#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/49/2014947.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014947_Fobs loop_ _publ_author_name 'Banerjee, Sangeeta Ray' 'Zubieta, Jon' _publ_section_title ; A new tricarbonylrhenium(I) compound incorporating the tridentate ligand N,N-bispicolyl-2-ethanolamine ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m275 _journal_page_last m277 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.881 _cell_angle_gamma 90.000 _cell_length_a 14.9624 _cell_length_b 16.5768 _cell_length_c 18.1167 _exptl_crystal_F_000 2400.00 _reflns_d_resolution_high 0.6800 _[local]_cod_data_source_file tr1108Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p21c in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 622.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 21.55 56.80 96.02 o 2 0 0 184023.11 214898.67 14111.09 o 3 0 0 4323.97 4143.02 171.46 o 4 0 0 20951.78 23506.82 775.66 o 5 0 0 9238.17 7370.79 292.05 o 6 0 0 2530.38 3853.36 313.47 o 7 0 0 51966.31 48502.62 1576.51 o 8 0 0 117541.09 115746.18 3660.82 o 9 0 0 3946.62 4198.91 338.07 o 10 0 0 53122.95 50777.92 2103.05 o 11 0 0 2035.83 2151.73 314.12 o 12 0 0 22376.35 22926.49 1111.66 o 13 0 0 1643.27 2166.09 369.13 o 14 0 0 7616.73 8259.28 629.56 o 15 0 0 63188.16 63267.40 3267.05 o 16 0 0 552.25 1360.74 409.64 o 17 0 0 24458.29 25419.06 1359.34 o 18 0 0 32.71 284.21 423.15 o 19 0 0 5411.96 5536.17 714.89 o 20 0 0 268.56 445.45 532.71 o 1 1 0 15333.87 15304.90 585.07 o 2 1 0 16902.53 21112.07 640.95 o 3 1 0 94599.51 102271.98 2767.94 o 4 1 0 48050.34 52794.66 1301.25 o 5 1 0 64711.64 65490.24 1612.00 o 6 1 0 16156.67 16613.38 462.97 o 7 1 0 38553.18 38634.17 995.92 o 8 1 0 2224.77 2090.37 144.06 o 9 1 0 338.68 661.48 105.59 o 10 1 0 38773.09 35468.31 952.45 o 11 1 0 403.16 311.31 157.84 o 12 1 0 21486.47 19572.63 698.39 o 13 1 0 18669.92 17348.61 660.24 o 14 1 0 14129.70 13557.18 582.67 o 15 1 0 11870.19 11325.67 546.19 o 16 1 0 892.77 700.80 266.13 o 17 1 0 430.22 493.71 275.32 o 18 1 0 5844.10 6198.81 505.69 o 19 1 0 9.40 290.38 324.83 o 20 1 0 7460.58 8111.33 677.34 o 0 2 0 33284.75 37495.85 1730.67 o 1 2 0 122914.13 154927.89 9303.19 o 2 2 0 555.43 879.91 55.60 o 3 2 0 86915.69 99425.34 3746.06 o 4 2 0 40951.23 39485.36 986.09 o 5 2 0 146.37 334.53 79.53 o 6 2 0 24670.05 24894.29 662.09 o 7 2 0 997.00 931.53 108.78 o 8 2 0 78.82 217.30 136.96 