#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014991.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014991_Fobs loop_ _publ_author_name 'Senge, Mathias O.' 'Smith, Kevin M.' _publ_section_title ; Hydrogen-bonding patterns in six derivatives of 2,4-dimethylpyrrole ; _journal_coeditor_code FG1869 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o537 _journal_page_last o541 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.310 _cell_angle_gamma 90.000 _cell_length_a 8.1500 _cell_length_b 16.0400 _cell_length_c 7.9080 _exptl_crystal_F_000 448.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file fg1869IVsup5.hkl _[local]_cod_data_source_block 4 #BEGIN Tags that were not found in dictionaries: _shelx_title ' MS165 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 112.29 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 143.62 135.84 5.60 o 2 0 0 80.16 68.88 3.82 o 3 0 0 4964.29 4675.21 290.38 o 4 0 0 1572.30 1484.04 86.30 o 5 0 0 651.89 612.29 28.56 o 6 0 0 30.55 32.80 1.49 o 7 0 0 706.20 672.12 36.44 o 8 0 0 221.74 206.80 13.74 o 9 0 0 26.88 25.53 1.56 o 10 0 0 70.97 66.15 6.42 o 1 1 0 314.96 309.63 29.32 o 2 1 0 11.35 9.75 0.73 o 3 1 0 25.53 26.75 2.32 o 4 1 0 1.85 2.78 0.15 o 5 1 0 109.16 91.68 6.20 o 6 1 0 275.76 238.89 16.56 o 7 1 0 130.51 121.06 7.04 o 8 1 0 6.45 7.35 0.34 o 9 1 0 26.73 23.55 1.51 o 10 1 0 13.61 11.43 0.47 o 0 2 0 4117.72 3602.24 3.16 o 1 2 0 4367.33 4301.38 356.39 o 2 2 0 3117.58 2892.08 251.27 o 3 2 0 196.95 186.00 13.77 o 4 2 0 29.20 33.37 2.38 o 5 2 0 537.04 554.33 42.33 o 6 2 0 119.22 100.51 7.07 o 7 2 0 10.33 9.81 0.71 o 8 2 0 10.81 7.04 0.55 o 9 2 0 42.87 39.82 2.00 o 10 2 0 0.89 0.49 0.27 o 1 3 0 1.35 3.15 0.33 o 2 3 0 3473.43 3229.65 299.18 o 3 3 0 1871.68 1796.23 182.70 o 4 3 0 762.06 813.32 40.95 o 5 3 0 29.73 23.20 2.56 o 6 3 0 499.59 430.73 29.09 o 7 3 0 1.43 1.29 1.07 o 8 3 0 558.24 498.43 38.57 o 9 3 0 47.24 46.97 4.04 o 10 3 0 0.64 0.58 0.28 o 0 4 0 723.06 568.77 1.57 o 1 4 0 117.75 105.45 8.30 o 2 4 0 653.20 636.97 92.32 o 3 4 0 393.04 372.52 40.92 o 4 4 0 165.74 183.94 17.52 o 5 4 0 1.40 2.97 0.24 o 6 4 0 1.95 4.56 0.87 o 7 4 0 20.93 19.62 2.34 o 8 4 0 142.73 121.57 8.85 o 9 4 0 9.97 8.71 0.39 o 10 4 0 0.87 0.91 0.28 o 1 5 0 520.81 576.53 40.92 o 2 5 0 341.33 350.02 45.40 o 3 5 0 123.94 