#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/51/2015193.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015193_Fobs loop_ _publ_author_name 'Pavan Kumar, K. V. P.' 'Kumara Swamy, K. C.' _publ_section_title ; Two phosphate--imidazole complexes with and without a hydrogen-bonded guest molecule ; _journal_coeditor_code SK1869 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o668 _journal_page_last o670 _journal_volume 61 _journal_year 2005 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.542 _cell_angle_gamma 90.000 _cell_length_a 29.3332 _cell_length_b 9.9415 _cell_length_c 23.3483 _exptl_crystal_F_000 2520.00 _reflns_d_resolution_high 0.7508 _[local]_cod_data_source_file sk1869IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' kck53_m in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 584.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10594.93 10674.95 298.06 o 4 0 0 585.92 625.03 46.43 o 6 0 0 10750.52 10379.86 387.35 o 8 0 0 107536.40 125529.96 2898.83 o 10 0 0 26127.91 29699.80 469.96 o 12 0 0 10401.07 10007.44 149.84 o 14 0 0 95.60 229.99 39.82 o 16 0 0 1935.17 2426.19 71.66 o 18 0 0 11229.27 12042.75 147.05 o 20 0 0 12423.64 13043.46 592.51 o 22 0 0 5472.58 5750.37 147.23 o 24 0 0 1756.59 1668.91 124.40 o 26 0 0 2505.78 2447.86 148.35 o 28 0 0 26.52 93.84 79.43 o 30 0 0 82.59 48.25 78.21 o 32 0 0 673.53 846.63 120.45 o 34 0 0 422.31 433.57 107.82 o 36 0 0 106.62 31.90 125.36 o 1 1 0 7744.74 7520.18 51.17 o 3 1 0 4404.85 5731.02 94.02 o 5 1 0 56845.68 63788.43 1517.83 o 7 1 0 4876.83 4652.32 123.86 o 9 1 0 20097.26 24202.97 428.73 o 11 1 0 12634.75 13231.52 245.45 o 13 1 0 9483.96 10503.44 144.42 o 15 1 0 1492.00 1215.61 40.77 o 17 1 0 1789.75 2050.03 52.33 o 19 1 0 3939.91 3985.60 109.25 o 21 1 0 1025.86 1110.82 58.67 o 23 1 0 207.19 208.62 44.14 o 25 1 0 57.31 62.62 46.60 o 27 1 0 39.23 35.43 50.21 o 29 1 0 395.91 404.44 67.74 o 31 1 0 10.39 29.39 56.31 o 33 1 0 2.99 3.03 57.57 o 35 1 0 94.74 123.95 67.25 o 0 2 0 196.74 319.76 18.43 o 2 2 0 25797.65 25601.66 187.40 o 4 2 0 115301.89 120248.62 1442.62 o 6 2 0 3036.87 3266.52 51.48 o 8 2 0 1671.22 1551.79 42.91 o 10 2 0 30.27 0.73 14.34 o 12 2 0 277.17 404.45 23.15 o 14 2 0 26760.99 31296.75 617.25 o 16 2 0 8442.81 8224.54 159.32 o 18 2 0 4472.10 4179.35 189.84 o 20 2 0 90.01 55.87 37.98 o 22 2 0 8701.03 8355.82 181.50 o 24 2 0 1201.34 1263.41 65.96 o 26 2 0 170.68 155.69 52.38 o 28 2 0 332.74 313.82 64.29 o 30 2 0 986.65 1005.16 85.70 o 32 2 0 8.43 68.94 59.62 o 34 2 0 93.43 112.99 63.96 o 1 3 0 1283.82 1305.55 29.37 o 3 3 0 438.12 347.65 19.21 o 5 3 0 2626.78 1969.38 34.74 o 7 3 0 22930.62 24953.53 398.91 o 9 3 0 33170.32 39504.26 867.07 o 11 3 0 0.20 8.49 15.93 o 13 3 0 1811.36 1645.46 54.19 o 15 3 0 11613.19 12560.91 385.45 o 17 3 0 353.83 261.39 40.73 o 19 3 0 9195.35 9941.50 325.44 o 21 3 0 1439.35 1360.46 69.77 o 23 3 0 93.72 17.99 40.14 o 25 3 0 335.36 359.37 50.49 o 27 3 0 120.31 199.42 49.53 o 29 3 0 80.59 68.57 52.14 o 31 3 0 1280.79 1307.09 96.68 o 33 3 0 21.42 20.03 69.70 o 0 4 0 2786.96 2266.38 62.24 o 2 4 0 20.42 21.65 15.41 o 4 4 0 1089.53 1221.93 31.89 o 6 4 0 426.79 427.57 23.13 o 8 4 0 13307.14 15401.19 281.20 o 10 4 0 39.40 36.76 19.07 o 12 4 0 404.04 309.99 24.35 o 14 4 0 133.40 51.57 