#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/50/2015039.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015039_Fobs loop_ _publ_author_name 'Blewett, Gavin' 'Bredenkamp, Martin W.' 'Koch, Klaus R.' _publ_section_title ; Polymorphism in bipodal O,O'-dimethyl N,N'-(m-phenylenedicarbonyl)bis(thiocarbamate) ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o469 _journal_page_last o472 _journal_volume 61 _journal_year 2005 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.435 _cell_angle_gamma 90.000 _cell_length_a 19.3359 _cell_length_b 8.2864 _cell_length_c 8.6590 _exptl_crystal_F_000 648.00 _reflns_d_resolution_high 0.7802 _[local]_cod_data_source_file rb1007Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2F001WM in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 277.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 84.33 97.17 6.73 o 4 0 0 9705.74 9982.06 326.79 o 6 0 0 7552.38 7683.73 168.87 o 8 0 0 114.24 96.25 9.89 o 10 0 0 0.32 7.97 7.54 o 12 0 0 3693.77 3507.79 123.40 o 14 0 0 2667.87 2550.32 97.27 o 16 0 0 3278.37 3162.33 118.92 o 18 0 0 3335.81 3108.69 120.82 o 20 0 0 421.42 384.26 37.08 o 22 0 0 31.11 18.71 17.94 o 24 0 0 566.32 517.58 45.01 o 1 1 0 7810.47 8185.41 123.45 o 3 1 0 1520.44 1494.31 22.08 o 5 1 0 6674.79 7470.27 114.92 o 7 1 0 1813.92 1725.52 30.88 o 9 1 0 6010.56 6015.34 95.66 o 11 1 0 1098.65 1031.13 35.45 o 13 1 0 1683.94 1658.67 39.93 o 15 1 0 0.51 -5.09 9.82 o 17 1 0 56.04 54.98 13.81 o 19 1 0 119.34 129.41 47.34 o 21 1 0 465.68 410.56 33.42 o 23 1 0 7.51 38.54 13.32 o 0 2 0 2749.60 2838.80 64.58 o 2 2 0 2721.18 2477.44 35.57 o 4 2 0 667.20 634.07 12.23 o 6 2 0 32.36 25.52 4.07 o 8 2 0 830.98 948.15 21.02 o 10 2 0 3227.98 3446.27 51.95 o 12 2 0 123.23 144.79 9.92 o 14 2 0 0.58 0.36 5.55 o 16 2 0 1498.00 1498.53 49.26 o 18 2 0 40.22 39.65 13.89 o 20 2 0 11.67 17.46 12.25 o 22 2 0 0.29 1.35 11.50 o 24 2 0 0.06 7.50 17.07 o 1 3 0 86.94 109.51 15.62 o 3 3 0 366.78 373.92 9.10 o 5 3 0 694.82 724.87 13.39 o 7 3 0 2088.85 2224.44 34.80 o 9 3 0 2953.40 2834.48 43.85 o 11 3 0 0.95 4.58 4.56 o 13 3 0 265.56 256.09 13.98 o 15 3 0 93.74 106.78 9.63 o 17 3 0 44.75 47.55 26.22 o 19 3 0 120.33 129.57 19.40 o 21 3 0 864.65 785.11 36.80 o 23 3 0 0.53 11.19 12.59 o 0 4 0 28426.43 30777.25 652.86 o 2 4 0 5.64 31.68 4.73 o 4 4 0 4649.17 4465.66 71.86 o 6 4 0 4629.79 4453.63 56.52 o 8 4 0 1180.60 1164.02 21.71 o 10 4 0 329.08 275.97 10.40 o 12 4 0 3233.12 2968.09 89.74 