#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014965.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014965_Fobs loop_ _publ_author_name 'Sharma, Raj Pal' 'Bala, Ritu' 'Sharma, Rajni' 'Bond, Andrew D.' _publ_section_title ; Second-sphere coordination in anion binding: sodium hexaamminecobalt(III) tetrakis(4-fluorobenzoate) monohydrate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m356 _journal_page_last m358 _journal_volume 61 _journal_year 2005 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.349 _cell_angle_gamma 90.000 _cell_length_a 16.1930 _cell_length_b 33.4500 _cell_length_c 6.5169 _exptl_crystal_F_000 1568.00 _reflns_d_resolution_high 0.7563 _[local]_cod_data_source_file bg1006Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rs0401 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 485.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 235973.73 244481.84 2791.04 o 6 0 0 5001.04 5214.11 57.26 o 8 0 0 15787.54 14984.33 174.79 o 10 0 0 7593.39 7379.48 89.30 o 12 0 0 5677.85 5485.06 77.13 o 14 0 0 132.64 85.89 12.84 o 16 0 0 6631.21 6517.89 236.40 o 3 1 0 34.70 25.68 1.65 o 5 1 0 1044.03 1099.40 10.56 o 7 1 0 4294.02 4448.63 36.63 o 9 1 0 613.30 581.73 8.74 o 11 1 0 330.40 320.07 8.62 o 13 1 0 73.62 75.82 7.99 o 15 1 0 16.15 10.13 11.19 o 17 1 0 2.17 -4.55 14.18 o 4 2 0 1265.98 1269.84 12.32 o 6 2 0 523.03 551.99 8.24 o 8 2 0 12288.29 12963.40 102.56 o 10 2 0 7320.46 7330.29 62.85 o 12 2 0 1599.67 1718.21 22.59 o 14 2 0 301.48 278.06 11.91 o 16 2 0 580.34 634.73 20.17 o 3 3 0 1020.32 1010.64 10.13 o 5 3 0 1653.02 1572.15 14.93 o 7 3 0 2326.44 2413.79 22.63 o 9 3 0 1170.90 1226.79 13.31 o 11 3 0 144.96 161.05 7.17 o 13 3 0 627.63 688.42 19.26 o 15 3 0 13.51 8.99 10.14 o 17 3 0 82.10 78.59 24.35 o 2 4 0 18824.80 18935.25 176.46 o 4 4 0 13402.72 13873.60 120.99 o 6 4 0 74.18 84.53 6.31 o 8 4 0 20897.43 20713.21 161.80 o 10 4 0 1845.44 1737.01 23.19 o 12 4 0 6327.85 6433.66 62.98 o 14 4 0 2333.21 2391.86 28.88 o 16 4 0 1492.82 1494.64 29.02 o 3 5 0 1771.12 1901.39 19.54 o 5 5 0 243.53 249.30 5.54 o 7 5 0 12520.45 13520.34 123.44 o 9 5 0 625.69 652.02 9.29 o 11 5 0 2341.42 2466.48 27.42 o 13 5 0 927.38 983.74 16.58 o 15 5 0 1169.78 1215.79 22.15 o 17 5 0 1151.27 1126.52 31.48 o 0 6 0 3357.24 2627.07 31.01 o 2 6 0 6075.59 6101.99 80.37 o 4 6 0 21276.96 20313.32 182.56 o 6 6 0 509.69 438.84 7.34 o 8 6 0 7677.46 8783.59 