#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/51/2015162.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015162_Fobs loop_ _publ_author_name 'Pelosi, G.' 'Pelizzi, C.' 'Belicchi Ferrari, M.' 'Rodr\'iguez-Arg\"uelles, M. C.' 'Vieito, C.' 'Sanmart\'in, J.' _publ_section_title ; Isatin 3-semicarbazone and 1-methylisatin 3-semicarbazone ; _journal_coeditor_code HJ1061 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o589 _journal_page_last o592 _journal_volume 61 _journal_year 2005 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 3.9840 _cell_length_b 20.9300 _cell_length_c 12.1220 _exptl_crystal_F_000 455.87 _reflns_d_resolution_high 0.8993 _[local]_cod_data_source_file hj1061IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' II P 21 21 21 R = 0.03' _shelx_refln_list_code 4 _shelx_f_calc_maximum 158.82 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 496.50 500.83 24.86 o 4 0 0 7.72 9.30 4.10 o 1 1 0 4174.94 4092.64 51.99 o 2 1 0 54.34 47.96 2.02 o 3 1 0 59.85 62.72 2.61 o 4 1 0 24.74 30.93 3.42 o 0 2 0 131.09 151.87 2.74 o 1 2 0 1494.34 1426.20 18.42 o 2 2 0 193.58 204.65 3.66 o 3 2 0 15.40 15.08 1.87 o 4 2 0 0.88 1.49 2.67 o 1 3 0 25223.46 24236.18 60.96 o 2 3 0 456.47 458.76 7.61 o 3 3 0 41.01 38.34 2.22 o 4 3 0 2.81 2.44 2.55 o 0 4 0 2899.85 2842.97 21.97 o 1 4 0 9257.31 9043.65 72.14 o 2 4 0 2185.54 2212.98 35.52 o 3 4 0 1.89 1.96 1.86 o 4 4 0 3.25 3.72 2.56 o 1 5 0 444.69 432.21 8.00 o 2 5 0 63.23 51.47 2.48 o 3 5 0 2.94 2.13 1.84 o 4 5 0 0.45 2.22 2.46 o 0 6 0 2649.97 2616.51 49.18 o 1 6 0 197.31 187.34 2.92 o 2 6 0 1638.67 1587.31 11.67 o 3 6 0 124.38 129.66 4.06 o 4 6 0 6.60 8.94 2.66 o 1 7 0 1178.68 1215.59 12.42 o 2 7 0 843.02 810.82 14.26 o 3 7 0 241.76 240.70 5.30 o 4 7 0 9.65 10.21 2.76 o 0 8 0 852.90 891.19 8.39 o 1 8 0 329.55 338.55 5.85 o 2 8 0 437.71 428.62 6.11 o 3 8 0 30.20 25.02 2.52 o 4 8 0 41.44 43.28 3.78 o 1 9 0 356.37 336.78 4.96 o 2 9 0 32.43 31.21 2.15 o 3 9 0 0.37 0.67 1.93 o 4 9 0 59.44 69.09 4.69 o 0 10 0 3260.45 3511.89 49.39 o 1 10 0 9.42 7.17 1.34 o 2 10 0 7.75 7.44 1.70 o 3 10 0 24.99 21.25 2.43 o 4 10 0 11.76 