#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/50/2015044.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015044_Fobs loop_ _publ_author_name 'Gainsford, Graeme J.' 'Kemmitt, Tim' _publ_section_title ; catena-Poly[sodium(I)-\m-tetraethoxyborato] ; _journal_coeditor_code SF1008 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m417 _journal_page_last m418 _journal_volume 61 _journal_year 2005 _space_group_IT_number 18 _symmetry_space_group_name_Hall 'P 2 2ab' _symmetry_space_group_name_H-M 'P 21 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.6330 _cell_length_b 15.2720 _cell_length_c 5.7440 _exptl_crystal_F_000 232.00 _reflns_d_resolution_high 0.8009 _[local]_cod_data_source_file sf1008Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tkhe in P21212 (note data collected as P2 21 21) merg FRIEDELS' _shelx_refln_list_code 4 _shelx_f_calc_maximum 61.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 285.56 267.91 10.43 o 4 0 0 34.99 41.88 8.32 o 6 0 0 5.57 9.86 7.47 o 8 0 0 96.67 85.85 9.41 o 1 1 0 3786.40 3649.55 53.75 o 2 1 0 533.01 532.29 10.66 o 3 1 0 209.15 208.10 4.95 o 4 1 0 0.91 0.94 4.51 o 5 1 0 51.23 57.63 4.93 o 6 1 0 0.01 -2.34 4.88 o 7 1 0 88.44 95.84 7.34 o 8 1 0 4.42 10.41 9.95 o 9 1 0 9.70 35.62 10.33 o 0 2 0 3475.38 3175.80 66.38 o 1 2 0 0.03 0.82 2.35 o 2 2 0 1457.80 1464.01 30.89 o 3 2 0 24.19 24.08 3.25 o 4 2 0 6.21 6.96 3.93 o 5 2 0 22.10 22.85 4.78 o 6 2 0 0.23 -1.57 5.29 o 7 2 0 47.67 51.88 5.73 o 8 2 0 108.04 97.99 10.46 o 9 2 0 68.87 75.62 16.70 o 1 3 0 3164.06 3053.56 153.65 o 2 3 0 554.77 535.15 8.95 o 3 3 0 11.93 5.77 3.21 o 4 3 0 0.26 -2.59 4.27 o 5 3 0 13.67 18.87 6.84 o 6 3 0 79.75 81.64 6.44 o 7 3 0 50.31 42.30 5.52 o 8 3 0 22.95 30.96 10.71 o 9 3 0 78.79 72.22 10.01 o 0 4 0 319.05 290.30 9.88 o 1 4 0 1179.92 1136.09 19.36 o 2 4 0 1916.35 1910.85 28.74 o 3 4 0 391.80 391.37 8.71 o 4 4 0 84.96 77.00 4.56 o 5 4 0 35.34 41.61 8.06 o 6 4 0 27.00 27.84 5.45 o 7 4 0 18.09 17.08 5.33 o 8 4 0 58.62 54.04 7.56 o 9 4 0 36.95 31.39 8.69 o 1 5 0 371.26 360.24 6.14 o 2 5 0 281.08 274.71 8.15 o 3 5 0 257.07 225.72 5.41 o 4 5 0 168.10 172.59 5.78 o 5 5 0 50.49 45.07 5.05 o 6 5 0 175.17 150.97 6.91 o 7 5 0 92.60 97.10 8.69 o 8 5 0 94.77 99.04 16.43 o 9 5 0 56.42 63.27 10.52 o 0 6 0 344.93 310.87 8.22 o 1 6 0 19.24 20.95 3.28 o 2 6 0 85.82 76.16 5.17 o 3 6 0 0.28 4.88 5.06 o 4 6 0 108.45 107.68 5.76 o 5 6 0 163.16 149.29 6.47 o 6 6 0 394.26 386.35 10.92 o 7 6 0 3.75 9.73 7.14 o 8 6 0 8.76 9.97 16.16 o 9 6 0 8.42 26.18 10.86 o 2 7 0 218.43 220.73 7.21 o 3 7 0 144.26 151.27 4.93 o 4 7 0 108.16 111.51 5.63 o 5 7 0 529.97 475.77 