107.39 13.84 o 4 5 0 7.45 6.67 0.63 o 5 5 0 26.32 28.77 3.14 o 6 5 0 9.12 9.61 0.97 o 7 5 0 245.67 234.29 17.61 o 8 5 0 0.04 0.32 0.22 o 9 5 0 62.63 49.59 3.74 o 10 5 0 20.10 21.54 1.04 o 0 6 0 454.65 500.22 1.81 o 1 6 0 5.14 5.91 0.40 o 2 6 0 2643.78 2607.30 273.22 o 3 6 0 68.58 100.42 14.63 o 4 6 0 43.47 45.98 5.43 o 5 6 0 142.97 154.22 17.11 o 6 6 0 481.95 443.56 43.39 o 7 6 0 159.39 156.29 15.05 o 8 6 0 9.87 9.11 0.39 o 9 6 0 1.69 1.78 0.34 o 10 6 0 53.42 56.46 3.62 o 1 7 0 815.34 741.88 48.00 o 2 7 0 10.30 14.46 0.51 o 3 7 0 111.67 109.36 15.57 o 4 7 0 65.62 57.84 6.44 o 5 7 0 19.57 21.14 2.67 o 6 7 0 12.06 9.28 1.09 o 7 7 0 27.53 32.24 2.21 o 8 7 0 1.59 2.15 0.27 o 9 7 0 0.56 0.73 0.67 o 0 8 0 8035.96 7532.39 8.80 o 1 8 0 392.41 353.56 14.94 o 2 8 0 512.58 616.05 56.40 o 3 8 0 1344.32 1409.91 168.35 o 4 8 0 92.43 100.82 14.45 o 5 8 0 46.23 54.03 7.42 o 6 8 0 473.96 483.26 53.72 o 7 8 0 528.31 485.53 38.95 o 8 8 0 9.16 9.13 0.54 o 9 8 0 24.57 24.84 1.83 o 1 9 0 509.37 548.20 24.02 o 2 9 0 3.00 2.56 0.35 o 3 9 0 1.28 3.31 0.53 o 4 9 0 8.24 11.63 1.29 o 5 9 0 53.05 59.34 7.66 o 6 9 0 135.37 120.33 13.31 o 7 9 0 24.16 21.70 2.19 o 8 9 0 8.48 8.00 0.50 o 9 9 0 5.33 5.64 0.44 o 0 10 0 604.50 583.15 2.58 o 1 10 0 3.39 5.49 0.46 o 2 10 0 129.39 132.06 10.36 o 3 10 0 49.36 63.91 7.19 o 4 10 0 3.81 5.67 0.64 o 5 10 0 244.57 241.57 31.73 o 6 10 0 85.91 84.23 9.22 o 7 10 0 7.08 7.25 0.89 o 8 10 0 4.36 4.69 0.35 o 9 10 0 0.06 0.14 0.35 o 1 11 0 307.49 307.07 9.93 o 2 11 0 22.34 23.21 2.13 o 3 11 0 381.55 370.10 38.59 o 4 11 0 228.32 246.26 33.00 o 5 11 0 122.69 111.43 13.75 o 6 11 0 48.75 46.62 5.76 o 7 11 0 69.02 71.60 7.88 o 8 11 0 34.60 29.12 2.66 o 0 12 0 16.75 23.34 0.61 o 1 12 0 20.63 22.98 0.44 o 2 12 0 0.01 0.31 0.16 o 3 12 0 146.26 128.86 13.03 o 4 12 0 20.93 21.70 2.03 o 5 12 0 1.86 3.10 0.72 o 6 12 0 51.38 46.46 5.50 o 7 12 0 28.26 26.56 2.76 o 8 12 0 3.60 2.27 0.33 o 1 13 0 69.55 67.76 1.95 o 2 13 0 21.30 12.39 0.70 o 3 13 0 739.13 692.78 68.50 o 4 13 0 70.25 66.21 8.00 o 5 13 0 73.43 71.52 9.97 o 6 13 0 1.04 1.73 0.26 o 7 13 0 2.71 4.14 0.71 o 8 13 0 35.84 36.85 3.23 o 0 14 0 220.68 187.83 1.82 o 1 14 0 176.94 159.36 4.40 o 2 14 0 40.50 33.59 1.75 o 3 14 0 257.05 242.22 20.96 o 4 14 0 271.79 246.20 26.79 o 5 14 0 13.83 17.62 1.26 o 6 14 0 0.76 