#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:03:18 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180817 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/48/2014890.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014890_Fobs loop_ _publ_author_name 'Iyer, Vijay Mahadevan' 'Stoeckli-Evans, Helen' 'D'Al\'eo, Anthony' 'Cola, Luisa De' 'Belser, Peter' _publ_section_title ; Packing effects in 4,4'-bis(4-hydroxybutyl)-2,2'-bipyridine and 4,4'-bis(4-bromobutyl)-2,2'-bipyridine ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o259 _journal_page_last o261 _journal_volume 61 _journal_year 2005 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.3566 _cell_length_b 14.2463 _cell_length_c 14.7789 _exptl_crystal_F_000 856.00 _reflns_d_resolution_high 0.8388 _cod_data_source_file sk1818IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' IYER01-2 IPDS2 -1200DEGC DIFABS' _shelx_refln_list_code 4 _shelx_f_calc_maximum 335.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 46366.24 42065.82 884.21 o 4 0 0 51948.96 51772.26 659.33 o 6 0 0 406.22 362.17 38.14 o 8 0 0 1292.39 1268.09 69.38 o 2 1 0 10755.91 10258.07 129.83 o 4 1 0 29104.99 27434.40 290.07 o 6 1 0 13301.08 12277.40 239.50 o 8 1 0 3371.82 3721.96 52.33 o 0 2 0 6298.72 5962.73 140.02 o 2 2 0 23988.58 21495.13 117.19 o 4 2 0 3780.94 3019.21 49.61 o 6 2 0 132.32 169.99 25.88 o 8 2 0 9.45 12.97 27.19 o 2 3 0 7622.07 8057.99 97.38 o 4 3 0 11374.16 9736.97 54.66 o 6 3 0 13061.36 12372.27 84.58 o 8 3 0 7005.96 7037.36 81.66 o 0 4 0 43994.63 47059.29 921.53 o 2 4 0 18598.53 16635.94 581.34 o 4 4 0 8569.73 8161.62 170.09 o 6 4 0 15.76 40.58 29.92 o 8 4 0 1052.51 1021.79 39.30 o 2 5 0 8588.26 8563.12 88.98 o 4 5 0 14274.90 13608.81 152.52 o 6 5 0 11043.13 10490.82 105.58 o 8 5 0 5502.10 5647.44 145.61 o 0 6 0 30475.49 31076.25 161.68 o 2 6 0 29337.06 29407.57 680.92 o 4 6 0 10274.90 9803.37 74.54 o 6 6 0 564.50 530.53 34.09 o 8 6 0 89.22 85.90 56.22 o 2 7 0 4049.40 4139.13 62.12 o 4 7 0 3360.75 2929.83 40.38 o 6 7 0 5892.85 5909.87 153.56 o 8 7 0 658.00 674.57 40.17 o 0 8 0 40271.96 42351.51 491.39 o 2 8 0 16871.01 16404.74 337.64 o 4 8 0 3500.48 3125.26 84.69 o 6 8 0 343.00 334.31 31.25 o 8 8 0 1597.90 1391.56 64.02 o 2 9 0 