#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:03:18 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180817 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/48/2014888.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014888_Fobs loop_ _publ_author_name 'Glidewell, Christopher' 'Low, John N.' 'Skakle, Janet M. S.' 'Wardell, James L.' _publ_section_title ; Three isomeric N-(nitrophenyl)succinimides: isolated molecules, hydrogen-bonded sheets and a hydrogen-bonded three-dimensional framework ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o216 _journal_page_last o220 _journal_volume 61 _journal_year 2005 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.135 _cell_angle_gamma 90.000 _cell_length_a 10.3731 _cell_length_b 11.5900 _cell_length_c 7.9761 _exptl_crystal_F_000 456.00 _reflns_d_resolution_high 0.7673 _cod_data_source_file sk1817IIIsup4.hkl _cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' 741 R = 0.07 C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 192.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14925.04 13132.97 317.95 o 4 0 0 176.55 206.37 11.61 o 6 0 0 1379.10 1382.91 52.20 o 8 0 0 720.25 781.48 32.90 o 10 0 0 555.56 620.98 30.05 o 12 0 0 145.09 149.96 38.51 o 3 1 0 143.97 140.72 4.80 o 5 1 0 24.63 27.94 3.12 o 7 1 0 244.30 218.60 8.93 o 9 1 0 609.80 697.66 17.58 o 11 1 0 146.31 148.58 14.73 o 0 2 0 8158.97 7239.92 205.96 o 2 2 0 127.16 178.63 4.63 o 4 2 0 3929.16 4146.97 90.15 o 6 2 0 39.21 33.43 3.99 o 8 2 0 306.37 278.01 10.66 o 10 2 0 28.15 22.86 13.59 o 12 2 0 9.18 35.34 17.35 o 1 3 0 3807.51 3633.25 65.79 o 3 3 0 75.68 62.99 3.55 o 5 3 0 1706.62 1924.13 46.05 o 7 3 0 339.93 308.10 9.02 o 9 3 0 166.09 159.41 10.29 o 11 3 0 1.09 26.63 15.33 o 0 4 0 26.45 16.12 2.98 o 2 4 0 3594.31 3631.12 80.35 o 4 4 0 98.65 91.96 4.37 o 6 4 0 3.54 2.06 5.35 o 8 4 0 679.61 661.44 19.87 o 10 4 0 16.71 -3.54 12.12 o 12 4 0 25.41 48.76 22.48 o 1 5 0 21.36 40.01 3.93 o 3 5 0 60.77 52.83 5.01 o 5 5 0 14.51 11.71 4.49 o 7 5 0 259.44 234.18 8.71 o 9 5 0 8.82 17.03 9.41 o 11 5 0 1.78 -20.50 20.50 o 0 6 0 54.29 61.61 4.06 o 2 6 0 1347.46 1392.39 28.09 o 4 6 0 84.42 81.31 4.66 o 6 6 0 52.89 54.45 5.79 o 8 6 0 191.50 182.39 13.26 o 10 6 0 10.49 5.62 14.49 o 1 7 0 18.74 15.87 3.07 o 3 7 0 108.44 106.39 5.26 o 5 7 0 415.70 436.40 