11.78 o 6 7 0 5.59 8.45 5.51 o 7 7 0 35.01 35.09 7.61 o 8 7 0 3.70 9.34 7.72 o 0 8 0 32.94 30.49 6.11 o 1 8 0 2.69 8.81 4.26 o 2 8 0 90.85 80.49 7.54 o 3 8 0 212.29 235.44 6.61 o 4 8 0 110.77 112.58 6.37 o 5 8 0 87.00 84.52 6.74 o 6 8 0 383.83 365.94 16.31 o 7 8 0 1.39 -1.26 8.48 o 8 8 0 13.15 8.65 8.49 o 1 9 0 7.13 9.57 3.62 o 2 9 0 16.12 11.50 3.73 o 3 9 0 124.83 132.27 5.93 o 4 9 0 74.76 73.57 6.17 o 5 9 0 562.52 550.78 12.76 o 6 9 0 0.79 1.57 7.09 o 7 9 0 20.89 24.56 7.82 o 8 9 0 33.78 60.57 23.07 o 0 10 0 77.35 90.24 6.32 o 1 10 0 24.57 32.42 5.48 o 2 10 0 24.82 15.81 4.47 o 3 10 0 157.74 134.54 7.45 o 4 10 0 713.99 708.51 22.25 o 5 10 0 0.01 2.22 5.62 o 6 10 0 7.93 7.00 7.20 o 7 10 0 17.55 26.09 7.85 o 8 10 0 12.74 15.58 8.62 o 1 11 0 2.71 8.77 4.19 o 2 11 0 86.92 92.46 6.62 o 3 11 0 416.67 384.77 10.22 o 4 11 0 35.65 34.31 5.85 o 5 11 0 29.40 39.47 6.63 o 6 11 0 1.65 1.92 7.29 o 7 11 0 56.01 56.24 8.29 o 0 12 0 4.86 11.22 9.81 o 1 12 0 17.77 17.92 4.84 o 2 12 0 20.71 26.35 5.58 o 3 12 0 76.35 65.76 6.29 o 4 12 0 416.00 394.87 10.86 o 5 12 0 2.12 -1.05 7.66 o 6 12 0 1.28 -4.04 7.63 o 7 12 0 0.82 5.85 8.34 o 1 13 0 21.39 21.50 6.94 o 2 13 0 110.00 106.09 7.18 o 3 13 0 185.36 182.90 16.69 o 4 13 0 1.02 0.58 5.28 o 5 13 0 23.15 21.65 12.97 o 6 13 0 0.50 15.47 12.74 o 0 14 0 60.05 60.98 7.39 o 1 14 0 38.27 50.23 5.86 o 2 14 0 77.24 85.92 9.84 o 3 14 0 4.46 17.00 6.14 o 4 14 0 21.90 6.67 7.28 o 5 14 0 21.87 14.96 7.97 o 6 14 0 20.91 33.21 9.31 o 1 15 0 97.11 99.66 9.66 o 2 15 0 12.88 13.96 5.63 o 3 15 0 11.40 14.02 6.32 o 4 15 0 24.63 35.33 9.34 o 5 15 0 49.00 43.35 9.58 o 0 16 0 86.49 94.39 16.29 o 1 16 0 0.07 4.75 6.84 o 2 16 0 54.82 80.38 12.96 o 3 16 0 26.56 41.03 10.08 o 4 16 0 7.37 3.00 10.18 o 5 16 0 18.37 27.10 9.85 o 1 17 0 48.73 68.05 15.02 o 2 17 0 68.63 65.85 6.71 o 3 17 0 26.48 23.29 11.76 o 4 17 0 2.62 9.95 9.10 o 0 18 0 5.53 8.05 12.50 o 1 18 0 58.15 68.02 10.19 o 2 18 0 62.94 68.98 9.59 o 3 18 0 5.12 -4.71 9.38 o 0 0 1 8.50 6.64 2.38 o 1 0 1 380.89 442.87 8.61 o 2 0 1 0.01 6.59 2.77 o 3 0 1 546.80 588.28 10.36 o 4 0 1 129.68 166.06 7.49 o 5 0 1 302.02 270.76 7.13 o 6 0 1 42.10 44.35 5.86 o 7 0 1 0.31 -0.35 5.72 o 8 0 1 107.89 106.85 15.49 o 9 0 1 14.67 38.42 16.19 o 0 1 1 2716.76 2728.40 39.32 o 1 1 1 176.23 188.76 3.21 o 2 1 1 673.84 676.47 12.05 o 3 1 1 85.15 99.04 2.67 o 4 1 1 368.90 379.35 5.23 o 5 1 1 17.85 22.22 3.60 o 6 1 1 98.70 99.65 4.52 o 7 1 1 51.56 54.31 4.28 o 8 1 1 0.36 1.92 5.49 o 9 1 1 17.26 21.23 9.78 o 0 2 1 314.51 323.87 5.25 o 1 2 1 3734.43 3790.20 42.76 o 2 2 1 558.84 550.63 6.50 o 3 2 1 363.14 392.51 5.49 o 4 2 1 29.64 