#------------------------------------------------------------------------------
#$Date: 2016-04-02 22:03:18 +0300 (Sat, 02 Apr 2016) $
#$Revision: 180817 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/48/2014895.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2014895_Fobs
loop_
_publ_author_name
'Glidewell, Christopher'
'Low, John N.'
'Skakle, Janet M. S.'
'Wardell, James L.'
_publ_section_title
;
Supramolecular structures of four isomorphous anilinium
2-carboxy-4-nitrobenzoate salts:
4-X-C~6~H~4~NH~3~^+^·C~8~H~4~NO~6~^{-^} (X = H,
Cl, Br and I)
;
_journal_issue 5
_journal_name_full 'Acta Crystallographica Section C'
_journal_page_first o276
_journal_page_last o280
_journal_volume 61
_journal_year 2005
_space_group_IT_number 15
_symmetry_space_group_name_Hall '-C 2yc'
_symmetry_space_group_name_H-M 'C 1 2/c 1'
_cell_angle_alpha 90.000
_cell_angle_beta 98.134
_cell_angle_gamma 90.000
_cell_length_a 12.8131
_cell_length_b 7.5521
_cell_length_c 28.1140
_exptl_crystal_F_000 1264.00
_reflns_d_resolution_high 0.8080
_cod_data_source_file sk1823Isup2.hkl
_cod_data_source_block I
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' 316'
_shelx_refln_list_code 4
_shelx_f_calc_maximum 485.86
_shelx_f_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 4743.77 4744.30 168.58 o
4 0 0 236056.70 247123.58 7854.98 o
6 0 0 1882.32 1812.21 67.12 o
8 0 0 1062.42 1185.62 61.11 o
10 0 0 2775.56 3153.89 166.76 o
14 0 0 73.25 811.62 141.53 o
1 1 0 219.00 345.41 19.47 o
3 1 0 27015.46 26717.61 580.05 o
5 1 0 4209.56 5080.64 115.47 o
7 1 0 12179.50 12896.11 297.43 o
9 1 0 1165.84 1216.93 50.43 o
11 1 0 9215.20 10003.93 321.92 o
13 1 0 1.58 -4.56 45.91 o
15 1 0 785.38 485.79 85.26 o
0 2 0 27142.64 23991.04 916.01 o
2 2 0 1988.32 1728.91 58.51 o
4 2 0 3772.06 3329.04 84.20 o
6 2 0 605.59 614.70 25.52 o
8 2 0 1298.80 1177.87 44.72 o
10 2 0 207.25 298.34 38.63 o
12 2 0 802.79 857.86 68.86 o
14 2 0 550.94 480.99 136.95 o
1 3 0 4930.19 4445.39 159.05 o
3 3 0 2634.55 2896.76 95.55 o
5 3 0 23.86 72.27 16.98 o
7 3 0 8.32 32.54 26.14 o
9 3 0 428.15 589.51 41.19 o
11 3 0 109.16 139.87 53.27 o
13 3 0 435.96 382.78 79.54 o
0 4 0 1843.02 2145.22 110.96 o
2 4 0 46.66 73.11 13.18 o
4 4 0 0.00 100.42 22.05 o
6 4 0 507.21 589.07 41.89 o
8 4 0 1814.48 2000.96 96.38 o
10 4 0 921.94 1024.98 82.90 o
12 4 0 270.53 211.26 70.94 o
14 4 0 137.18 137.69 89.59 o
1 5 0 332.26 346.68 29.34 o