o 9 2 0 26999.23 25020.56 698.68 o 10 2 0 2088.44 2487.16 278.19 o 11 2 0 18079.75 16034.57 587.30 o 12 2 0 961.26 1261.37 214.76 o 13 2 0 3993.14 4912.79 355.76 o 14 2 0 7220.33 7553.33 574.38 o 15 2 0 163.17 -28.35 218.22 o 16 2 0 6846.40 6399.72 453.02 o 17 2 0 1176.75 1277.45 309.88 o 18 2 0 6365.85 6428.29 510.71 o 19 2 0 635.37 1115.80 357.01 o 20 2 0 949.31 588.56 373.27 o 1 3 0 4773.06 4557.28 304.32 o 2 3 0 2267.56 1865.35 135.82 o 3 3 0 2848.57 3379.65 284.76 o 4 3 0 292982.00 307441.97 7378.17 o 5 3 0 82507.78 85283.19 2089.14 o 6 3 0 31930.19 32811.84 852.61 o 7 3 0 35148.13 34846.04 910.06 o 8 3 0 14247.08 13788.47 422.64 o 9 3 0 2541.92 2753.34 208.81 o 10 3 0 35886.37 35190.30 953.96 o 11 3 0 43122.70 39488.86 1068.76 o 12 3 0 338.49 274.02 174.61 o 13 3 0 1395.69 1678.88 250.32 o 14 3 0 19.46 165.36 210.19 o 15 3 0 1177.36 1490.88 276.52 o 16 3 0 843.98 1748.18 317.81 o 17 3 0 667.22 2551.84 355.45 o 18 3 0 2819.44 3759.03 424.97 o 19 3 0 8815.54 10698.36 646.34 o 20 3 0 1456.44 1735.49 483.76 o 0 4 0 254489.92 305111.47 9431.85 o 1 4 0 941.71 1097.49 86.94 o 2 4 0 11442.42 15935.61 832.95 o 3 4 0 22375.01 23260.52 548.01 o 4 4 0 190.38 419.29 59.29 o 5 4 0 1040.19 1374.28 145.84 o 6 4 0 29747.32 30264.16 795.89 o 7 4 0 11524.79 10742.13 345.01 o 8 4 0 23494.06 23183.49 650.01 o 9 4 0 578.58 495.07 146.42 o 10 4 0 10999.38 9553.79 354.66 o 11 4 0 1094.58 1118.96 166.74 o 12 4 0 2008.60 2513.05 346.82 o 13 4 0 1575.45 2087.15 267.07 o 14 4 0 8875.81 8282.43 452.29 o 15 4 0 17444.11 17547.62 715.50 o 16 4 0 197.06 96.89 247.08 o 17 4 0 1849.54 1749.85 333.07 o 18 4 0 276.15 316.79 305.00 o 19 4 0 187.43 303.61 386.43 o 1 5 0 2229.22 3024.63 142.38 o 2 5 0 25237.15 24327.84 583.28 o 3 5 0 21084.54 23999.22 544.01 o 4 5 0 52689.60 51529.85 1173.39 o 5 5 0 18964.68 18589.85 465.08 o 6 5 0 19641.24 19201.50 540.18 o 7 5 0 157.86 384.19 103.47 o 8 5 0 14024.60 13743.96 433.76 o 9 5 0 8290.12 7494.19 302.45 o 10 5 0 5208.19 5167.07 258.73 o 11 5 0 5473.11 5444.55 279.10 o 12 5 0 8426.27 8218.46 682.04 o 13 5 0 4664.92 4944.51 364.08 o 14 5 0 3404.77 4502.39 566.12 o 15 5 0 3587.94 4582.93 612.41 o 16 5 0 1329.22 2220.19 322.82 o 17 5 0 15.11 452.14 292.26 o 18 5 0 2.35 1232.34 405.68 o 19 5 0 2037.97 2422.72 488.57 o 0 6 0 10249.58 12147.41 454.29 o 1 6 0 120355.26 121368.43 2970.37 o 2 6 0 527.75 869.57 97.50 o 3 6 0 95948.62 95395.86 1958.09 