41.10 3.24 o 5 2 1 246.06 245.69 5.08 o 6 2 1 47.17 46.19 4.22 o 7 2 1 9.83 14.72 4.32 o 8 2 1 35.84 32.89 5.17 o 9 2 1 0.29 7.11 11.46 o 0 3 1 129.96 120.21 3.62 o 1 3 1 252.47 236.76 3.84 o 2 3 1 548.21 565.21 6.24 o 3 3 1 259.90 284.86 8.21 o 4 3 1 279.26 293.04 4.57 o 5 3 1 20.49 17.85 3.39 o 6 3 1 85.91 76.50 4.63 o 7 3 1 129.84 119.07 5.38 o 8 3 1 8.80 5.39 5.37 o 9 3 1 20.69 15.29 9.21 o 0 4 1 4.14 5.73 2.21 o 1 4 1 214.58 202.55 3.34 o 2 4 1 3.39 4.36 1.83 o 3 4 1 826.21 887.53 8.82 o 4 4 1 6.41 4.40 2.54 o 5 4 1 90.06 91.50 4.21 o 6 4 1 50.71 55.26 5.63 o 7 4 1 86.42 79.31 4.90 o 8 4 1 21.15 26.76 5.19 o 9 4 1 9.24 25.36 7.88 o 0 5 1 817.78 787.53 10.49 o 1 5 1 560.59 559.44 6.85 o 2 5 1 1460.12 1583.95 14.56 o 3 5 1 121.73 126.34 3.42 o 4 5 1 277.82 268.97 4.83 o 5 5 1 65.87 61.06 4.22 o 6 5 1 42.35 40.64 4.61 o 7 5 1 5.51 4.37 4.13 o 8 5 1 12.49 10.98 5.11 o 9 5 1 15.41 44.42 10.53 o 0 6 1 4.44 6.79 2.10 o 1 6 1 296.22 286.94 3.28 o 2 6 1 341.98 347.61 5.04 o 3 6 1 300.75 328.10 4.97 o 4 6 1 166.80 158.96 4.18 o 5 6 1 20.04 18.36 4.18 o 6 6 1 9.37 7.62 4.54 o 7 6 1 55.51 55.71 4.84 o 8 6 1 8.55 22.42 6.01 o 0 7 1 279.43 290.94 6.92 o 1 7 1 34.22 41.36 3.43 o 2 7 1 347.01 346.56 4.96 o 3 7 1 111.94 105.71 3.46 o 4 7 1 124.25 114.85 3.94 o 5 7 1 80.39 81.20 5.33 o 6 7 1 136.53 132.00 5.77 o 7 7 1 68.27 69.57 6.17 o 8 7 1 14.28 25.63 6.54 o 0 8 1 170.28 180.24 3.97 o 1 8 1 357.26 359.65 4.61 o 2 8 1 12.74 13.90 2.42 o 3 8 1 182.22 182.62 4.25 o 4 8 1 0.05 0.17 3.13 o 5 8 1 99.45 106.04 7.28 o 6 8 1 37.31 38.08 4.43 o 7 8 1 0.96 6.04 4.60 o 8 8 1 13.63 31.65 9.44 o 0 9 1 257.73 240.88 5.99 o 1 9 1 58.88 67.07 2.94 o 2 9 1 183.55 179.87 4.18 o 3 9 1 168.65 167.45 4.37 o 4 9 1 34.02 30.27 4.19 o 5 9 1 16.95 14.22 4.32 o 6 9 1 0.07 5.34 4.43 o 7 9 1 12.87 16.99 5.48 o 8 9 1 7.11 13.52 6.24 o 0 10 1 0.03 2.02 3.66 o 1 10 1 229.90 226.39 4.67 o 2 10 1 24.17 26.33 3.56 o 3 10 1 23.54 27.33 3.68 o 4 10 1 32.40 31.99 4.58 o 5 10 1 93.74 92.32 5.17 o 6 10 1 15.26 26.00 4.95 o 7 10 1 0.66 14.21 4.92 o 8 10 1 28.66 33.79 8.79 o 0 11 1 194.96 196.56 9.31 o 1 11 1 1.33 4.93 3.73 o 2 11 1 42.62 40.77 4.68 o 3 11 1 38.46 36.71 4.47 o 4 11 1 112.64 121.04 5.65 o 5 11 1 13.26 13.98 4.33 o 6 11 1 34.02 38.49 5.06 o 7 11 1 6.34 18.00 5.08 o 0 12 1 40.01 40.44 4.79 o 1 12 1 101.55 97.61 4.33 o 2 12 1 37.85 40.18 3.94 o 3 12 1 106.76 90.99 5.43 o 4 12 1 33.58 31.81 4.73 o 5 12 1 14.02 16.70 4.81 o 6 12 1 0.34 6.75 4.76 o 7 12 1 1.24 12.95 10.26 o 0 13 1 13.26 9.51 5.12 o 1 13 1 90.56 87.07 4.85 o 2 13 1 86.08 87.82 4.91 o 3 13 1 20.05 20.52 4.18 o 4 13 1 4.16 7.98 4.59 o 5 13 