12.68 4.69 o 1 11 0 183.00 179.29 3.35 o 2 11 0 27.08 25.74 2.06 o 3 11 0 219.20 228.61 5.65 o 0 12 0 8.36 5.30 1.76 o 1 12 0 166.96 158.55 3.39 o 2 12 0 1.52 0.18 1.87 o 3 12 0 35.73 38.07 3.27 o 1 13 0 231.94 243.38 4.48 o 2 13 0 81.11 85.04 3.57 o 3 13 0 90.95 90.22 4.23 o 0 14 0 460.44 463.29 12.08 o 1 14 0 106.72 104.60 3.06 o 2 14 0 0.64 2.12 2.04 o 3 14 0 0.11 1.60 2.54 o 1 15 0 56.23 54.31 2.53 o 2 15 0 265.14 262.68 5.89 o 3 15 0 0.01 -0.88 2.62 o 0 16 0 27.20 26.06 3.25 o 1 16 0 63.81 66.63 2.89 o 2 16 0 1.91 3.02 2.29 o 3 16 0 2.82 3.41 3.20 o 1 17 0 229.46 238.76 5.36 o 2 17 0 96.79 94.57 4.09 o 3 17 0 2.15 -0.63 3.28 o 0 18 0 12.73 10.25 3.24 o 1 18 0 59.29 60.72 3.26 o 2 18 0 1.97 2.32 2.43 o 1 19 0 57.50 56.79 3.73 o 2 19 0 13.08 14.39 2.74 o 0 20 0 364.28 378.81 10.38 o 1 20 0 0.01 -0.33 2.44 o 2 20 0 13.95 13.29 2.83 o 1 21 0 18.30 15.35 2.93 o 0 22 0 1.37 -2.26 3.52 o 1 22 0 29.40 33.84 3.61 o 1 0 1 810.67 843.34 9.41 o 2 0 1 89.19 91.17 2.52 o 3 0 1 24.37 24.54 2.13 o 4 0 1 4.28 1.72 2.61 o 0 1 1 510.52 520.81 5.05 o 1 1 1 2690.53 2745.93 13.70 o 2 1 1 174.83 179.32 2.49 o 3 1 1 124.19 129.44 2.53 o 4 1 1 15.10 15.19 2.07 o 0 2 1 1358.45 1299.48 12.95 o 1 2 1 1171.36 1240.65 13.25 o 2 2 1 180.72 178.43 3.47 o 3 2 1 19.51 18.32 1.37 o 4 2 1 21.72 22.06 2.08 o 0 3 1 7781.76 7683.04 36.36 o 1 3 1 2786.60 2792.93 15.54 o 2 3 1 806.63 811.72 6.50 o 3 3 1 52.10 52.56 1.77 o 4 3 1 3.80 4.21 1.74 o 0 4 1 96.52 80.21 1.70 o 1 4 1 1051.43 1012.82 9.21 o 2 4 1 646.82 665.80 7.35 o 3 4 1 53.99 51.96 1.88 o 4 4 1 6.74 8.15 1.86 o 0 5 1 71.25 68.24 1.43 o 1 5 1 2396.80 2342.36 14.70 o 2 5 1 203.08 218.78 3.19 o 3 5 1 26.49 23.79 1.66 o 4 5 1 18.54 17.13 2.09 o 0 6 1 308.22 332.75 3.18 o 1 6 1 1122.45 1109.10 8.19 o 2 6 1 853.71 843.78 6.50 o 3 6 1 21.30 20.46 1.64 o 4 6 1 11.15 12.55 2.03 o 0 7 1 13.09 19.43 3.44 o 1 7 1 755.16 786.63 5.45 o 2 7 1 1598.82 1600.90 14.43 o 3 7 1 274.35 292.91 4.08 o 4 7 1 5.37 4.59 1.91 o 0 8 1 1884.64 1963.46 20.21 o 1 8 1 189.41 191.51 2.19 o 2 8 1 304.22 320.41 3.55 o 3 8 1 140.96 130.72 4.77 o 4 8 1 1.08 0.96 2.03 o 0 9 1 120.69 