o 4 6 0 26531.92 24870.99 555.44 o 5 6 0 1364.54 2045.43 131.84 o 6 6 0 58841.20 55904.16 1284.68 o 7 6 0 1974.94 1500.78 142.81 o 8 6 0 653.51 591.15 126.59 o 9 6 0 60728.09 57300.98 1483.70 o 10 6 0 2704.67 3045.51 226.05 o 11 6 0 40980.75 40569.01 1108.78 o 12 6 0 4092.86 3693.60 265.63 o 13 6 0 3785.53 3961.43 338.71 o 14 6 0 33469.75 32217.94 1098.28 o 15 6 0 3234.90 3766.50 370.09 o 16 6 0 20227.20 19899.28 940.64 o 17 6 0 1440.04 1025.87 368.12 o 18 6 0 14024.01 13729.55 822.11 o 19 6 0 855.99 1746.46 478.60 o 1 7 0 4685.06 5127.09 213.18 o 2 7 0 5815.86 5679.91 228.68 o 3 7 0 33249.87 32707.91 865.81 o 4 7 0 198979.19 191615.86 3896.72 o 5 7 0 207.79 310.24 73.59 o 6 7 0 78171.78 76366.03 1898.44 o 7 7 0 4474.39 4006.67 171.84 o 8 7 0 16900.50 18308.13 554.45 o 9 7 0 7716.71 7018.81 303.55 o 10 7 0 14110.92 15147.23 505.10 o 11 7 0 58435.76 54108.85 1440.41 o 12 7 0 11582.35 10510.88 424.19 o 13 7 0 10776.16 9824.37 479.27 o 14 7 0 8286.98 7832.55 538.48 o 15 7 0 1971.23 1997.55 395.03 o 16 7 0 1758.82 2395.69 396.27 o 17 7 0 467.85 3155.37 458.37 o 18 7 0 1188.26 1826.92 444.72 o 19 7 0 12034.44 14232.18 889.61 o 0 8 0 55659.44 66393.30 2150.07 o 1 8 0 22992.10 21600.27 550.81 o 2 8 0 40506.63 43251.87 1131.93 o 3 8 0 938.02 944.48 144.84 o 4 8 0 3671.39 3637.09 176.86 o 5 8 0 2467.64 2216.83 253.99 o 6 8 0 21076.21 19152.80 466.90 o 7 8 0 7400.26 6284.98 230.18 o 8 8 0 11798.80 10337.52 373.98 o 9 8 0 12660.22 11172.12 405.39 o 10 8 0 7028.12 7023.72 324.06 o 11 8 0 1585.79 2096.16 257.52 o 12 8 0 2719.30 3090.22 302.20 o 13 8 0 1284.05 1602.81 361.21 o 14 8 0 1252.52 855.58 365.74 o 15 8 0 2018.82 2223.07 379.66 o 16 8 0 2776.85 3169.63 439.78 o 17 8 0 6198.12 6248.58 663.28 o 18 8 0 1896.90 1805.21 423.58 o 19 8 0 3244.82 2737.98 521.11 o 1 9 0 8113.45 8704.06 471.38 o 2 9 0 4305.83 5043.53 456.56 o 3 9 0 23248.90 23494.79 674.63 o 4 9 0 24179.08 22250.04 639.64 o 5 9 0 40921.32 40529.80 979.26 o 6 9 0 8228.47 7203.22 234.91 o 7 9 0 42620.93 42536.10 943.33 o 8 9 0 16410.89 14447.46 592.75 o 9 9 0 5504.66 5935.87 687.47 o 10 9 0 27465.48 23911.20 829.13 o 11 9 0 2667.52 2694.41 286.39 o 12 9 0 7810.36 7399.32 432.28 o 13 9 0 745.81 770.16 239.37 o 14 9 0 4271.33 4846.79 600.26 o 15 9 0 2935.96 3131.89 426.17 o 16 9 0 92.29 565.18 335.00 o 17 9 0 553.59 701.20 359.90 o 18 9 0 4810.75 5562.98 606.14 o 0 10 0 97982.95 117213.48 3744.01 o 