2630.73 2654.94 50.65 o 4 9 0 21328.46 19679.62 96.59 o 6 9 0 4725.25 4696.25 80.39 o 8 9 0 4464.93 4515.42 185.72 o 0 10 0 2682.88 2309.98 57.15 o 2 10 0 7709.56 7990.64 117.24 o 4 10 0 130.18 185.87 42.46 o 6 10 0 128.33 143.96 69.12 o 8 10 0 577.20 588.52 38.83 o 2 11 0 1178.22 1280.84 46.86 o 4 11 0 638.81 719.13 70.03 o 6 11 0 3144.89 2969.02 174.21 o 0 12 0 6801.18 6599.87 253.59 o 2 12 0 5215.13 5511.40 131.85 o 4 12 0 2173.71 2383.62 139.14 o 6 12 0 258.16 243.09 36.30 o 2 13 0 1108.74 1228.34 46.37 o 4 13 0 2857.30 2983.71 90.44 o 6 13 0 1696.44 1614.29 105.09 o 0 14 0 3186.99 3180.86 86.12 o 2 14 0 4935.39 5262.61 229.52 o 4 14 0 608.91 705.51 71.44 o 2 15 0 669.90 632.26 45.44 o 4 15 0 436.32 444.14 41.25 o 0 16 0 556.50 546.41 73.68 o 2 16 0 896.69 866.05 53.01 o 1 1 1 1248.93 1435.08 51.14 o 2 1 1 477.47 485.19 27.60 o 3 1 1 120.99 128.49 19.43 o 4 1 1 343.56 336.25 19.37 o 5 1 1 45.03 52.10 16.96 o 6 1 1 0.13 8.35 16.10 o 7 1 1 38.44 36.89 16.34 o 8 1 1 35.03 49.28 18.27 o 9 1 1 0.28 25.09 20.80 o 0 2 1 41.25 59.10 56.38 o 1 2 1 4400.81 4385.91 77.49 o 2 2 1 10.43 31.37 31.49 o 3 2 1 157.74 155.94 21.59 o 4 2 1 6.27 34.03 20.41 o 5 2 1 190.76 202.29 18.26 o 6 2 1 484.15 487.90 17.87 o 7 2 1 1.32 38.21 19.75 o 8 2 1 1.00 3.39 20.54 o 9 2 1 0.99 27.85 19.97 o 1 3 1 145.14 175.56 58.47 o 2 3 1 2014.94 2046.95 70.62 o 3 3 1 344.83 336.67 24.83 o 4 3 1 0.08 -15.65 25.57 o 5 3 1 53.16 50.63 21.16 o 6 3 1 178.35 178.62 20.59 o 7 3 1 1.22 18.92 19.49 o 8 3 1 32.49 55.46 25.29 o 9 3 1 100.59 55.59 23.49 o 0 4 1 2691.23 3047.46 98.32 o 1 4 1 978.96 1046.00 39.75 o 2 4 1 666.38 776.90 48.23 o 3 4 1 267.91 289.75 28.68 o 4 4 1 755.82 753.61 24.91 o 5 4 1 114.75 96.10 19.81 o 6 4 1 13.50 -8.82 21.24 o 7 4 1 11.70 12.85 25.43 o 8 4 1 114.66 125.22 23.22 o 9 4 1 78.23 62.10 24.63 o 1 5 1 230.88 231.03 33.90 o 2 5 1 1231.28 1238.87 52.90 o 3 5 1 26.47 29.01 34.10 o 4 5 1 0.21 1.11 22.90 o 5 5 1 237.69 231.77 23.74 o 6 5 1 633.14 667.53 22.28 o 7 5 1 99.49 73.53 21.60 o 8 5 1 23.14 15.33 22.39 o 9 5 1 23.53 17.97 26.67 o 0 6 1 1483.09 1538.78 50.82 o 1 6 1 53.42 42.57 39.36 o 2 6 1 540.77 640.32 43.89 o 3 6 1 288.38 371.61 42.85 o 4 6 1 253.53 242.90 26.26 o 5 6 1 343.12 355.66 22.33 o 6 6 1 183.46 224.35 