#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014948.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014948_Fobs loop_ _publ_author_name 'Besnard, C\'eline' 'Kloc, Christian' 'Siegrist, Theo' 'Svensson, Christer' 'Pluta, Krystian' _publ_section_title ; Azinyl sulfides. LXXXI. 14-Phenyl-7-thiapyrano[2,3-c;6,5-c']diquinoline-14-carbonitrile ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o377 _journal_page_last o379 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 75.724 _cell_angle_beta 84.369 _cell_angle_gamma 84.415 _cell_length_a 7.9135 _cell_length_b 9.3622 _cell_length_c 13.3280 _exptl_crystal_F_000 416.00 _reflns_d_resolution_high 0.9178 _[local]_cod_data_source_file tr1113Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' pluta7' _shelx_refln_list_code 4 _shelx_f_calc_maximum 39.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 247.52 283.57 14.69 o 4 0 0 160.49 153.38 3.27 o 5 0 0 96.20 122.34 2.62 o 6 0 0 84.80 88.17 1.90 o 7 0 0 12.41 15.80 0.66 o 8 0 0 2.81 2.75 0.55 o -8 1 0 7.57 6.46 0.24 o -7 1 0 24.05 25.67 1.44 o -6 1 0 49.98 53.57 6.91 o -5 1 0 93.24 100.35 6.51 o -4 1 0 98.89 106.89 5.78 o -3 1 0 28.70 34.44 0.75 o -2 1 0 123.75 106.20 3.04 o -1 1 0 225.78 192.62 5.79 o 2 1 0 312.98 248.83 7.48 o 4 1 0 157.74 175.80 14.21 o 5 1 0 172.20 172.63 3.69 o 6 1 0 24.29 25.21 2.98 o 7 1 0 0.06 0.03 0.11 o 8 1 0 14.15 15.33 0.56 o -8 2 0 3.68 3.44 0.47 o -7 2 0 46.85 53.77 3.06 o -6 2 0 107.22 107.57 2.32 o -5 2 0 10.26 10.07 0.32 o -3 2 0 207.59 198.90 4.24 o -2 2 0 64.10 68.53 14.92 o 3 2 0 157.30 187.01 13.65 o 4 2 0 501.66 509.17 10.82 o 5 2 0 7.64 9.72 0.62 o 6 2 0 29.33 31.87 0.76 o 7 2 0 3.16 2.73 0.49 o 8 2 0 99.37 96.44 7.01 o -7 3 0 6.61 6.05 0.21 o -6 3 0 6.16 6.29 0.43 o -5 3 0 104.57 105.71 2.27 o -4 3 0 558.82 557.11 11.84 o -3 3 0 73.41 81.61 1.75 o 1 3 0 345.64 276.48 8.31 o 2 3 0 160.72 161.41 5.28 o 3 3 0 43.03 42.70 3.74 o 4 3 0 37.70 30.26 2.24 o 5 3 0 13.21 14.56 1.80 o 6 3 0 43.69 48.76 1.08 o 7 3 0 32.73 31.64 1.33 o 8 3 0 0.39 0.16 0.16 o -7 4 0 3.22 3.52 0.20 o -6 4 0 2.40 3.02 0.17 o -5 4 0 1.37 1.12 0.11 o -4 4 0 4.04 3.41 0.16 o -3 4 0 30.15 29.59 3.06 o -2 4 0 654.82 709.07 21.29 o 0 4 0 1.81 0.75 0.08 o 1 4 0 48.23 39.86 3.35 o 2 4 0 206.38 198.31 21.66 o 3 4 0 61.70 52.43 3.11 o 4 4 0 85.66 84.11 2.47 o 5 4 0 43.31 