12.67 o 7 7 0 204.13 199.19 8.77 o 9 7 0 26.49 10.90 13.36 o 11 7 0 70.72 77.52 22.96 o 0 8 0 364.32 345.22 10.79 o 2 8 0 221.29 237.04 7.05 o 4 8 0 1060.72 1186.08 28.37 o 6 8 0 962.26 1018.00 26.31 o 8 8 0 10.60 3.06 11.04 o 10 8 0 4.82 9.56 18.94 o 1 9 0 6.63 3.57 4.24 o 3 9 0 160.15 139.97 7.16 o 5 9 0 88.45 76.92 7.13 o 7 9 0 393.99 405.83 19.28 o 9 9 0 0.19 4.04 18.05 o 0 10 0 79.40 58.31 6.62 o 2 10 0 33.61 40.16 6.14 o 4 10 0 12.76 6.52 7.08 o 6 10 0 35.71 56.07 11.98 o 8 10 0 14.36 35.53 16.17 o 1 11 0 246.22 168.91 7.44 o 3 11 0 16.31 11.12 7.91 o 5 11 0 104.03 112.10 10.66 o 7 11 0 111.12 126.28 16.39 o 0 12 0 71.05 75.93 13.32 o 2 12 0 59.48 58.75 8.58 o 4 12 0 21.63 23.11 11.15 o 6 12 0 0.05 -3.68 14.54 o 1 13 0 6.50 11.50 11.42 o 3 13 0 0.88 -5.27 12.12 o 5 13 0 53.36 72.11 14.87 o 0 14 0 0.18 37.45 25.67 o 2 14 0 3.49 -10.36 17.05 o 4 14 0 141.99 113.60 20.55 o 1 15 0 60.01 64.97 35.92 o -13 1 1 11.70 -12.45 20.51 o -11 1 1 45.27 44.78 11.79 o -9 1 1 499.20 483.75 13.99 o -7 1 1 474.38 431.38 10.88 o -5 1 1 187.44 176.56 4.89 o -3 1 1 8628.01 8270.05 153.53 o -1 1 1 246.55 168.50 50.05 o 1 1 1 63.07 67.79 2.74 o 3 1 1 50.17 32.31 2.87 o 5 1 1 37.67 32.23 3.70 o 7 1 1 0.00 1.08 4.32 o 9 1 1 154.65 145.09 9.85 o 11 1 1 55.54 47.08 15.58 o -12 2 1 57.89 86.73 18.39 o -10 2 1 34.10 38.03 8.34 o -8 2 1 199.38 176.14 9.17 o -6 2 1 1805.26 2006.24 45.60 o -4 2 1 4488.19 4719.32 86.99 o -2 2 1 16.54 42.30 2.50 o 0 2 1 0.25 13.37 1.76 o 2 2 1 109.69 106.62 4.13 o 4 2 1 1513.79 1729.56 37.64 o 6 2 1 0.02 4.12 3.83 o 8 2 1 12.72 20.57 5.41 o 10 2 1 26.70 34.24 12.33 o 12 2 1 10.99 17.44 20.00 o -11 3 1 91.08 103.35 13.38 o -9 3 1 284.29 265.53 10.23 o -7 3 1 321.60 323.17 9.63 o -5 3 1 2.18 0.30 3.13 o -3 3 1 2025.46 1961.51 40.85 o -1 3 1 271.84 272.35 4.88 o 1 3 1 666.05 645.52 13.00 o 3 3 1 1519.00 1482.99 32.90 o 5 3 1 89.40 89.75 5.09 o 7 3 1 1.58 10.18 4.96 o 9 3 1 136.42 108.11 10.78 o 11 3 1 158.78 204.92 21.74 o -12 4 1 2.43 -5.88 21.72 o -10 4 1 17.82 33.91 10.14 o -8 4 1 31.86 26.11 7.32 o -6 4 1 7.74 2.04 4.90 o -4 4 1 1884.58 1940.72 45.39 o -2 4 1 483.45 440.83 9.61 o 0 4 1 3427.83 3345.36 57.57 o 2 4 1 110.08 125.90 5.57 o 4 4 1 2.44 1.94 3.07 o 6 4 1 503.91 452.42 13.24 o 8 4 1 0.78 -5.65 8.65 o 10 4 1 10.15 6.95 14.21 o -11 5 1 20.93 40.35 17.16 o -9 5 1 210.56 198.51 14.66 o -7 5 1 6.72 0.36 6.17 o -5 5 1 285.99 255.18 9.02 o -3 5 1 368.97 336.96 8.01 o -1 5 1 7614.34 7643.58 124.65 o 1 5 1 572.25 568.21 10.86 o 3 5 1 530.85 485.81 18.68 o 5 5 1 162.99 127.22 5.39 o 7 5 1 1.78 6.21 5.66 o 9 5 1 172.85 144.22 14.40 o 11 5 1 6.31 16.47 21.48 o -12 6 1 203.97 143.83 28.01 o -10 6 1 132.25 134.90 15.04 o -8 6 1 0.00 3.95 6.89 o -6 6 1 109.49 114.27 6.05 o -4 6 1 957.88 1012.75 25.39 o -2 6 1 1032.84 1312.14 24.44 o 0 6 1 4669.78 5210.31 94.15 o 2 6 1 15.31 11.66 2.99 o 4 6 1 596.92 601.96 22.84 o 6 6 1 9.79 6.29 5.21 o 8 6 1 318.39 260.78 14.77 o 10 6 1 102.55 120.75 24.93 o -11 7 1 116.33 94.54 18.84 o -9 7 1 4.43 2.13 11.62 o -7 7 1 0.41 -6.35 6.35 o -5 7 1 133.02 135.21 8.39 o -3 7 1 0.51 6.83 3.60 o -1 7 1 517.09 512.92 9.75 o 1 7 1 354.52 352.77 7.81 o 3 7 1 8.91 3.28 3.54 o 5 7 1 89.75 94.04 5.77 o 7 7 1 226.78 236.89 15.79 o 9 7 1 23.31 22.78 15.22 o -10 8 1 32.07 54.23 16.07 o -8 8 1 422.94 332.09 20.06 o -6 8 1 606.66 642.23 18.97 o -4 8 1 483.42 499.55 13.25 o -2 8 1 1546.48 1619.64 31.17 o 0 8 1 10.75 9.09 3.68 o 2 8 1 61.96 76.47 7.23 o 4 8 1 3893.27 4790.32 107.42 o 6 8 1 366.63 351.85 12.49 o 8 8 1 108.31 96.12 14.02 o 10 8 1 1.65 1.04 22.11 o -9 9 1 4.36 14.05 15.43 o -7 9 1 150.52 144.42 11.18 o -5 9 1 368.41 353.81 11.23 o -3 9 1 194.91 164.94 14.43 o -1 9 1 5.33 14.52 4.04 o 1 9 1 28.08 27.59 4.27 o 3 9 1 370.23 388.68 10.01 o 5 9 1 158.43 165.18 8.96 o 7 9 1 5.93 2.74 23.47 o 9 9 1 30.08 64.02 21.09 o -8 10 1 3.06 11.29 14.30 o -6 10 1 1.81 59.91 30.24 o -4 10 1 65.62 51.67 6.72 o -2 10 1 450.72 461.35 11.77 o 0 10 1 5.16 6.16 5.22 o 2 10 1 200.07 197.76 7.44 o 4 10 1 388.34 454.20 16.60 o 6 10 1 3.06 36.49 16.80 o 8 10 1 46.65 40.40 18.32 o -9 11 1 50.66 65.90 41.47 o -7 11 1 60.85 71.35 13.09 o -5 11 1 37.73 23.80 9.44 o -3 11 1 193.25 177.97 9.29 o -1 11 1 193.20 167.86 7.98 o 1 11 1 41.76 45.37 8.04 o 3 11 1 0.54 5.42 7.44 o 5 11 1 80.50 88.27 12.62 o 7 11 1 148.60 135.29 17.92 o -8 12 1 37.02 83.47 79.45 o -6 12 1 19.87 40.01 14.65 o -4 12 1 131.87 143.31 12.24 o -2 12 1 0.00 15.66 8.92 o 0 12 1 102.79 102.71 12.83 o 2 12 1 37.16 46.58 9.22 o 4 12 1 32.31 54.42 13.10 o 6 12 1 124.37 142.25 18.38 o -5 13 1 65.29 67.05 15.74 o -3 13 1 5.46 15.15 13.05 o -1 13 1 0.98 10.67 13.51 o 1 13 1 1.43 