3 5 0 189.18 294.44 43.08 o
5 5 0 0.93 82.67 32.52 o
7 5 0 27.23 130.97 44.84 o
9 5 0 0.33 55.95 51.15 o
11 5 0 100.07 26.71 62.15 o
13 5 0 0.01 23.68 90.12 o
0 6 0 123.33 263.35 47.23 o
2 6 0 398.27 453.36 39.38 o
4 6 0 415.74 358.40 38.44 o
6 6 0 275.52 227.55 47.77 o
8 6 0 226.19 155.99 66.78 o
10 6 0 54.53 43.87 60.42 o
1 7 0 72.52 37.30 39.90 o
3 7 0 466.63 342.16 71.80 o
5 7 0 34.00 108.57 185.79 o
7 7 0 224.32 228.51 75.48 o
9 7 0 33.63 79.72 83.23 o
0 8 0 234.50 141.32 78.29 o
2 8 0 6.62 122.00 86.93 o
4 8 0 317.16 247.26 116.37 o
6 8 0 70.77 113.56 90.49 o
8 8 0 137.78 -52.36 172.59 o
1 9 0 59.07 48.13 81.08 o
3 9 0 3.86 -98.73 161.15 o
-15 1 1 2.69 52.80 92.42 o
-13 1 1 409.64 427.97 67.80 o
-11 1 1 1443.49 1503.18 67.83 o
-9 1 1 551.26 542.78 37.98 o
-7 1 1 16371.63 17452.31 410.72 o
-5 1 1 3244.43 2666.97 60.73 o
-3 1 1 30319.79 27313.61 579.21 o
1 1 1 4263.65 3686.06 122.08 o
3 1 1 12516.68 12109.70 275.71 o
5 1 1 6933.35 7506.70 171.17 o
7 1 1 742.53 732.60 37.34 o
9 1 1 19.53 51.96 23.26 o
11 1 1 2980.14 3432.94 136.79 o
13 1 1 304.01 298.16 62.94 o
15 1 1 781.31 417.57 102.31 o
-14 2 1 1748.57 2043.68 155.53 o
-12 2 1 108.38 151.57 58.09 o
-10 2 1 6.94 39.21 28.20 o
-8 2 1 1672.19 1720.20 60.28 o
-6 2 1 790.18 824.88 36.04 o
-4 2 1 608.25 636.07 23.61 o
-2 2 1 5.38 30.20 13.40 o
0 2 1 776.48 980.59 30.93 o
2 2 1 2747.43 2324.38 68.06 o
4 2 1 2814.74 2654.03 65.42 o
6 2 1 1772.23 1690.83 46.73 o
8 2 1 1506.81 1353.61 48.36 o
10 2 1 6255.21 6574.55 201.92 o
12 2 1 180.73 165.06 48.40 o
14 2 1 2370.02 2314.91 179.70 o
-13 3 1 755.47 639.24 83.32 o
-11 3 1 1.99 78.75 47.13 o
-9 3 1 295.11 344.65 32.95 o
-7 3 1 335.30 314.84 25.62 o
-5 3 1 830.90 828.56 36.46 o
-3 3 1 157.83 180.98 21.65 o
-1 3 1 5553.27 5102.82 144.99 o
1 3 1 4032.18 3947.87 127.05 o
3 3 1 7300.13 7065.75 227.10 o
5 3 1 2637.64 2604.84 84.21 o
7 3 1 1498.67 1478.52 50.58 o
9 3 1 145.66 128.58 32.24 o
11 3 1 0.05 44.21 38.10 o
13 3 1 2.13 -64.33 64.33 o
-14 4 1 0.66 -83.31 92.89 o
-12 4 1 28.72 115.07 73.43 o
-10 4 1 89.92 138.84 50.46 o
-8 4 1 1155.28 1197.10 57.62 o
-6 4 1 116.19 155.99 39.43 o
-4 4 1 4409.12 4686.33 187.46 o
-2 4 1 2445.57 2196.31 64.68 o
0 4 1 9.40 88.97 15.09 o
2 4 1 1910.14 1606.14 53.01 o
4 4 1 0.21 18.84 21.44 o
6 4 1 2103.30 2035.37 92.84 o
8 4 1 114.52 159.39 32.48 o
10 4 1 958.41 1209.65 121.63 o
12 4 1 569.05 607.98 94.33 o
