#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/49/2014931.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014931_Fobs loop_ _publ_author_name 'Harding, David J.' 'Adams, Harry' 'Tuntulani, Thawatchai' _publ_section_title ; B---N bond cleavage by cobalt(II) in acetato(3,5-diphenylpyrazole)[tris(3,5-diphenylpyrazolyl)borato]cobalt(II) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m301 _journal_page_last m303 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 84.568 _cell_angle_beta 66.500 _cell_angle_gamma 67.199 _cell_length_a 13.5669 _cell_length_b 14.0474 _cell_length_c 15.4195 _exptl_crystal_F_000 1050.00 _reflns_d_resolution_high 0.7684 _[local]_cod_data_source_file sq1208Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' IMW235 IN P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 277.97 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ 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1 0 200.92 196.95 5.73 o 3 1 0 123.55 111.06 5.98 o 4 1 0 1981.24 2070.24 28.35 o 5 1 0 2596.87 2662.11 33.50 o 6 1 0 318.69 311.69 10.98 o 7 1 0 1714.93 1654.02 26.15 o 8 1 0 1799.04 1852.55 39.86 o 9 1 0 2277.16 2293.04 47.40 o 10 1 0 1383.42 1381.72 38.99 o 11 1 0 592.87 702.79 33.53 o 12 1 0 41.80 61.67 22.74 o 13 1 0 17.29 13.64 22.51 o 14 1 0 0.11 25.01 27.81 o 15 1 0 0.48 6.54 44.79 o -13 2 0 21.82 20.93 29.73 o -12 2 0 379.05 387.04 41.25 o -11 2 0 690.70 814.64 51.27 o -10 2 0 2.18 -11.56 16.84 o -9 2 0 57.74 50.43 16.17 o -8 2 0 299.18 306.11 21.97 o -7 2 0 1035.96 992.13 29.76 o -6 2 0 22.09 16.24 6.83 o -5 2 0 3835.89 4107.23 46.38 o -4 2 0 14.71 24.36 5.54 o -3 2 0 17662.06 19226.20 193.34 o -2 2 0 33.70 44.02 4.60 o -1 2 0 531.44 508.46 9.63 o 0 2 0 3072.33 3109.19 27.08 o 1 2 0 112.65 115.16 4.24 o 2 2 0 2903.53 3063.10 40.16 o 3 2 0 64.82 70.29 7.01 o 4 2 0 1015.70 951.40 20.37 o 5 2 0 10.47 3.96 4.60 o 6 2 0 3822.64 4001.43 47.97 o 7 2 0 7473.21 8122.70 73.81 o 8 2 0 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44.44 o 14 3 0 236.10 314.69 38.00 o 15 3 0 7.73 23.18 27.97 o -12 4 0 70.15 126.66 32.42 o -11 4 0 23.35 -13.36 25.72 o -10 4 0 26.84 43.50 22.94 o -9 4 0 41.98 17.72 21.68 o -8 4 0 730.38 746.76 31.13 o -7 4 0 3.96 1.65 12.05 o -6 4 0 210.05 175.73 15.78 o -5 4 0 872.82 795.25 20.17 o -4 4 0 779.00 778.69 20.41 o -3 4 0 1623.39 1812.35 26.81 o -2 4 0 2230.96 2289.22 29.17 o -1 4 0 558.00 581.60 16.84 