74.51 o 10 6 0 5433.23 5507.14 48.24 o 12 6 0 1463.01 1366.79 18.84 o 14 6 0 7107.71 7559.17 81.77 o 16 6 0 3003.18 3140.50 46.05 o 1 7 0 2.95 -1.50 1.50 o 3 7 0 161.24 156.90 3.77 o 5 7 0 29.66 36.25 2.84 o 7 7 0 263.60 287.13 6.99 o 9 7 0 0.25 -0.07 4.13 o 11 7 0 375.77 413.31 11.04 o 13 7 0 2.67 2.13 7.54 o 15 7 0 4.50 9.50 10.43 o 17 7 0 2.25 -4.99 16.83 o 0 8 0 751.85 915.48 14.49 o 2 8 0 19504.45 19595.83 170.01 o 4 8 0 183.46 228.94 5.19 o 6 8 0 3257.55 3252.99 30.68 o 8 8 0 9646.43 9934.90 88.66 o 10 8 0 543.04 469.61 10.63 o 12 8 0 4222.18 4178.22 43.12 o 14 8 0 655.01 636.39 16.69 o 16 8 0 1060.52 1071.71 26.56 o 1 9 0 2699.45 2564.82 23.55 o 3 9 0 632.40 654.89 8.08 o 5 9 0 1772.23 1694.94 17.34 o 7 9 0 966.34 982.22 12.35 o 9 9 0 278.48 268.90 7.37 o 11 9 0 6.06 6.50 6.15 o 13 9 0 26.11 26.94 7.89 o 15 9 0 614.30 583.97 17.18 o 17 9 0 398.27 367.66 21.30 o 0 10 0 1378.13 1618.64 23.59 o 2 10 0 25095.52 25474.38 220.58 o 4 10 0 12393.42 12744.13 171.60 o 6 10 0 17.11 13.24 3.44 o 8 10 0 1903.39 1981.49 21.09 o 10 10 0 318.42 248.01 7.94 o 12 10 0 3997.00 4146.24 43.30 o 14 10 0 428.34 434.43 13.61 o 16 10 0 1446.01 1549.71 35.02 o 1 11 0 2813.64 2866.69 28.09 o 3 11 0 3151.87 3096.46 28.86 o 5 11 0 690.12 793.12 10.44 o 7 11 0 17371.73 18877.88 213.52 o 9 11 0 585.80 651.67 11.91 o 11 11 0 1562.99 1595.12 22.24 o 13 11 0 206.30 195.50 10.49 o 15 11 0 138.37 114.70 11.83 o 17 11 0 7.84 6.10 17.41 o 0 12 0 34914.98 34865.01 398.99 o 2 12 0 32866.38 33623.96 290.33 o 4 12 0 249.29 135.91 7.90 o 6 12 0 92.34 33.47 3.94 o 8 12 0 3999.92 3478.89 33.85 o 10 12 0 2919.37 2764.99 30.42 o 12 12 0 1443.32 1435.08 19.97 o 14 12 0 50.14 51.89 10.35 o 16 12 0 289.36 322.55 19.77 o 1 13 0 1798.13 1806.14 19.00 o 3 13 0 5431.21 5301.35 48.00 o 5 13 0 1594.25 1577.61 18.32 o 7 13 0 3772.90 3750.15 35.87 o 9 13 0 922.70 925.62 14.25 o 11 13 0 1058.15 1112.98 18.46 o 13 13 0 130.71 138.46 10.28 o 15 13 0 65.76 54.11 15.57 o 17 13 0 8.53 -6.40 21.24 o 0 14 0 84995.39 90258.52 1884.38 o 2 14 0 29646.05 31685.59 274.50 o 4 14 0 3615.68 3584.25 41.30 o 6 14 0 2015.68 1925.00 20.30 o 8 14 0 4703.15 4815.24 44.17 o 10 14 0 7165.28 7533.26 78.67 o 12 14 0 1754.38 1845.30 34.66 o 14 14 0 676.45 664.87 23.30 o 16 14 0 1619.21 1663.91 42.30 o 1 15 0 126.63 97.40 4.27 o 3 15 0 14683.84 15311.45 149.21 o 5 15 0 169.37 140.06 4.99 o 7 15 0 1153.65 1075.22 14.57 o 9 