#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014957.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014957_Fobs loop_ _publ_author_name 'You, Zhong-Lu' _publ_section_title ; Bis[\m-N,N'-bis(3-methylsalicylidene)propane-1,3-diaminato]dicobalt(II) 0.28-hydrate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m359 _journal_page_last m360 _journal_volume 61 _journal_year 2005 _space_group_IT_number 92 _symmetry_space_group_name_Hall 'P 4abw 2nw' _symmetry_space_group_name_H-M 'P 41 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.3810 _cell_length_b 10.3810 _cell_length_c 32.5130 _exptl_crystal_F_000 1528.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file av1247Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P 41 21 2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 260.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, -z+3/4' '-x+1/2, y+1/2, -z+1/4' '-y, -x, -z+1/2' 'y, x, -z' 'y+1/2, -x+1/2, z+3/4' '-y+1/2, x+1/2, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 162.64 242.40 8.12 o 0 2 0 1590.41 1806.38 46.36 o 1 2 0 7809.92 8407.00 148.26 o 2 2 0 2296.14 2324.87 59.82 o 1 3 0 3076.59 3130.79 56.76 o 2 3 0 309.96 348.03 8.26 o 3 3 0 31523.34 33867.91 839.70 o 0 4 0 19.30 14.82 3.59 o 1 4 0 1547.22 1411.40 27.18 o 2 4 0 5.16 18.37 2.71 o 3 4 0 4549.17 4902.63 88.48 o 4 4 0 1862.48 2001.81 54.15 o 1 5 0 7182.71 7444.58 133.14 o 2 5 0 492.74 632.47 14.45 o 3 5 0 1242.11 1044.12 21.68 o 4 5 0 5409.71 5349.94 101.68 o 5 5 0 667.71 642.89 29.05 o 0 6 0 273.71 212.49 14.68 o 1 6 0 1.93 10.72 3.38 o 2 6 0 6937.05 7078.20 127.48 o 3 6 0 2095.62 2015.31 41.25 o 4 6 0 950.20 864.24 25.70 o 5 6 0 3088.34 2974.12 71.07 o 6 6 0 920.93 919.28 39.23 o 1 7 0 879.74 848.73 19.35 o 2 7 0 487.51 453.09 13.72 o 3 7 0 31.48 48.56 6.75 o 4 7 0 3.69 1.39 6.05 o 5 7 0 348.74 335.11 16.23 o 6 7 0 314.96 297.58 15.92 o 7 7 0 2694.41 2765.41 97.60 o 0 8 0 4172.43 3998.98 106.11 o 1 8 0 1011.32 1006.53 24.01 o 2 8 0 193.33 216.88 10.70 o 3 8 0 1793.23 1716.36 44.62 o 4 8 0 801.40 753.04 28.36 o 5 8 0 179.94 199.83 13.54 o 6 8 0 266.75 275.58 16.77 o 7 8 0 136.65 141.07 13.03 o 8 8 0 19.12 4.40 12.24 o 1 9 0 825.76 800.88 24.45 o 2 9 0 103.24 81.84 9.21 o 3 9 0 511.41 515.67 20.70 o 4 9 0 375.83 372.05 18.23 o 5 9 0 383.30 346.84 18.22 o 6 9 0 379.42 423.78 20.65 o 7 9 0 1470.48 1488.26 43.37 o 8 9 0 993.98 926.32 32.25 