14 4 1 2.16 -77.97 98.65 o
-13 5 1 0.12 15.12 81.66 o
-11 5 1 59.57 115.69 73.48 o
-9 5 1 71.27 34.32 49.10 o
-7 5 1 22.22 9.21 43.13 o
-5 5 1 2033.99 2043.79 95.13 o
-3 5 1 901.30 1013.38 56.73 o
-1 5 1 3035.84 3122.35 114.81 o
1 5 1 354.88 402.90 31.15 o
3 5 1 840.62 871.45 43.66 o
5 5 1 474.39 370.26 43.85 o
7 5 1 1964.50 1923.35 126.25 o
9 5 1 41.77 98.21 51.43 o
11 5 1 129.06 177.92 88.93 o
13 5 1 43.01 -32.91 92.73 o
-12 6 1 104.97 -115.90 205.63 o
-10 6 1 60.87 75.18 63.67 o
-8 6 1 51.34 122.08 52.11 o
-6 6 1 44.40 30.19 43.49 o
-4 6 1 329.97 268.74 33.89 o
-2 6 1 272.10 333.55 37.96 o
0 6 1 429.42 457.07 39.10 o
2 6 1 2109.24 2059.76 87.35 o
4 6 1 174.26 159.86 36.99 o
6 6 1 641.27 516.19 54.18 o
8 6 1 178.70 186.72 50.39 o
10 6 1 85.97 32.05 82.36 o
-9 7 1 81.08 40.42 83.09 o
-7 7 1 163.00 95.32 88.90 o
-5 7 1 5.24 -35.19 69.12 o
-3 7 1 341.76 591.39 104.38 o
-1 7 1 138.74 68.87 48.04 o
1 7 1 54.89 60.11 41.71 o
3 7 1 13.17 51.98 54.73 o
5 7 1 1237.90 1415.26 152.10 o
7 7 1 1206.93 910.57 141.93 o
9 7 1 253.27 103.06 132.04 o
-8 8 1 0.09 146.66 209.70 o
-6 8 1 63.72 34.65 103.60 o
-4 8 1 796.78 985.99 225.58 o
-2 8 1 0.36 48.29 58.35 o
0 8 1 179.39 144.40 53.61 o
2 8 1 218.04 32.92 79.43 o
4 8 1 5.08 99.87 97.89 o
6 8 1 29.52 45.75 157.34 o
-3 9 1 0.42 214.78 120.59 o
-1 9 1 61.16 92.06 134.21 o
1 9 1 1.76 46.75 122.64 o
3 9 1 12.97 93.82 105.03 o
-14 0 2 299.12 248.91 73.16 o
-12 0 2 108.89 61.13 60.57 o
-10 0 2 4786.52 4945.42 227.48 o
-8 0 2 7127.43 7971.85 285.03 o
-6 0 2 10001.37 11194.80 341.58 o
-4 0 2 36508.18 38911.83 1178.45 o
-2 0 2 213.06 234.81 16.60 o
2 0 2 21468.83 21323.35 864.17 o
4 0 2 111618.37 116411.84 3735.73 o
6 0 2 1211.78 1243.26 74.51 o
8 0 2 37168.46 44750.55 1553.44 o
10 0 2 1451.36 1642.55 96.64 o
12 0 2 116.47 175.55 55.88 o
14 0 2 65.74 209.80 101.95 o
-15 1 2 569.88 310.30 76.73 o
-13 1 2 43.82 50.69 40.44 o
-11 1 2 393.05 414.47 40.68 o
-9 1 2 9.94 62.40 24.95 o
-7 1 2 16408.90 18052.36 398.07 o
-5 1 2 7938.19 9126.86 197.46 o
-3 1 2 60544.20 58478.88 1361.82 o
-1 1 2 882.62 1132.49 38.37 o
1 1 2 29574.05 26555.31 833.13 o
3 1 2 43423.14 45381.22 1149.20 o
5 1 2 18814.57 20119.74 454.26 o
7 1 2 141.50 259.09 20.09 o
9 1 2 835.99 1005.82 44.84 o
11 1 2 497.73 625.10 48.89 o
13 1 2 685.47 578.64 83.31 o
15 1 2 767.48 416.47 106.72 o
-14 2 2 716.57 599.71 104.43 o
-12 2 2 6.56 73.29 53.81 o
-10 2 2 1993.76 1916.06 80.13 o