122.92 3.60 o 1 9 1 106.68 108.63 1.71 o 2 9 1 112.74 113.89 4.81 o 3 9 1 86.57 86.44 2.55 o 4 9 1 42.91 43.96 2.86 o 0 10 1 376.39 383.23 4.76 o 1 10 1 329.03 344.13 6.68 o 2 10 1 199.13 202.10 3.25 o 3 10 1 393.42 415.97 6.12 o 0 11 1 0.23 2.27 1.21 o 1 11 1 545.02 594.40 7.00 o 2 11 1 20.60 21.22 1.37 o 3 11 1 62.40 65.94 2.69 o 0 12 1 338.32 339.03 5.58 o 1 12 1 215.85 208.51 3.68 o 2 12 1 0.97 0.75 1.21 o 3 12 1 33.09 29.04 2.12 o 0 13 1 620.23 659.28 7.28 o 1 13 1 1.99 2.46 0.93 o 2 13 1 113.20 112.67 2.78 o 3 13 1 15.98 14.01 2.09 o 0 14 1 7.45 6.93 1.30 o 1 14 1 60.12 57.94 1.62 o 2 14 1 173.95 184.15 3.49 o 3 14 1 15.32 13.51 2.12 o 0 15 1 57.96 53.07 2.32 o 1 15 1 57.42 59.35 1.85 o 2 15 1 3.82 2.38 1.52 o 3 15 1 15.75 16.24 2.17 o 0 16 1 53.89 52.81 2.32 o 1 16 1 153.24 151.08 2.68 o 2 16 1 46.11 42.33 2.15 o 3 16 1 0.82 1.65 1.99 o 0 17 1 23.62 24.45 2.45 o 1 17 1 11.23 10.91 1.44 o 2 17 1 16.10 15.95 1.83 o 3 17 1 3.55 3.44 2.31 o 0 18 1 66.59 75.95 3.54 o 1 18 1 103.80 102.57 2.94 o 2 18 1 20.99 22.60 2.00 o 0 19 1 0.00 0.74 2.12 o 1 19 1 34.31 28.80 2.25 o 2 19 1 1.47 0.46 1.72 o 0 20 1 21.04 22.26 2.77 o 1 20 1 0.09 -1.14 1.79 o 2 20 1 1.63 2.28 2.02 o 0 21 1 102.09 107.11 4.43 o 1 21 1 11.06 13.67 2.09 o 0 22 1 21.32 23.46 3.05 o 1 22 1 26.43 24.58 2.40 o 0 23 1 30.37 24.82 3.39 o 0 0 2 277.14 303.32 11.85 o 1 0 2 2726.72 2610.38 39.12 o 2 0 2 6.85 6.86 1.33 o 3 0 2 293.66 288.62 5.13 o 4 0 2 1.61 2.06 2.80 o 0 1 2 73.74 56.46 1.10 o 1 1 2 1918.51 1849.18 13.39 o 2 1 2 71.80 73.80 1.64 o 3 1 2 29.48 28.18 1.52 o 4 1 2 31.31 31.30 2.74 o 0 2 2 291.95 222.46 2.18 o 1 2 2 46.30 46.50 1.03 o 2 2 2 10.27 9.98 0.96 o 3 2 2 1.34 1.41 1.15 o 4 2 2 13.07 16.55 2.30 o 0 3 2 4028.63 3718.00 31.09 o 1 3 2 407.82 378.64 6.22 o 2 3 2 130.22 147.42 2.19 o 3 3 2 5.35 3.45 1.25 o 4 3 2 3.08 3.32 2.15 o 0 4 2 628.38 531.20 3.48 o 1 4 2 50.66 52.74 1.07 o 2 4 2 817.38 825.19 10.38 o 3 4 2 40.88 41.29 1.77 o 4 4 2 31.64 34.60 2.50 o 0 5 2 814.41 786.55 8.79 o 1 5 2 314.20 292.11 3.42 o 2 5 2 18.41 18.30 1.17 o 3 5 2 79.58 79.23 2.35 o 4 5 2 0.82 3.00 2.00 o 0 6 2 278.39 258.86 