 8.07 11.64 1.18 o 5 7 1 10.66 12.08 0.62 o 6 7 1 388.75 382.16 4.85 o 7 7 1 219.93 217.05 2.04 o 8 7 1 190.44 186.38 2.10 o 9 7 1 164.48 163.19 2.04 o 10 7 1 21.65 22.45 0.70 o -10 8 1 163.15 161.52 2.23 o -9 8 1 52.39 52.78 1.64 o -8 8 1 55.71 55.51 0.74 o -7 8 1 443.11 434.64 2.56 o -6 8 1 60.07 60.06 0.95 o -5 8 1 15.09 15.73 0.64 o -4 8 1 2.33 2.13 0.65 o -3 8 1 13.27 14.34 0.64 o -2 8 1 36.31 38.90 0.69 o -1 8 1 64.55 65.44 1.39 o 0 8 1 267.19 272.23 1.62 o 1 8 1 569.27 564.34 3.72 o 2 8 1 155.38 158.49 1.89 o 3 8 1 183.26 188.96 1.32 o 4 8 1 278.81 270.30 2.11 o 5 8 1 67.81 67.63 0.98 o 6 8 1 232.66 234.67 1.55 o 7 8 1 82.53 83.64 0.88 o 8 8 1 21.72 22.54 0.68 o 9 8 1 19.95 20.73 0.74 o -8 9 1 350.90 341.49 3.88 o -7 9 1 107.66 106.84 1.12 o -6 9 1 2.36 3.37 0.68 o -5 9 1 750.11 746.79 6.00 o -4 9 1 583.14 578.74 4.52 o -3 9 1 386.93 388.14 3.04 o -2 9 1 98.38 101.15 1.37 o -1 9 1 308.09 318.13 2.40 o 0 9 1 156.70 164.28 1.89 o 1 9 1 36.48 40.39 0.93 o 2 9 1 123.51 122.23 2.15 o 3 9 1 105.67 106.76 0.77 o 4 9 1 21.03 18.45 0.66 o 5 9 1 193.57 190.22 2.29 o 6 9 1 143.53 144.72 1.52 o 7 9 1 13.48 15.33 0.71 o 8 9 1 392.68 379.96 3.09 o -6 10 1 299.36 296.20 2.56 o -5 10 1 0.04 1.08 0.70 o -4 10 1 0.99 2.13 0.71 o -3 10 1 16.93 17.13 0.76 o -2 10 1 408.99 415.12 4.33 o -1 10 1 11.00 13.62 0.73 o 0 10 1 554.15 566.07 4.72 o 1 10 1 91.53 92.46 0.87 o 2 10 1 325.86 326.06 2.13 o 3 10 1 669.55 669.11 5.26 o 4 10 1 135.17 135.08 2.37 o 5 10 1 158.29 156.24 3.12 o 6 10 1 0.18 0.58 0.72 o -4 11 1 19.49 22.66 1.81 o -3 11 1 326.26 315.46 9.99 o -2 11 1 49.47 49.87 1.69 o -1 11 1 106.77 110.00 2.98 o 0 11 1 98.09 99.11 1.54 o 1 11 1 0.67 0.75 0.77 o 2 11 1 144.81 146.03 2.02 o 3 11 1 447.03 430.76 6.97 o -13 0 2 550.07 533.58 5.52 o -12 0 2 10.83 13.09 1.11 o -11 0 2 16.85 19.12 1.09 o -10 0 2 2010.49 2013.32 19.10 o -9 0 2 150.01 152.58 2.09 o -8 0 2 1630.00 1574.34 2.39 o -7 0 2 4.96 8.89 0.92 o -6 0 2 4378.96 4285.88 56.12 o -5 0 2 405.20 416.44 4.44 o -4 0 2 8.10 6.78 1.01 o -3 0 2 6197.28 6128.55 11.92 o -2 0 2 4759.20 4704.56 19.36 o -1 0 2 490.95 574.11 6.70 o 0 0 2 643.24 635.10 3.09 o 1 0 2 0.15 7.18 1.27 o 2 0 2 1242.26 1346.72 6.53 o 3 0 2 4604.06 4174.44 74.50 o 4 0 2 143.63 141.87 1.12 o 5 0 2 4519.18 4236.23 49.21 o 6 0 2 118.85 125.21 3.73 o 7 0 2 1999.63 1950.56 22.15 o 8 0 2 644.00 645.77 5.25 o 9 0 2 7.68 8.96 0.78 o 10 0 2 669.72 650.52 9.16 o 11 0 2 143.48 140.71 1.67 o 12 0 2 111.80 113.40 2.56 o -13 1 2 407.96 405.20 1.87 o -12 1 2 1.94 6.16 1.40 o -11 1 2 845.26 840.51 6.35 o -10 1 2 81.27 83.80 0.66 o -9 1 2 548.53 548.55 3.66 o -8 1 2 23.09 23.46 0.60 o -7 1 2 1413.23 1405.82 8.79 o -6 1 2 819.79 838.58 6.08 o -5 1 2 1719.53 1711.26 12.81 o -4 1 2 536.13 554.41 4.22 o -3 1 2 4455.62 4388.95 40.39 o -2 1 2 