42.89 4.76 o 6 4 0 279.49 307.96 6.57 o 7 4 0 16.03 16.49 0.43 o 8 4 0 12.42 8.71 0.29 o -7 5 0 35.29 42.42 1.00 o -6 5 0 54.41 53.83 8.68 o -5 5 0 48.57 50.44 1.56 o -4 5 0 20.77 24.15 2.77 o -3 5 0 45.82 43.54 0.95 o -2 5 0 26.82 27.09 1.97 o -1 5 0 22.68 25.58 1.14 o 1 5 0 90.29 82.78 2.02 o 2 5 0 31.60 29.70 2.20 o 3 5 0 0.25 0.16 0.09 o 4 5 0 178.61 236.01 77.29 o 5 5 0 4.22 4.08 0.17 o 6 5 0 109.88 149.27 4.53 o 7 5 0 15.76 17.09 1.68 o -6 6 0 1.24 0.95 0.29 o -5 6 0 75.33 64.66 2.57 o -4 6 0 64.30 71.54 7.84 o -3 6 0 17.70 19.82 2.07 o -2 6 0 5.67 6.08 0.17 o 2 6 0 97.01 99.34 3.00 o 3 6 0 49.82 46.90 1.66 o 4 6 0 191.09 201.36 11.67 o 5 6 0 37.42 39.94 0.90 o 6 6 0 143.45 133.27 10.34 o 7 6 0 5.72 4.31 0.36 o -5 7 0 58.63 71.69 3.31 o -4 7 0 13.75 16.15 2.25 o -3 7 0 195.27 172.78 24.85 o 4 7 0 34.00 35.34 0.80 o 5 7 0 53.78 54.34 4.90 o 6 7 0 13.75 11.19 1.05 o -6 -7 1 162.20 170.08 12.93 o -5 -7 1 150.40 152.74 17.25 o -4 -7 1 7.88 8.16 0.29 o -3 -7 1 8.06 7.41 0.31 o 3 -7 1 70.10 43.22 6.27 o 4 -7 1 0.42 -0.18 0.29 o 5 -7 1 0.11 0.18 0.69 o -6 -6 1 6.16 5.69 0.38 o -5 -6 1 23.46 26.67 2.90 o -4 -6 1 22.32 25.12 2.29 o -3 -6 1 23.21 23.21 1.09 o -2 -6 1 0.09 0.15 0.19 o -1 -6 1 202.81 199.61 6.00 o 0 -6 1 6.03 7.15 0.27 o 1 -6 1 218.44 233.98 11.66 o 2 -6 1 166.43 149.87 5.05 o 3 -6 1 89.26 84.79 5.74 o 4 -6 1 78.10 65.09 1.43 o 5 -6 1 9.62 10.44 0.96 o 6 -6 1 0.07 -0.14 0.24 o -7 -5 1 1.22 0.77 0.34 o -5 -5 1 26.85 28.36 1.40 o -4 -5 1 23.09 19.88 0.47 o -3 -5 1 66.91 64.06 1.47 o -2 -5 1 25.88 22.92 2.01 o -1 -5 1 38.77 30.31 2.29 o 0 -5 1 390.10 407.97 22.92 o 1 -5 1 42.23 46.32 2.27 o 2 -5 1 171.12 137.08 4.50 o 3 -5 1 56.66 51.78 3.09 o 4 -5 1 10.35 8.74 1.42 o 5 -5 1 2.49 2.30 0.18 o 6 -5 1 0.34 0.67 0.21 o -7 -4 1 20.52 22.37 1.18 o -6 -4 1 124.08 115.70 4.97 o -5 -4 1 66.59 61.90 9.84 o -4 -4 1 38.66 38.12 2.12 o -3 -4 1 159.36 148.36 18.95 o -2 -4 1 44.35 52.02 1.12 o -1 -4 1 198.13 175.43 10.28 o 0 -4 1 69.70 66.81 3.14 o 2 -4 1 284.50 286.07 28.38 o 3 -4 1 551.18 631.78 30.72 o 4 -4 1 0.49 0.22 0.11 o 5 -4 1 70.83 70.90 1.54 o 6 -4 1 0.37 0.46 0.15 o 7 -4 1 16.48 15.21 2.96 o -8 -3 1 0.33 0.24 0.17 o -7 -3 1 53.74 59.35 3.03 o -6 -3 1 3.85 3.52 0.26 o -5 -3 1 36.57 32.75 2.03 o -4 -3 1 822.10 923.04 27.72 o -3 -3 1 656.04 752.91 22.61 o -2 -3 1 58.09 61.50 2.02 o -1 -3 1 524.63 448.46 13.47 o 0 -3 1 23.11 23.01 0.80 o 3 -3 1 103.99 118.60 4.00 o 4 -3 1 250.48 242.58 5.17 o 5 -3 1 1.03 0.99 0.12 o 6 -3 1 3.21 3.56 0.32 o 7 -3 1 1.17 1.09 0.23 o -8 -2 1 18.62 18.39 1.05 o -7 -2 1 92.43 100.50 3.96 o -6 -2 1 33.19 31.81 1.20 o -5 -2 1 4.18 3.06 0.23 o -4 -2 1 9.69 11.12 0.57 o -2 -2 1 175.07 191.67 11.00 o 0 -2 1 54.52 51.10 4.51 o 3 -2 1 163.38 143.94 7.01 o 4 -2 1 3.97 2.59 0.11 o 5 -2 1 3.41 4.51 0.26 o 6 -2 1 0.32 0.57 0.12 o 7 -2 1 241.81 264.45 25.69 o 8 -2 1 26.96 28.48 0.66 o -8 -1 1 17.53 17.92 1.11 o -7 -1 1 8.22 7.10 0.86 o -6 -1 1 125.84 123.80 2.66 o -5 -1 1 0.32 0.39 0.11 o -4 -1 1 395.42 416.12 23.35 o -3 -1 1 46.91 53.89 2.91 o -1 -1 1 66.51 66.18 3.31 o 0 -1 1 18.51 15.00 0.33 o 2 -1 1 226.00 204.96 4.36 o 3 -1 1 80.87 81.51 2.57 o 4 -1 1 232.60 256.75 5.47 o 5 -1 1 77.99 92.54 7.82 o 6 -1 1 86.60 99.06 2.13 o 7 -1 1 81.06 86.40 1.87 o 8 -1 1 172.06 184.26 8.00 o -8 0 1 13.14 15.11 0.88 o -7 0 1 1.88 0.94 0.32 o -6 0 1 114.24 121.18 6.00 o -5 0 1 8.14 7.43 0.49 o -4 0 1 211.00 173.07 5.67 o 4 0 1 268.96 283.27 17.02 o 5 0 1 143.37 167.24 27.44 o 6 0 1 6.57 6.80 0.19 o 7 0 1 96.01 98.71 2.20 o 8 0 1 31.90 28.86 1.72 o -8 1 1 6.58 7.75 0.90 o -7 1 1 27.57 25.81 1.38 o -6 1 1 170.09 175.00 5.21 o -5 1 1 98.46 86.97 3.53 o -4 1 1 70.68 91.27 7.59 o -3 1 1 251.90 268.78 5.72 o -1 1 1 42.87 32.91 0.70 o 0 1 1 0.66 1.49 0.52 o 2 1 1 293.45 247.99 7.46 o 3 1 1 130.77 122.54 2.62 o 4 1 1 24.81 32.60 2.79 o 5 1 1 79.64 71.22 1.65 o 6 1 1 36.10 42.99 3.53 o 7 1 1 34.83 35.25 3.40 o 8 1 1 26.05 24.71 0.58 o -8 2 1 19.53 20.44 1.47 o -7 2 1 8.05 8.81 0.25 o -6 2 1 105.25 105.59 5.34 o -5 2 1 52.83 48.50 2.56 o -3 2 1 238.50 268.93 15.80 o 1 2 1 75.93 66.49 2.22 o 3 2 1 39.43 39.16 3.29 o 4 2 1 2.87 1.25 0.08 o 5 2 1 132.66 133.20 13.08 o 6 2 1 202.47 209.83 4.48 o 7 2 1 0.54 1.49 0.12 o 8 2 1 0.27 0.78 0.58 o -7 3 1 0.06 0.25 0.18 o -6 3 1 55.54 65.48 2.01 o -5 3 1 191.62 210.73 50.23 o -4 3 1 41.88 45.68 1.00 o -2 3 1 55.34 60.94 6.25 o 1 3 1 8.84 7.74 0.60 o 2 3 1 4.20 3.26 0.11 o 3 3 1 0.16 0.24 0.06 o 4 3 1 138.78 121.46 11.63 o 5 3 1 157.09 141.45 10.16 o 6 3 1 173.97 179.42 4.44 o 7 3 1 7.92 5.95 0.57 o 8 3 1 43.71 43.55 2.28 o -7 4 1 5.55 3.78 0.18 o -6 4 1 56.07 60.35 1.77 o -5 4 1 80.54 83.90 1.81 o -4 4 1 0.06 0.13 0.09 o -3 4 1 52.62 