0.36 0.27 o 7 14 0 19.58 21.32 3.07 o 1 15 0 330.85 315.08 8.43 o 2 15 0 1.70 1.68 0.24 o 3 15 0 23.39 23.35 2.23 o 4 15 0 245.78 237.70 27.82 o 5 15 0 1.80 2.99 0.42 o 6 15 0 110.30 109.55 11.72 o 7 15 0 59.64 64.50 7.28 o 0 16 0 0.16 0.34 0.32 o 1 16 0 254.19 230.01 5.18 o 2 16 0 17.01 20.89 0.95 o 3 16 0 26.93 26.86 0.84 o 4 16 0 69.19 64.39 5.05 o 5 16 0 27.75 32.64 4.08 o 6 16 0 61.66 67.51 7.86 o 1 17 0 8.89 11.13 0.43 o 2 17 0 0.85 1.31 0.25 o 3 17 0 0.91 1.96 0.29 o 4 17 0 2.10 2.64 0.47 o 5 17 0 11.80 14.96 2.16 o 6 17 0 42.26 42.49 5.96 o 0 18 0 211.51 209.96 2.27 o 1 18 0 1.74 0.88 0.27 o 2 18 0 85.01 80.19 3.64 o 3 18 0 41.40 37.50 3.28 o 4 18 0 4.15 4.24 0.35 o 5 18 0 48.65 48.48 5.54 o 1 19 0 17.42 19.65 0.57 o 2 19 0 11.20 10.77 0.46 o 3 19 0 0.69 0.68 0.76 o 4 19 0 67.74 69.53 6.91 o 0 20 0 27.31 25.53 0.93 o 1 20 0 0.62 0.80 0.40 o 2 20 0 9.57 9.78 0.46 o -10 1 1 11.14 10.77 0.66 o -9 1 1 11.39 7.10 0.53 o -8 1 1 77.59 60.49 1.14 o -7 1 1 0.29 1.09 0.28 o -6 1 1 725.24 678.65 3.09 o -5 1 1 113.36 104.63 1.09 o -4 1 1 2981.65 2671.49 5.01 o -3 1 1 69.08 58.43 0.63 o -2 1 1 890.81 796.70 1.96 o -1 1 1 149.53 157.85 0.69 o 0 1 1 623.96 632.54 1.25 o 1 1 1 2771.29 3180.32 3.47 o 2 1 1 294.88 325.19 1.28 o 3 1 1 143.68 171.26 1.11 o 4 1 1 23.94 21.54 0.47 o 5 1 1 1425.74 1436.90 4.15 o 6 1 1 20.32 21.12 0.60 o 7 1 1 210.73 206.90 1.91 o 8 1 1 26.43 23.72 0.75 o 9 1 1 7.74 6.62 0.54 o 10 1 1 0.00 -0.08 0.37 o -10 2 1 33.09 31.96 1.00 o -9 2 1 1.30 2.47 0.40 o -8 2 1 334.86 296.21 2.46 o -7 2 1 220.14 201.77 1.86 o -6 2 1 54.71 46.33 0.83 o -5 2 1 6.42 1.86 0.23 o -4 2 1 12.84 17.77 0.42 o -3 2 1 374.01 317.14 1.49 o -2 2 1 199.58 216.71 1.04 o -1 2 1 397.96 345.97 1.11 o 0 2 1 6206.62 6361.73 5.04 o 1 2 1 1314.55 1523.77 2.47 o 2 2 1 73.09 83.69 0.67 o 3 2 1 866.30 889.96 2.57 o 4 2 1 60.67 67.42 0.82 o 5 2 1 73.50 69.80 0.93 o 6 2 1 22.24 19.36 0.58 o 7 2 1 140.19 135.32 1.56 o 8 2 1 20.05 20.76 0.72 o 9 2 1 102.82 104.62 1.63 o 10 2 1 11.14 13.23 0.72 o -10 3 1 6.18 7.13 0.54 o -9 3 1 10.01 14.04 0.66 o -8 3 1 204.67 165.03 1.85 o -7 3 1 69.82 60.23 1.05 o -6 3 1 1.86 3.44 0.31 o -5 3 1 157.84 143.92 1.31 o -4 3 1 185.94 219.09 1.44 o -3 3 1 313.11 291.90 1.47 o -2 3 1 610.79 484.79 1.66 o -1 3 1 15.63 18.64 0.29 o 0 3 1 720.94 675.04 1.63 