-8 2 2 36.21 45.10 19.30 o
-6 2 2 3030.48 3136.64 88.39 o
-4 2 2 642.33 671.39 26.07 o
0 2 2 4135.98 4569.20 142.22 o
2 2 2 12965.46 11817.75 337.82 o
4 2 2 433.47 591.47 23.74 o
6 2 2 4594.27 5142.98 127.68 o
8 2 2 122.24 145.75 20.62 o
10 2 2 259.85 392.33 50.58 o
12 2 2 21.19 7.42 54.80 o
14 2 2 313.75 319.60 62.86 o
-13 3 2 771.84 969.82 110.94 o
-11 3 2 1042.40 950.22 93.79 o
-9 3 2 9.79 25.74 27.79 o
-7 3 2 807.88 911.90 53.55 o
-5 3 2 342.91 330.64 22.44 o
-3 3 2 268.85 339.55 44.99 o
-1 3 2 3028.87 3173.45 100.05 o
1 3 2 39.90 68.58 11.48 o
3 3 2 9026.21 8996.12 292.55 o
5 3 2 4357.66 4558.79 130.63 o
7 3 2 5836.98 6274.32 177.79 o
9 3 2 1899.48 2075.85 73.78 o
11 3 2 336.62 247.91 52.14 o
13 3 2 644.34 659.21 106.23 o
-14 4 2 21.13 18.03 71.07 o
-12 4 2 22.34 95.53 76.45 o
-10 4 2 121.27 170.72 45.27 o
-8 4 2 51.93 78.75 34.27 o
-6 4 2 810.08 788.10 59.98 o
-4 4 2 3058.90 3350.76 120.35 o
-2 4 2 891.84 907.35 31.99 o
0 4 2 2161.39 2769.04 92.73 o
2 4 2 35.79 48.86 12.87 o
4 4 2 493.07 474.28 35.15 o
6 4 2 244.68 314.29 37.98 o
8 4 2 319.01 370.62 28.85 o
10 4 2 61.25 83.73 47.08 o
12 4 2 37.93 77.02 70.55 o
14 4 2 5.07 -216.05 216.05 o
-13 5 2 2.53 132.62 73.47 o
-11 5 2 0.00 15.52 67.88 o
-9 5 2 167.40 236.63 67.38 o
-7 5 2 38.22 2.04 40.97 o
-5 5 2 637.73 618.72 47.70 o
-3 5 2 206.26 193.60 33.13 o
-1 5 2 2847.12 2909.76 91.54 o
1 5 2 531.43 489.95 34.35 o
3 5 2 895.50 928.40 44.56 o
5 5 2 356.67 399.56 43.28 o
7 5 2 8.99 81.44 48.35 o
9 5 2 502.45 488.62 63.22 o
11 5 2 118.24 102.96 61.32 o
13 5 2 524.46 371.03 151.08 o
-12 6 2 89.02 237.91 133.70 o
-10 6 2 0.76 22.33 68.25 o
-8 6 2 0.27 12.54 45.98 o
-6 6 2 298.15 255.38 44.56 o
-4 6 2 0.54 44.77 29.17 o
-2 6 2 167.92 192.64 19.98 o
0 6 2 77.20 147.19 33.40 o
2 6 2 75.69 161.30 35.30 o
4 6 2 36.83 20.76 35.83 o
6 6 2 202.60 117.70 40.99 o
8 6 2 43.44 28.04 43.86 o
10 6 2 782.93 820.02 99.18 o
-9 7 2 42.39 167.80 111.33 o
-7 7 2 123.24 212.12 86.66 o
-5 7 2 0.47 7.63 103.29 o
-3 7 2 78.69 16.69 61.09 o
-1 7 2 594.61 665.57 66.83 o
1 7 2 140.22 153.69 48.61 o
3 7 2 198.08 233.40 102.05 o
5 7 2 173.66 54.23 110.26 o
7 7 2 26.65 98.02 65.63 o
9 7 2 44.47 123.02 127.60 o
-8 8 2 156.44 358.39 151.74 o
-6 8 2 6.90 88.74 117.33 o
-4 8 2 254.92 345.37 111.73 o
-2 8 2 248.94 336.70 69.97 o
0 8 2 46.06 151.99 51.89 o
2 8 2 221.38 307.82 86.73 o
4 8 2 49.56 76.30 101.17 o