o 0 4 0 4020.66 4129.98 39.56 o 1 4 0 90.53 77.14 5.63 o 2 4 0 550.01 535.74 10.93 o 3 4 0 64.27 65.32 5.49 o 4 4 0 1996.05 1967.23 25.16 o 5 4 0 1148.30 1132.62 20.27 o 6 4 0 117.45 167.83 26.26 o 7 4 0 1408.68 1306.35 24.40 o 8 4 0 1078.61 1069.24 23.47 o 9 4 0 778.54 712.30 20.72 o 10 4 0 49.13 40.74 15.48 o 11 4 0 745.15 733.57 30.49 o 12 4 0 97.80 78.81 17.47 o 13 4 0 217.81 210.55 30.05 o 14 4 0 0.10 8.56 24.17 o 15 4 0 13.00 -8.68 31.88 o -12 5 0 475.91 455.05 49.87 o -11 5 0 345.61 384.24 44.68 o -10 5 0 194.74 170.64 34.10 o -9 5 0 69.49 76.44 25.32 o -8 5 0 542.38 598.94 81.23 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0 2451.21 2516.67 43.82 o 8 7 0 2377.32 2401.50 37.04 o 9 7 0 1252.62 1219.31 26.59 o 10 7 0 720.53 686.39 26.74 o 11 7 0 308.36 324.89 24.76 o 12 7 0 5.08 17.42 18.02 o 13 7 0 25.81 16.69 16.67 o 14 7 0 17.45 36.81 19.19 o 15 7 0 3.60 -9.77 25.03 o 16 7 0 203.72 283.10 54.47 o -10 8 0 2.20 -12.41 45.56 o -9 8 0 328.91 394.58 45.00 o -8 8 0 294.48 323.66 39.46 o -7 8 0 251.24 193.50 29.29 o -6 8 0 55.62 36.94 16.90 o -5 8 0 453.90 422.73 37.40 o -4 8 0 609.92 643.96 23.36 o -3 8 0 629.53 647.51 21.65 o -2 8 0 912.17 843.42 22.76 o -1 8 0 2905.26 2962.40 47.36 o 0 8 0 3747.57 3820.68 47.94 o 1 8 0 79.24 111.86 11.69 o 2 8 0 5.99 18.18 7.48 o 3 8 0 4018.03 4134.58 47.48 o 4 8 0 75.89 43.40 7.62 o 5 8 0 1040.79 1143.19 22.33 o 6 8 0 18.97 15.49 7.96 o 7 8 0 168.54 175.70 15.43 o 8 8 0 35.16 42.84 10.46 o 9 8 0 3.89 -0.39 9.42 o 10 8 0 166.47 154.66 17.67 o 11 8 0 1341.09 1254.53 47.96 o 12 8 0 532.89 636.58 68.19 o 13 8 0 8.15 10.53 20.45 o 14 8 0 806.71 920.27 48.97 o 15 8 0 367.95 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10 0 55.91 30.85 10.97 o 0 10 0 2032.55 2017.77 37.28 o 1 10 0 405.66 424.69 33.34 o 2 10 0 112.66 103.62 12.08 o 3 10 0 1611.42 1649.56 30.96 o 4 10 0 1616.16 1647.56 36.96 o 5 10 0 3242.29 3326.01 54.63 o 6 10 0 3709.45 3730.26 58.67 o 7 10 0 70.46 62.39 14.78 o 8 10 0 59.21 57.35 13.66 o 9 10 0 176.31 143.49 17.13 o 10 10 0 708.79 738.24 31.35 o 11 10 0 145.33 127.82 24.59 o 12 10 0 865.58 878.70 34.84 o 13 10 0 292.86 289.93 37.53 o 14 10 0 184.28 273.83 65.00 o 15 10 0 267.21 320.64 38.89 o -8 11 0 17.83 26.07 53.91 o -7 11 0 56.63 -3.92 32.76 o -6 11 0 8.02 37.54 28.83 o -5 11 0 234.35 274.58 37.06 o -4 11 0 2.82 -15.13 16.58 o -3 11 0 2.33 -4.06 14.58 o -2 11 0 1.61 12.98 12.79 o -1 11 