o 9 9 0 68.74 104.17 23.92 o 0 10 0 206.45 216.70 19.39 o 1 10 0 31.79 25.17 8.12 o 2 10 0 32.01 54.26 9.96 o 3 10 0 28.44 9.32 7.80 o 4 10 0 115.98 128.38 12.43 o 5 10 0 570.16 598.85 25.11 o 6 10 0 536.12 544.79 24.29 o 7 10 0 53.41 83.26 12.27 o 8 10 0 31.01 47.39 11.53 o 9 10 0 80.55 58.19 17.51 o 1 11 0 0.90 -4.02 9.34 o 2 11 0 69.76 85.58 12.03 o 3 11 0 202.74 194.23 18.68 o 4 11 0 198.56 211.96 18.48 o 5 11 0 11.17 22.65 13.34 o 6 11 0 710.00 776.91 30.12 o 7 11 0 58.56 84.76 13.86 o 0 12 0 12.12 51.37 33.16 o 1 12 0 393.73 354.90 33.84 o 2 12 0 30.47 23.61 12.92 o 3 12 0 55.47 52.09 12.51 o 4 12 0 247.75 277.95 21.12 o 5 12 0 114.49 115.03 17.47 o 6 12 0 838.79 929.89 47.94 o 1 13 0 102.46 152.76 35.90 o 2 13 0 67.55 83.53 21.43 o 3 13 0 67.72 78.95 25.72 o 0 1 1 36516.82 39194.12 686.73 o 1 1 1 19021.89 20612.14 443.12 o -1 2 1 4446.71 4730.12 85.35 o 0 2 1 187.21 216.81 5.24 o 1 2 1 4030.52 4345.52 83.55 o 2 2 1 3379.27 3427.20 61.95 o -2 3 1 4037.33 4151.03 76.42 o -1 3 1 8247.67 8437.07 149.79 o 0 3 1 46.74 49.05 2.75 o 1 3 1 8214.85 8449.45 149.08 o 2 3 1 3838.43 3912.84 71.86 o 3 3 1 7850.16 8072.31 143.37 o -3 4 1 11817.59 12623.03 224.57 o -2 4 1 4639.08 4625.09 86.76 o -1 4 1 1813.87 1913.78 35.02 o 0 4 1 39.17 34.22 2.92 o 1 4 1 1683.14 1779.16 34.52 o 2 4 1 4572.94 4542.98 82.49 o 3 4 1 12067.82 12804.08 246.78 o 4 4 1 8413.74 9128.35 162.68 o -4 5 1 3763.37 3700.13 71.52 o -3 5 1 646.66 645.79 16.05 o -2 5 1 7217.55 7193.76 128.13 o -1 5 1 181.83 163.42 6.68 o 0 5 1 9.60 30.74 4.45 o 1 5 1 168.26 141.96 6.50 o 2 5 1 7156.44 7118.12 128.30 o 3 5 1 682.79 685.99 15.11 o 4 5 1 3859.49 3669.87 71.27 o 5 5 1 1486.15 1333.87 32.79 o -5 6 1 340.00 326.25 15.47 o -4 6 1 1917.91 1711.74 42.06 o -3 6 1 337.03 322.43 10.82 o -2 6 1 45.28 58.94 4.72 o -1 6 1 327.78 292.28 10.69 o 0 6 1 28.78 54.96 4.50 o 1 6 1 401.56 398.51 10.55 o 2 6 1 65.95 69.96 5.04 o 3 6 1 338.51 317.88 11.61 o 4 6 1 2005.69 1852.46 45.13 o 5 6 1 388.85 415.56 16.55 o 6 6 1 1102.79 1006.26 29.73 o -6 7 1 676.10 620.97 23.06 o -5 7 1 657.36 643.29 22.33 o -4 7 1 122.88 120.83 9.91 o -3 7 1 990.63 980.72 22.54 o -2 7 1 3255.95 3137.96 64.72 o -1 7 1 655.44 648.07 16.39 o 0 7 1 6.47 0.64 3.87 o 1 7 1 721.80 716.95 16.72 o 2 7 1 3255.19 3092.82 64.67 o 3 7 1 905.34 884.93 26.92 o 4 7 1 141.07 136.60 10.25 o 5 7 1 643.64 639.66 22.31 o 6 7 1 660.82 641.26 