1 6.36 8.74 4.76 o 6 13 1 16.71 8.22 6.58 o 0 14 1 28.40 28.39 6.34 o 1 14 1 12.28 6.15 3.55 o 2 14 1 23.98 31.97 4.44 o 3 14 1 57.28 62.65 5.36 o 4 14 1 37.13 43.56 5.23 o 5 14 1 1.02 10.94 6.68 o 6 14 1 3.58 12.09 10.24 o 0 15 1 0.50 9.71 10.49 o 1 15 1 69.28 68.82 4.56 o 2 15 1 25.47 25.11 5.38 o 3 15 1 39.60 37.44 8.02 o 4 15 1 6.62 17.48 5.94 o 5 15 1 20.49 23.77 7.50 o 0 16 1 86.86 88.57 8.59 o 1 16 1 4.85 2.71 4.77 o 2 16 1 21.05 24.48 5.94 o 3 16 1 9.21 8.03 5.53 o 4 16 1 8.41 11.80 5.92 o 5 16 1 0.12 3.40 13.50 o 0 17 1 7.36 14.79 7.87 o 1 17 1 23.89 27.88 4.93 o 2 17 1 7.54 8.15 5.71 o 3 17 1 8.12 5.56 5.97 o 4 17 1 5.27 4.88 7.36 o 0 18 1 13.80 30.99 9.92 o 1 18 1 0.58 7.17 6.16 o 2 18 1 12.84 22.00 5.81 o 1 0 2 98.26 100.04 3.56 o 2 0 2 176.12 165.64 4.18 o 3 0 2 17.72 22.91 3.48 o 4 0 2 775.68 816.03 12.36 o 5 0 2 34.68 28.89 7.19 o 6 0 2 111.22 128.51 9.81 o 7 0 2 83.37 74.79 8.57 o 8 0 2 20.21 23.02 7.92 o 9 0 2 7.27 21.11 8.85 o 0 1 2 1.86 0.23 1.82 o 1 1 2 480.83 513.40 5.64 o 2 1 2 187.09 200.82 3.34 o 3 1 2 199.54 221.97 4.60 o 4 1 2 81.28 82.28 3.29 o 5 1 2 365.88 358.87 7.32 o 6 1 2 29.47 45.91 5.51 o 7 1 2 110.39 124.28 6.69 o 8 1 2 76.67 64.81 6.40 o 9 1 2 0.31 8.86 8.14 o 0 2 2 597.87 562.71 7.70 o 1 2 2 7.33 11.97 2.21 o 2 2 2 679.87 715.12 7.11 o 3 2 2 178.96 186.60 3.96 o 4 2 2 611.39 644.03 7.68 o 5 2 2 207.62 218.34 5.94 o 6 2 2 154.27 146.61 6.60 o 7 2 2 68.69 77.82 6.02 o 8 2 2 23.55 20.60 5.63 o 9 2 2 7.13 13.88 9.59 o 0 3 2 124.24 129.09 3.69 o 1 3 2 736.42 765.20 7.22 o 2 3 2 64.61 66.63 4.05 o 3 3 2 1508.70 1540.67 14.72 o 4 3 2 166.51 171.52 4.29 o 5 3 2 81.63 81.34 4.87 o 6 3 2 22.43 18.13 5.49 o 7 3 2 68.82 73.43 6.03 o 8 3 2 5.46 8.85 5.44 o 9 3 2 12.22 23.94 6.07 o 0 4 2 240.77 230.00 3.96 o 1 4 2 124.62 118.61 2.59 o 2 4 2 1185.15 1297.78 11.53 o 3 4 2 247.67 254.63 5.02 o 4 4 2 214.20 221.61 4.86 o 5 4 2 11.78 12.73 4.31 o 6 4 2 160.09 157.94 5.86 o 7 4 2 1.33 -1.32 5.19 o 8 4 2 26.91 28.49 5.61 o 0 5 2 59.75 67.28 3.35 o 1 5 2 695.81 695.50 6.09 o 2 5 2 28.52 25.45 2.24 o 3 5 2 478.44 508.70 7.29 o 4 5 2 102.95 109.09 4.74 o 5 5 2 204.23 194.22 6.20 o 6 5 2 37.50 34.23 4.78 o 7 5 2 86.29 78.98 6.17 o 8 5 2 10.45 14.23 6.49 o 0 6 2 27.62 27.37 6.63 o 1 6 2 140.98 145.12 2.57 o 2 6 2 1207.39 1208.42 10.57 o 3 6 2 2.87 4.00 2.38 o 4 6 2 103.47 106.05 4.92 o 5 6 2 11.58 11.28 4.34 o 6 6 2 90.49 84.11 5.11 o 7 6 2 36.63 40.51 5.76 o 8 6 2 24.11 31.22 6.18 o 0 7 2 7.32 13.06 3.09 o 1 7 2 928.89 951.57 7.34 o 2 7 2 147.55 148.97 3.50 o 3 7 2 244.13 236.30 5.67 o 4 7 2 18.70 17.43 3.84 o 5 7 2 98.56 111.41 10.06 o 6 7 2 40.92 