2.77 o 1 6 2 35.43 31.09 0.93 o 2 6 2 59.25 59.51 1.60 o 3 6 2 72.72 78.50 2.39 o 4 6 2 2.61 2.88 2.06 o 0 7 2 327.63 329.49 3.70 o 1 7 2 414.38 402.71 5.43 o 2 7 2 43.38 39.55 1.43 o 3 7 2 0.54 0.85 1.36 o 4 7 2 25.80 26.09 2.62 o 0 8 2 203.69 189.29 2.63 o 1 8 2 665.56 718.54 7.45 o 2 8 2 6.80 5.82 1.08 o 3 8 2 64.35 61.02 2.21 o 4 8 2 5.14 6.07 2.30 o 0 9 2 13.15 14.31 1.21 o 1 9 2 268.73 279.10 3.54 o 2 9 2 88.44 94.85 1.94 o 3 9 2 0.68 0.96 1.53 o 4 9 2 43.81 45.89 3.03 o 0 10 2 168.53 165.42 2.71 o 1 10 2 22.17 19.70 1.10 o 2 10 2 35.06 34.23 1.37 o 3 10 2 49.07 50.91 2.44 o 0 11 2 734.93 765.89 8.51 o 1 11 2 25.53 22.94 1.14 o 2 11 2 2.66 2.68 1.21 o 3 11 2 103.17 101.04 3.09 o 0 12 2 24.54 21.71 1.70 o 1 12 2 76.17 84.33 1.74 o 2 12 2 94.91 89.55 2.52 o 3 12 2 30.31 30.77 3.50 o 0 13 2 263.99 277.15 4.31 o 1 13 2 28.60 29.84 1.28 o 2 13 2 40.67 37.40 2.26 o 3 13 2 3.75 4.64 1.89 o 0 14 2 34.34 31.36 1.68 o 1 14 2 46.52 47.01 1.56 o 2 14 2 15.44 11.07 1.58 o 3 14 2 0.59 0.02 1.87 o 0 15 2 11.04 12.32 1.65 o 1 15 2 244.68 241.05 3.00 o 2 15 2 30.76 26.87 1.85 o 3 15 2 31.39 27.87 5.08 o 0 16 2 2.75 3.61 1.58 o 1 16 2 8.77 9.33 1.42 o 2 16 2 69.64 64.85 3.70 o 3 16 2 0.48 1.91 1.94 o 0 17 2 20.66 18.52 1.91 o 1 17 2 27.93 30.14 1.78 o 2 17 2 5.04 5.69 1.73 o 0 18 2 65.38 59.35 3.25 o 1 18 2 26.37 24.26 1.81 o 2 18 2 51.43 48.64 2.57 o 0 19 2 132.50 154.65 4.92 o 1 19 2 26.64 23.51 1.98 o 2 19 2 4.84 5.34 1.93 o 0 20 2 108.92 112.78 4.46 o 1 20 2 2.05 2.74 1.85 o 2 20 2 18.32 21.92 2.35 o 0 21 2 25.78 26.99 3.05 o 1 21 2 17.12 15.29 2.15 o 0 22 2 15.24 15.96 2.81 o 1 22 2 28.30 31.68 2.56 o 0 23 2 0.12 -0.92 3.95 o 1 0 3 24.39 22.86 1.49 o 2 0 3 30.67 30.99 1.75 o 3 0 3 15.75 14.32 1.90 o 4 0 3 0.03 -0.40 3.49 o 0 1 3 119.82 149.14 2.31 o 1 1 3 161.42 158.38 4.96 o 2 1 3 99.22 93.79 1.83 o 3 1 3 38.69 38.49 1.66 o 4 1 3 9.18 8.97 2.48 o 0 2 3 61.27 50.89 1.71 o 1 2 3 68.90 66.97 2.60 o 2 2 3 35.93 34.92 1.26 o 3 2 3 54.09 53.51 1.85 o 4 2 3 32.08 31.83 3.06 o 0 3 3 1871.02 1802.91 21.52 o 1 3 3 53.12 59.30 1.74 o 2 3 3 54.04 53.71 2.39 o 3 3 3 35.54 35.51 1.71 o 4 3 3 