23.25 o 7 7 1 230.58 247.78 15.29 o -7 8 1 925.93 895.81 29.84 o -6 8 1 212.43 253.05 15.41 o -5 8 1 2371.73 2261.17 57.90 o -4 8 1 262.04 270.02 16.34 o -3 8 1 21.12 17.65 6.86 o -2 8 1 42.24 56.83 6.26 o -1 8 1 988.71 987.66 23.57 o 0 8 1 65.58 80.91 6.59 o 1 8 1 978.68 951.64 23.21 o 2 8 1 34.76 37.35 7.22 o 3 8 1 12.85 5.21 7.52 o 4 8 1 308.17 325.19 15.99 o 5 8 1 2366.08 2301.12 58.10 o 6 8 1 270.42 263.03 15.65 o 7 8 1 950.15 901.97 32.53 o 8 8 1 137.42 158.89 14.18 o -8 9 1 394.30 426.99 22.23 o -7 9 1 360.22 386.74 20.45 o -6 9 1 473.68 474.76 21.76 o -5 9 1 147.30 134.87 12.10 o -4 9 1 106.21 93.32 10.70 o -3 9 1 693.44 693.47 23.72 o -2 9 1 177.81 156.17 11.32 o -1 9 1 67.73 72.10 7.59 o 0 9 1 1.94 -2.78 5.30 o 1 9 1 39.75 39.46 7.42 o 2 9 1 124.82 117.02 12.59 o 3 9 1 652.40 639.59 23.63 o 4 9 1 132.95 147.98 12.01 o 5 9 1 101.16 104.87 12.53 o 6 9 1 442.56 441.13 21.40 o 7 9 1 353.34 389.69 21.41 o 8 9 1 369.56 391.09 23.70 o 9 9 1 220.63 218.11 17.22 o -9 10 1 298.01 404.88 40.73 o -8 10 1 427.38 448.02 31.73 o -7 10 1 137.87 140.24 14.33 o -6 10 1 548.28 558.34 24.37 o -5 10 1 425.74 467.91 21.62 o -4 10 1 413.25 408.10 19.65 o -3 10 1 64.47 74.09 9.83 o -2 10 1 134.81 128.44 12.18 o -1 10 1 34.31 35.93 8.86 o 0 10 1 277.48 261.57 14.17 o 1 10 1 46.55 24.75 8.75 o 2 10 1 129.05 113.15 11.85 o 3 10 1 82.12 83.85 10.69 o 4 10 1 405.18 357.10 19.01 o 5 10 1 391.38 409.87 20.85 o 6 10 1 479.91 492.75 23.85 o 7 10 1 136.59 145.62 14.73 o 8 10 1 378.22 429.65 23.25 o 9 10 1 286.13 303.96 29.71 o -7 11 1 253.19 294.90 21.01 o -6 11 1 121.48 135.17 14.92 o -5 11 1 31.41 36.40 10.70 o -4 11 1 678.42 685.53 29.06 o -3 11 1 275.12 251.13 17.17 o -2 11 1 184.46 208.84 15.70 o -1 11 1 71.70 69.44 12.39 o 0 11 1 333.91 303.35 20.16 o 1 11 1 69.76 66.78 13.81 o 2 11 1 178.96 185.39 15.38 o 3 11 1 268.17 253.00 17.80 o 4 11 1 708.06 701.91 29.25 o 5 11 1 42.26 32.09 10.16 o 6 11 1 108.22 138.33 14.13 o 7 11 1 279.16 309.34 20.02 o -6 12 1 36.94 88.57 20.16 o -5 12 1 541.05 639.36 44.46 o -4 12 1 3.77 16.13 14.23 o -3 12 1 89.12 123.21 17.76 o -2 12 1 63.15 47.48 23.50 o -1 12 1 73.40 50.98 19.04 o 0 12 1 340.41 426.68 37.69 o 1 12 1 77.63 97.50 18.20 o 2 12 1 68.32 82.57 14.08 o 3 12 1 63.07 51.32 11.34 o 4 12 1 4.85 -0.54 10.49 o 5 12 1 516.46 538.27 29.65 o 6 12 1 45.64 83.05 16.16 o -3 13 1 134.04 145.68 29.42 o -2 13 1 65.22 62.72 