45.87 5.03 o 7 7 2 40.27 37.18 5.48 o 8 7 2 8.02 14.06 6.05 o 0 8 2 735.53 737.92 10.77 o 1 8 2 82.93 82.02 3.03 o 2 8 2 264.50 258.25 4.59 o 3 8 2 39.44 39.61 4.28 o 4 8 2 119.29 112.66 5.08 o 5 8 2 28.32 24.00 4.23 o 6 8 2 30.08 26.84 4.82 o 7 8 2 41.17 41.61 5.49 o 8 8 2 2.29 6.26 7.42 o 0 9 2 0.97 2.59 3.29 o 1 9 2 351.05 347.11 5.17 o 2 9 2 13.98 11.75 3.69 o 3 9 2 132.33 129.55 5.74 o 4 9 2 14.03 18.79 4.24 o 5 9 2 90.57 83.22 5.10 o 6 9 2 39.02 33.63 4.60 o 7 9 2 32.96 41.12 5.99 o 0 10 2 453.08 435.38 10.00 o 1 10 2 195.63 194.64 4.69 o 2 10 2 111.60 113.05 4.82 o 3 10 2 2.48 5.04 5.53 o 4 10 2 79.20 76.57 4.63 o 5 10 2 0.38 1.70 4.39 o 6 10 2 11.02 23.57 5.27 o 7 10 2 10.79 12.69 5.71 o 0 11 2 7.07 4.18 8.71 o 1 11 2 135.06 137.49 5.54 o 2 11 2 39.65 31.29 4.68 o 3 11 2 124.73 112.61 5.93 o 4 11 2 33.54 29.11 4.60 o 5 11 2 23.22 34.96 5.92 o 6 11 2 1.93 6.17 4.92 o 7 11 2 4.69 9.35 7.86 o 0 12 2 100.86 98.02 8.25 o 1 12 2 39.20 38.68 4.58 o 2 12 2 143.71 138.68 8.60 o 3 12 2 39.02 41.09 4.64 o 4 12 2 24.50 28.10 4.81 o 5 12 2 12.19 18.05 5.14 o 6 12 2 1.04 16.67 5.13 o 0 13 2 42.91 37.57 6.32 o 1 13 2 90.35 103.34 5.21 o 2 13 2 26.49 24.06 4.72 o 3 13 2 71.43 66.36 5.34 o 4 13 2 37.39 38.27 5.57 o 5 13 2 13.85 7.50 5.83 o 6 13 2 2.41 11.03 6.34 o 0 14 2 99.75 108.11 17.52 o 1 14 2 87.12 81.98 5.64 o 2 14 2 66.80 69.00 7.41 o 3 14 2 34.15 34.39 5.31 o 4 14 2 38.67 33.34 5.73 o 5 14 2 9.40 16.27 5.77 o 0 15 2 143.26 137.82 30.36 o 1 15 2 31.30 40.39 5.78 o 2 15 2 0.31 5.12 5.50 o 3 15 2 34.75 35.51 5.39 o 4 15 2 18.27 16.23 5.77 o 5 15 2 18.78 23.97 7.65 o 0 16 2 4.00 -0.16 6.77 o 1 16 2 37.50 32.76 5.39 o 2 16 2 26.06 25.67 6.45 o 3 16 2 2.35 12.89 6.08 o 4 16 2 5.72 18.21 9.58 o 0 17 2 37.26 40.46 8.20 o 1 17 2 8.20 17.18 5.48 o 2 17 2 1.30 7.09 5.24 o 3 17 2 9.39 25.12 7.38 o 0 18 2 1.33 7.15 12.37 o 1 18 2 4.35 20.06 5.81 o 0 0 3 28.01 31.17 4.64 o 1 0 3 1243.84 1283.01 12.74 o 2 0 3 35.91 40.67 4.68 o 3 0 3 0.77 0.69 3.53 o 4 0 3 155.65 157.64 6.86 o 5 0 3 72.79 75.97 7.44 o 6 0 3 87.67 93.68 7.61 o 7 0 3 0.22 0.43 9.12 o 8 0 3 10.48 25.70 8.50 o 0 1 3 1111.03 1241.02 17.75 o 1 1 3 4.16 5.47 1.76 o 2 1 3 674.84 667.87 7.39 o 3 1 3 22.82 23.39 3.08 o 4 1 3 170.27 176.91 5.05 o 5 1 3 70.17 68.61 5.35 o 6 1 3 3.76 0.40 4.13 o 7 1 3 28.27 27.44 5.30 o 8 1 3 19.24 22.20 6.02 o 0 2 3 55.74 61.95 2.91 o 1 2 3 1078.23 1130.67 10.29 o 2 2 3 2.52 1.04 2.43 o 3 2 3 8.99 8.41 2.90 o 4 2 3 71.37 66.04 5.21 o 5 2 3 28.04 30.62 5.75 o 6 2 3 6.30 7.76 5.19 o 7 2 3 4.82 3.45 4.85 o 8 2 3 5.19 8.62 5.38 o 0 3 3 950.83 915.96 10.49 o 1 3 3 38.51 35.85 2.58 o 2 3 3 119.94 