60.78 4.89 o -2 4 1 370.55 362.37 10.89 o -1 4 1 61.57 57.95 3.18 o 2 4 1 27.24 33.00 2.60 o 3 4 1 671.52 529.65 15.91 o 4 4 1 0.29 0.39 0.10 o 5 4 1 67.70 70.70 1.53 o 6 4 1 26.85 25.89 0.97 o 7 4 1 48.89 47.64 1.41 o 8 4 1 18.60 18.86 0.66 o -7 5 1 12.97 9.53 0.36 o -6 5 1 5.91 7.26 1.04 o -5 5 1 67.35 86.13 2.63 o -4 5 1 1.06 1.03 0.10 o -3 5 1 64.04 68.94 1.95 o -2 5 1 72.80 77.56 5.12 o -1 5 1 23.79 22.35 1.22 o 2 5 1 23.79 30.37 1.47 o 3 5 1 24.11 16.90 2.72 o 4 5 1 78.63 83.96 1.80 o 5 5 1 0.03 0.24 0.12 o 6 5 1 77.58 96.30 2.94 o 7 5 1 23.27 21.97 2.07 o -6 6 1 1.84 2.64 0.37 o -5 6 1 106.88 92.37 2.00 o -4 6 1 14.76 15.04 1.32 o -3 6 1 66.86 62.72 5.51 o -2 6 1 11.75 12.35 2.55 o 3 6 1 131.69 166.47 6.31 o 4 6 1 33.26 39.74 6.94 o 5 6 1 923.84 1335.89 36.15 o 6 6 1 18.76 19.62 1.32 o 7 6 1 6.82 5.47 0.30 o -5 7 1 15.81 17.08 1.58 o -4 7 1 66.47 73.64 3.43 o -3 7 1 0.01 -0.05 0.13 o 4 7 1 35.70 36.68 1.16 o 5 7 1 28.06 26.07 2.53 o 6 7 1 5.28 5.57 0.43 o -5 -7 2 0.40 1.19 0.30 o -4 -7 2 42.96 37.45 0.86 o -3 -7 2 8.89 8.68 0.28 o -2 -7 2 47.42 54.19 3.67 o 1 -7 2 90.69 85.62 2.71 o 2 -7 2 0.63 -0.17 0.33 o 3 -7 2 92.16 93.43 2.56 o 4 -7 2 0.20 1.09 0.21 o 5 -7 2 24.61 24.85 0.64 o -6 -6 2 41.46 40.93 0.96 o -5 -6 2 8.56 9.53 0.30 o -4 -6 2 86.87 80.44 11.34 o -3 -6 2 2.06 2.02 0.14 o -2 -6 2 245.15 272.81 6.00 o -1 -6 2 95.57 95.08 9.82 o 0 -6 2 4.38 5.76 0.31 o 1 -6 2 13.77 12.29 0.31 o 2 -6 2 94.42 92.27 1.99 o 3 -6 2 34.95 37.57 2.03 o 4 -6 2 0.66 -0.09 0.17 o 5 -6 2 8.34 7.23 0.80 o 6 -6 2 42.45 49.28 6.74 o -7 -5 2 26.46 27.83 2.02 o -6 -5 2 58.72 59.02 1.88 o -5 -5 2 102.20 104.95 2.27 o -4 -5 2 74.01 76.61 3.10 o -3 -5 2 1.67 1.23 0.24 o -2 -5 2 19.19 18.58 0.42 o -1 -5 2 200.55 221.61 4.72 o 0 -5 2 24.32 26.25 2.72 o 1 -5 2 0.28 0.03 0.08 o 2 -5 2 27.70 33.52 3.38 o 3 -5 2 14.06 10.16 1.97 o 4 -5 2 0.03 0.13 0.13 o 5 -5 2 77.54 86.12 2.64 o 6 -5 2 177.08 199.11 12.21 o -7 -4 2 4.70 5.95 0.29 o -6 -4 2 58.74 46.31 1.01 o -5 -4 2 10.20 10.36 0.39 o -4 -4 2 2.84 2.76 0.13 o -3 -4 2 62.45 73.76 5.09 o -2 -4 2 13.19 17.18 2.48 o -1 -4 2 683.19 846.53 25.42 o 2 -4 2 371.11 398.31 8.47 o 3 -4 2 46.11 42.15 4.51 o 4 -4 2 0.43 0.77 0.12 o 5 -4 2 13.87 15.15 0.57 o 6 -4 2 221.52 223.73 4.78 o 7 -4 2 13.71 11.83 0.81 o -8 -3 2 0.52 0.36 0.18 o -7 -3 2 0.00 0.07 0.22 o -6 -3 2 53.10 