21.36 11.90 o 3 13 1 6.60 -2.88 19.82 o 5 13 1 9.00 18.41 19.09 o -4 14 1 21.88 6.39 17.33 o -2 14 1 0.03 -11.97 20.32 o 0 14 1 7.88 8.22 18.48 o 2 14 1 121.03 78.80 30.03 o 4 14 1 40.74 23.60 28.34 o -1 15 1 5.08 18.85 28.55 o -12 0 2 183.92 175.63 25.45 o -10 0 2 450.97 440.27 22.08 o -8 0 2 58.74 50.44 7.31 o -6 0 2 187.70 182.83 8.61 o -4 0 2 15496.32 16572.38 446.99 o -2 0 2 37191.46 35621.19 913.49 o 0 0 2 25822.66 24261.86 617.60 o 2 0 2 4499.10 4653.78 141.12 o 4 0 2 48.41 62.29 5.19 o 6 0 2 0.42 12.12 5.68 o 8 0 2 2277.43 2625.60 124.75 o 10 0 2 141.91 142.73 28.64 o -13 1 2 136.73 143.45 22.42 o -11 1 2 111.94 152.27 13.13 o -9 1 2 7.24 15.19 5.27 o -7 1 2 173.93 180.50 6.06 o -5 1 2 134.23 148.30 4.50 o -3 1 2 1909.64 2040.66 41.18 o -1 1 2 758.95 789.93 16.93 o 1 1 2 546.07 544.65 14.51 o 3 1 2 167.90 179.32 5.30 o 5 1 2 1087.90 1132.08 27.39 o 7 1 2 836.80 830.14 24.34 o 9 1 2 118.20 101.37 13.81 o 11 1 2 36.76 44.70 17.62 o -12 2 2 103.95 109.72 18.79 o -10 2 2 264.05 254.17 16.52 o -8 2 2 1049.65 1070.81 35.29 o -6 2 2 611.60 594.81 13.24 o -4 2 2 180.54 190.15 4.98 o -2 2 2 219.53 256.34 5.85 o 0 2 2 7734.42 7568.32 161.94 o 2 2 2 0.64 -2.71 2.81 o 4 2 2 781.60 825.97 20.17 o 6 2 2 232.93 220.47 9.50 o 8 2 2 219.60 229.96 11.41 o 10 2 2 0.13 -5.47 13.15 o -13 3 2 12.28 30.72 29.36 o -11 3 2 0.00 14.59 9.86 o -9 3 2 171.69 146.29 7.45 o -7 3 2 7.37 9.61 3.85 o -5 3 2 0.17 2.92 2.94 o -3 3 2 2513.11 2500.73 52.19 o -1 3 2 60.51 52.17 2.38 o 1 3 2 540.98 578.35 12.04 o 3 3 2 3490.58 3871.20 85.82 o 5 3 2 950.48 1035.80 30.17 o 7 3 2 20.19 9.49 8.75 o 9 3 2 0.12 11.24 11.32 o 11 3 2 4.40 13.04 17.20 o -12 4 2 32.29 38.94 23.52 o -10 4 2 103.59 88.04 10.82 o -8 4 2 84.66 71.24 5.60 o -6 4 2 110.95 113.16 6.52 o -4 4 2 556.66 587.76 14.46 o -2 4 2 1574.44 1637.33 30.86 o 0 4 2 1034.98 1035.71 19.87 o 2 4 2 207.86 211.41 6.50 o 4 4 2 785.70 779.35 24.47 o 6 4 2 33.30 30.63 5.36 o 8 4 2 314.86 260.96 19.66 o 10 4 2 59.79 50.11 14.63 o -11 5 2 22.74 13.85 15.31 o -9 5 2 5.33 8.91 7.44 o -7 5 2 618.26 552.32 17.38 o -5 5 2 83.66 92.10 5.15 o -3 5 2 240.76 212.65 5.53 o -1 5 2 596.27 637.60 11.68 o 1 5 2 0.00 -1.11 2.77 o 3 5 2 106.10 101.12 6.55 o 5 5 2 14.53 15.87 5.47 o 7 5 2 79.91 74.60 8.16 o 9 5 2 0.00 1.92 13.43 o 11 5 2 0.06 -25.83 50.24 o -12 6 2 4.34 