1 10 0 11895.80 18014.88 1495.05 o 2 10 0 1969.15 2269.49 177.47 o 3 10 0 9267.58 9923.57 891.87 o 4 10 0 13112.08 13171.89 437.81 o 5 10 0 6719.61 6274.86 279.97 o 6 10 0 20023.88 19480.80 541.39 o 7 10 0 2202.82 2290.51 215.28 o 8 10 0 12944.50 13456.69 479.22 o 9 10 0 7843.86 7882.16 362.05 o 10 10 0 1253.73 1505.65 216.40 o 11 10 0 10767.41 10974.70 510.53 o 12 10 0 2117.75 2280.27 343.07 o 13 10 0 552.53 373.41 229.93 o 14 10 0 13074.05 13638.73 748.87 o 15 10 0 11110.17 10940.69 681.60 o 16 10 0 2363.18 2788.89 446.95 o 17 10 0 1273.69 1132.22 506.88 o 18 10 0 813.74 38.51 482.79 o 1 11 0 4647.50 4871.17 242.12 o 2 11 0 870.89 1008.82 146.67 o 3 11 0 3066.52 3087.29 215.76 o 4 11 0 34640.34 31450.63 888.88 o 5 11 0 4453.19 4621.11 256.11 o 6 11 0 845.11 993.85 186.01 o 7 11 0 2390.43 2376.91 224.80 o 8 11 0 156.82 159.11 161.20 o 9 11 0 179.02 288.69 206.63 o 10 11 0 65.38 35.94 166.63 o 11 11 0 5236.28 6044.72 361.46 o 12 11 0 3547.82 3604.52 315.79 o 13 11 0 370.74 485.66 216.20 o 14 11 0 1511.64 2129.97 324.72 o 15 11 0 170.09 723.92 274.12 o 16 11 0 1.58 30.97 269.40 o 17 11 0 1128.98 1394.67 373.90 o 18 11 0 17.33 -134.41 337.03 o 0 12 0 99729.27 117081.85 5723.49 o 1 12 0 17.37 5436.70 608.16 o 2 12 0 56433.86 57953.14 1532.73 o 3 12 0 4172.70 4933.93 691.69 o 4 12 0 3709.35 3696.43 248.24 o 5 12 0 139.74 161.20 132.77 o 6 12 0 940.43 821.80 199.64 o 7 12 0 9666.43 8739.83 436.71 o 8 12 0 15796.58 14628.70 533.44 o 9 12 0 6364.02 5630.66 335.00 o 10 12 0 15135.40 14273.31 543.35 o 11 12 0 163.30 -49.71 186.00 o 12 12 0 9429.51 9064.75 448.46 o 13 12 0 3600.00 3976.84 343.62 o 14 12 0 1960.31 2259.45 334.47 o 15 12 0 7765.07 7824.45 773.58 o 16 12 0 254.37 783.87 305.76 o 17 12 0 9562.56 10303.57 1164.23 o 1 13 0 14713.56 14570.98 601.97 o 2 13 0 10540.02 10567.51 497.45 o 3 13 0 27674.64 26399.25 791.15 o 4 13 0 5415.08 5106.72 282.56 o 5 13 0 56759.58 53337.08 1437.65 o 6 13 0 2.43 51.54 161.44 o 7 13 0 46360.05 40775.53 1498.80 o 8 13 0 6775.17 6641.28 440.94 o 9 13 0 3024.29 3846.94 346.18 o 10 13 0 40076.11 36382.00 1074.99 o 11 13 0 29.86 38.78 191.20 o 12 13 0 7612.73 8001.65 442.71 o 13 13 0 6950.32 6675.31 427.77 o 14 13 0 6518.36 6502.98 518.10 o 15 13 0 6129.91 6026.19 496.79 o 16 13 0 61.38 608.96 302.07 o 17 13 0 259.61 -123.79 268.53 o 0 14 0 73383.78 76824.16 5250.07 o 1 14 0 9767.31 14398.25 622.30 o 2 14 0 10168.90 11417.44 