15 0 570.92 583.86 11.86 o 11 15 0 1485.51 1470.58 21.80 o 13 15 0 25.48 20.02 9.53 o 15 15 0 252.86 259.83 18.22 o 17 15 0 0.16 12.24 22.46 o 0 16 0 144087.97 155642.66 1774.80 o 2 16 0 15.69 28.63 4.72 o 4 16 0 36222.51 38336.95 349.93 o 6 16 0 1116.23 962.09 13.44 o 8 16 0 7499.12 7449.24 72.01 o 10 16 0 5175.75 5247.57 56.84 o 12 16 0 2919.33 2987.85 52.62 o 14 16 0 752.91 734.64 20.92 o 16 16 0 2412.33 2496.54 47.56 o 1 17 0 1005.46 1066.70 13.38 o 3 17 0 358.13 293.26 6.82 o 5 17 0 3442.22 3581.44 36.38 o 7 17 0 176.86 164.40 6.68 o 9 17 0 347.90 343.14 9.62 o 11 17 0 318.29 306.48 11.06 o 13 17 0 0.15 5.24 11.18 o 15 17 0 39.65 1.39 15.44 o 17 17 0 50.92 48.26 23.84 o 0 18 0 1880.17 1387.66 28.29 o 2 18 0 2672.73 2444.13 25.78 o 4 18 0 2909.16 2532.64 26.87 o 6 18 0 3128.10 2858.62 46.83 o 8 18 0 4226.15 4215.31 43.19 o 10 18 0 5563.51 5681.35 61.32 o 12 18 0 3265.28 3406.34 53.97 o 14 18 0 3590.91 3772.18 52.41 o 16 18 0 971.16 1028.49 36.84 o 1 19 0 213.56 198.04 5.92 o 3 19 0 0.07 -4.33 4.33 o 5 19 0 0.28 -4.67 4.67 o 7 19 0 1062.43 1044.53 15.39 o 9 19 0 431.40 409.79 14.12 o 11 19 0 608.67 632.64 17.86 o 13 19 0 241.48 261.29 16.26 o 15 19 0 106.88 100.64 17.42 o 0 20 0 29793.25 31738.46 653.20 o 2 20 0 5376.02 5813.36 60.33 o 4 20 0 8876.35 8982.04 85.48 o 6 20 0 279.46 266.58 10.89 o 8 20 0 203.57 185.18 8.61 o 10 20 0 927.11 837.16 19.06 o 12 20 0 558.42 572.57 21.46 o 14 20 0 4064.12 4194.38 57.38 o 16 20 0 1082.96 1089.25 32.97 o 1 21 0 40.36 40.29 5.05 o 3 21 0 1194.95 1162.73 22.53 o 5 21 0 40.14 25.00 5.48 o 7 21 0 3807.51 3869.73 40.39 o 9 21 0 810.93 798.09 16.27 o 11 21 0 3907.39 4106.18 53.35 o 13 21 0 499.14 466.43 19.82 o 15 21 0 10.07 3.78 16.89 o 0 22 0 525.09 483.87 16.84 o 2 22 0 1626.82 1370.17 18.25 o 4 22 0 68.41 84.61 6.40 o 6 22 0 9216.44 9201.90 134.68 o 8 22 0 163.21 148.34 11.16 o 10 22 0 10623.33 11213.11 137.74 o 12 22 0 64.81 42.74 13.94 o 14 22 0 2422.15 2669.02 48.52 o 16 22 0 186.01 188.76 25.93 o 1 23 0 7.93 8.32 5.19 o 3 23 0 2210.14 2125.31 37.05 o 5 23 0 570.82 532.79 12.31 o 7 23 0 225.02 207.06 12.87 o 9 23 0 2335.47 2386.70 34.48 o 11 23 0 12.62 -9.14 12.84 o 13 23 0 142.71 140.79 23.74 o 15 23 0 0.92 16.92 21.92 o 0 24 0 1665.82 1522.93 31.82 o 2 24 0 10640.86 11314.06 114.33 o 4 24 0 132.81 109.59 8.39 o 6 24 0 94.58 113.64 14.38 o 8 24 0 6363.54 6535.39 78.25 o 10 24 0 210.15 236.09 15.78 o 12 24 