#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/49/2014984.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014984_Fobs loop_ _publ_author_name 'Alley, Steven' 'Gallagher, John F.' 'Hooper, Vincent M.' 'Kenny, Peter T. M.' 'Lough, Alan J.' _publ_section_title ; Methyl 2-(4-ferrocenylbenzamido)thiophene-3-carboxylate and ethyl 2-(4-ferrocenylbenzamido)-1,3-thiazole-4-acetate, a unique ferrocene derivative containing a thiazole moiety ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m365 _journal_page_last m369 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 91.811 _cell_angle_beta 106.096 _cell_angle_gamma 92.735 _cell_length_a 12.7466 _cell_length_b 12.8752 _cell_length_c 13.5661 _exptl_crystal_F_000 984.00 _reflns_d_resolution_high 0.7690 _[local]_cod_data_source_file fg1846IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title 'FG1846 - revised (II) structural refinement [18-5-2005]' _shelx_refln_list_code 4 _shelx_f_calc_maximum 207.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1125.93 1100.56 44.49 o 3 0 0 5003.21 5304.61 125.49 o 4 0 0 7263.14 7277.72 196.55 o 5 0 0 341.16 302.73 13.06 o 6 0 0 3999.73 3771.81 83.29 o 7 0 0 4868.57 5311.72 226.83 o 8 0 0 1785.34 1743.07 58.61 o 9 0 0 432.00 441.62 17.63 o 10 0 0 841.59 832.98 32.46 o 11 0 0 783.97 866.56 64.22 o 12 0 0 1062.66 1016.93 84.92 o 13 0 0 0.10 -20.80 40.16 o 14 0 0 0.79 -4.49 38.48 o 15 0 0 335.52 225.60 88.44 o -15 1 0 47.49 -48.72 82.08 o -14 1 0 47.86 54.54 54.54 o -13 1 0 5.52 -2.91 45.54 o -12 1 0 173.83 148.67 38.83 o -11 1 0 571.30 523.09 51.59 o -10 1 0 1541.67 1586.79 49.12 o -9 1 0 1129.85 1220.02 43.25 o -8 1 0 76.87 106.48 10.49 o -7 1 0 185.41 195.29 19.61 o -6 1 0 9101.86 8886.77 382.68 o -5 1 0 306.64 270.51 12.39 o -4 1 0 971.52 1103.12 30.28 o -3 1 0 727.32 743.27 22.82 o -2 1 0 11153.08 11120.63 240.91 o 2 1 0 5800.30 5319.71 123.16 o 3 1 0 2695.42 2433.86 57.73 o 4 1 0 2333.59 2230.29 51.38 o 5 1 0 193.34 137.08 16.41 o 6 1 0 2.34 23.77 9.97 o 7 1 0 26.75 32.59 9.17 o 8 1 0 1451.74 1431.34 56.34 o 9 1 0 1958.81 2171.85 51.55 o 10 1 0 178.18 174.45 10.76 o 11 1 0 131.73 109.44 43.29 o 12 1 0 28.57 50.37 46.20 o 13 1 0 1538.81 1631.25 246.51 o 14 1 0 19.49 2.87 101.67 o 15 1 0 1.49 -21.45 64.07 o -15 2 0 56.58 36.27 84.73 o -14 2 0 271.31 196.74 63.55 o -13 2 0 79.12 33.10 48.45 o -12 2 0 319.55 385.81 78.38 o -11 2 0 3.11 -1.06 8.06 o -10 2 0 1577.58 1600.37 49.53 o -9 2 0 691.55 693.13 29.71 o -8 2 0 8417.89 8478.22 199.77 o -7 2 0 323.63 340.45 16.01 o -6 2 0 49.95 81.91 10.95 o -5 2 0 2169.71 2067.93 61.76 o -4 2 0 3632.16 3605.59 148.74 o -3 2 0 1015.94 932.72 38.66 o -2 2 0 3688.20 3681.65 113.89 o -1 2 0 1268.69 1221.48 66.64 o 0 2 0 59.58 70.92 14.56 o 1 2 0 12.25 26.73 24.89 o 2 2 0 20174.89 18874.88 651.76 o 3 2 0 620.22 669.25 22.16 o 4 2 0 1104.92 1023.15 30.98 o 5 2 0 2282.56 2235.75 70.49 o 6 2 0 3740.30 3663.05 86.30 o 7 2 0 4189.90 4138.85 168.07 o 8 2 0 399.88 466.11 43.80 o 9 2 0 164.60 167.36 12.55 o 10 2 0 367.29 399.70 18.87 o 11 2 0 198.66 203.21 14.98 o 12 2 0 4.31 -37.16 53.09 o 13 2 0 144.58 140.47 57.65 o 14 2 0 5.93 -48.98 55.07 o 15 2 0 129.83 186.93 76.52 o -15 3 0 2.64 -60.37 60.37 o -14 3 0 1204.67 1251.55 162.90 o -13 3 0 183.09 114.39 54.02 o -12 3 0 3.84 1.99 8.08 o -11 3 0 79.00 83.64 12.99 o -10 3 0 1339.95 1354.99 48.60 o -9 3 0 1110.12 1117.29 42.15 o -8 3 0 196.57 179.56 16.25 o -7 3 0 210.59 182.24 16.07 o -6 3 0 1367.29 1405.88 45.91 o -5 3 0 1145.29 1119.27 44.12 o -4 3 0 2432.60 2298.32 84.30 o -3 3 0 456.86 420.49 28.19 o -2 3 0 6415.07 6058.32 188.28 o -1 3 0 6275.46 6157.96 213.09 o 0 3 0 8901.71 8309.55 240.51 o 1 3 0 13216.05 13023.50 375.87 o 2 3 0 2526.38 2577.95 73.56 o 3 3 0 534.65 539.05 25.37 o 4 3 0 193.17 194.16 29.75 o 5 3 0 6100.25 5457.01 119.35 o 6 3 0 2152.01 2196.18 60.51 o 7 3 0 677.06 742.08 28.58 o 8 3 0 2680.43 2810.67 111.64 o 9 3 0 73.37 93.21 20.26 o 10 3 0 188.03 186.65 15.56 o 11 3 0 2.55 4.14 16.20 o 12 3 0 111.44 102.67 12.17 o 13 3 0 80.90 28.54 123.52 o 14 3 0 34.84 -9.27 61.43 o 15 3 0 80.03 95.05 79.70 o -15 4 0 51.63 -9.00 63.28 o -14 4 0 84.50 135.03 72.02 o -13 4 0 64.44 52.30 18.56 o -12 4 0 885.30 905.19 86.38 o -11 4 0 1.17 2.72 13.18 o -10 4 0 90.20 84.89 13.65 o -9 4 0 550.10 577.75 31.55 o -8 4 0 150.17 170.60 16.06 o -7 4 0 429.48 414.75 25.22 o -6 4 0 366.64 295.79 20.87 o -5 4 0 24.36 28.01 16.66 o -4 4 0 3314.09 3518.91 122.36 o -3 4 0 2473.20 2682.11 93.27 o -2 4 0 4907.43 4841.20 158.74 o -1 4 0 1624.77 1412.06 62.87 o 0 4 0 8548.68 9157.03 269.27 o 1 4 0 515.98 487.85 31.80 o 2 4 0 954.65 996.89 42.68 o 3 4 0 2632.48 2341.35 