540.08 o 3 14 0 1710.71 2603.26 766.50 o 4 14 0 1014.69 1473.94 195.04 o 5 14 0 315.02 264.43 140.98 o 6 14 0 2.07 -118.91 137.89 o 7 14 0 22767.75 20766.73 784.82 o 8 14 0 32400.67 28056.71 986.55 o 9 14 0 2453.25 1936.77 323.16 o 10 14 0 5483.49 5648.39 436.15 o 11 14 0 399.77 391.83 213.84 o 12 14 0 205.12 111.04 214.87 o 13 14 0 0.50 445.05 228.82 o 14 14 0 371.48 299.85 351.43 o 15 14 0 8014.18 7257.72 535.48 o 16 14 0 2089.81 2828.42 707.18 o 1 15 0 0.59 194.72 202.81 o 2 15 0 20281.03 20017.77 777.45 o 3 15 0 395.55 682.71 246.26 o 4 15 0 26035.08 25534.77 1005.00 o 5 15 0 65.30 88.02 237.23 o 6 15 0 17644.94 15577.53 653.04 o 7 15 0 2248.54 2174.18 296.69 o 8 15 0 10778.46 10686.91 568.99 o 9 15 0 3923.40 3825.66 389.46 o 10 15 0 41.54 174.29 284.26 o 11 15 0 4897.20 4848.85 437.72 o 12 15 0 452.42 172.04 244.22 o 13 15 0 8040.69 8363.83 531.21 o 14 15 0 811.31 824.17 289.20 o 15 15 0 498.31 1042.01 319.00 o 0 16 0 42137.99 43376.00 2800.33 o 1 16 0 20759.85 20864.26 819.78 o 2 16 0 3414.08 4049.04 431.91 o 3 16 0 16898.27 16693.42 701.34 o 4 16 0 3696.85 4003.54 368.97 o 5 16 0 665.99 387.92 238.48 o 6 16 0 4532.10 4434.27 799.17 o 7 16 0 46.23 -96.28 272.48 o 8 16 0 964.06 780.85 323.93 o 9 16 0 3254.18 3054.57 441.58 o 10 16 0 761.94 541.40 260.38 o 11 16 0 9059.43 8940.09 539.83 o 12 16 0 6943.58 6765.53 505.57 o 13 16 0 1780.57 1839.57 415.15 o 14 16 0 7786.55 7706.95 535.71 o 15 16 0 2285.45 2397.14 475.53 o 1 17 0 1019.27 1475.72 288.75 o 2 17 0 1942.38 2295.41 383.56 o 3 17 0 360.89 536.41 250.63 o 4 17 0 12122.15 11978.59 812.90 o 5 17 0 2743.11 2363.42 329.84 o 6 17 0 10.16 306.62 302.37 o 7 17 0 2778.03 2468.42 417.62 o 8 17 0 37.15 59.29 285.35 o 9 17 0 45.68 25.88 291.14 o 10 17 0 4036.00 3750.35 470.10 o 11 17 0 2070.53 2071.10 407.28 o 12 17 0 236.46 22.48 248.99 o 13 17 0 459.97 381.01 265.48 o 14 17 0 125.65 584.83 284.44 o 0 18 0 1154.25 2514.46 474.12 o 1 18 0 14404.00 12616.10 806.45 o 2 18 0 482.36 511.75 257.05 o 3 18 0 7581.44 7649.65 522.16 o 4 18 0 1245.54 1431.29 329.41 o 5 18 0 170.63 811.09 414.35 o 6 18 0 1165.96 719.89 629.32 o 7 18 0 4073.35 4320.91 612.19 o 8 18 0 3358.47 2977.68 453.54 o 9 18 0 2936.62 2472.79 648.11 o 10 18 0 82.81 -140.27 297.64 o 11 18 0 3761.85 3799.89 495.58 o 12 18 0 910.73 991.98 365.27 o 13 18 0 4182.57 4207.65 715.94 o 1 19 0 27.20 298.23 251.70 o 2 19 0 9235.03 9320.10 543.58 o 3 19 