0 3460.92 3581.39 57.39 o 14 24 0 42.75 54.98 21.42 o 16 24 0 338.02 309.60 40.55 o 1 25 0 229.01 209.90 9.05 o 3 25 0 394.95 373.08 10.43 o 5 25 0 1235.41 1252.51 18.93 o 7 25 0 1322.04 1346.97 23.24 o 9 25 0 4.91 -9.74 11.21 o 11 25 0 12.42 14.25 13.92 o 13 25 0 200.39 200.30 18.46 o 15 25 0 18.99 43.92 23.76 o 0 26 0 23.68 19.54 15.21 o 2 26 0 6047.00 5883.72 69.59 o 4 26 0 3027.43 3103.05 37.28 o 6 26 0 1121.01 1083.35 20.54 o 8 26 0 412.73 383.66 19.91 o 10 26 0 10.88 24.97 15.80 o 12 26 0 2051.30 2014.56 39.50 o 14 26 0 165.17 191.12 24.78 o 1 27 0 284.93 298.07 13.16 o 3 27 0 1023.19 1033.71 16.99 o 5 27 0 637.67 663.29 16.36 o 7 27 0 121.42 107.75 13.07 o 9 27 0 56.03 40.18 12.36 o 11 27 0 239.71 221.56 16.79 o 13 27 0 48.56 28.72 20.96 o 15 27 0 208.49 178.54 37.34 o 0 28 0 4000.71 4075.96 94.46 o 2 28 0 5476.56 6342.88 87.91 o 4 28 0 380.24 396.04 14.42 o 6 28 0 4529.09 4776.22 69.13 o 8 28 0 836.34 843.36 48.76 o 10 28 0 4744.77 4976.45 74.06 o 12 28 0 277.50 308.60 29.96 o 14 28 0 157.39 155.37 25.96 o 1 29 0 183.01 143.97 11.34 o 3 29 0 76.29 90.51 12.65 o 5 29 0 1832.54 1743.33 35.02 o 7 29 0 106.71 94.55 12.49 o 9 29 0 449.98 450.83 18.55 o 11 29 0 208.14 221.40 17.57 o 13 29 0 0.86 -21.26 22.47 o 0 30 0 1249.93 1410.02 46.74 o 2 30 0 6162.07 5895.93 115.48 o 4 30 0 232.58 275.66 17.04 o 6 30 0 929.16 943.30 28.75 o 8 30 0 801.34 779.95 29.02 o 10 30 0 788.11 914.08 33.22 o 12 30 0 1209.50 1255.96 59.60 o 14 30 0 531.75 621.43 47.73 o 1 31 0 118.82 100.35 15.08 o 3 31 0 896.92 859.64 27.01 o 5 31 0 63.87 64.10 14.77 o 7 31 0 158.41 110.40 16.84 o 9 31 0 240.76 210.65 21.39 o 11 31 0 24.62 6.16 20.07 o 13 31 0 0.10 -13.85 34.87 o 0 32 0 5874.17 5907.88 142.44 o 2 32 0 7754.09 7723.14 203.89 o 4 32 0 2416.17 2475.36 50.27 o 6 32 0 2337.97 2376.61 49.92 o 8 32 0 601.60 626.36 27.74 o 10 32 0 1502.60 1622.35 62.56 o 12 32 0 691.60 817.77 49.46 o 1 33 0 238.47 235.45 17.48 o 3 33 0 14.79 11.06 23.00 o 5 33 0 345.62 301.27 19.84 o 7 33 0 58.37 46.89 17.21 o 9 33 0 322.92 380.53 24.31 o 11 33 0 57.27 60.09 30.91 o 13 33 0 15.23 -2.47 37.34 o 0 34 0 5472.85 5548.33 136.25 o 2 34 0 32.96 116.67 16.43 o 4 34 0 2642.14 2671.12 54.46 o 6 34 0 731.32 685.65 28.58 o 8 34 0 434.10 372.58 23.42 o 10 34 0 980.07 909.38 36.80 o 12 34 0 126.07 115.57 50.82 o 1 35 0 33.94 31.74 15.73 o 3 35 0 70.88 37.99 16.08 o 5 35 0 4.61 13.50 16.87 o 7 35 0 1.60 4.67 