41.03 o -1 13 1 287.05 353.10 44.37 o 0 13 1 79.16 72.67 25.43 o 1 13 1 273.95 261.03 39.88 o 2 13 1 64.13 105.24 23.17 o 3 13 1 162.37 165.99 30.42 o 0 1 2 8897.65 10225.15 187.91 o 1 1 2 43075.68 46905.11 1005.62 o -1 2 2 1211.25 1257.49 21.70 o 0 2 2 1436.21 1514.36 27.79 o 1 2 2 969.05 1010.56 21.84 o 2 2 2 14457.48 15091.16 277.50 o -2 3 2 9815.38 9893.87 179.31 o -1 3 2 2725.87 2876.09 54.87 o 0 3 2 3715.78 3808.86 68.38 o 1 3 2 2707.72 2870.07 51.97 o 2 3 2 9244.19 9400.26 169.67 o 3 3 2 3582.63 3968.59 71.83 o -3 4 2 609.86 607.37 15.28 o -2 4 2 8842.20 9192.17 172.31 o -1 4 2 734.67 764.33 16.04 o 0 4 2 3109.87 3173.28 57.89 o 1 4 2 722.38 751.18 15.90 o 2 4 2 8984.49 9360.29 158.32 o 3 4 2 700.16 677.06 15.13 o 4 4 2 16463.32 17630.48 311.28 o -4 5 2 1374.34 1364.30 29.78 o -3 5 2 3838.97 3811.96 73.44 o -2 5 2 1396.70 1415.70 28.91 o -1 5 2 849.30 1033.85 20.37 o 0 5 2 66.24 125.27 5.46 o 1 5 2 739.74 884.95 19.55 o 2 5 2 1497.49 1529.09 30.27 o 3 5 2 3852.84 3797.84 69.82 o 4 5 2 1468.46 1451.98 29.93 o 5 5 2 568.13 617.90 18.63 o -5 6 2 1626.22 1502.33 39.54 o -4 6 2 41.47 69.17 6.86 o -3 6 2 571.65 601.38 15.99 o -2 6 2 2614.80 2458.63 46.24 o -1 6 2 1408.19 1366.45 27.27 o 0 6 2 356.66 325.33 9.74 o 1 6 2 1336.77 1293.69 26.89 o 2 6 2 2517.51 2358.99 47.77 o 3 6 2 633.51 623.54 15.68 o 4 6 2 65.10 80.47 8.12 o 5 6 2 1591.25 1491.50 39.55 o 6 6 2 148.19 154.84 11.39 o -6 7 2 101.18 117.52 10.76 o -5 7 2 1166.68 1128.54 33.06 o -4 7 2 2365.10 2197.47 53.53 o -3 7 2 2108.56 2001.80 42.89 o -2 7 2 522.10 534.22 15.00 o -1 7 2 3105.80 3098.70 57.92 o 0 7 2 736.86 717.21 17.23 o 1 7 2 3033.02 2999.98 57.31 o 2 7 2 536.77 539.53 15.73 o 3 7 2 2231.42 2171.09 51.88 o 4 7 2 2174.41 2076.17 53.34 o 5 7 2 1282.18 1201.05 33.44 o 6 7 2 95.92 90.41 10.06 o 7 7 2 31.60 26.05 8.12 o -7 8 2 292.99 326.06 18.16 o -6 8 2 2335.92 2203.03 56.70 o -5 8 2 56.39 77.21 9.68 o -4 8 2 558.38 547.63 20.45 o -3 8 2 239.58 215.40 12.61 o -2 8 2 1171.13 1150.24 26.10 o -1 8 2 1783.33 1697.78 36.34 o 0 8 2 442.85 458.45 14.44 o 1 8 2 1760.80 1656.34 36.22 o 2 8 2 1081.21 1024.88 30.50 o 3 8 2 180.91 164.42 11.84 o 4 8 2 529.35 480.40 20.05 o 5 8 2 66.82 81.01 9.96 o 6 8 2 2308.52 2158.89 56.50 o 7 8 2 292.49 308.40 17.83 o 8 8 2 779.30 837.27 40.11 o -8 9 2 112.15 99.73 12.67 o -7 9 2 93.42 101.46 14.10 o -6 9 2 391.68 400.10 20.26 o -5 9 2 293.69 