70.81 o 4 4 0 959.66 839.66 43.43 o 5 4 0 1146.05 1038.13 53.07 o 6 4 0 548.27 606.66 26.49 o 7 4 0 120.17 138.30 16.67 o 8 4 0 550.62 552.50 38.09 o 9 4 0 2359.87 2393.52 73.67 o 10 4 0 360.85 398.27 24.56 o 11 4 0 257.44 270.42 20.53 o 12 4 0 104.32 90.57 16.24 o 13 4 0 121.89 16.05 83.67 o 14 4 0 209.50 181.38 76.79 o 15 4 0 3.47 12.18 78.26 o -15 5 0 12.76 116.76 101.93 o -14 5 0 126.51 106.17 19.24 o -13 5 0 136.84 164.97 19.20 o -12 5 0 5.50 18.32 19.15 o -11 5 0 33.44 9.88 19.83 o -10 5 0 48.05 48.30 22.31 o -9 5 0 110.23 134.92 18.84 o -8 5 0 824.11 865.12 37.02 o -7 5 0 2831.58 2950.19 90.73 o -6 5 0 504.52 510.97 48.73 o -5 5 0 3.13 35.39 30.45 o -4 5 0 970.07 909.21 47.47 o -3 5 0 845.94 683.43 38.70 o -2 5 0 713.42 687.36 39.80 o -1 5 0 2819.44 2606.86 94.42 o 0 5 0 6241.29 6248.91 200.13 o 1 5 0 3013.80 2544.27 104.19 o 2 5 0 118.50 138.36 22.50 o 3 5 0 181.88 135.15 30.73 o 4 5 0 5292.90 5340.63 138.90 o 5 5 0 227.97 202.20 21.33 o 6 5 0 509.14 546.76 43.79 o 7 5 0 1256.44 1265.93 51.41 o 8 5 0 588.79 650.31 35.02 o 9 5 0 1158.76 1237.44 65.86 o 10 5 0 1088.43 1113.08 78.68 o 11 5 0 636.44 687.19 38.30 o 12 5 0 959.74 966.74 46.06 o 13 5 0 173.57 176.50 18.03 o -15 6 0 384.09 271.68 95.59 o -14 6 0 97.29 78.60 23.30 o -13 6 0 93.26 117.15 23.31 o -12 6 0 137.39 93.54 51.94 o -11 6 0 3.85 -13.56 19.58 o -10 6 0 12.15 1.00 26.79 o -9 6 0 631.87 629.77 37.57 o -8 6 0 42.15 40.81 18.01 o -7 6 0 563.97 616.06 38.66 o -6 6 0 508.94 481.96 32.83 o -5 6 0 5158.87 4991.92 225.13 o -4 6 0 419.27 407.74 67.93 o -3 6 0 1950.80 2368.07 144.24 o -2 6 0 1393.90 1313.62 104.83 o -1 6 0 172.36 240.61 47.80 o 0 6 0 3094.79 2814.54 105.53 o 1 6 0 4747.55 4826.81 180.94 o 2 6 0 917.97 893.41 71.14 o 3 6 0 1615.83 1561.03 55.75 o 4 6 0 262.86 312.31 33.99 o 5 6 0 707.59 689.75 35.50 o 6 6 0 827.86 736.61 38.31 o 7 6 0 233.19 263.69 23.76 o 8 6 0 1459.82 1537.82 62.31 o 9 6 0 1.91 3.49 15.53 o 10 6 0 197.52 207.00 24.89 o 11 6 0 5.12 28.42 28.12 o 12 6 0 387.60 382.50 43.66 o 13 6 0 50.61 36.97 18.80 o -14 7 0 26.43 44.48 82.87 o -13 7 0 16.13 7.68 22.53 o -12 7 0 119.89 112.14 21.46 o -11 7 0 557.57 624.07 40.16 o -10 7 0 44.34 31.65 17.39 o -9 7 0 11.50 5.18 17.33 o -8 7 0 856.53 943.51 58.69 o -7 7 0 1046.80 1069.59 56.55 o -6 7 0 92.42 110.09 38.00 o -5 7 0 28.38 42.15 