o 14 4 0 1285.40 1210.02 28.60 o 16 4 0 833.22 808.27 26.80 o 18 4 0 486.03 526.53 22.65 o 20 4 0 154.72 158.85 26.47 o 22 4 0 4.13 14.14 12.94 o 1 5 0 109.32 147.55 7.84 o 3 5 0 1.02 2.60 3.53 o 5 5 0 275.54 291.30 8.37 o 7 5 0 183.33 212.16 10.31 o 9 5 0 104.25 112.61 8.58 o 11 5 0 1255.91 1118.01 60.60 o 13 5 0 655.53 689.75 49.10 o 15 5 0 94.01 85.70 11.51 o 17 5 0 33.39 32.87 9.62 o 19 5 0 307.11 358.68 20.36 o 21 5 0 108.91 127.80 24.49 o 0 6 0 1229.02 1039.01 32.86 o 2 6 0 12.27 15.93 5.39 o 4 6 0 457.11 377.73 13.32 o 6 6 0 643.07 641.45 15.24 o 8 6 0 378.21 382.43 14.66 o 10 6 0 3830.98 3622.92 119.43 o 12 6 0 14.05 24.60 8.78 o 14 6 0 365.76 401.04 23.42 o 16 6 0 1716.88 1805.92 70.84 o 18 6 0 84.03 113.20 15.75 o 20 6 0 203.15 260.02 21.92 o 1 7 0 791.12 705.06 20.00 o 3 7 0 2087.49 1851.59 52.90 o 5 7 0 304.14 293.59 15.30 o 7 7 0 315.93 309.14 16.24 o 9 7 0 632.00 660.10 23.30 o 11 7 0 0.02 3.51 9.14 o 13 7 0 537.22 557.12 28.32 o 15 7 0 604.06 635.85 34.54 o 17 7 0 6.84 39.13 11.18 o 0 8 0 8.85 31.99 16.47 o 2 8 0 727.54 594.25 68.00 o 4 8 0 183.16 168.48 16.74 o 6 8 0 599.22 570.27 30.01 o 8 8 0 447.45 476.64 20.72 o 10 8 0 102.23 150.30 30.92 o 12 8 0 563.98 632.36 54.46 o 14 8 0 24.83 64.81 19.06 o 16 8 0 40.56 91.10 14.79 o 1 9 0 25.40 8.77 10.66 o 3 9 0 2.87 3.21 10.43 o 5 9 0 493.26 489.31 27.46 o 7 9 0 39.89 69.76 21.73 o 9 9 0 85.57 88.48 22.68 o 11 9 0 21.24 13.28 16.47 o 0 10 0 862.06 869.68 54.33 o 2 10 0 4.18 13.29 10.77 o 4 10 0 540.59 576.07 52.56 o 6 10 0 212.62 254.05 34.24 o -23 1 1 1594.47 1487.60 55.49 o -21 1 1 390.30 396.73 27.59 o -19 1 1 961.60 851.50 37.31 o -17 1 1 401.40 368.54 24.15 o -15 1 1 383.73 328.19 25.96 o -13 1 1 347.94 315.32 20.09 o -11 1 1 1804.48 1800.32 50.67 o -9 1 1 3107.40 3480.16 84.21 o -7 1 1 5278.66 5294.68 102.40 o -5 1 1 76912.79 84686.23 1477.56 o -3 1 1 2292.43 2935.94 39.54 o -1 1 1 7.00 7.93 2.49 o 1 1 1 17539.88 20055.06 300.87 o 3 1 1 1271.67 1334.67 22.37 o 5 1 1 2755.92 2664.65 39.21 o 7 1 1 2361.41 2173.87 33.72 o 9 1 1 22.88 32.37 4.56 o 11 1 1 7835.15 7857.50 111.76 o 13 1 1 405.24 371.69 14.95 o 15 1 1 199.46 194.33 14.02 o 17 1 1 49.96 61.99 10.99 o 19 1 1 641.60 600.11 30.46 o 21 1 1 1125.22 1086.34 80.97 o 23 1 1 10.22 25.29 12.34 o -24 2 1 50.67 78.55 23.59 o -22 2 1 2.14 12.73 13.44 o -20 2 1 6.08 6.78 12.92 o -18 2 1 672.16 656.51 32.15 o -16 2 1 46.05 43.17 13.44 o -14 2 1 4328.78 4275.38 85.35 o -12 2 1 54.21 44.24 6.37 o -10 2 1 4623.75 4866.43 79.63 o -8 2 1 799.69 969.86 20.80 o -6 2 1 2328.34 2670.88 45.09 o -4 2 1 283.71 336.28 8.65 o -2 2 1 179.27 211.17 7.61 o 0 2 1 640.07 568.62 11.79 o 2 2 1 17562.08 18964.64 254.55 o 4 2 1 2326.71 2350.52 31.66 o 6 2 1 4319.42 4305.13 56.04 o 8 2 1 2477.32 2423.98 34.10 o 10 2 1 638.95 591.36 13.47 o 12 2 1 373.25 339.14 12.85 o 14 2 1 3400.37 3079.07 55.77 o 16 2 1 818.89 770.01 26.34 o 18 2 1 751.92 697.85 26.26 o 20 2 1 594.14 624.99 31.31 o 22 2 1 481.53 474.40 28.38 o -23 3 1 463.72 467.73 30.88 o -21 3 1 7.34 6.87 21.39 o -19 3 1 1080.35 1026.01 75.24 o -17 3 1 886.48 899.79 37.07 o -15 3 1 1130.08 1159.50 32.97 o -13 3 1 0.12 0.69 5.47 o -11 3 1 1525.33 1395.81 29.28 o -9 3 1 1760.76 1755.16 29.62 o -7 3 1 9.27 13.84 4.31 o -5 3 1 11162.11 12167.43 144.41 o -3 3 1 959.06 1025.26 23.65 o -1 3 1 879.82 730.59 15.41 o 1 3 1 4894.26 4964.34 77.80 o 3 3 1 12.86 -3.52 3.52 o 5 3 1 25.44 9.74 3.57 o 7 3 1 2872.27 2841.59 42.91 o 9 3 1 0.01 1.22 3.73 o 11 3 1 938.97 1091.99 24.45 o 13 3 1 55.59 68.62 7.80 o 15 3 1 11.74 14.79 6.59 o 17 3 1 1.01 -3.21 8.11 o 19 3 1 411.32 394.94 20.61 o 21 3 1 501.81 491.68 28.22 o 23 3 1 29.34 43.12 18.37 o -22 4 1 58.65 50.93 15.04 o -20 4 1 272.60 266.85 23.66 o -18 4 1 213.15 236.09 21.58 o -16 4 1 1385.67 1375.90 55.44 o -14 4 1 47.84 42.46 9.41 o -12 4 1 30.00 33.26 6.98 o -10 4 1 29.61 14.93 5.06 o -8 4 1 145.51 128.16 6.88 o -6 4 1 423.54 425.73 9.58 o -4 4 1 4.52 9.49 4.34 o -2 4 1 1028.57 976.79 20.23 o 0 4 1 29.62 35.91 4.71 o 2 4 1 2346.00 2380.44 60.01 o 4 4 1 590.75 513.04 10.28 o 6 4 1 110.80 132.03 7.00 o 8 4 1 202.00 210.67 8.62 o 10 4 1 616.81 647.88 17.92 o 12 4 1 451.46 438.17 15.30 o 14 4 1 264.54 278.44 13.47 o 16 4 1 441.55 377.04 16.28 o 18 4 1 1.98 1.96 8.81 o 20 4 1 607.32 611.75 44.50 o -21 5 1 133.54 173.83 26.34 o -19 5 1 363.51 388.40 35.44 o -17 5 1 165.25 163.62 14.64 o -15 5 1 2277.41 2162.94 52.20 o -13 5 1 1374.44 1338.06 31.09 o -11 5 1 2490.91 2291.15 44.16 o -9 5 1 1418.23 1334.46 31.96 o -7 5 1 2955.99 2825.40 42.82 o -5 5 1 6805.59 6984.91 111.54 o -3 5 1 1341.61 1533.09 36.96 o -1 5 1 973.69 736.44 17.48 o 1 5 1 1864.45 1798.12 33.43 o 3 5 1 803.73 759.49 19.70 o 5 5 1 3375.67 3170.11 41.99 o 7 5 1 3187.25 2991.05 46.73 o 9 5 1 746.30 742.35 24.43 o 11 5 1 8776.04 8993.80 144.22 o 13 5 1 16.65 27.37 14.96 o 15 5 1 1056.82 1024.44 83.56 o 17 5 1 315.92 349.73 22.41 o 19 5 1 9.60 33.98 16.38 o -20 6 1 441.28 