5.14 23.30 o -10 6 2 24.53 28.08 11.40 o -8 6 2 17.01 19.43 6.83 o -6 6 2 690.93 691.22 20.97 o -4 6 2 913.13 926.48 22.21 o -2 6 2 256.15 251.16 6.15 o 0 6 2 1167.66 1204.56 22.94 o 2 6 2 0.39 8.79 3.62 o 4 6 2 116.67 96.97 6.69 o 6 6 2 20.77 21.76 6.25 o 8 6 2 43.63 68.88 11.69 o 10 6 2 25.71 48.04 24.14 o -11 7 2 61.83 60.94 20.82 o -9 7 2 69.35 52.44 12.17 o -7 7 2 0.01 -1.53 7.35 o -5 7 2 961.33 1026.63 29.67 o -3 7 2 130.91 118.76 4.75 o -1 7 2 40.62 47.73 3.53 o 1 7 2 127.27 117.64 4.95 o 3 7 2 45.07 52.26 6.11 o 5 7 2 45.06 45.45 6.10 o 7 7 2 177.43 171.05 11.72 o 9 7 2 0.98 29.71 28.98 o -10 8 2 31.25 47.57 16.60 o -8 8 2 483.92 468.57 21.74 o -6 8 2 924.28 1034.09 27.37 o -4 8 2 164.15 158.31 6.35 o -2 8 2 26.47 24.36 3.81 o 0 8 2 16.57 15.15 3.81 o 2 8 2 1096.63 1154.11 24.62 o 4 8 2 652.73 655.10 17.69 o 6 8 2 104.87 92.94 9.43 o 8 8 2 16.03 28.38 17.00 o -9 9 2 31.11 27.84 15.24 o -7 9 2 258.11 289.59 15.16 o -5 9 2 472.07 485.72 13.58 o -3 9 2 14.97 13.91 5.03 o -1 9 2 57.37 51.43 4.42 o 1 9 2 1945.68 2189.13 45.60 o 3 9 2 594.21 607.93 14.87 o 5 9 2 40.93 51.38 13.00 o 7 9 2 0.01 19.89 15.71 o 9 9 2 0.12 7.50 27.03 o -10 10 2 0.66 8.96 29.48 o -8 10 2 230.52 221.30 17.16 o -6 10 2 87.82 108.74 19.50 o -4 10 2 106.26 114.96 7.54 o -2 10 2 236.57 214.94 7.21 o 0 10 2 47.40 47.22 5.48 o 2 10 2 0.92 -1.14 5.83 o 4 10 2 34.50 36.22 8.99 o 6 10 2 85.79 101.15 15.45 o 8 10 2 29.17 3.20 21.92 o -9 11 2 0.04 37.25 25.72 o -7 11 2 36.07 23.39 14.39 o -5 11 2 53.25 53.30 9.36 o -3 11 2 377.16 321.84 12.67 o -1 11 2 88.06 58.04 10.64 o 1 11 2 87.17 80.67 7.12 o 3 11 2 55.98 61.05 14.87 o 5 11 2 13.79 28.30 14.32 o 7 11 2 161.66 148.51 21.38 o -8 12 2 21.51 10.12 33.45 o -6 12 2 33.53 36.99 14.49 o -4 12 2 21.92 30.71 11.83 o -2 12 2 38.98 21.25 8.79 o 0 12 2 17.67 33.83 8.89 o 2 12 2 52.11 61.40 11.37 o 4 12 2 67.06 80.15 15.33 o 6 12 2 11.85 -16.50 18.99 o -5 13 2 19.94 17.10 19.15 o -3 13 2 16.48 14.03 15.60 o -1 13 2 33.20 26.52 12.65 o 1 13 2 16.74 27.71 12.81 o 3 13 2 145.87 149.65 20.68 o 5 13 2 19.35 2.00 24.37 o -4 14 2 28.13 46.85 29.57 o -2 14 2 16.36 36.59 20.84 o 0 14 2 2.67 -2.34 15.63 o 2 14 2 14.48 -4.82 15.05 o -13 1 3 1.09 -5.05 22.18 o -11 1 3 46.87 53.50 11.49 o -9 1 3 89.53 61.72 6.44 o -7 1 3 1824.55 1955.35 47.50 o -5 1 3 289.13 279.88 8.39 