26.08 o -4 7 0 1008.86 944.80 57.03 o -3 7 0 2555.14 2634.58 107.41 o -2 7 0 3046.07 2916.98 118.27 o -1 7 0 3908.83 4097.03 139.00 o 0 7 0 2485.78 2499.07 186.33 o 1 7 0 330.74 336.83 31.68 o 2 7 0 1115.17 1174.02 57.23 o 3 7 0 1326.05 1202.44 59.83 o 4 7 0 417.58 338.38 27.66 o 5 7 0 680.92 710.86 37.62 o 6 7 0 2122.82 2254.65 100.07 o 7 7 0 57.44 53.00 24.27 o 8 7 0 1821.63 1852.92 77.03 o 9 7 0 390.20 377.53 33.91 o 10 7 0 241.74 224.93 27.38 o 11 7 0 23.60 -0.61 17.60 o 12 7 0 0.57 11.65 17.40 o 13 7 0 72.86 125.50 34.95 o -14 8 0 9.59 -2.91 82.08 o -13 8 0 787.97 883.83 72.92 o -12 8 0 270.60 201.30 35.37 o -11 8 0 0.48 31.28 19.92 o -10 8 0 1277.87 1312.48 68.17 o -9 8 0 375.14 358.92 34.35 o -8 8 0 204.54 165.50 34.43 o -7 8 0 189.46 198.79 30.32 o -6 8 0 414.06 410.63 74.02 o -5 8 0 61.87 82.78 24.03 o -4 8 0 2674.40 2758.89 114.17 o -3 8 0 1455.30 1439.62 81.38 o -2 8 0 1621.65 1771.72 83.12 o -1 8 0 921.12 935.80 72.32 o 0 8 0 2557.26 2601.47 208.17 o 1 8 0 7.40 -24.81 24.81 o 2 8 0 2080.77 2089.72 95.66 o 3 8 0 16.56 24.72 22.24 o 4 8 0 57.04 54.84 21.53 o 5 8 0 101.94 99.81 32.95 o 6 8 0 665.85 724.85 42.56 o 7 8 0 178.64 213.00 28.08 o 8 8 0 106.05 145.79 30.92 o 9 8 0 252.32 236.46 33.51 o 10 8 0 276.15 267.84 34.37 o 11 8 0 91.27 74.99 28.91 o 12 8 0 56.30 16.96 30.49 o -13 9 0 47.89 79.84 32.19 o -12 9 0 276.79 309.47 47.70 o -11 9 0 319.52 278.19 36.78 o -10 9 0 2.00 5.62 23.74 o -9 9 0 60.04 32.58 19.95 o -8 9 0 1812.28 2013.95 108.64 o -7 9 0 25.65 17.07 21.44 o -6 9 0 125.80 75.75 26.11 o -5 9 0 296.20 349.77 89.24 o -4 9 0 764.23 785.89 60.01 o -3 9 0 50.17 51.79 27.14 o -2 9 0 183.12 118.35 30.23 o -1 9 0 29.00 38.25 22.93 o 0 9 0 4593.07 4519.31 173.73 o 1 9 0 22.00 -8.84 33.23 o 2 9 0 3.83 -22.84 22.84 o 3 9 0 763.23 879.56 61.77 o 4 9 0 579.15 582.96 44.46 o 5 9 0 121.19 91.13 30.32 o 6 9 0 4.58 6.32 20.25 o 7 9 0 9.32 22.89 26.95 o 8 9 0 6.77 29.22 24.63 o 9 9 0 219.43 211.95 33.16 o 10 9 0 469.16 457.65 61.47 o 11 9 0 14.31 -6.06 26.83 o 12 9 0 1.00 29.39 44.22 o -13 10 0 4.31 -33.12 38.29 o -12 10 0 3.75 -20.15 23.28 o -11 10 0 142.05 148.59 31.67 o -10 10 0 121.20 88.18 27.63 o -9 10 0 120.59 78.88 38.26 o -8 10 0 444.96 429.60 48.08 o -7 10 0 102.97 34.02 27.13 o -6 10 0 341.45 406.46 47.81 o -5 10 0 127.83 81.60 59.31 o -4 10 0 42.92 