122.75 3.39 o 3 3 3 48.09 58.58 3.38 o 4 3 3 7.52 8.66 4.37 o 5 3 3 130.88 123.83 5.14 o 6 3 3 30.38 19.90 4.46 o 7 3 3 7.22 20.16 6.69 o 8 3 3 35.69 51.19 7.06 o 0 4 3 110.85 115.23 2.94 o 1 4 3 425.32 436.31 5.17 o 2 4 3 2.34 0.86 2.64 o 3 4 3 61.07 61.41 3.47 o 4 4 3 163.87 143.01 5.66 o 5 4 3 9.28 10.60 3.88 o 6 4 3 77.34 75.18 5.29 o 7 4 3 30.11 39.73 5.16 o 8 4 3 5.31 15.92 5.63 o 0 5 3 151.97 149.76 3.88 o 1 5 3 10.25 9.30 2.37 o 2 5 3 125.09 122.54 3.70 o 3 5 3 6.97 3.59 3.47 o 4 5 3 113.10 110.53 5.65 o 5 5 3 66.33 62.50 4.57 o 6 5 3 33.77 30.75 4.82 o 7 5 3 3.14 12.17 4.94 o 8 5 3 16.15 15.43 6.25 o 0 6 3 44.11 44.81 3.69 o 1 6 3 7.71 14.94 2.53 o 2 6 3 38.10 40.23 3.22 o 3 6 3 70.88 80.65 4.05 o 4 6 3 20.50 23.33 5.00 o 5 6 3 52.19 53.29 4.07 o 6 6 3 36.25 35.90 5.04 o 7 6 3 41.85 39.25 5.37 o 8 6 3 5.29 16.31 7.69 o 0 7 3 41.24 43.54 3.98 o 1 7 3 50.60 42.92 2.71 o 2 7 3 11.58 12.59 3.46 o 3 7 3 9.06 10.71 3.89 o 4 7 3 147.71 136.42 6.28 o 5 7 3 18.16 13.48 3.73 o 6 7 3 48.83 41.02 5.16 o 7 7 3 9.53 26.45 7.45 o 0 8 3 211.74 206.93 6.18 o 1 8 3 77.64 75.14 3.43 o 2 8 3 121.38 112.40 3.46 o 3 8 3 113.15 111.07 5.69 o 4 8 3 4.40 5.26 3.54 o 5 8 3 105.87 95.96 4.88 o 6 8 3 28.17 31.09 9.07 o 7 8 3 18.58 25.03 5.35 o 0 9 3 116.02 116.36 5.48 o 1 9 3 88.58 100.07 3.88 o 2 9 3 81.18 79.49 4.04 o 3 9 3 23.34 24.42 3.61 o 4 9 3 162.35 159.42 5.18 o 5 9 3 2.72 -0.33 4.26 o 6 9 3 42.76 51.54 5.57 o 7 9 3 8.43 15.01 6.95 o 0 10 3 52.89 60.13 5.11 o 1 10 3 37.32 29.87 3.86 o 2 10 3 113.23 99.83 4.46 o 3 10 3 50.79 51.96 3.79 o 4 10 3 15.53 19.45 3.97 o 5 10 3 98.59 83.95 5.32 o 6 10 3 7.73 14.92 4.47 o 7 10 3 16.17 30.83 5.93 o 0 11 3 50.98 52.59 7.00 o 1 11 3 24.60 29.68 4.46 o 2 11 3 9.99 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324.22 7.98 o 5 0 4 59.94 69.88 6.36 o 6 0 4 102.75 111.52 8.50 o 7 0 4 27.59 7.72 14.44 o 0 1 4 0.10 0.12 4.06 o 1 1 4 12.53 11.35 2.77 o 2 1 4 1.86 -3.20 3.20 o 3 1 4 555.68 531.11 7.92 o 4 1 4 34.68 37.15 3.28 o 5 1 4 173.65 161.95 5.48 o 6 1 4 127.89 117.06 6.12 o 7 1 4 21.01 30.21 4.94 o 0 2 4 0.48 7.09 4.57 o 1 2 4 0.79 -3.12 3.12 o 2 2 4 230.94 223.14 5.63 o 3 2 4 20.00 19.84 3.88 o 4 2 4 296.88 302.61 6.31 o 5 2 4 11.25 12.78 3.75 o 6 2 4 77.68 75.59 5.73 o 7 2 4 17.65 18.40 6.37 o 0 3 4 5.17 9.78 3.61 o 1 3 4 134.00 145.57 4.73 o 2 3 4 18.94 13.50 3.51 o 3 3 4 303.61 286.27 6.64 o 4 3 4 16.55 15.62 3.79 o 5 3 4 238.67 214.67 5.92 o 6 3 4 11.91 17.59 4.48 o 7 3 4 23.78 27.57 5.40 o 0 4 4 26.67 30.41 3.68 o 1 4 4 6.71 14.68 3.04 o 2 4 4 485.34 487.35 9.06 o 3 4 4 37.28 30.61 4.09 o 4 4 4 213.72 201.37 5.58 o 5 4 4 