545.94 29.73 o -18 6 1 232.63 295.17 18.88 o -16 6 1 8.62 24.30 9.04 o -14 6 1 304.99 299.64 17.55 o -12 6 1 56.87 64.15 8.62 o -10 6 1 301.05 324.66 14.26 o -8 6 1 122.18 103.84 7.62 o -6 6 1 32.92 25.06 5.38 o -4 6 1 714.22 626.89 17.39 o -2 6 1 2522.32 2300.66 42.40 o 0 6 1 0.43 3.13 4.83 o 2 6 1 3296.35 3124.18 62.44 o 4 6 1 252.15 227.44 12.90 o 6 6 1 2400.66 2273.69 49.80 o 8 6 1 1294.94 1231.95 32.25 o 10 6 1 290.92 327.92 38.42 o 12 6 1 92.60 84.27 14.57 o 14 6 1 1083.73 1079.10 40.30 o 16 6 1 1066.35 1092.59 41.53 o 18 6 1 81.27 115.08 19.70 o -17 7 1 221.64 332.04 47.21 o -15 7 1 644.31 677.43 31.43 o -13 7 1 12.45 25.52 9.90 o -11 7 1 389.01 380.80 16.30 o -9 7 1 65.30 59.14 7.21 o -7 7 1 213.21 215.41 10.16 o -5 7 1 65.20 38.64 8.67 o -3 7 1 81.86 66.70 9.34 o -1 7 1 6.22 13.35 7.19 o 1 7 1 5.83 3.29 6.73 o 3 7 1 305.32 282.55 15.16 o 5 7 1 508.74 435.92 18.34 o 7 7 1 464.65 419.58 20.62 o 9 7 1 153.95 178.96 17.41 o 11 7 1 1105.68 1164.69 50.66 o 13 7 1 18.50 36.95 11.63 o 15 7 1 64.86 97.81 15.46 o 17 7 1 45.38 78.22 16.08 o -16 8 1 220.60 306.91 34.41 o -14 8 1 212.85 302.51 34.24 o -12 8 1 1.02 -5.61 12.33 o -10 8 1 708.70 636.95 30.88 o -8 8 1 526.89 455.01 25.70 o -6 8 1 1.61 -4.08 9.56 o -4 8 1 516.96 498.02 27.21 o -2 8 1 737.04 666.11 36.60 o 0 8 1 343.92 315.49 16.44 o 2 8 1 280.86 257.93 15.29 o 4 8 1 503.19 463.23 20.05 o 6 8 1 87.64 85.40 14.83 o 8 8 1 402.88 460.14 28.16 o 10 8 1 2.62 -0.14 8.62 o 12 8 1 0.37 28.34 10.38 o 14 8 1 14.26 14.23 16.13 o -11 9 1 386.69 570.88 44.15 o -9 9 1 138.28 177.13 27.68 o -7 9 1 724.73 684.35 33.04 o -5 9 1 249.81 266.21 28.41 o -3 9 1 28.51 11.11 10.53 o -1 9 1 1459.18 1317.02 47.05 o 1 9 1 145.25 158.85 17.73 o 3 9 1 3.62 0.50 10.27 o 5 9 1 762.33 827.86 52.17 o 7 9 1 310.49 215.33 30.01 o 9 9 1 107.26 154.89 22.85 o 11 9 1 1382.63 1588.89 66.19 o -6 10 1 41.33 53.94 15.60 o -4 10 1 230.82 237.78 22.29 o -2 10 1 132.24 164.04 19.57 o 0 10 1 25.03 42.10 13.59 o 2 10 1 385.93 394.41 26.82 o 4 10 1 322.89 345.46 37.34 o 6 10 1 58.77 63.73 23.20 o -24 0 2 353.10 381.33 41.57 o -22 0 2 417.78 390.39 37.94 o -20 0 2 272.14 216.36 31.39 o -18 0 2 558.68 545.78 42.51 o -16 0 2 2006.25 2134.23 90.55 o -14 0 2 68.48 95.38 19.75 o -12 0 2 5223.30 5198.08 175.32 o -10 0 2 14671.41 16015.34 496.46 o -8 0 2 1369.68 1705.90 65.37 o -6 0 2 4533.25 6014.99 191.01 o -4 0 2 69351.30 80997.44 2458.65 o -2 0 2 16.42 10.43 6.73 o 2 0 2 1423.85 1737.03 33.33 o 4 0 2 