18.18 o 9 35 0 0.13 -6.33 20.45 o 11 35 0 379.76 378.84 39.57 o 0 36 0 5012.92 5051.78 127.60 o 2 36 0 1031.00 1012.25 32.26 o 4 36 0 1014.57 999.22 36.35 o 6 36 0 576.75 613.98 27.19 o 8 36 0 481.21 483.03 31.16 o 10 36 0 2307.32 2463.94 83.33 o 1 37 0 0.37 0.49 16.87 o 3 37 0 84.47 86.28 18.61 o 5 37 0 127.64 128.07 20.37 o 7 37 0 19.12 5.84 20.07 o 9 37 0 130.52 152.08 34.87 o 0 38 0 2902.70 2810.39 83.09 o 2 38 0 489.23 338.36 37.34 o 4 38 0 166.03 125.10 20.28 o 6 38 0 222.69 224.00 23.25 o 8 38 0 732.69 696.06 31.64 o 1 39 0 231.84 261.31 22.64 o 3 39 0 0.01 -8.67 25.72 o 5 39 0 496.86 517.83 34.50 o 7 39 0 6.14 -7.26 22.11 o 9 39 0 136.60 80.86 36.60 o 0 40 0 722.63 568.26 39.32 o 2 40 0 404.68 341.08 24.83 o 4 40 0 11.19 37.30 21.51 o 6 40 0 157.15 195.91 25.09 o 8 40 0 656.42 614.01 45.25 o 1 41 0 174.75 161.52 23.08 o 3 41 0 34.78 25.77 21.50 o 5 41 0 54.50 26.72 22.99 o 7 41 0 55.63 55.64 35.36 o 0 42 0 707.74 624.89 43.52 o 2 42 0 710.59 563.00 29.80 o 4 42 0 189.69 173.28 25.35 o 1 43 0 23.42 12.86 23.08 o 3 43 0 92.52 101.21 24.83 o 0 44 0 831.93 990.62 59.35 o 2 44 0 1160.89 1164.22 61.33 o -17 1 1 282.63 278.48 16.01 o -15 1 1 7789.69 8089.90 78.97 o -13 1 1 4206.82 4166.09 42.97 o -11 1 1 18188.53 17931.43 178.72 o -9 1 1 7247.22 7579.49 83.40 o -7 1 1 16.84 41.08 3.33 o -5 1 1 68192.81 73488.05 642.48 o -3 1 1 14056.70 15998.36 149.63 o 1 1 1 12054.90 13942.31 132.86 o 3 1 1 1306.14 1609.21 14.55 o 5 1 1 61669.66 65458.66 527.99 o 7 1 1 571.88 462.94 7.70 o 9 1 1 10083.96 10474.23 88.06 o 11 1 1 212.31 199.02 7.66 o 13 1 1 2448.70 2465.60 46.36 o 15 1 1 7347.58 7431.66 92.47 o 17 1 1 1082.58 1173.85 59.60 o -18 2 1 47.63 36.67 21.12 o -16 2 1 55.80 53.89 11.99 o -14 2 1 649.51 664.23 19.36 o -12 2 1 920.82 888.98 15.87 o -10 2 1 470.58 460.49 8.73 o -8 2 1 1288.98 1252.28 15.52 o -6 2 1 188.27 215.40 5.21 o -4 2 1 2.07 -1.89 1.89 o -2 2 1 3931.18 3926.27 43.07 o 0 2 1 771.52 722.55 13.64 o 2 2 1 2902.12 3088.83 24.44 o 4 2 1 2304.39 2327.19 20.64 o 6 2 1 459.51 440.08 7.18 o 8 2 1 41.82 35.77 4.17 o 10 2 1 2.11 -4.92 4.92 o 12 2 1 906.78 953.84 19.95 o 14 2 1 35.00 34.61 11.57 o 16 2 1 218.79 208.23 16.27 o 18 2 1 4.13 16.08 24.30 o -17 3 1 128.56 127.94 14.11 o -15 3 1 5194.46 5258.88 54.65 o -13 3 1 9701.85 10050.82 95.28 o -11 3 1 13462.02 13102.87 131.87 o -9 3 1 1007.22 736.56 15.04 o -7 3 1 4798.66 4554.65 42.21 o -5 3 1 