6 8 2 18.97 43.21 96.08 o
-3 9 2 51.72 663.15 283.91 o
-1 9 2 269.57 146.52 211.86 o
1 9 2 12.80 40.08 81.28 o
3 9 2 37.83 92.99 105.42 o
-15 1 3 984.20 774.67 104.52 o
-13 1 3 72.89 66.23 47.41 o
-11 1 3 1233.00 1170.16 58.99 o
-9 1 3 544.46 474.28 33.09 o
-7 1 3 187.31 253.55 26.44 o
-5 1 3 1270.82 1446.37 38.22 o
-3 1 3 4596.13 4114.17 106.21 o
-1 1 3 507.09 311.31 15.27 o
1 1 3 27278.52 23030.72 665.97 o
3 1 3 4710.06 5432.80 138.08 o
5 1 3 1145.86 942.55 33.04 o
7 1 3 6644.38 7206.94 177.38 o
9 1 3 333.19 330.23 31.94 o
11 1 3 521.80 544.18 44.03 o
13 1 3 1.18 -21.37 43.61 o
15 1 3 46.30 -62.29 201.53 o
-14 2 3 339.88 341.15 92.84 o
-12 2 3 133.58 113.64 44.92 o
-10 2 3 2947.02 2746.28 112.91 o
-8 2 3 30.40 52.16 18.42 o
-6 2 3 692.79 865.77 33.30 o
-4 2 3 2854.97 3095.52 89.77 o
-2 2 3 6430.30 5869.95 163.60 o
0 2 3 2220.17 1591.35 47.73 o
2 2 3 172.06 286.37 21.28 o
4 2 3 2438.74 2636.56 74.85 o
6 2 3 1887.78 1910.55 52.22 o
8 2 3 1192.35 1242.72 46.00 o
10 2 3 460.50 397.92 38.39 o
12 2 3 253.88 121.44 44.26 o
14 2 3 234.07 112.82 60.77 o
-15 3 3 299.08 -100.08 415.45 o
-13 3 3 166.84 211.46 65.11 o
-11 3 3 82.45 173.13 49.42 o
-9 3 3 610.73 796.87 49.08 o
-7 3 3 159.20 120.62 29.86 o
-5 3 3 174.72 125.79 14.76 o
-3 3 3 3529.25 3274.06 94.37 o
-1 3 3 6548.75 6751.26 184.48 o
1 3 3 738.50 701.64 30.90 o
3 3 3 538.04 609.56 24.45 o
5 3 3 154.45 205.37 16.99 o
7 3 3 2258.99 2289.74 70.27 o
9 3 3 0.38 125.60 31.15 o
11 3 3 539.29 578.70 70.97 o
13 3 3 98.29 42.06 70.84 o
-14 4 3 76.46 129.56 85.83 o
-12 4 3 882.40 835.49 93.02 o
-10 4 3 318.62 371.20 74.41 o
-8 4 3 29.64 34.61 24.19 o
-6 4 3 3310.96 3638.75 180.59 o
-4 4 3 566.87 515.59 39.49 o
-2 4 3 705.67 603.83 25.72 o
0 4 3 9529.21 10003.32 313.33 o
2 4 3 339.65 256.88 22.64 o
4 4 3 4284.64 4641.22 167.31 o
6 4 3 390.04 364.17 35.99 o
8 4 3 186.13 181.10 34.77 o
10 4 3 31.85 15.90 56.99 o
12 4 3 258.76 165.49 79.77 o
-13 5 3 18.60 85.55 90.00 o
-11 5 3 965.76 1004.29 136.49 o
-9 5 3 1.24 -2.13 54.80 o
-7 5 3 57.54 118.63 47.56 o
-5 5 3 973.34 849.24 93.77 o
-3 5 3 366.52 332.82 18.64 o
-1 5 3 1784.26 1730.52 64.91 o
1 5 3 25.23 55.45 25.87 o
3 5 3 144.96 157.56 30.46 o
5 5 3 925.23 1021.77 61.00 o
7 5 3 45.78 89.28 38.52 o
9 5 3 29.00 80.22 74.40 o
11 5 3 4.09 -73.16 73.16 o
-12 6 3 92.00 302.78 130.79 o
-10 6 3 8.64 29.39 59.61 o
-8 6 3 182.51 174.45 58.54 o
-6 6 3 64.16 152.08 43.22 o