40.18 3.16 o -5 -3 2 168.90 185.70 3.97 o -4 -3 2 20.82 24.03 1.03 o -3 -3 2 389.58 402.39 23.89 o -2 -3 2 134.33 124.82 12.83 o -1 -3 2 423.70 441.01 9.37 o 0 -3 2 205.31 195.01 10.10 o 2 -3 2 144.29 140.43 28.37 o 3 -3 2 96.34 93.49 2.57 o 4 -3 2 52.19 45.90 1.64 o 5 -3 2 194.42 198.97 19.76 o 6 -3 2 0.22 0.40 0.15 o 7 -3 2 3.46 3.12 0.28 o -8 -2 2 3.19 3.17 0.63 o -7 -2 2 0.05 0.05 0.11 o -6 -2 2 53.62 50.40 10.56 o -5 -2 2 5.80 7.01 1.25 o -3 -2 2 10.36 8.81 0.36 o -2 -2 2 15.94 18.86 0.55 o 0 -2 2 416.61 390.89 29.60 o 1 -2 2 491.00 527.45 15.84 o 2 -2 2 112.61 95.73 2.05 o 3 -2 2 73.68 76.62 5.39 o 4 -2 2 235.69 233.09 6.50 o 5 -2 2 22.71 17.79 0.42 o 6 -2 2 59.83 66.42 2.10 o 7 -2 2 18.15 18.18 0.49 o 8 -2 2 77.64 69.83 2.96 o -8 -1 2 1.48 0.64 0.16 o -7 -1 2 29.78 31.43 1.05 o -6 -1 2 195.54 189.79 4.06 o -5 -1 2 314.06 316.39 19.57 o -4 -1 2 13.45 13.84 0.32 o 2 -1 2 118.58 120.45 3.71 o 3 -1 2 90.16 85.53 8.48 o 4 -1 2 4.47 4.34 0.14 o 5 -1 2 4.05 3.55 0.14 o 6 -1 2 16.93 17.76 0.42 o 7 -1 2 99.00 118.75 4.46 o 8 -1 2 186.57 182.58 5.26 o -8 0 2 1.96 1.27 0.61 o -7 0 2 7.72 6.84 0.21 o -6 0 2 1.85 1.97 0.33 o -5 0 2 68.06 69.91 4.34 o -4 0 2 225.03 232.82 17.64 o -3 0 2 14.60 10.63 0.55 o 2 0 2 451.55 392.33 11.79 o 3 0 2 447.73 439.95 9.35 o 4 0 2 23.11 29.79 0.66 o 5 0 2 140.00 132.84 6.50 o 6 0 2 48.85 48.16 1.94 o 7 0 2 10.77 8.88 0.57 o 8 0 2 30.76 29.05 4.03 o -8 1 2 10.41 8.01 1.71 o -7 1 2 16.73 17.59 0.42 o -6 1 2 437.03 500.22 20.94 o -5 1 2 131.11 139.03 7.18 o -4 1 2 292.64 334.28 24.06 o -3 1 2 181.42 194.65 4.15 o -2 1 2 161.61 126.15 12.90 o 1 1 2 60.44 47.04 10.96 o 3 1 2 2.81 3.20 0.27 o 5 1 2 226.44 237.94 5.08 o 6 1 2 108.66 96.60 2.08 o 7 1 2 128.64 126.82 6.00 o 8 1 2 31.11 25.20 0.58 o -8 2 2 14.37 11.35 1.27 o -7 2 2 75.36 74.44 2.07 o -6 2 2 35.71 34.00 3.66 o -5 2 2 276.06 292.43 6.23 o -4 2 2 96.55 103.97 7.33 o -3 2 2 4.54 2.99 0.72 o -2 2 2 107.63 89.15 1.90 o -1 2 2 1.49 1.37 0.07 o 1 2 2 62.68 55.08 7.46 o 2 2 2 55.69 42.82 4.85 o 3 2 2 655.75 734.78 22.07 o 4 2 2 252.68 291.74 12.12 o 5 2 2 193.09 171.45 7.53 o 6 2 2 48.26 58.55 4.45 o 7 2 2 61.41 64.16 1.42 o 8 2 2 0.56 0.17 0.15 o -7 3 2 0.06 -0.12 0.14 o -6 3 2 6.12 7.47 0.22 o -5 3 2 80.90 93.26 10.95 o -4 3 2 190.72 205.14 20.19 o -3 3 2 324.01 366.98 18.71 o -2 3 2 0.04 0.23 0.06 o -1 3 