0 743.67 799.35 28.20 o 0 11 0 2329.66 2444.47 50.94 o 1 11 0 86.71 76.91 14.79 o 2 11 0 60.88 28.32 12.63 o 3 11 0 115.59 113.91 15.01 o 4 11 0 2.08 10.26 10.76 o 5 11 0 379.26 420.57 23.36 o 6 11 0 206.79 222.38 18.74 o 7 11 0 392.77 460.23 24.64 o 8 11 0 288.52 283.28 20.89 o 9 11 0 123.93 108.77 14.85 o 10 11 0 4.17 15.57 14.74 o 11 11 0 16.56 18.63 16.13 o 12 11 0 4.70 11.00 22.23 o 13 11 0 635.02 679.50 65.45 o 14 11 0 290.09 340.48 55.76 o 15 11 0 196.36 259.05 52.70 o -7 12 0 6.28 -31.47 54.39 o -6 12 0 59.16 12.35 50.92 o -5 12 0 379.64 395.76 68.35 o -4 12 0 431.50 549.82 66.17 o -3 12 0 241.85 214.26 47.13 o -2 12 0 471.18 567.33 34.49 o -1 12 0 1271.26 1292.11 39.45 o 0 12 0 184.10 179.90 53.18 o 1 12 0 42.92 68.07 18.84 o 2 12 0 44.93 30.79 16.30 o 3 12 0 105.08 102.31 18.54 o 4 12 0 519.12 574.69 32.10 o 5 12 0 292.55 342.09 70.69 o 6 12 0 5.48 1.42 14.63 o 7 12 0 703.50 668.50 41.72 o 8 12 0 1132.56 1148.25 43.87 o 9 12 0 35.03 -0.66 14.87 o 10 12 0 888.65 928.71 41.75 o 11 12 0 1619.20 1594.13 59.23 o 12 12 0 48.65 37.79 24.09 o 13 12 0 47.89 3.73 26.78 o 14 12 0 34.74 -19.45 38.98 o 15 12 0 45.92 12.91 44.87 o -5 13 0 47.82 47.29 51.00 o -4 13 0 20.51 34.38 48.50 o -2 13 0 1.06 11.38 23.89 o -1 13 0 7.65 -12.39 18.81 o 0 13 0 759.54 798.80 51.33 o 1 13 0 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15 0 2.99 -17.18 21.08 o 4 15 0 136.62 177.16 47.25 o 5 15 0 691.40 804.95 44.17 o 6 15 0 1.67 -17.41 22.88 o 7 15 0 422.82 450.63 41.88 o 8 15 0 102.66 76.09 22.61 o 9 15 0 39.57 74.40 23.87 o 10 15 0 12.65 -9.38 22.12 o 11 15 0 93.87 73.48 24.83 o 12 15 0 2.42 -1.31 25.14 o 13 15 0 4.72 20.76 28.49 o 0 16 0 13.22 18.26 28.00 o 1 16 0 1.42 2.94 26.95 o 2 16 0 447.49 424.27 76.99 o 3 16 0 1058.99 1139.17 51.91 o 4 16 0 32.86 47.93 21.99 o 5 16 0 247.92 222.88 54.35 o 6 16 0 507.28 546.41 43.44 o 7 16 0 349.81 371.12 37.24 o 8 16 0 28.88 16.59 24.50 o 9 16 0 2.68 -7.68 23.01 o 10 16 0 102.03 121.45 31.68 o 11 16 0 223.39 229.44 50.36 o 12 16 0 91.52 137.84 56.41 o 1 17 0 18.92 14.77 31.12 o 2 17 0 7.63 14.33 28.13 o 3 17 0 0.70 0.08 25.85 o 4 17 0 4.67 24.49 24.48 o 5 17 0 0.11 -14.90 24.24 o 6 17 0 4.85 4.36 24.47 o 7 17 0 14.33 22.54 28.29 o 8 17 0 88.52 84.93 29.62 o 9 17 0 75.53 62.36 28.34 o 10 17 0 45.15 38.25 47.69 o 5 18 0 33.98 48.99 37.20 o -5 -18 1 501.95 448.54 56.49 o -9 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