22.32 o 7 6 1 96.04 111.79 29.98 o 8 6 1 9.47 1.37 22.09 o 9 6 1 407.95 396.83 28.15 o 1 7 1 462.46 516.09 39.05 o 2 7 1 178.85 198.46 28.94 o 3 7 1 53.11 43.91 32.43 o 4 7 1 104.32 119.28 24.71 o 5 7 1 976.23 1006.71 26.53 o 6 7 1 9.94 29.15 23.95 o 7 7 1 155.60 175.03 24.73 o 8 7 1 286.23 266.15 23.51 o 9 7 1 166.61 109.12 28.89 o 0 8 1 142.70 204.32 40.80 o 1 8 1 427.45 467.78 31.09 o 2 8 1 226.66 261.71 31.93 o 3 8 1 236.76 247.52 27.79 o 4 8 1 217.38 204.32 32.14 o 5 8 1 161.44 145.69 28.02 o 6 8 1 57.58 47.62 22.03 o 7 8 1 4.29 -13.01 25.17 o 8 8 1 217.46 168.80 26.55 o 1 9 1 495.72 509.37 35.28 o 2 9 1 30.72 42.52 29.59 o 3 9 1 207.14 262.51 30.47 o 4 9 1 21.17 101.40 33.39 o 5 9 1 24.59 12.28 30.67 o 6 9 1 38.42 59.35 24.76 o 7 9 1 7.91 27.05 24.44 o 8 9 1 66.48 112.45 28.45 o 0 10 1 1131.04 1093.58 39.10 o 1 10 1 63.48 64.40 34.05 o 2 10 1 174.70 210.37 29.75 o 3 10 1 149.79 189.47 28.69 o 4 10 1 678.49 655.38 32.46 o 5 10 1 329.99 310.92 23.54 o 6 10 1 408.12 422.50 27.42 o 7 10 1 101.73 132.12 26.51 o 8 10 1 53.88 58.92 29.87 o 1 11 1 10.37 38.80 34.50 o 2 11 1 18.54 22.50 30.52 o 3 11 1 165.82 221.39 35.55 o 4 11 1 37.28 61.68 24.62 o 5 11 1 8.32 8.16 24.47 o 6 11 1 43.33 46.74 30.40 o 7 11 1 42.71 57.51 26.25 o 0 12 1 438.20 357.62 39.47 o 1 12 1 4.89 67.07 31.67 o 2 12 1 4.12 29.49 32.12 o 3 12 1 8.54 56.66 41.87 o 4 12 1 154.42 172.77 29.85 o 5 12 1 34.30 43.99 27.93 o 6 12 1 69.65 111.52 22.53 o 7 12 1 84.45 99.11 29.50 o 1 13 1 383.46 352.65 32.54 o 2 13 1 30.90 51.55 28.80 o 3 13 1 501.83 587.44 32.75 o 4 13 1 77.08 128.07 31.69 o 5 13 1 286.29 294.73 26.19 o 6 13 1 56.98 73.08 26.07 o 0 14 1 5.47 104.78 48.72 o 1 14 1 34.66 15.05 33.84 o 2 14 1 645.71 649.17 31.97 o 3 14 1 4.77 1.40 27.96 o 4 14 1 3.79 18.01 29.72 o 5 14 1 43.02 79.44 31.31 o 1 15 1 84.12 72.47 32.72 o 2 15 1 34.26 58.33 33.57 o 3 15 1 2.91 49.83 32.30 o 4 15 1 66.82 53.55 32.20 o 0 16 1 121.08 88.14 58.72 o 1 16 1 61.29 17.53 33.95 o 2 16 1 140.47 119.16 32.16 o 3 16 1 47.55 36.00 35.47 o 1 0 2 218.57 261.52 71.23 o 2 0 2 523.37 551.36 35.97 o 3 0 2 10102.57 8998.70 136.74 o 4 0 2 1420.93 1400.09 28.90 o 5 0 2 10299.91 9051.50 126.61 o 6 0 2 112.80 137.47 24.44 o 7 0 2 9008.61 8304.94 222.33 o 8 0 2 16.85 17.62 26.63 