22811.95 23032.93 322.09 o -3 3 1 133609.95 136329.73 1161.62 o -1 3 1 18757.01 18931.51 182.20 o 1 3 1 152212.25 161381.06 1290.76 o 3 3 1 33755.19 36294.32 293.83 o 5 3 1 20805.80 21611.59 176.04 o 7 3 1 1269.90 1195.33 13.11 o 9 3 1 2892.57 2536.05 24.53 o 11 3 1 478.29 499.31 12.06 o 13 3 1 7444.77 7743.25 94.03 o 15 3 1 997.69 983.94 23.99 o 17 3 1 5531.22 5655.96 102.38 o -18 4 1 114.24 94.97 17.83 o -16 4 1 538.22 513.47 26.66 o -14 4 1 4.61 3.10 7.73 o -12 4 1 187.23 186.17 10.75 o -10 4 1 1.76 2.82 4.22 o -8 4 1 301.48 260.38 6.10 o -6 4 1 541.68 634.52 12.09 o -4 4 1 92.64 88.04 6.62 o -2 4 1 3146.07 3253.37 28.84 o 0 4 1 2162.34 2225.56 18.89 o 2 4 1 1321.60 1400.72 13.28 o 4 4 1 959.70 921.04 9.76 o 6 4 1 1118.14 1149.16 12.34 o 8 4 1 28.41 31.04 4.21 o 10 4 1 218.68 200.67 6.72 o 12 4 1 1403.90 1409.90 24.73 o 14 4 1 483.95 451.88 16.18 o 16 4 1 1.28 3.62 14.27 o 18 4 1 145.34 159.07 26.49 o -17 5 1 110.96 69.73 13.81 o -15 5 1 21.20 22.99 9.75 o -13 5 1 176.62 115.72 8.73 o -11 5 1 8096.87 8235.66 84.69 o -9 5 1 5169.51 5213.52 45.69 o -7 5 1 7072.40 7452.54 78.36 o -5 5 1 3005.76 2852.17 28.39 o -3 5 1 12607.73 13085.42 122.44 o -1 5 1 12524.84 13332.86 100.77 o 1 5 1 9385.45 10245.74 88.06 o 3 5 1 1586.09 1526.41 14.79 o 5 5 1 19659.49 20348.67 165.86 o 7 5 1 9831.50 9627.71 80.20 o 9 5 1 6164.62 6715.80 57.70 o 11 5 1 134.34 132.27 7.89 o 13 5 1 101.93 121.84 11.42 o 15 5 1 80.88 80.87 13.62 o 17 5 1 1022.03 1060.30 38.47 o -18 6 1 24.02 16.51 17.22 o -16 6 1 317.01 299.01 15.02 o -14 6 1 275.89 261.21 13.27 o -12 6 1 120.50 119.55 7.93 o -10 6 1 1161.36 1272.85 15.44 o -8 6 1 785.99 866.60 11.15 o -6 6 1 790.34 889.67 10.56 o -4 6 1 292.13 269.10 4.82 o -2 6 1 261.86 270.76 4.00 o 0 6 1 66.22 69.85 2.19 o 2 6 1 2.60 4.37 2.74 o 4 6 1 28.97 39.14 3.75 o 6 6 1 292.15 346.05 6.64 o 8 6 1 145.81 173.24 5.75 o 10 6 1 1031.64 1072.69 16.17 o 12 6 1 7.52 6.69 9.53 o 14 6 1 750.09 769.04 20.46 o 16 6 1 3.33 0.12 14.25 o 18 6 1 117.00 97.43 36.85 o -17 7 1 83.78 88.52 16.18 o -15 7 1 133.63 154.20 16.71 o -13 7 1 756.78 718.37 15.38 o -11 7 1 9413.28 9731.19 102.50 o -9 7 1 1218.61 1072.87 14.14 o -7 7 1 4871.77 4761.72 58.42 o -5 7 1 5722.61 6255.07 55.86 o -3 7 1 21472.73 22679.83 196.67 o -1 7 1 6937.12 7637.96 66.95 o 1 7 1 37294.81 40029.08 389.09 o 3 7 1 1272.59 1258.85 12.80 o 5 7 1 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