287.60 16.94 o -4 9 2 485.14 557.81 21.99 o -3 9 2 1358.60 1340.17 35.26 o -2 9 2 1204.50 1116.82 30.73 o -1 9 2 341.09 369.87 14.47 o 0 9 2 106.94 107.30 8.61 o 1 9 2 382.47 393.36 18.19 o 2 9 2 1291.38 1221.34 38.22 o 3 9 2 1136.63 1074.51 33.98 o 4 9 2 499.80 527.88 21.90 o 5 9 2 367.50 388.09 18.99 o 6 9 2 418.23 415.25 20.63 o 7 9 2 86.07 85.58 12.04 o 8 9 2 120.81 118.80 13.43 o 9 9 2 268.06 311.40 19.89 o -9 10 2 297.99 257.30 31.07 o -8 10 2 52.14 66.53 13.22 o -7 10 2 844.74 919.75 31.95 o -6 10 2 516.00 505.80 23.48 o -5 10 2 153.98 160.13 13.89 o -4 10 2 375.15 354.08 19.37 o -3 10 2 300.10 304.22 16.63 o -2 10 2 1142.11 1067.10 42.04 o -1 10 2 35.88 47.98 8.90 o 0 10 2 662.30 711.59 24.40 o 1 10 2 39.54 47.99 9.60 o 2 10 2 1306.94 1127.59 35.55 o 3 10 2 320.08 310.98 17.12 o 4 10 2 384.97 377.60 19.73 o 5 10 2 193.76 198.69 15.21 o 6 10 2 511.26 507.52 23.67 o 7 10 2 808.16 832.02 33.46 o 8 10 2 36.76 48.91 11.68 o 9 10 2 294.47 322.75 29.45 o -7 11 2 31.51 41.06 11.89 o -6 11 2 56.48 74.83 12.76 o -5 11 2 590.37 604.17 27.75 o -4 11 2 24.71 42.17 11.27 o -3 11 2 242.32 248.33 19.04 o -2 11 2 115.57 136.93 14.58 o -1 11 2 36.89 29.10 12.57 o 0 11 2 95.73 106.77 13.74 o 1 11 2 38.07 27.05 10.79 o 2 11 2 110.19 124.45 13.50 o 3 11 2 254.80 226.61 17.06 o 4 11 2 10.56 27.81 10.30 o 5 11 2 588.59 583.75 25.81 o 6 11 2 51.55 79.25 12.15 o 7 11 2 21.36 44.46 11.54 o -6 12 2 113.53 115.42 22.82 o -5 12 2 6.04 11.98 12.31 o -4 12 2 46.85 38.26 12.59 o -3 12 2 126.37 118.02 19.76 o -2 12 2 47.29 46.95 18.82 o -1 12 2 110.63 124.46 24.60 o 0 12 2 665.59 746.84 49.73 o 1 12 2 100.85 160.03 21.12 o 2 12 2 42.37 25.23 11.57 o 3 12 2 113.38 154.13 15.21 o 4 12 2 34.82 55.31 11.76 o 5 12 2 4.56 22.44 11.34 o 6 12 2 100.62 115.62 18.55 o -3 13 2 73.83 38.65 30.11 o -2 13 2 101.04 83.94 20.92 o -1 13 2 213.52 262.48 37.74 o 0 13 2 166.88 238.20 42.46 o 1 13 2 206.58 195.45 27.68 o 2 13 2 113.29 142.59 20.86 o 3 13 2 63.52 51.08 16.14 o 0 1 3 42709.64 46916.01 857.45 o 1 1 3 27.47 24.27 2.06 o -1 2 3 4741.73 4982.63 91.85 o 0 2 3 8507.49 9338.49 164.99 o 1 2 3 4618.58 4878.48 91.28 o 2 2 3 3102.83 3235.65 64.13 o -2 3 3 4870.23 5501.45 104.67 o -1 3 3 6067.27 6314.08 110.59 o 0 3 3 1017.77 961.90 18.85 o 1 3 3 5810.59 6066.69 109.65 o 2 3 3 5077.15 5702.48 100.21 o 3 3 3 140.33 186.11 6.23 o -3 4 3 4116.20 3992.15 79.02 o -2 4 3 1195.94 1169.94 