60.63 46.82 5.90 o 6 4 4 34.71 40.47 4.74 o 7 4 4 6.16 16.09 5.12 o 0 5 4 111.40 107.56 5.15 o 1 5 4 306.25 278.36 5.16 o 2 5 4 8.01 7.37 3.94 o 3 5 4 329.53 314.90 6.49 o 4 5 4 29.50 26.70 4.96 o 5 5 4 43.57 46.80 5.74 o 6 5 4 21.33 28.54 4.92 o 7 5 4 30.97 46.13 5.50 o 0 6 4 453.71 467.15 8.08 o 1 6 4 104.75 102.74 3.84 o 2 6 4 279.87 273.98 5.44 o 3 6 4 9.50 14.27 4.26 o 4 6 4 66.11 63.23 5.99 o 5 6 4 44.01 37.50 5.88 o 6 6 4 34.98 44.33 4.89 o 7 6 4 4.11 13.99 5.22 o 0 7 4 344.35 332.27 6.97 o 1 7 4 267.76 257.19 5.64 o 2 7 4 11.93 15.09 3.65 o 3 7 4 169.75 163.86 7.03 o 4 7 4 2.49 -1.58 5.07 o 5 7 4 13.79 14.22 5.24 o 6 7 4 28.19 35.28 6.54 o 7 7 4 12.55 17.85 5.84 o 0 8 4 209.61 213.66 6.74 o 1 8 4 81.58 74.51 3.42 o 2 8 4 210.19 209.82 5.39 o 3 8 4 2.50 -0.66 4.18 o 4 8 4 10.86 3.41 5.39 o 5 8 4 0.17 4.33 3.80 o 6 8 4 33.07 28.90 5.22 o 0 9 4 10.76 7.05 4.13 o 1 9 4 240.69 232.82 5.26 o 2 9 4 71.07 68.17 3.78 o 3 9 4 18.61 15.50 4.45 o 4 9 4 1.10 3.45 5.58 o 5 9 4 27.00 38.95 5.03 o 6 9 4 8.94 19.09 5.88 o 0 10 4 193.97 195.57 6.91 o 1 10 4 8.02 -1.65 3.01 o 2 10 4 94.18 96.54 4.47 o 3 10 4 35.42 33.12 4.04 o 4 10 4 10.74 21.73 4.89 o 5 10 4 0.31 8.70 4.68 o 6 10 4 17.99 27.73 5.56 o 0 11 4 59.94 62.93 9.46 o 1 11 4 162.24 158.45 5.26 o 2 11 4 69.97 65.57 4.29 o 3 11 4 34.22 45.10 4.62 o 4 11 4 5.57 13.55 4.21 o 5 11 4 1.53 6.73 5.72 o 0 12 4 166.35 179.30 10.03 o 1 12 4 30.58 35.83 5.92 o 2 12 4 18.32 27.41 5.06 o 3 12 4 25.43 18.11 5.18 o 4 12 4 40.53 40.24 5.72 o 5 12 4 4.44 6.90 6.05 o 0 13 4 26.25 25.99 7.42 o 1 13 4 56.71 59.25 5.52 o 2 13 4 3.25 10.88 4.93 o 3 13 4 18.07 26.54 5.51 o 4 13 4 9.92 0.03 5.57 o 0 14 4 22.66 28.32 7.77 o 1 14 4 6.10 8.01 5.02 o 2 14 4 37.74 51.58 5.63 o 3 14 4 0.66 10.85 8.85 o 0 15 4 2.53 -1.57 7.53 o 1 15 4 38.47 35.19 6.13 o 2 15 4 8.93 13.48 6.65 o 0 0 5 0.10 7.55 6.71 o 1 0 5 6.11 10.93 4.60 o 2 0 5 22.93 21.12 6.24 o 3 0 5 8.49 6.65 5.41 o 4 0 5 32.80 29.03 6.44 o 5 0 5 57.10 52.41 6.27 o 6 0 5 38.35 44.94 8.03 o 0 1 5 14.21 5.82 4.55 o 1 1 5 1.93 2.74 3.21 o 2 1 5 40.01 39.01 4.01 o 3 1 5 107.53 103.37 4.39 o 4 1 5 53.96 51.06 3.63 o 5 1 5 7.63 10.10 4.53 o 6 1 5 28.31 35.46 5.46 o 0 2 5 13.51 11.38 4.83 o 1 2 5 51.28 55.59 3.62 o 2 2 5 0.22 -0.07 3.60 o 3 2 5 166.77 161.97 5.62 o 4 2 5 77.05 72.27 4.55 o 5 2 5 28.98 33.35 3.41 o 6 2 5 13.03 15.85 4.55 o 0 3 5 0.13 2.26 4.46 o 1 3 5 4.02 3.58 3.33 o 2 3 5 173.42 169.30 5.02 o 3 3 5 6.57 10.89 4.06 o 4 3 5 50.80 43.26 4.58 o 5 3 5 15.27 16.69 5.55 o 6 3 5 13.70 13.11 4.74 o 0 4 5 10.22 21.12 5.27 o 1 4 5 116.99 119.81 3.99 o 2 4 5 8.78 10.73 3.60 o 3 4 5 171.80 