2.30 1.77 2.20 o 0 4 3 50.58 51.55 1.42 o 1 4 3 452.98 476.65 3.09 o 2 4 3 104.25 102.18 1.81 o 3 4 3 12.06 10.37 1.35 o 4 4 3 7.95 10.02 2.38 o 0 5 3 33.56 35.02 1.39 o 1 5 3 15.12 13.45 0.89 o 2 5 3 104.50 105.64 1.86 o 3 5 3 2.96 2.48 1.30 o 4 5 3 8.75 7.57 2.12 o 0 6 3 167.68 177.92 2.50 o 1 6 3 268.41 255.40 5.71 o 2 6 3 122.09 129.95 2.12 o 3 6 3 5.79 3.38 1.42 o 4 6 3 11.80 16.47 2.36 o 0 7 3 2466.61 2477.55 11.03 o 1 7 3 380.80 374.91 3.71 o 2 7 3 88.61 87.94 1.82 o 3 7 3 1.32 0.59 1.45 o 4 7 3 1.42 3.35 2.37 o 0 8 3 254.25 243.46 3.23 o 1 8 3 41.18 40.20 1.22 o 2 8 3 51.75 48.89 1.49 o 3 8 3 52.49 48.41 2.19 o 4 8 3 1.19 3.02 2.33 o 0 9 3 153.35 169.46 2.89 o 1 9 3 71.81 80.66 1.65 o 2 9 3 84.00 74.17 1.74 o 3 9 3 48.85 50.83 2.41 o 0 10 3 280.13 333.65 3.88 o 1 10 3 702.66 693.68 6.98 o 2 10 3 4.16 2.75 0.96 o 3 10 3 23.81 22.39 1.98 o 0 11 3 106.95 103.33 2.40 o 1 11 3 333.83 356.05 4.19 o 2 11 3 12.26 11.10 1.25 o 3 11 3 5.32 5.57 1.75 o 0 12 3 25.56 25.93 1.57 o 1 12 3 3.60 3.85 0.99 o 2 12 3 107.66 113.46 2.58 o 3 12 3 2.22 3.49 2.45 o 0 13 3 216.52 224.14 3.90 o 1 13 3 55.27 56.58 2.04 o 2 13 3 310.05 320.10 5.16 o 3 13 3 39.44 41.37 2.51 o 0 14 3 176.07 200.83 3.97 o 1 14 3 39.09 36.12 1.46 o 2 14 3 39.82 38.67 2.21 o 3 14 3 10.98 9.02 2.04 o 0 15 3 0.21 2.76 1.53 o 1 15 3 232.06 238.32 3.11 o 2 15 3 14.61 13.85 1.81 o 3 15 3 12.50 11.97 2.29 o 0 16 3 45.34 42.75 2.35 o 1 16 3 212.35 213.88 4.54 o 2 16 3 13.04 11.59 1.83 o 3 16 3 15.73 17.65 2.46 o 0 17 3 53.56 50.90 2.59 o 1 17 3 89.39 85.54 2.51 o 2 17 3 77.35 70.87 2.79 o 0 18 3 106.57 120.26 4.65 o 1 18 3 21.26 21.27 1.77 o 2 18 3 38.65 39.05 2.78 o 0 19 3 344.96 380.32 7.29 o 1 19 3 10.34 10.03 1.87 o 2 19 3 4.91 4.78 1.93 o 0 20 3 7.97 12.11 2.65 o 1 20 3 114.41 119.10 3.31 o 2 20 3 8.03 4.92 2.04 o 0 21 3 48.44 48.50 3.82 o 1 21 3 8.08 14.50 2.39 o 0 22 3 0.29 3.16 2.62 o 1 22 3 29.52 31.63 2.74 o 0 0 4 1326.14 1430.94 17.71 o 1 0 4 0.36 0.72 1.06 o 2 0 4 542.41 562.34 7.42 o 3 0 4 0.59 -0.57 1.58 o 4 0 4 8.24 6.11 3.72 o 0 1 4 0.00 -0.06 0.94 o 1 1 4 68.67 70.64 1.60 o 2 1 4 40.76 39.72 1.38 o 3 1 4 