26.82 o -1 4 3 9433.04 9937.58 171.73 o 0 4 3 61.71 51.18 3.34 o 1 4 3 8899.37 9371.81 170.62 o 2 4 3 1460.20 1467.37 26.24 o 3 4 3 4026.81 3852.95 74.45 o 4 4 3 2305.55 2431.09 48.02 o -4 5 3 104.14 115.38 7.03 o -3 5 3 1453.09 1350.88 28.45 o -2 5 3 135.23 135.60 5.92 o -1 5 3 1721.96 1610.06 31.38 o 0 5 3 5645.82 5834.66 105.07 o 1 5 3 1737.77 1600.54 31.26 o 2 5 3 146.51 142.08 5.75 o 3 5 3 1417.93 1299.55 26.48 o 4 5 3 114.20 123.26 7.05 o 5 5 3 9651.84 9221.02 191.65 o -5 6 3 349.96 359.58 16.04 o -4 6 3 115.75 116.78 7.56 o -3 6 3 5784.76 5738.07 103.08 o -2 6 3 1451.46 1442.92 28.04 o -1 6 3 3554.43 3541.44 68.55 o 0 6 3 525.79 400.14 11.05 o 1 6 3 3881.32 3948.45 69.88 o 2 6 3 1458.73 1418.29 31.87 o 3 6 3 5710.37 5604.09 113.99 o 4 6 3 115.16 124.05 9.49 o 5 6 3 394.28 395.46 22.14 o 6 6 3 74.33 84.27 9.24 o -6 7 3 1313.12 1266.05 36.68 o -5 7 3 1041.49 1048.36 29.06 o -4 7 3 1161.95 1068.30 31.44 o -3 7 3 97.48 116.98 8.16 o -2 7 3 1464.78 1450.21 30.08 o -1 7 3 2324.93 2327.78 43.01 o 0 7 3 1803.62 1875.73 37.14 o 1 7 3 2041.31 2013.41 44.02 o 2 7 3 1491.65 1426.30 32.72 o 3 7 3 79.60 87.85 8.76 o 4 7 3 1254.74 1177.37 32.06 o 5 7 3 853.13 836.10 27.76 o 6 7 3 1333.05 1347.30 37.24 o 7 7 3 1.89 9.08 7.67 o -7 8 3 368.02 370.68 19.43 o -6 8 3 163.28 206.34 14.30 o -5 8 3 50.88 42.39 8.62 o -4 8 3 267.75 288.74 14.85 o -3 8 3 1280.36 1211.24 32.85 o -2 8 3 2460.78 2434.31 49.57 o -1 8 3 288.75 274.02 11.07 o 0 8 3 106.84 109.99 7.65 o 1 8 3 243.65 226.35 10.37 o 2 8 3 2388.63 2340.46 58.41 o 3 8 3 1161.71 1102.57 32.59 o 4 8 3 230.48 212.12 13.80 o 5 8 3 43.36 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8 715.40 743.58 24.77 o 5 7 8 1590.00 1574.24 42.72 o 6 7 8 33.04 31.04 8.07 o 7 7 8 773.92 760.13 26.65 o -7 8 8 4.53 11.52 9.18 o -6 8 8 89.31 104.99 12.23 o -5 8 8 559.58 565.33 23.71 o -4 8 8 1762.34 1677.44 47.76 o -3 8 8 1088.92 1054.57 27.65 o -2 8 8 951.45 902.76 22.41 o -1 8 8 282.15 282.32 20.47 o 0 8 8 1287.73 1325.17 29.94 o 1 8 8 317.41 314.71 14.60 o 2 8 8 851.21 837.44 28.47 o 3 8 8 1206.62 1181.49 32.80 o 4 8 8 1796.15 1690.95 45.22 o 5 8 8 539.88 528.13 22.50 o 6 8 8 98.32 102.75 11.28 o 7 8 8 7.34 13.66 8.62 o 8 8 8 46.92 45.84 11.38 o -8 9 8 133.42 161.78 17.82 o -7 9 8 410.93 431.96 25.92 o -6 9 8 348.29 386.96 23.50 o -5 9 8 347.85 341.86 21.84 o -4 9 8 178.03 195.18 15.88 o -3 9 8 42.74 15.43 