393.19 402.52 2.64 o -1 1 2 4126.09 3983.61 44.44 o 0 1 2 4105.03 3980.01 26.74 o 1 1 2 1838.69 1890.37 24.16 o 3 1 2 2.31 20.88 5.13 o 4 1 2 90.23 75.51 0.70 o 5 1 2 27.11 37.75 5.82 o 6 1 2 295.21 288.34 1.98 o 7 1 2 47.84 48.27 0.63 o 8 1 2 986.89 997.13 6.46 o 9 1 2 68.61 70.75 1.35 o 10 1 2 1178.01 1179.14 7.07 o 11 1 2 147.63 146.27 1.48 o 12 1 2 49.65 50.42 1.02 o -13 2 2 181.54 186.84 2.39 o -12 2 2 25.01 27.29 0.64 o -11 2 2 21.53 22.47 0.62 o -10 2 2 465.04 463.48 3.79 o -9 2 2 21.44 22.09 0.62 o -8 2 2 935.45 939.43 7.37 o -7 2 2 96.48 110.86 0.90 o -6 2 2 915.67 902.05 6.34 o -5 2 2 216.70 279.41 19.47 o -4 2 2 112.10 128.88 1.40 o -3 2 2 4281.06 4331.12 37.93 o -2 2 2 3307.22 3335.58 31.16 o -1 2 2 774.65 770.87 5.95 o 0 2 2 32.44 39.57 0.98 o 1 2 2 1118.80 1071.01 8.79 o 2 2 2 621.21 641.67 7.31 o 3 2 2 14.67 11.09 0.64 o 4 2 2 41.28 43.90 0.85 o 5 2 2 3723.25 3590.08 26.42 o 6 2 2 69.34 71.17 0.94 o 7 2 2 291.92 285.70 1.94 o 8 2 2 199.98 203.82 2.09 o 9 2 2 0.02 1.18 0.79 o 10 2 2 289.96 290.85 2.72 o 11 2 2 72.43 77.44 1.24 o 12 2 2 102.81 104.79 0.80 o -13 3 2 23.26 22.02 0.74 o -12 3 2 15.14 14.30 0.69 o -11 3 2 63.07 64.18 1.98 o -10 3 2 549.54 537.47 5.44 o -9 3 2 14.36 15.10 0.57 o -8 3 2 215.73 211.05 2.33 o -7 3 2 39.01 39.30 0.69 o -6 3 2 23.70 26.46 0.66 o -5 3 2 661.82 670.82 6.11 o -4 3 2 0.05 0.81 0.65 o -3 3 2 77.67 78.12 0.93 o -2 3 2 319.55 337.80 1.95 o -1 3 2 213.68 214.57 2.31 o 0 3 2 673.45 692.97 7.34 o 1 3 2 16.28 16.56 0.68 o 2 3 2 446.19 439.91 5.05 o 3 3 2 1209.07 1287.23 8.91 o 4 3 2 0.28 2.45 0.59 o 5 3 2 723.24 764.13 6.38 o 6 3 2 0.34 4.59 1.30 o 7 3 2 32.22 36.10 0.60 o 8 3 2 116.05 123.33 3.03 o 9 3 2 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576.27 579.65 6.76 o -2 5 2 263.37 251.45 3.30 o -1 5 2 219.01 202.60 2.52 o 0 5 2 2504.01 2549.83 36.85 o 1 5 2 672.42 698.77 11.52 o 2 5 2 39.62 33.76 1.13 o 3 5 2 77.33 82.23 1.46 o 4 5 2 310.71 329.71 3.80 o 5 5 2 22.29 26.43 0.81 o 6 5 2 4.87 10.39 1.83 o 7 5 2 0.07 0.19 0.87 o 8 5 2 1002.59 997.02 9.06 o 9 5 2 125.60 123.01 1.66 o 10 5 2 25.04 27.78 0.68 o 11 5 2 43.47 48.25 0.79 o -11 6 2 162.88 164.52 3.27 o -10 6 2 338.97 343.61 6.85 o -9 6 2 57.66 53.76 1.41 o -8 6 2 1288.30 1236.07 18.29 o -7 6 2 17.51 20.33 0.77 o -6 6 2 1259.46 1272.88 9.84 o -5 6 2 906.59 883.37 8.17 o -4 6 2 15.51 21.74 2.43 o -3 6 2 47.56 48.41 0.91 o -2 6 2 27.25 33.12 0.71 o -1 6 2 649.84 671.19 7.29 o 0 6 2 1849.80 1881.97 24.12 o 1 6 2 101.91 100.30 1.71 o 2 6 2 57.27 52.20 0.74 o 3 6 2 1616.82 1578.03 12.58 o 4 6 2 67.56 73.35 0.85 o 5 6 2 826.39 855.85 6.62 o 6 6 2 207.92 199.65 1.84 o 7 6 2 1329.73 1299.43 13.44 o 8 6 2 97.69 100.39 1.63 o 9 6 2 3.40 2.61 0.65 o 10 6 2 216.97 216.60 2.22 o -11 7 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