84.13 91.00 2.32 o 4 1 4 5.84 4.79 2.37 o 0 2 4 1498.76 1471.63 12.23 o 1 2 4 216.84 225.36 4.49 o 2 2 4 61.51 57.80 1.49 o 3 2 4 6.04 4.27 1.39 o 4 2 4 13.66 15.94 2.66 o 0 3 4 51.68 57.83 1.55 o 1 3 4 1138.06 1166.37 22.33 o 2 3 4 198.69 202.02 2.38 o 3 3 4 28.57 24.54 1.74 o 4 3 4 2.84 3.13 2.34 o 0 4 4 135.00 125.44 2.13 o 1 4 4 121.48 111.73 3.63 o 2 4 4 56.37 64.60 1.62 o 3 4 4 9.74 8.93 1.53 o 4 4 4 16.17 18.72 2.70 o 0 5 4 383.64 393.89 3.74 o 1 5 4 295.78 292.22 2.74 o 2 5 4 208.54 214.58 2.74 o 3 5 4 40.46 42.00 2.02 o 4 5 4 3.36 1.95 2.24 o 0 6 4 1834.01 1878.58 12.82 o 1 6 4 372.01 376.91 7.15 o 2 6 4 9.07 9.00 1.02 o 3 6 4 34.85 32.03 1.89 o 4 6 4 6.19 7.31 2.51 o 0 7 4 95.73 94.42 2.13 o 1 7 4 321.44 351.57 3.06 o 2 7 4 3.75 3.64 1.02 o 3 7 4 12.69 12.40 1.71 o 4 7 4 30.51 40.91 3.07 o 0 8 4 63.33 68.23 1.93 o 1 8 4 461.64 508.98 7.68 o 2 8 4 105.74 108.66 3.29 o 3 8 4 5.80 5.17 1.59 o 0 9 4 450.67 444.11 5.52 o 1 9 4 14.01 14.99 2.11 o 2 9 4 111.80 109.41 2.90 o 3 9 4 3.63 3.10 1.80 o 0 10 4 172.63 167.49 3.01 o 1 10 4 108.05 112.22 1.96 o 2 10 4 74.71 72.33 2.13 o 3 10 4 104.97 109.05 3.81 o 0 11 4 491.70 539.96 5.35 o 1 11 4 16.69 18.69 1.19 o 2 11 4 40.96 40.85 1.84 o 3 11 4 71.58 77.99 4.17 o 0 12 4 192.04 196.56 3.40 o 1 12 4 262.92 271.61 5.53 o 2 12 4 28.51 30.39 1.71 o 3 12 4 18.99 18.30 2.17 o 0 13 4 0.82 2.05 1.29 o 1 13 4 133.17 134.05 2.33 o 2 13 4 57.31 51.24 3.07 o 3 13 4 2.36 3.45 2.02 o 0 14 4 70.82 69.29 2.61 o 1 14 4 108.45 109.22 2.27 o 2 14 4 49.30 44.09 2.12 o 3 14 4 4.84 4.77 2.10 o 0 15 4 55.81 56.43 2.59 o 1 15 4 11.66 11.17 1.34 o 2 15 4 97.61 96.72 3.01 o 3 15 4 2.07 0.20 2.12 o 0 16 4 412.86 441.93 7.78 o 1 16 4 86.89 83.44 2.22 o 2 16 4 7.19 6.18 1.76 o 0 17 4 9.14 9.81 1.92 o 1 17 4 0.01 1.73 1.54 o 2 17 4 7.69 7.95 1.85 o 0 18 4 24.64 21.77 2.23 o 1 18 4 44.08 43.46 2.80 o 2 18 4 4.81 4.98 1.90 o 0 19 4 0.69 1.29 2.26 o 1 19 4 28.59 33.98 2.25 o 2 19 4 5.32 6.03 2.03 o 0 20 4 0.14 0.25 2.35 o 1 20 4 92.70 94.28 5.84 o 0 21 4 5.03 7.74 2.64 o 1 21 4 0.06 -0.08 2.08 o 0 22 4 1.06 0.34 2.74 o 1 0 5 431.84 428.28 11.27 o 2 0 5 940.47 