13717.20 15572.11 271.34 o 6 0 2 7311.30 7555.85 134.78 o 8 0 2 332.64 355.48 19.68 o 10 0 2 34.91 15.78 11.77 o 12 0 2 261.53 243.55 18.93 o 14 0 2 1289.83 1215.36 41.27 o 16 0 2 4799.72 4714.53 118.48 o 18 0 2 46.10 25.53 12.89 o 20 0 2 1.95 -5.00 14.83 o 22 0 2 4177.35 4148.00 157.38 o -23 1 2 9.51 24.81 14.24 o -21 1 2 123.97 139.24 42.86 o -19 1 2 190.97 197.12 20.67 o -17 1 2 294.66 311.62 23.16 o -15 1 2 271.41 314.84 21.95 o -13 1 2 0.96 1.25 9.29 o -11 1 2 287.33 292.01 18.41 o -9 1 2 2689.54 2686.15 89.34 o -7 1 2 14.81 12.70 7.22 o -5 1 2 13426.80 15923.44 316.16 o -3 1 2 4154.77 4567.45 82.74 o -1 1 2 1802.77 2152.17 40.59 o 1 1 2 572.35 539.74 24.57 o 3 1 2 1921.52 1841.16 30.97 o 5 1 2 4470.26 4744.90 67.30 o 7 1 2 2223.13 2180.48 60.43 o 9 1 2 7614.13 8002.18 112.72 o 11 1 2 7.79 13.37 4.92 o 13 1 2 1712.22 1591.79 35.33 o 15 1 2 309.11 264.29 13.96 o 17 1 2 114.84 106.60 10.89 o 19 1 2 5.72 5.84 12.07 o 21 1 2 112.11 141.11 15.36 o 23 1 2 108.22 177.41 19.47 o -24 2 2 9.00 21.00 15.66 o -22 2 2 26.14 31.77 30.18 o -20 2 2 592.70 540.19 31.39 o -18 2 2 22.96 6.02 12.51 o -16 2 2 87.92 74.61 10.39 o -14 2 2 308.77 302.33 19.80 o -12 2 2 1731.28 1506.11 103.76 o -10 2 2 802.19 791.67 22.95 o -8 2 2 618.99 636.97 27.87 o -6 2 2 155.28 132.67 6.30 o -4 2 2 75.09 90.72 13.47 o -2 2 2 900.89 894.84 36.44 o 0 2 2 99.90 97.64 5.32 o 2 2 2 11.24 11.48 3.52 o 4 2 2 29.22 36.61 3.08 o 6 2 2 16372.23 18741.79 254.57 o 8 2 2 57.38 74.50 5.92 o 10 2 2 121.74 118.71 9.99 o 12 2 2 377.22 435.19 13.24 o 14 2 2 6.66 1.18 6.63 o 16 2 2 3.43 -0.77 8.76 o 18 2 2 0.01 8.92 8.81 o 20 2 2 0.08 -3.51 8.62 o 22 2 2 194.42 200.22 17.28 o -23 3 2 12.26 52.85 16.06 o -21 3 2 1035.65 1047.01 45.09 o -19 3 2 393.63 393.62 27.35 o -17 3 2 852.00 740.16 86.49 o -15 3 2 1034.90 1004.94 30.37 o -13 3 2 96.17 120.58 9.67 o -11 3 2 47.65 56.45 7.04 o -9 3 2 371.13 317.82 12.13 o -7 3 2 908.51 856.88 16.88 o -5 3 2 4202.09 4590.33 74.17 o -3 3 2 14383.96 15619.57 236.91 o -1 3 2 0.43 5.60 3.27 o 1 3 2 7476.72 8153.16 125.51 o 3 3 2 458.57 420.17 9.51 o 5 3 2 26.66 65.99 6.25 o 7 3 2 152.75 140.10 6.81 o 9 3 2 1996.39 1828.75 31.38 o 11 3 2 408.42 359.05 13.35 o 13 3 2 1764.99 1686.23 34.77 o 15 3 2 1408.49 1314.93 35.92 o 17 3 2 38.97 29.79 11.31 o 19 3 2 138.45 183.64 15.66 o 21 3 2 94.56 137.35 18.85 o -22 4 2 102.46 139.03 19.47 o -20 4 2 41.19 30.49 13.73 o -18 4 2 515.61 533.86 29.81 o -16 4 2 2217.27 2043.23 62.41 o -14 4 2 