o 9 0 2 4980.77 5175.12 125.69 o 1 1 2 19804.56 17290.02 341.15 o 2 1 2 56.56 50.39 25.07 o 3 1 2 18649.86 16247.61 98.45 o 4 1 2 4.74 36.65 20.21 o 5 1 2 1088.75 904.45 19.56 o 6 1 2 5.00 -0.54 17.49 o 7 1 2 31.46 49.81 19.22 o 8 1 2 15.54 31.33 18.99 o 9 1 2 773.35 801.49 25.19 o 0 2 2 106.03 176.69 56.20 o 1 2 2 30945.40 30119.60 558.95 o 2 2 2 566.24 669.35 33.67 o 3 2 2 7973.38 6789.76 96.09 o 4 2 2 27.49 58.71 19.76 o 5 2 2 24611.25 23206.59 122.96 o 6 2 2 197.70 218.00 19.89 o 7 2 2 9153.58 8862.25 147.28 o 8 2 2 83.62 107.87 20.11 o 9 2 2 1945.28 2140.18 32.51 o 1 3 2 112453.15 110118.73 889.95 o 2 3 2 609.88 659.79 34.81 o 3 3 2 34448.30 33615.88 550.56 o 4 3 2 58.65 81.44 21.61 o 5 3 2 6255.09 5872.48 83.73 o 6 3 2 390.96 388.18 20.55 o 7 3 2 13.02 13.84 19.06 o 8 3 2 1.58 14.05 21.00 o 9 3 2 559.78 603.72 22.28 o 0 4 2 4294.34 4819.56 89.92 o 1 4 2 33.13 55.63 32.28 o 2 4 2 1029.55 1197.32 44.52 o 3 4 2 13069.22 12413.07 235.28 o 4 4 2 35.00 39.82 22.69 o 5 4 2 12978.06 12213.55 120.40 o 6 4 2 107.31 134.94 19.47 o 7 4 2 2571.37 2744.95 40.44 o 8 4 2 154.32 178.44 21.38 o 9 4 2 2013.70 2078.90 48.93 o 1 5 2 37391.93 37140.53 672.67 o 2 5 2 55.25 78.56 38.29 o 3 5 2 7764.39 6712.59 83.06 o 4 5 2 538.28 556.19 25.40 o 5 5 2 3062.53 2948.44 52.78 o 6 5 2 2.81 15.63 23.37 o 7 5 2 144.16 177.56 22.37 o 8 5 2 33.72 42.67 29.90 o 9 5 2 678.91 678.95 23.79 o 0 6 2 5.36 62.00 45.69 o 1 6 2 3385.55 3603.27 83.72 o 2 6 2 1267.92 1384.45 57.63 o 3 6 2 12527.24 11999.90 60.76 o 4 6 2 24.74 42.77 25.59 o 5 6 2 15381.01 14609.09 239.44 o 6 6 2 139.60 97.16 24.68 o 7 6 2 8605.83 8541.83 99.60 o 8 6 2 70.88 58.61 23.72 o 9 6 2 2027.17 2097.75 54.64 o 1 7 2 13149.65 12650.79 196.23 o 2 7 2 7.61 40.79 36.31 o 3 7 2 11091.81 10617.88 218.87 o 4 7 2 52.83 61.35 34.41 o 5 7 2 47.09 46.38 21.15 o 6 7 2 3.02 -0.32 26.11 o 7 7 2 15.83 15.71 24.19 o 8 7 2 0.14 -3.10 24.98 o 9 7 2 1526.33 1503.79 166.51 o 0 8 2 74.33 143.00 39.34 o 1 8 2 201.64 193.12 31.59 o 2 8 2 145.92 171.84 31.22 o 3 8 2 5131.06 5042.94 108.24 o 4 8 2 11.73 -25.65 25.65 o 5 8 2 3933.38 3699.31 68.82 o 6 8 2 33.42 31.82 23.52 o 7 8 2 4584.54 4743.56 85.23 o 8 8 2 24.35 67.34 23.47 o 1 9 2 13154.86 13221.12 232.52 o 2 9 2 11.73 43.35 31.59 o 3 9 