o 1 3 1 4183.11 4685.11 4.92 o 2 3 1 748.61 859.19 2.27 o 3 3 1 601.47 617.42 2.20 o 4 3 1 542.12 615.20 2.47 o 5 3 1 36.11 36.58 0.70 o 6 3 1 80.71 81.42 1.12 o 7 3 1 187.34 186.56 1.84 o 8 3 1 76.43 77.91 1.31 o 9 3 1 181.67 182.92 2.15 o 10 3 1 1.69 3.06 0.48 o -10 4 1 20.28 24.45 0.90 o -9 4 1 28.81 28.22 0.88 o -8 4 1 24.41 25.60 0.77 o -7 4 1 9.87 9.34 0.48 o -6 4 1 205.54 203.88 1.74 o -5 4 1 3.10 3.03 0.26 o -4 4 1 104.14 94.16 0.98 o -3 4 1 2390.04 2215.11 4.30 o -2 4 1 666.88 576.47 1.92 o -1 4 1 302.94 286.63 1.22 o 0 4 1 38.90 33.82 0.41 o 1 4 1 54.92 81.01 0.66 o 2 4 1 359.26 385.63 1.60 o 3 4 1 0.00 0.27 0.15 o 4 4 1 788.94 885.91 3.04 o 5 4 1 106.74 122.15 1.26 o 6 4 1 99.01 95.96 1.23 o 7 4 1 192.22 191.80 1.89 o 8 4 1 9.81 12.50 0.61 o 9 4 1 43.94 46.73 1.15 o 10 4 1 6.76 7.76 0.62 o -10 5 1 10.07 10.56 0.67 o -9 5 1 82.20 76.57 1.41 o -8 5 1 30.76 26.92 0.81 o -7 5 1 67.11 56.05 1.03 o -6 5 1 262.91 230.97 1.89 o -5 5 1 44.59 36.69 0.71 o -4 5 1 205.01 202.06 1.47 o -3 5 1 45.70 44.44 0.63 o -2 5 1 288.05 311.67 1.49 o -1 5 1 295.88 277.42 1.30 o 0 5 1 1066.49 1047.70 2.49 o 1 5 1 599.52 680.89 2.07 o 2 5 1 223.61 268.43 1.41 o 3 5 1 188.74 226.66 1.43 o 4 5 1 293.23 327.35 1.90 o 5 5 1 0.27 -0.07 0.22 o 6 5 1 91.41 92.42 1.23 o 7 5 1 175.75 172.93 1.82 o 8 5 1 46.71 45.13 1.04 o 9 5 1 157.62 156.20 2.03 o 10 5 1 61.73 66.02 1.45 o -10 6 1 27.38 25.40 0.93 o -9 6 1 9.68 10.58 0.61 o -8 6 1 201.95 167.18 1.94 o -7 6 1 18.92 13.47 0.56 o -6 6 1 282.58 226.75 1.91 o -5 6 1 1902.94 1653.04 4.78 o -4 6 1 177.48 214.82 1.56 o -3 6 1 5.39 3.86 0.23 o -2 6 1 2929.76 2836.56 4.92 o -1 6 1 481.42 514.71 1.92 o 0 6 1 0.04 2.61 0.17 o 1 6 1 0.28 1.07 0.14 o 2 6 1 83.57 118.32 1.00 o 3 6 1 525.06 683.47 2.59 o 4 6 1 16.35 27.95 0.60 o 5 6 1 35.41 43.59 0.81 o 6 6 1 667.86 705.36 3.42 o 7 6 1 220.50 226.48 2.11 o 8 6 1 2.72 3.32 0.43 o 9 6 1 81.49 91.81 1.59 o -9 7 1 6.97 9.18 0.59 o -8 7 1 46.10 39.18 0.99 o -7 7 1 42.26 38.00 0.90 o -6 7 1 496.61 422.49 2.67 o -5 7 1 13.50 8.16 0.41 o -4 7 1 0.48 1.07 0.20 o -3 7 1 61.55 52.56 0.75 o -2 7 1 0.49 0.89 0.16 o -1 7 1 191.49 165.43 1.17 o 0 7 1 29.05 42.22 0.59 o 1 7 1 27.41 25.61 0.48 o 2 7 1 77.32 70.49 0.82 o 3 7 1 303.66 368.86 1.99 o 4 7 1 56.86 55.44 0.86 o 5 7 1 4.30 9.88 0.45 o 6 7 1 47.49 