-4 6 3 574.89 599.38 45.29 o
-2 6 3 244.10 201.54 26.34 o
0 6 3 39.63 20.43 32.55 o
2 6 3 154.38 110.87 26.44 o
4 6 3 144.46 153.56 34.73 o
6 6 3 38.31 51.82 41.15 o
8 6 3 376.99 347.47 66.30 o
10 6 3 1399.51 1195.06 177.69 o
-9 7 3 0.18 39.86 112.74 o
-7 7 3 4.52 67.55 86.00 o
-5 7 3 824.02 978.69 123.46 o
-3 7 3 173.28 155.45 74.05 o
-1 7 3 2325.60 2271.72 186.44 o
1 7 3 33.11 35.52 44.75 o
3 7 3 1591.58 1530.89 180.93 o
5 7 3 767.28 804.32 95.54 o
7 7 3 1659.83 1311.90 160.48 o
9 7 3 31.76 78.61 100.16 o
-8 8 3 75.78 7.88 122.26 o
-6 8 3 111.26 146.92 122.35 o
-4 8 3 412.60 619.17 266.12 o
-2 8 3 17.90 53.26 46.09 o
0 8 3 81.89 89.25 56.66 o
2 8 3 0.70 20.75 80.34 o
4 8 3 332.78 217.09 112.35 o
6 8 3 0.00 -83.12 99.64 o
-3 9 3 31.96 88.20 111.39 o
-1 9 3 41.95 -71.93 128.49 o
1 9 3 3.65 -85.52 85.52 o
3 9 3 0.62 24.41 76.70 o
-14 0 4 125.97 92.32 77.10 o
-12 0 4 1.02 14.63 61.05 o
-10 0 4 211.78 149.68 39.21 o
-8 0 4 997.20 1080.53 69.29 o
-6 0 4 990.16 951.77 46.49 o
-4 0 4 551.43 797.93 36.54 o
-2 0 4 1009.99 997.76 45.86 o
2 0 4 1185.39 1576.76 85.74 o
4 0 4 280.13 396.40 31.73 o
6 0 4 35.21 42.49 24.65 o
8 0 4 1727.35 1821.33 105.01 o
10 0 4 1814.25 1927.55 145.50 o
12 0 4 5346.24 6218.15 343.81 o
14 0 4 1.17 70.08 114.63 o
-15 1 4 10.72 -54.16 64.55 o
-13 1 4 65.58 -4.50 54.02 o
-11 1 4 1.91 -29.02 32.59 o
-9 1 4 193.11 223.64 28.46 o
-7 1 4 247.62 333.15 21.30 o
-5 1 4 557.30 654.64 33.00 o
-3 1 4 4535.71 3942.90 112.14 o
-1 1 4 2331.28 1983.73 71.30 o
1 1 4 33888.73 32378.37 900.76 o
3 1 4 7896.25 7223.19 218.80 o
5 1 4 49.58 40.78 13.14 o
7 1 4 3113.59 3623.11 98.76 o
9 1 4 79.32 123.44 25.50 o
11 1 4 2561.07 2949.21 115.55 o
13 1 4 293.71 261.83 81.37 o
15 1 4 107.51 -80.53 95.37 o
-14 2 4 233.87 160.62 111.53 o
-12 2 4 13.51 28.47 48.18 o
-10 2 4 19.97 3.83 33.13 o
-8 2 4 1131.52 1039.00 43.38 o
-6 2 4 1823.46 1847.64 56.74 o
-4 2 4 541.89 466.04 21.61 o
-2 2 4 4022.00 3858.62 112.76 o
0 2 4 9050.55 8380.71 226.44 o
2 2 4 8316.88 8048.55 269.54 o
4 2 4 5600.30 5255.32 146.98 o
6 2 4 1586.72 1497.12 48.29 o
8 2 4 8.97 54.83 18.89 o
10 2 4 1105.04 1197.97 65.05 o
12 2 4 164.55 120.63 51.06 o
14 2 4 571.11 319.50 133.50 o
-15 3 4 28.19 -127.83 271.33 o
-13 3 4 424.95 244.13 73.90 o
-11 3 4 933.19 933.26 69.95 o
-9 3 4 107.73 79.21 31.00 o
-7 3 4 632.24 581.23 32.93 o
-5 3 4 0.92 6.67 21.89 o
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