37.58 25.97 o -3 10 0 88.73 86.80 32.29 o -2 10 0 13.75 -21.96 27.04 o -1 10 0 715.58 723.65 55.07 o 0 10 0 524.49 564.38 48.45 o 1 10 0 176.46 156.95 32.09 o 2 10 0 2.49 -28.86 28.86 o 3 10 0 20.71 51.75 33.64 o 4 10 0 181.70 196.22 30.98 o 5 10 0 244.25 218.47 58.10 o 6 10 0 123.55 106.28 29.60 o 7 10 0 220.02 148.98 32.60 o 8 10 0 28.36 35.77 47.69 o 9 10 0 242.81 226.61 38.54 o 10 10 0 414.29 367.31 46.07 o 11 10 0 78.67 78.79 36.29 o -12 11 0 157.03 62.35 64.61 o -11 11 0 8.33 75.53 44.66 o -10 11 0 143.16 81.80 44.94 o -9 11 0 8.69 22.15 33.63 o -8 11 0 260.02 193.90 54.28 o -7 11 0 417.84 395.51 43.87 o -6 11 0 75.90 99.16 55.34 o -5 11 0 982.19 941.97 74.07 o -4 11 0 1191.53 1185.50 107.02 o -3 11 0 28.84 11.71 29.10 o -2 11 0 63.28 58.68 43.03 o -1 11 0 414.86 342.64 52.30 o 0 11 0 5.07 -15.48 25.90 o 1 11 0 89.27 48.69 74.14 o 2 11 0 429.53 444.83 52.30 o 3 11 0 182.06 112.62 41.37 o 4 11 0 254.49 234.21 32.67 o 5 11 0 529.50 517.92 52.41 o 6 11 0 43.63 17.40 28.32 o 7 11 0 608.57 604.35 54.07 o 8 11 0 0.46 4.32 33.86 o 9 11 0 2.08 9.88 32.48 o 10 11 0 85.82 91.97 37.72 o 11 11 0 231.93 267.96 61.96 o -11 12 0 169.20 192.80 53.11 o -10 12 0 82.05 44.24 35.56 o -9 12 0 21.99 -12.55 41.83 o -8 12 0 241.19 310.62 49.30 o -7 12 0 323.95 348.93 57.06 o -6 12 0 778.07 707.97 75.04 o -5 12 0 14.35 1.99 28.85 o -4 12 0 389.32 416.27 63.11 o -3 12 0 264.42 345.02 54.21 o -2 12 0 1.04 -15.15 34.03 o -1 12 0 603.91 540.55 55.43 o 0 12 0 379.49 310.84 50.66 o 1 12 0 718.67 757.42 94.28 o 2 12 0 14.28 15.01 39.71 o 3 12 0 327.01 339.43 54.65 o 4 12 0 5.28 6.91 27.58 o 5 12 0 87.26 115.42 34.28 o 6 12 0 18.91 21.50 41.67 o 7 12 0 197.01 200.28 49.31 o 8 12 0 333.11 379.44 64.49 o 9 12 0 37.32 140.06 73.08 o 10 12 0 66.58 29.39 49.78 o -10 13 0 19.85 202.02 86.58 o -9 13 0 307.42 392.42 74.94 o -8 13 0 79.66 114.95 48.46 o -7 13 0 282.55 174.40 46.53 o -6 13 0 64.23 92.29 41.55 o -5 13 0 33.39 7.44 42.50 o -4 13 0 25.22 87.45 49.51 o -3 13 0 698.11 623.01 73.66 o -2 13 0 197.47 149.39 125.77 o -1 13 0 63.37 97.34 54.41 o 0 13 0 230.18 156.18 52.48 o 1 13 0 1885.78 2103.62 202.56 o 2 13 0 267.57 246.07 49.16 o 3 13 0 381.84 381.29 62.61 o 4 13 0 47.50 55.03 34.37 o 5 13 0 433.58 417.42 72.95 o 6 13 0 0.30 62.22 82.87 o 7 13 0 50.81 55.95 79.96 o 8 13 0 309.19 328.87 90.29 o 9 