990.02 11.53 o 3 0 5 3.52 4.54 2.07 o 4 0 5 28.33 36.56 4.04 o 0 1 5 391.43 406.40 4.08 o 1 1 5 190.17 181.82 3.99 o 2 1 5 52.34 54.74 1.74 o 3 1 5 8.46 7.98 1.50 o 4 1 5 13.28 12.05 2.53 o 0 2 5 192.76 208.42 2.82 o 1 2 5 66.92 70.48 1.67 o 2 2 5 9.86 8.58 1.13 o 3 2 5 52.05 49.22 2.25 o 4 2 5 1.71 1.55 4.31 o 0 3 5 0.01 0.09 0.96 o 1 3 5 1106.01 1146.28 13.73 o 2 3 5 87.86 88.74 3.12 o 3 3 5 143.91 153.97 3.57 o 4 3 5 0.62 -1.30 2.29 o 0 4 5 93.40 102.20 2.22 o 1 4 5 484.67 500.34 5.27 o 2 4 5 11.19 10.94 1.05 o 3 4 5 2.95 1.66 1.51 o 4 4 5 14.68 15.29 2.63 o 0 5 5 264.69 268.92 4.65 o 1 5 5 15.84 15.99 0.99 o 2 5 5 111.77 109.29 5.26 o 3 5 5 43.69 44.04 2.21 o 4 5 5 31.42 35.52 4.01 o 0 6 5 186.98 203.90 3.32 o 1 6 5 26.33 25.08 2.83 o 2 6 5 193.70 200.07 4.97 o 3 6 5 3.20 1.82 1.53 o 0 7 5 173.23 183.37 2.98 o 1 7 5 60.15 55.43 1.73 o 2 7 5 18.77 17.55 1.21 o 3 7 5 60.96 63.37 2.68 o 0 8 5 841.10 895.20 12.22 o 1 8 5 21.60 19.19 1.06 o 2 8 5 65.04 59.84 1.83 o 3 8 5 89.58 93.85 3.43 o 0 9 5 3.11 4.52 1.36 o 1 9 5 23.45 22.20 1.07 o 2 9 5 61.92 58.23 1.80 o 3 9 5 3.36 3.17 1.90 o 0 10 5 9.94 6.94 1.31 o 1 10 5 70.52 66.46 2.06 o 2 10 5 147.22 144.57 3.26 o 3 10 5 27.94 24.90 2.35 o 0 11 5 11.82 14.22 1.52 o 1 11 5 97.02 96.41 2.25 o 2 11 5 35.75 34.10 1.77 o 3 11 5 0.09 0.87 1.92 o 0 12 5 14.23 12.40 1.48 o 1 12 5 66.68 64.68 1.77 o 2 12 5 82.04 76.26 2.90 o 3 12 5 21.41 23.37 2.69 o 0 13 5 1.67 0.87 1.35 o 1 13 5 107.52 102.95 3.90 o 2 13 5 28.74 25.60 1.76 o 3 13 5 9.61 9.18 2.08 o 0 14 5 3.97 2.47 1.64 o 1 14 5 134.16 132.38 2.88 o 2 14 5 61.67 57.23 2.35 o 3 14 5 5.11 5.16 2.14 o 0 15 5 93.76 93.16 3.18 o 1 15 5 57.46 55.91 2.03 o 2 15 5 26.76 24.31 1.96 o 0 16 5 10.15 9.39 1.95 o 1 16 5 22.33 22.55 1.72 o 2 16 5 14.87 16.06 1.96 o 0 17 5 34.58 36.16 2.53 o 1 17 5 49.41 45.71 2.28 o 2 17 5 27.25 23.48 2.29 o 0 18 5 171.71 175.74 4.45 o 1 18 5 61.00 59.88 2.54 o 2 18 5 8.75 7.09 3.05 o 0 19 5 19.96 21.60 2.44 o 1 19 5 6.92 6.79 2.10 o 0 20 5 0.18 2.01 2.54 o 1 20 5 4.17 4.32 1.90 o 0 21 5 53.97 53.93 4.01 o 0 0 6 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