51.10 0.98 o 7 7 1 301.02 310.40 2.52 o 8 7 1 16.44 18.36 0.74 o 9 7 1 0.13 -0.39 0.41 o -9 8 1 54.48 58.10 1.29 o -8 8 1 11.74 11.04 0.59 o -7 8 1 2.71 4.29 0.41 o -6 8 1 56.86 53.47 1.00 o -5 8 1 22.71 20.90 0.61 o -4 8 1 20.05 15.40 0.48 o -3 8 1 79.39 81.82 0.98 o -2 8 1 33.92 41.50 0.66 o -1 8 1 32.85 40.60 0.63 o 0 8 1 246.00 274.48 1.58 o 1 8 1 11.67 17.16 0.43 o 2 8 1 72.89 75.70 0.89 o 3 8 1 155.47 159.65 1.38 o 4 8 1 10.16 10.65 0.44 o 5 8 1 269.27 306.67 2.20 o 6 8 1 342.93 359.04 2.56 o 7 8 1 64.85 63.84 1.20 o 8 8 1 4.48 4.48 0.49 o 9 8 1 2.13 2.17 0.43 o -9 9 1 45.42 44.42 1.17 o -8 9 1 5.98 5.15 0.47 o -7 9 1 173.41 170.12 1.92 o -6 9 1 828.87 693.65 3.60 o -5 9 1 291.45 251.30 2.02 o -4 9 1 462.08 410.87 2.41 o -3 9 1 99.13 100.56 1.13 o -2 9 1 418.63 364.51 2.03 o -1 9 1 0.83 0.57 0.16 o 0 9 1 283.93 311.04 1.80 o 1 9 1 911.66 963.47 3.22 o 2 9 1 190.86 220.90 1.60 o 3 9 1 360.40 392.69 2.24 o 4 9 1 117.31 120.10 1.33 o 5 9 1 377.45 438.29 2.70 o 6 9 1 331.84 349.86 2.59 o 7 9 1 183.93 198.09 2.10 o 8 9 1 12.54 15.69 0.72 o 9 9 1 3.10 4.07 0.53 o -9 10 1 0.00 0.17 0.37 o -8 10 1 44.31 39.31 1.05 o -7 10 1 205.66 185.95 2.06 o -6 10 1 19.67 13.44 0.59 o -5 10 1 113.49 97.42 1.31 o -4 10 1 214.78 201.13 1.76 o -3 10 1 201.35 184.43 1.60 o -2 10 1 9.20 6.80 0.33 o -1 10 1 459.70 437.40 2.28 o 0 10 1 322.09 333.23 1.97 o 1 10 1 0.18 0.18 0.20 o 2 10 1 200.15 220.81 1.68 o 3 10 1 205.63 228.28 1.79 o 4 10 1 6.20 6.61 0.40 o 5 10 1 44.19 48.04 0.96 o 6 10 1 4.69 8.20 0.51 o 7 10 1 108.81 102.57 1.56 o 8 10 1 89.72 96.01 1.64 o 9 10 1 8.14 8.31 0.66 o -8 11 1 6.36 4.97 0.50 o -7 11 1 85.02 77.68 1.38 o -6 11 1 4.19 4.08 0.40 o -5 11 1 22.30 19.41 0.65 o -4 11 1 116.64 106.47 1.34 o -3 11 1 74.04 54.51 0.92 o -2 11 1 1.65 2.03 0.25 o -1 11 1 24.70 23.54 0.58 o 0 11 1 57.13 48.26 0.84 o 1 11 1 331.52 343.14 2.13 o 2 11 1 85.30 90.49 1.14 o 3 11 1 97.18 103.99 1.27 o 4 11 1 725.47 801.43 3.68 o 5 11 1 2.85 2.09 0.34 o 6 11 1 7.29 8.33 0.53 o 7 11 1 107.87 115.15 1.70 o 8 11 1 72.00 76.92 1.49 o -8 12 1 10.29 9.21 0.61 o -7 12 1 87.03 78.45 1.43 o -6 12 1 72.15 70.97 1.27 o -5 12 1 117.50 91.88 1.37 o -4 12 1 0.12 1.11 0.30 o -3 12 1 2469.53 2054.90 5.87 o -2 12 1 664.68 661.00 3.18 o -1 12 1 126.39 114.01 1.30 o 0 12 1 1177.26 1127.25 4.05 o 1 12 