176.93 5.94 o 4 4 5 17.14 18.03 4.32 o 5 4 5 19.12 28.96 5.87 o 6 4 5 9.33 16.20 4.55 o 0 5 5 6.38 10.75 4.56 o 1 5 5 21.30 22.64 2.95 o 2 5 5 192.51 185.52 5.34 o 3 5 5 11.13 15.11 4.29 o 4 5 5 26.71 37.55 5.55 o 5 5 5 41.80 49.95 7.12 o 6 5 5 16.44 31.48 4.76 o 0 6 5 121.07 113.13 8.02 o 1 6 5 181.89 190.03 4.41 o 2 6 5 42.07 41.54 4.60 o 3 6 5 105.79 109.75 5.92 o 4 6 5 4.70 9.50 4.94 o 5 6 5 36.28 35.27 6.94 o 6 6 5 26.42 32.13 5.10 o 0 7 5 110.74 96.42 5.72 o 1 7 5 24.17 26.62 3.27 o 2 7 5 117.42 118.19 5.49 o 3 7 5 10.65 10.72 5.63 o 4 7 5 0.67 1.26 4.69 o 5 7 5 10.01 10.41 8.04 o 0 8 5 2.10 15.99 6.74 o 1 8 5 77.49 75.26 4.10 o 2 8 5 2.09 2.11 4.33 o 3 8 5 4.18 6.70 4.45 o 4 8 5 0.02 8.84 6.14 o 5 8 5 1.42 6.77 6.39 o 0 9 5 77.73 79.67 6.93 o 1 9 5 22.86 25.11 3.89 o 2 9 5 19.76 34.90 4.47 o 3 9 5 0.28 5.58 4.52 o 4 9 5 4.09 2.73 7.59 o 5 9 5 0.71 10.50 6.77 o 0 10 5 16.69 11.71 5.19 o 1 10 5 27.65 22.68 3.91 o 2 10 5 22.87 16.73 6.15 o 3 10 5 42.44 31.86 6.78 o 4 10 5 0.42 -2.55 7.55 o 0 11 5 11.59 6.43 12.39 o 1 11 5 23.21 34.75 4.75 o 2 11 5 20.78 42.55 6.02 o 3 11 5 42.32 34.26 4.63 o 4 11 5 4.80 7.13 8.50 o 0 12 5 54.13 64.52 8.74 o 1 12 5 8.41 14.61 5.40 o 2 12 5 5.70 29.57 12.17 o 3 12 5 9.46 21.19 6.19 o 0 13 5 5.17 17.03 11.33 o 1 13 5 17.16 4.89 5.89 o 2 13 5 3.87 11.97 5.63 o 0 0 6 133.04 126.89 10.28 o 1 0 6 40.93 42.26 5.71 o 2 0 6 388.70 387.94 10.07 o 3 0 6 6.36 0.94 6.15 o 4 0 6 1.86 6.12 7.46 o 5 0 6 5.03 -10.94 10.94 o 0 1 6 17.72 21.01 5.05 o 1 1 6 371.00 373.66 6.90 o 2 1 6 23.99 21.60 3.66 o 3 1 6 19.87 18.37 4.45 o 4 1 6 18.78 28.66 4.38 o 5 1 6 0.41 10.18 4.53 o 0 2 6 441.37 438.85 10.39 o 1 2 6 20.67 23.03 3.67 o 2 2 6 102.47 103.63 4.55 o 3 2 6 8.17 4.13 3.99 o 4 2 6 0.18 4.53 4.08 o 5 2 6 22.19 16.42 4.21 o 0 3 6 15.24 9.39 7.84 o 1 3 6 192.54 189.79 5.25 o 2 3 6 10.42 10.60 3.49 o 3 3 6 43.15 48.89 4.95 o 4 3 6 44.85 53.46 5.70 o 5 3 6 9.43 13.34 7.22 o 0 4 6 378.71 383.88 10.00 o 1 4 6 22.73 23.99 3.76 o 2 4 6 21.90 18.36 3.67 o 3 4 6 11.66 24.98 5.23 o 4 4 6 10.74 16.71 4.69 o 0 5 6 18.20 20.31 5.33 o 1 5 6 62.77 57.49 4.23 o 2 5 6 7.15 9.15 3.96 o 3 5 6 28.08 25.22 5.37 o 4 5 6 15.87 20.34 5.58 o 0 6 6 2.49 3.02 5.08 o 1 6 6 6.70 18.09 4.21 o 2 6 6 51.59 57.98 5.04 o 3 6 6 2.68 -4.96 4.96 o 4 6 6 84.62 85.26 6.21 o 0 7 6 13.08 7.34 6.32 o 1 7 6 11.58 9.64 4.34 o 2 7 6 0.40 1.86 4.30 o 3 7 6 70.04 80.96 6.59 o 0 8 6 4.69 2.02 8.20 o 1 8 6 38.42 43.00 4.55 o 2 8 6 10.43 -0.20 5.14 o 3 8 6 2.55 5.87 5.14 o 0 9 6 0.39 7.72 6.08 o 1 9 6 5.59 0.10 4.26 o 2 9 6 62.73 68.56 6.98 o 0 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