0 998.33 1145.83 296.67 o 4 19 0 30223.06 26938.74 1018.87 o 5 19 0 203.52 136.85 324.90 o 6 19 0 18117.70 16538.54 902.14 o 7 19 0 4758.10 4053.51 506.36 o 8 19 0 11556.98 10791.51 745.57 o 9 19 0 6095.89 4784.24 548.81 o 10 19 0 1416.86 862.17 355.15 o 11 19 0 9525.58 8495.71 1207.67 o 12 19 0 1487.08 1130.46 366.45 o 0 20 0 42.52 226.31 363.47 o 1 20 0 16133.94 17098.35 765.09 o 2 20 0 2643.70 3240.49 391.95 o 3 20 0 6375.62 7229.01 564.83 o 4 20 0 387.52 -114.00 308.50 o 5 20 0 57.55 145.11 326.95 o 6 20 0 8672.01 7290.57 1100.74 o 7 20 0 633.21 378.69 338.75 o 8 20 0 897.53 -182.70 317.73 o 9 20 0 8778.50 7870.89 671.65 o 10 20 0 1967.61 1491.59 392.74 o 11 20 0 5756.35 4784.68 551.79 o 1 21 0 1304.87 2341.15 361.40 o 2 21 0 43.13 406.00 290.53 o 3 21 0 6932.74 6926.43 526.85 o 4 21 0 3590.62 4304.05 527.00 o 5 21 0 7096.22 6967.28 653.53 o 6 21 0 104.81 -460.05 460.05 o 7 21 0 4604.39 4230.76 531.92 o 8 21 0 1417.83 754.06 342.43 o 9 21 0 437.64 391.63 343.51 o 10 21 0 1139.58 1132.22 341.21 o 0 22 0 16238.51 17712.02 1150.92 o 1 22 0 67.78 329.07 295.87 o 2 22 0 13313.41 14544.18 730.90 o 3 22 0 6119.67 5905.09 499.17 o 4 22 0 4207.28 4179.56 538.71 o 5 22 0 1108.03 1164.08 751.25 o 6 22 0 126.81 -295.45 339.08 o 7 22 0 462.82 178.12 408.32 o 8 22 0 2447.15 2011.85 649.04 o 1 23 0 768.22 572.74 317.05 o 2 23 0 2.06 133.59 360.47 o 3 23 0 353.01 724.51 367.68 o 4 23 0 2071.14 1576.53 408.68 o 5 23 0 1081.49 1271.65 415.09 o 6 23 0 607.61 1469.26 434.80 o 0 24 0 501.20 911.67 470.36 o 1 24 0 223.10 1682.37 364.67 o 2 24 0 1606.32 837.15 323.91 o 3 24 0 74.22 1412.78 355.09 o -20 1 1 1099.68 1612.84 400.90 o -19 1 1 10.99 1054.62 337.19 o -18 1 1 2616.73 3337.95 394.77 o -17 1 1 58.00 250.60 249.99 o -16 1 1 2115.76 3000.12 332.08 o -15 1 1 441.02 311.41 214.07 o -14 1 1 3969.86 4442.23 348.63 o -13 1 1 28046.25 26511.82 892.11 o -12 1 1 8730.12 8816.17 409.39 o -11 1 1 9928.23 9757.95 520.00 o -10 1 1 10219.53 9727.72 333.74 o -9 1 1 8076.41 7126.46 263.73 o -8 1 1 19774.68 18216.84 515.09 o -7 1 1 16775.00 15996.03 453.70 o -6 1 1 153014.27 154632.94 3732.28 o -5 1 1 766.37 672.62 73.69 o -4 1 1 2344.68 2751.86 145.66 o -3 1 1 477.42 707.30 56.26 o -2 1 1 537.55 916.28 56.93 o -1 1 1 3856.84 3220.97 125.71 o 0 1 1 439.73 386.05 54.24 o 1 1 1 1723.89 1770.06 149.62 o 2 1 1 137788.41 151663.45 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