1 669.69 624.16 3.03 o 2 12 1 116.95 127.20 1.41 o 3 12 1 59.91 86.99 1.22 o 4 12 1 1253.99 1335.18 4.94 o 5 12 1 0.85 3.04 0.39 o 6 12 1 13.11 14.62 0.67 o 7 12 1 14.86 17.16 0.76 o 8 12 1 188.67 206.43 2.46 o -8 13 1 4.72 4.40 0.51 o -7 13 1 10.23 10.36 0.62 o -6 13 1 9.90 9.06 0.56 o -5 13 1 22.16 18.90 0.69 o -4 13 1 127.92 123.07 1.55 o -3 13 1 114.81 106.39 1.40 o -2 13 1 10.27 6.66 0.41 o -1 13 1 82.04 59.63 1.00 o 0 13 1 30.49 24.94 0.75 o 1 13 1 0.82 0.61 0.31 o 2 13 1 3.88 3.78 0.35 o 3 13 1 436.20 448.45 2.85 o 4 13 1 98.77 108.15 1.48 o 5 13 1 0.15 -0.23 0.34 o 6 13 1 29.93 33.79 0.94 o 7 13 1 0.66 1.47 0.41 o 8 13 1 6.79 9.74 0.68 o -7 14 1 57.14 58.05 1.32 o -6 14 1 12.64 11.50 0.62 o -5 14 1 258.24 240.41 2.35 o -4 14 1 352.47 293.01 2.48 o -3 14 1 37.33 28.10 0.79 o -2 14 1 341.03 302.96 2.36 o -1 14 1 220.18 179.00 1.78 o 0 14 1 235.89 219.58 1.97 o 1 14 1 395.10 383.83 2.61 o 2 14 1 240.38 224.68 2.04 o 3 14 1 39.90 42.76 0.95 o 4 14 1 114.87 112.13 1.56 o 5 14 1 112.94 121.90 1.70 o 6 14 1 49.27 61.10 1.29 o 7 14 1 0.52 1.39 0.43 o -7 15 1 24.85 23.59 0.89 o -6 15 1 24.74 23.54 0.87 o -5 15 1 29.81 23.65 0.81 o -4 15 1 60.83 60.87 1.20 o -3 15 1 8.81 6.07 0.45 o -2 15 1 7.73 5.12 0.41 o -1 15 1 59.30 52.83 1.04 o 0 15 1 138.49 119.07 1.52 o 1 15 1 49.44 36.71 0.97 o 2 15 1 20.37 23.12 0.74 o 3 15 1 31.33 34.98 0.90 o 4 15 1 16.93 16.97 0.70 o 5 15 1 143.19 162.62 2.03 o 6 15 1 43.67 46.85 1.17 o 7 15 1 19.32 23.77 0.92 o -6 16 1 3.47 3.48 0.48 o -5 16 1 24.98 22.43 0.84 o -4 16 1 9.69 10.04 0.58 o -3 16 1 0.71 0.44 0.32 o -2 16 1 1.93 2.89 0.39 o -1 16 1 10.76 9.96 0.53 o 0 16 1 8.73 10.02 0.55 o 1 16 1 7.87 6.36 0.50 o 2 16 1 8.20 9.49 0.56 o 3 16 1 2.56 3.56 0.43 o 4 16 1 4.91 5.82 0.51 o 5 16 1 140.59 154.10 2.04 o 6 16 1 114.53 126.35 1.94 o -6 17 1 44.25 40.81 1.16 o -5 17 1 18.15 18.09 0.79 o -4 17 1 36.58 31.37 0.96 o -3 17 1 3.72 3.28 0.42 o -2 17 1 1.58 1.67 0.36 o -1 17 1 13.52 9.03 0.56 o 0 17 1 46.15 37.38 0.97 o 1 17 1 0.22 0.69 0.34 o 2 17 1 28.59 23.38 0.81 o 3 17 1 14.26 14.50 0.69 o 4 17 1 3.29 3.81 0.49 o 5 17 1 15.12 17.75 0.80 o -5 18 1 48.72 45.61 1.21 o -4 18 1 3.40 4.04 0.48 o -3 18 1 20.14 17.04 0.75 o -2 18 1 5.28 6.33 0.51 o -1 18 1 26.90 26.80 0.88 o 0 18 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