2 344.32 276.46 8.30 o 2 3 2 25.86 29.23 1.69 o 3 3 2 332.30 367.62 11.05 o 4 3 2 101.15 105.99 13.66 o 5 3 2 35.13 37.03 1.56 o 6 3 2 4.55 7.11 0.47 o 7 3 2 51.72 50.11 3.22 o 8 3 2 75.89 64.81 5.51 o -7 4 2 22.79 21.56 0.52 o -6 4 2 48.12 44.03 5.74 o -5 4 2 0.69 0.88 0.12 o -4 4 2 171.62 191.02 5.74 o -3 4 2 17.85 20.35 2.94 o -2 4 2 281.65 261.61 11.83 o 2 4 2 44.12 49.42 1.06 o 3 4 2 14.39 8.19 0.65 o 4 4 2 0.28 0.09 0.07 o 5 4 2 2.20 1.24 0.11 o 6 4 2 0.01 0.07 0.13 o 7 4 2 72.88 63.49 9.58 o 8 4 2 1.07 1.32 0.25 o -7 5 2 27.36 22.80 2.96 o -6 5 2 122.87 126.81 2.73 o -5 5 2 2.21 2.02 0.17 o -4 5 2 63.51 57.38 2.01 o -3 5 2 64.04 55.77 1.20 o -2 5 2 91.26 93.95 9.74 o 2 5 2 2.05 4.08 0.16 o 4 5 2 1.27 1.23 0.09 o 5 5 2 151.38 146.25 10.97 o 6 5 2 3.40 4.80 0.26 o 7 5 2 6.01 6.06 0.25 o -6 6 2 32.80 27.65 0.98 o -5 6 2 13.78 10.88 0.50 o -4 6 2 82.60 83.27 5.04 o -3 6 2 154.49 182.96 6.24 o -2 6 2 67.71 59.50 1.83 o 3 6 2 20.34 22.34 0.50 o 4 6 2 9.48 8.56 0.90 o 5 6 2 297.27 300.20 11.50 o 6 6 2 45.98 34.18 8.43 o 7 6 2 5.99 6.05 0.59 o -5 7 2 0.49 1.49 0.27 o -4 7 2 36.53 36.55 0.83 o -3 7 2 0.91 0.62 0.19 o 4 7 2 1.30 1.36 0.22 o 5 7 2 54.66 59.17 1.32 o 6 7 2 41.25 39.47 1.77 o -4 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314.84 26.01 o 0 3 13 5.80 5.29 0.26 o 1 3 13 27.42 23.87 1.19 o 2 3 13 15.04 16.10 1.35 o 3 3 13 15.72 15.75 0.42 o 4 3 13 33.28 32.20 1.05 o -2 4 13 23.55 23.32 3.41 o -1 4 13 2.50 2.08 0.33 o 0 4 13 26.46 24.64 3.53 o 1 4 13 37.08 37.14 0.87 o 2 4 13 34.23 38.65 1.19 o 3 4 13 36.02 33.65 1.17 o 4 4 13 24.62 24.35 4.52 o -2 5 13 43.33 39.90 5.04 o -1 5 13 12.92 12.90 0.53 o 0 5 13 27.75 30.69 5.64 o 1 5 13 27.69 20.73 6.49 o 2 5 13 46.13 48.81 2.08 o 3 5 13 7.97 9.33 1.40 o -1 6 13 13.27 16.35 0.77 o 0 6 13 8.00 10.19 1.68 o 1 6 13 13.54 15.48 2.01 o 2 6 13 0.30 0.67 0.72 o 3 6 13 31.38 35.44 1.22 o 1 0 14 8.15 8.86 0.31 o -1 1 14 3.90 3.68 0.40 o 0 1 14 28.75 24.43 0.84 o 1 1 14 49.91 50.18 9.81 o 2 1 14 0.16 0.55 0.21 o -1 2 14 118.78 123.67 10.37 o 0 2 14 7.06 4.66 0.74 o 1 2 14 1.63 1.56 0.56 o 2 2 14 13.05 9.86 0.93 o -1 3 14 27.37 26.85 0.96 o 0 3 14 84.30 89.70 17.93 o 1 3 14 1.53 1.76 0.31 o 2 3 14 8.86 7.06 0.39 o 3 3 14 2.33 1.09 0.29 o 0 4 14 61.62 57.96 15.64 o 1 4 14 8.00 5.24 0.30 o 2 4 14 50.01 44.48 3.12 o 1 5 14 35.24 39.76 0.94 o