2 6721.96 6854.93 152.14 o 4 9 2 100.61 63.24 27.14 o 5 9 2 2944.19 2938.96 39.51 o 6 9 2 78.92 115.41 26.76 o 7 9 2 4.57 -3.54 25.54 o 8 9 2 44.33 37.61 29.14 o 0 10 2 195.93 194.24 37.75 o 1 10 2 1573.96 1636.09 34.27 o 2 10 2 35.73 55.37 33.88 o 3 10 2 2960.63 2918.12 94.30 o 4 10 2 53.55 83.19 28.30 o 5 10 2 3393.37 3356.43 73.68 o 6 10 2 4.93 15.67 25.00 o 7 10 2 2979.96 2831.00 60.06 o 1 11 2 11947.99 12156.00 276.60 o 2 11 2 35.23 5.84 35.74 o 3 11 2 7162.88 7671.69 173.75 o 4 11 2 11.29 0.80 35.28 o 5 11 2 121.76 160.17 22.85 o 6 11 2 6.47 4.56 26.24 o 7 11 2 4.71 60.65 30.44 o 0 12 2 47.78 55.58 33.72 o 1 12 2 8.08 44.52 36.86 o 2 12 2 510.51 545.26 36.73 o 3 12 2 5314.50 5439.69 124.82 o 4 12 2 6.08 -4.73 28.26 o 5 12 2 2640.48 2791.12 56.18 o 6 12 2 33.70 34.93 23.66 o 1 13 2 2469.68 2638.09 68.76 o 2 13 2 2.79 51.98 32.13 o 3 13 2 221.48 289.45 30.45 o 4 13 2 215.83 271.62 32.95 o 5 13 2 269.82 284.69 25.59 o 6 13 2 6.62 47.02 22.81 o 0 14 2 0.68 -42.84 42.84 o 1 14 2 18.87 33.57 32.57 o 2 14 2 18.28 43.11 32.23 o 3 14 2 1260.76 1329.63 31.84 o 4 14 2 0.63 48.47 33.37 o 5 14 2 1296.40 1317.84 68.10 o 1 15 2 2330.54 2283.65 55.84 o 2 15 2 0.36 29.79 34.50 o 3 15 2 1679.41 1706.36 60.53 o 4 15 2 96.02 98.87 30.76 o 0 16 2 17.96 32.52 59.66 o 1 16 2 156.94 112.06 32.21 o 2 16 2 3.42 25.26 31.46 o 3 16 2 322.79 274.15 41.51 o 1 1 3 3712.13 4054.85 96.29 o 2 1 3 701.45 727.79 27.72 o 3 1 3 6.89 37.60 23.06 o 4 1 3 0.36 17.04 19.51 o 5 1 3 555.24 610.66 18.51 o 6 1 3 46.67 19.90 18.19 o 7 1 3 57.89 58.46 21.03 o 8 1 3 12.59 26.20 20.55 o 9 1 3 125.76 125.41 25.01 o 0 2 3 2718.57 2396.11 133.06 o 1 2 3 6723.27 7382.26 291.29 o 2 2 3 1859.82 1967.29 37.40 o 3 2 3 201.37 270.10 25.92 o 4 2 3 296.42 310.31 23.37 o 5 2 3 55.56 85.45 19.31 o 6 2 3 4.79 49.90 23.14 o 7 2 3 35.26 39.07 18.34 o 8 2 3 7.11 21.07 21.11 o 9 2 3 59.71 39.02 24.16 o 1 3 3 6330.73 6610.62 246.31 o 2 3 3 80.08 100.35 29.36 o 3 3 3 1118.44 1244.61 28.98 o 4 3 3 106.73 126.90 21.84 o 5 3 3 64.83 63.97 21.35 o 6 3 3 64.71 94.98 18.98 o 7 3 3 436.39 408.16 22.06 o 8 3 3 30.45 11.20 19.44 o 9 3 3 5.54 15.17 28.53 o 0 4 3 2295.76 2419.70 65.06 o 1 4 3 1083.31 1212.57 34.04 o 2 4 3 534.95 551.18 33.73 o 3 4 3 2374.41 2509.26 70.13 o 