297.89 276.70 13.65 o -12 4 2 2738.73 2618.35 49.26 o -10 4 2 2629.66 2545.79 47.29 o -8 4 2 1312.34 1414.62 25.12 o -6 4 2 0.50 24.86 6.11 o -4 4 2 4347.13 4792.24 77.67 o -2 4 2 0.11 1.73 3.61 o 0 4 2 3816.41 3530.18 58.00 o 2 4 2 3775.87 3728.51 50.91 o 4 4 2 170.36 133.65 8.04 o 6 4 2 1691.72 1385.52 24.14 o 8 4 2 342.82 337.02 12.31 o 10 4 2 718.97 728.42 19.44 o 12 4 2 319.07 300.40 13.41 o 14 4 2 0.61 1.48 6.96 o 16 4 2 1720.53 1672.44 54.42 o 18 4 2 174.96 195.49 21.69 o 20 4 2 30.15 24.67 23.02 o -21 5 2 55.37 92.68 17.16 o -19 5 2 4.36 18.87 21.73 o -17 5 2 80.97 106.96 14.42 o -15 5 2 29.01 22.84 7.71 o -13 5 2 4.30 2.65 6.34 o -11 5 2 61.31 61.54 8.22 o -9 5 2 915.98 829.30 18.25 o -7 5 2 150.59 164.73 8.16 o -5 5 2 571.05 592.28 18.60 o -3 5 2 221.92 195.68 9.19 o -1 5 2 123.57 132.51 7.63 o 1 5 2 292.07 250.64 12.44 o 3 5 2 1729.88 1578.80 35.99 o 5 5 2 1158.21 1123.56 24.62 o 7 5 2 1542.00 1496.18 56.79 o 9 5 2 2106.37 2034.70 46.78 o 11 5 2 134.37 127.33 11.66 o 13 5 2 12.37 8.05 7.50 o 15 5 2 87.54 105.05 14.79 o 17 5 2 91.87 126.51 22.68 o 19 5 2 124.81 155.22 24.58 o -20 6 2 729.35 794.86 57.04 o -18 6 2 491.04 546.30 31.10 o -16 6 2 18.26 18.19 8.61 o -14 6 2 808.55 744.34 22.85 o -12 6 2 1079.12 1063.06 27.25 o -10 6 2 602.12 553.88 15.48 o -8 6 2 1054.44 992.71 23.17 o -6 6 2 462.37 422.43 17.94 o -4 6 2 9.36 10.89 7.00 o -2 6 2 89.46 87.18 9.33 o 0 6 2 1468.08 1175.62 68.01 o 2 6 2 937.81 902.56 50.33 o 4 6 2 112.68 116.39 13.53 o 6 6 2 10933.02 10839.59 191.30 o 8 6 2 661.74 599.47 42.13 o 10 6 2 359.05 331.05 21.26 o 12 6 2 702.31 727.87 32.13 o 14 6 2 3.14 10.31 9.57 o 16 6 2 210.71 216.14 18.93 o 18 6 2 408.42 458.60 37.43 o -17 7 2 223.31 229.66 21.56 o -15 7 2 714.36 734.05 34.66 o -13 7 2 22.01 26.65 12.76 o -11 7 2 86.04 80.22 11.63 o -9 7 2 763.64 756.65 21.19 o -7 7 2 1697.84 1538.57 41.46 o -5 7 2 0.16 2.59 7.21 o -3 7 2 3726.54 3555.12 74.12 o -1 7 2 198.94 179.25 12.89 o 1 7 2 3234.10 2984.87 63.86 o 3 7 2 763.98 728.01 24.07 o 5 7 2 46.03 42.35 8.86 o 7 7 2 208.35 194.95 17.94 o 9 7 2 1008.45 933.38 46.35 o 11 7 2 907.09 900.12 39.32 o 13 7 2 561.66 634.57 79.77 o 15 7 2 754.28 810.27 36.04 o 17 7 2 119.71 191.10 27.25 o -16 8 2 364.56 440.66 39.06 o -14 8 2 0.03 -3.36 13.71 o -12 8 2 830.68 860.11 53.47 o -10 8 2 53.88 71.85 9.52 o -8 8 2 61.66 61.50 8.76 o -6 8 2 877.01 794.47 45.74 o -4 8 2 224.88 182.40 13.91 o -2 8 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