8.94 o -2 9 8 38.93 50.69 8.17 o -1 9 8 2084.18 1997.18 48.24 o 0 9 8 2198.54 2053.54 52.29 o 1 9 8 2121.63 2026.65 55.30 o 2 9 8 28.51 39.06 9.08 o 3 9 8 38.90 41.16 8.94 o 4 9 8 159.09 159.68 13.06 o 5 9 8 378.61 400.30 19.72 o 6 9 8 366.65 408.26 20.77 o 7 9 8 429.75 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124.81 23.72 o -3 12 9 38.71 48.50 20.13 o -2 12 9 90.88 86.23 21.57 o -1 12 9 12.27 -2.41 15.22 o 0 12 9 117.20 91.98 18.37 o 1 12 9 16.57 17.70 11.35 o 2 12 9 122.97 109.74 17.85 o 3 12 9 45.25 61.56 12.70 o 4 12 9 114.17 114.98 15.06 o 5 12 9 3.63 15.83 10.96 o -1 13 9 3.81 35.83 34.07 o 0 13 9 256.26 256.06 30.69 o 1 13 9 4.64 27.86 17.78 o 2 13 9 148.71 135.29 21.05 o 0 1 10 31.86 61.95 4.25 o 1 1 10 25936.40 27398.48 480.82 o -1 2 10 5810.13 6044.02 101.48 o 0 2 10 391.95 375.56 9.46 o 1 2 10 5305.40 5568.73 106.71 o 2 2 10 8434.78 8635.22 153.37 o -2 3 10 2257.88 2079.84 38.59 o -1 3 10 2968.02 3118.26 54.58 o 0 3 10 21860.38 23116.23 406.32 o 1 3 10 2979.13 3077.35 59.37 o 2 3 10 2173.01 1977.00 39.52 o 3 3 10 197.57 183.79 6.94 o -3 4 10 190.77 230.22 8.14 o -2 4 10 4969.46 5067.69 91.51 o -1 4 10 3436.68 3658.99 67.58 o 0 4 10 329.89 426.28 11.35 o 1 4 10 3489.36 3745.21 67.92 o 2 4 10 4858.96 4976.34 90.37 o 3 4 10 214.70 226.41 8.40 o 4 4 10 1552.30 1513.84 33.88 o -4 5 10 459.47 448.37 13.80 o -3 5 10 2154.03 2200.34 43.47 o -2 5 10 562.67 535.73 13.45 o -1 5 10 3243.24 3192.62 59.66 o 0 5 10 6025.27 5921.50 106.95 o 1 5 10 3271.28 3224.22 59.62 o 2 5 10 543.75 510.05 12.52 o 3 5 10 2031.99 2031.36 45.13 o 4 5 10 404.40 378.52 13.41 o 5 5 10 1461.74 1336.16 31.58 o -5 6 10 1536.85 1534.90 33.81 o -4 6 10 322.69 331.76 12.88 o -3 6 10 1124.63 1068.67 24.62 o -2 6 10 3932.79 3831.12 69.83 o -1 6 10 2309.67 2321.87 45.59 o 0 6 10 1493.11 1438.16 29.39 o 1 6 10 2391.85 2420.78 47.81 o 2 6 10 3917.94 3626.72 113.66 o 3 6 10 1139.60 1048.73 27.51 o 4 6 10 351.69 357.00 15.05 o 5 6 10 1255.21 1219.72 34.13 o 6 6 10 1290.04 1286.58 33.67 o -6 7 10 859.51 867.64 29.14 o -5 7 10 11.45 9.34 6.86 o -4 7 10 2027.60 1978.19 45.95 o -3 7 10 237.03 233.12 14.36 o -2 7 10 2028.06 1935.52 39.61 o -1 7 10 2010.92 1992.88 40.60 o 0 7 10 533.27 479.66 15.20 o 1 7 10 2176.41 2110.18 50.77 o 2 7 10 2145.79 2062.84 53.97 o 3 7 10 288.14 269.85 12.67 o 4 7 10 1932.58 1838.21 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