o -3 1 3 1993.19 1943.95 43.19 o -1 1 3 9987.24 10495.68 210.67 o 1 1 3 395.43 374.19 9.31 o 3 1 3 126.68 114.98 4.83 o 5 1 3 388.52 388.75 13.57 o 7 1 3 6.93 2.91 6.51 o 9 1 3 0.70 -9.71 12.73 o 11 1 3 14.38 20.47 23.29 o -12 2 3 3.00 10.68 17.90 o -10 2 3 355.28 393.85 15.82 o -8 2 3 1091.70 1167.49 27.30 o -6 2 3 1224.75 1295.76 28.41 o -4 2 3 3.83 2.50 2.64 o -2 2 3 934.13 961.92 23.30 o 0 2 3 130.63 134.64 5.92 o 2 2 3 27.74 27.52 3.29 o 4 2 3 183.07 187.12 6.69 o 6 2 3 3.73 7.76 5.36 o 8 2 3 74.36 97.83 10.70 o 10 2 3 24.10 33.12 17.60 o -13 3 3 18.70 25.16 27.74 o -11 3 3 52.13 53.34 11.65 o -9 3 3 173.12 165.62 7.47 o -7 3 3 300.94 289.44 8.99 o -5 3 3 67.09 52.72 4.11 o -3 3 3 1834.70 1863.17 39.78 o -1 3 3 244.34 247.65 7.74 o 1 3 3 2657.31 2875.92 64.10 o 3 3 3 112.51 116.45 5.87 o 5 3 3 2.52 7.01 4.91 o 7 3 3 119.45 113.41 9.06 o 9 3 3 1.51 -6.94 20.08 o -12 4 3 3.36 27.16 26.69 o -10 4 3 7.72 13.61 7.97 o -8 4 3 3.81 2.05 4.67 o -6 4 3 445.79 444.77 14.53 o -4 4 3 269.19 234.02 7.90 o -2 4 3 50.58 52.04 3.76 o 0 4 3 44.90 43.83 3.32 o 2 4 3 678.13 732.33 21.73 o 4 4 3 47.08 61.48 5.40 o 6 4 3 34.60 20.95 6.80 o 8 4 3 36.96 41.01 9.28 o 10 4 3 1.09 5.93 17.62 o -11 5 3 3.66 17.54 13.27 o -9 5 3 524.36 494.59 16.23 o -7 5 3 68.25 65.18 17.01 o -5 5 3 1005.88 984.16 27.27 o -3 5 3 15.52 10.32 2.92 o -1 5 3 163.57 178.82 7.27 o 1 5 3 1068.60 989.31 29.94 o 3 5 3 112.90 109.78 5.94 o 5 5 3 0.05 11.75 6.41 o 7 5 3 333.63 274.77 14.40 o 9 5 3 86.99 88.42 18.48 o -12 6 3 38.35 80.19 23.93 o -10 6 3 0.40 23.97 12.12 o -8 6 3 161.43 147.78 8.71 o -6 6 3 242.78 253.13 9.68 o -4 6 3 2025.95 2353.13 59.08 o -2 6 3 961.52 1018.69 20.08 o 0 6 3 556.07 518.14 19.05 o 2 6 3 2.35 4.94 3.95 o 4 6 3 643.15 550.70 19.13 o 6 6 3 27.80 14.27 11.34 o 8 6 3 150.80 149.66 17.96 o -11 7 3 6.39 8.50 17.86 o -9 7 3 321.47 335.78 17.13 o -7 7 3 0.01 11.39 6.82 o -5 7 3 56.73 48.49 5.43 o -3 7 3 226.51 216.78 6.55 o -1 7 3 690.94 712.24 17.04 o 1 7 3 30.28 33.15 5.81 o 3 7 3 105.83 92.86 5.66 o 5 7 3 426.70 449.39 14.98 o 7 7 3 14.56 10.59 13.12 o 9 7 3 54.46 66.34 31.58 o -10 8 3 206.08 185.34 23.68 o -8 8 3 96.29 132.37 13.60 o -6 8 3 86.14 87.05 6.86 o -4 8 3 0.78 3.58 4.84 o -2 8 3 0.87 11.87 3.91 o 0 8 3 1596.29 1818.15 36.09 o 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