13 0 286.31 277.50 96.38 o -9 14 0 107.56 135.56 69.11 o -8 14 0 4.02 -23.03 86.58 o -7 14 0 282.47 265.05 80.76 o -6 14 0 11.88 -22.95 37.81 o -5 14 0 43.94 99.83 102.33 o -4 14 0 119.25 60.54 39.32 o -3 14 0 216.54 222.87 45.57 o -2 14 0 0.06 -23.04 36.12 o -1 14 0 763.66 677.16 83.43 o 0 14 0 67.31 69.63 121.93 o 1 14 0 18.69 40.83 43.20 o 2 14 0 70.15 85.02 43.20 o 3 14 0 104.73 108.59 52.21 o 4 14 0 210.42 217.36 62.43 o 5 14 0 1.19 13.61 45.49 o 6 14 0 64.67 69.37 57.98 o 7 14 0 67.27 5.82 52.16 o -7 15 0 257.55 342.63 92.15 o -6 15 0 27.98 37.33 63.28 o -5 15 0 133.04 72.02 63.28 o -4 15 0 13.73 37.33 57.45 o -3 15 0 232.13 158.34 72.02 o -2 15 0 13.71 -40.24 60.37 o -1 15 0 149.03 40.25 83.41 o 0 15 0 186.81 178.46 63.28 o 1 15 0 144.17 72.02 69.11 o 2 15 0 49.17 109.35 60.37 o 3 15 0 89.07 40.25 69.11 o 4 15 0 261.05 247.84 69.11 o 5 15 0 0.94 5.82 83.67 o 6 15 0 3.59 14.56 69.37 o -5 16 0 183.64 89.23 69.11 o -4 16 0 1.86 -46.07 69.10 o -3 16 0 73.49 123.65 100.61 o -2 16 0 171.04 129.48 69.11 o -1 16 0 67.50 -5.82 94.79 o 0 16 0 3.26 -69.10 69.10 o 1 16 0 193.78 163.90 83.41 o 2 16 0 125.08 115.18 69.11 o 3 16 0 102.20 132.39 74.93 o -4 -16 1 123.81 97.70 74.67 o -3 -16 1 8.17 60.37 68.84 o -2 -16 1 14.40 23.03 68.84 o -1 -16 1 33.50 0.00 65.93 o 0 -16 1 59.65 137.94 97.70 o 1 -16 1 65.48 126.30 63.28 o 2 -16 1 0.72 140.59 100.61 o 3 -16 1 12.49 65.93 60.37 o 4 -16 1 263.23 370.44 100.62 o 5 -16 1 0.41 152.24 80.49 o -6 -15 1 1.70 51.89 69.10 o -5 -15 1 1.83 -5.82 63.28 o -4 -15 1 0.24 112.26 97.70 o -3 -15 1 2.33 25.95 54.54 o -2 -15 1 576.81 690.11 109.37 o -1 -15 1 272.99 273.00 97.71 o 0 -15 1 228.59 238.57 74.67 o 1 -15 1 245.75 290.21 83.41 o 2 -15 1 499.89 468.45 97.72 o 3 -15 1 292.87 321.72 83.41 o 4 -15 1 0.11 0.00 57.45 o 5 -15 1 73.97 -40.25 54.54 o 6 -15 1 2.36 25.95 63.28 o 7 -15 1 1.45 140.85 71.75 o -8 -14 1 10.72 -11.65 57.98 o -7 -14 1 0.62 -17.21 54.81 o -6 -14 1 12.32 37.60 86.58 o -5 -14 1 69.80 2.91 46.07 o -4 -14 1 75.32 31.46 43.53 o -3 -14 1 197.02 197.32 73.34 o -2 -14 1 211.12 238.59 57.99 o -1 -14 1 366.12 288.74 55.67 o 0 -14 1 612.23 624.73 72.35 o 1 -14 1 155.77 222.58 84.07 o 2 -14 1 276.95 177.01 81.03 o 3 -14 1 120.19 158.74 54.39 o 4 -14 1 284.09 201.61 47.72 o 5 -14 1 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