4 4 3 911.46 903.39 28.22 o 5 4 3 6.03 18.84 20.79 o 6 4 3 2.56 9.52 27.70 o 7 4 3 352.24 386.55 23.73 o 8 4 3 188.67 157.16 22.45 o 9 4 3 55.53 82.21 22.14 o 1 5 3 1438.92 1673.13 39.00 o 2 5 3 0.33 -0.55 37.66 o 3 5 3 266.87 281.58 28.29 o 4 5 3 17.54 22.40 22.55 o 5 5 3 1.28 6.26 21.49 o 6 5 3 0.63 -5.12 24.65 o 7 5 3 1328.40 1257.57 33.38 o 8 5 3 2.66 6.56 23.07 o 9 5 3 4.13 -16.44 25.61 o 0 6 3 165.34 237.34 50.21 o 1 6 3 639.96 763.12 40.74 o 2 6 3 229.28 267.78 33.12 o 3 6 3 892.77 1066.72 38.47 o 4 6 3 342.32 285.66 29.79 o 5 6 3 168.92 178.71 23.61 o 6 6 3 36.21 46.07 22.32 o 7 6 3 23.71 22.03 24.87 o 8 6 3 138.74 168.64 25.62 o 9 6 3 66.86 88.04 23.75 o 1 7 3 1664.73 1859.74 38.11 o 2 7 3 295.05 349.49 30.12 o 3 7 3 9.81 3.21 34.00 o 4 7 3 2.09 5.45 25.66 o 5 7 3 1514.72 1469.93 24.98 o 6 7 3 281.63 314.52 38.30 o 7 7 3 19.59 8.77 24.18 o 8 7 3 152.35 168.37 24.50 o 0 8 3 440.08 408.85 37.32 o 1 8 3 32.63 41.69 32.21 o 2 8 3 2.35 19.10 27.64 o 3 8 3 491.12 541.23 36.80 o 4 8 3 589.11 553.30 26.51 o 5 8 3 902.34 921.92 34.04 o 6 8 3 47.81 83.06 31.93 o 7 8 3 127.65 186.50 30.16 o 8 8 3 190.65 199.11 27.26 o 1 9 3 151.82 134.39 29.26 o 2 9 3 36.00 57.32 30.69 o 3 9 3 217.60 253.19 31.95 o 4 9 3 12.68 72.35 29.05 o 5 9 3 6.09 68.94 30.64 o 6 9 3 4.02 -14.76 28.10 o 7 9 3 45.91 38.47 24.35 o 8 9 3 6.99 39.44 27.32 o 0 10 3 902.66 892.33 43.87 o 1 10 3 94.25 110.47 30.34 o 2 10 3 71.45 97.23 38.94 o 3 10 3 2.56 6.69 31.84 o 4 10 3 530.38 557.39 27.60 o 5 10 3 47.04 57.88 27.36 o 6 10 3 530.39 516.98 33.49 o 7 10 3 60.80 84.12 24.57 o 1 11 3 329.56 389.68 36.32 o 2 11 3 40.25 113.71 35.13 o 3 11 3 612.30 661.89 31.00 o 4 11 3 74.18 42.65 26.40 o 5 11 3 11.32 67.50 23.74 o 6 11 3 2.57 28.64 25.03 o 7 11 3 45.18 67.63 25.82 o 0 12 3 130.49 114.23 49.84 o 1 12 3 10.36 50.48 37.13 o 2 12 3 211.92 249.01 32.52 o 3 12 3 411.84 463.91 35.79 o 4 12 3 111.24 137.56 25.70 o 5 12 3 139.23 110.15 27.27 o 6 12 3 26.48 38.55 24.06 o 1 13 3 145.86 135.77 31.81 o 2 13 3 37.70 40.12 33.88 o 3 13 3 234.12 247.13 28.24 o 4 13 3 4.77 32.50 30.61 o 5 13 3 271.85 239.48 26.15 o 6 13 3 145.01 111.56 21.85 o 0 14 3 14.20 -21.91 41.50 o 1 14 3 64.15 35.93 32.96 o 2 14 3 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