33.80 o 16 4 0 228.21 126.53 37.70 o 18 4 0 2643.35 2562.23 112.61 o 20 4 0 1164.03 1201.22 61.66 o 22 4 0 568.76 587.71 65.82 o 24 4 0 776.40 753.35 60.19 o 26 4 0 281.92 317.04 51.67 o 28 4 0 349.26 356.39 60.38 o 30 4 0 415.29 512.17 74.49 o 32 4 0 123.39 122.55 86.84 o 1 5 0 13276.28 13697.84 94.38 o 3 5 0 7090.31 6779.50 68.94 o 5 5 0 5657.18 5844.81 118.69 o 7 5 0 216.97 179.49 22.94 o 9 5 0 3399.22 3480.81 89.02 o 11 5 0 3735.77 3817.54 103.21 o 13 5 0 734.39 702.99 56.46 o 15 5 0 2570.56 2845.16 132.38 o 17 5 0 36.90 -32.57 38.61 o 19 5 0 1166.29 1131.14 63.03 o 21 5 0 93.51 59.99 41.62 o 23 5 0 64.33 45.38 43.39 o 25 5 0 64.98 75.93 48.52 o 27 5 0 237.85 286.82 67.06 o 29 5 0 0.00 -21.17 56.26 o 31 5 0 10.35 27.68 71.48 o 33 5 0 226.85 234.58 170.02 o 0 6 0 2367.71 2069.71 69.99 o 2 6 0 932.66 897.69 40.10 o 4 6 0 12856.98 13776.72 105.22 o 6 6 0 389.24 392.61 30.07 o 8 6 0 208.89 221.96 27.73 o 10 6 0 4311.94 4477.52 210.66 o 12 6 0 1979.56 1824.48 68.71 o 14 6 0 402.39 382.24 45.32 o 16 6 0 21.10 -4.67 38.92 o 18 6 0 551.61 500.03 50.56 o 20 6 0 293.25 304.14 48.92 o 22 6 0 402.33 441.77 59.50 o 24 6 0 26.10 56.67 55.15 o 26 6 0 88.48 174.44 62.56 o 28 6 0 0.03 6.42 63.33 o 30 6 0 142.32 216.05 71.21 o 1 7 0 9.45 -3.52 25.72 o 3 7 0 134.93 97.74 28.78 o 5 7 0 477.35 595.22 36.80 o 7 7 0 779.43 794.53 43.59 o 9 7 0 198.49 207.65 38.60 o 11 7 0 161.06 109.37 40.88 o 13 7 0 280.56 254.10 42.44 o 15 7 0 7.61 -27.52 36.87 o 17 7 0 258.45 229.99 49.20 o 19 7 0 611.78 606.32 68.60 o 21 7 0 87.19 48.78 52.81 o 23 7 0 0.29 5.80 52.80 o 25 7 0 1.81 3.16 56.46 o 27 7 0 39.67 8.92 59.00 o 29 7 0 117.47 25.72 101.37 o 0 8 0 15.45 -3.22 39.32 o 2 8 0 415.18 406.08 36.85 o 4 8 0 0.36 5.65 29.26 o 6 8 0 0.05 -12.93 30.83 o 8 8 0 482.47 540.62 50.69 o 10 8 0 2598.52 2402.11 94.33 o 12 8 0 2998.42 2841.25 109.21 o 14 8 0 533.49 544.66 64.36 o 16 8 0 549.95 548.96 66.85 o 18 8 0 478.72 460.76 67.94 o 20 8 0 488.19 501.83 70.22 o 22 8 0 1.50 2.92 53.30 o 24 8 0 653.14 711.52 84.69 o 26 8 0 120.54 129.73 70.17 o 1 9 0 288.14 284.80 36.82 o 3 9 0 701.95 683.31 50.38 o 5 9 0 659.25 650.60 49.91 o 7 9 0 1402.50 1380.62 77.75 o 9 9 0 237.34 288.46 54.91 o 11 9 0 282.57 290.56 56.87 o 13 9 0 177.43 107.03 50.88 o 15 9 0 459.95 498.24 67.96 o 17 9 0 139.72 99.43 54.74 o 19 9 0 165.07 220.19 61.14 o 21 9 0 804.68 769.75 84.61 o 23 9 0 332.15 383.29 78.15 o 0 10 0 1235.04 1274.10 89.72 o 2 10 0 2900.39 2971.69 87.48 o 4 10 0 1887.76 2106.50 133.22 o 6 10 0 228.31 205.65 54.62 o 8 10 0 324.18 460.98 62.92 o 10 10 0 207.60 280.49 58.61 o 12 10 0 19.15 -5.18 47.62 o 14 10 0 7.34 11.07 48.77 o 16 10 0 1387.62 1508.92 100.80 o 18 10 0 70.92 160.07 61.75 o 20 10 0 75.80 183.13 67.35 o 22 10 0 1.74 -3.00 112.22 o 1 11 0 0.23 -75.82 80.70 o 3 11 0 71.16 132.13 60.01 o 5 11 0 1373.22 1506.14 92.37 o 7 11 0 1089.72 1185.75 85.99 o 9 11 0 232.55 257.13 61.32 o 11 11 0 72.71 9.58 50.33 o 13 11 0 18.12 1.76 53.69 o 15 11 0 594.13 701.01 81.60 o 17 11 0 67.08 126.58 64.52 o 19 11 0 594.22 562.61 171.15 o 4 12 0 2.35 -23.65 103.97 o 6 12 0 305.48 330.87 97.72 o 8 12 0 654.47 734.89 95.58 o 10 12 0 141.49 92.66 71.78 o 12 12 0 236.65 318.90 71.57 o 14 12 0 76.77 74.95 83.50 o 5 13 0 42.24 -93.08 96.83 o -35 1 1 443.79 496.16 80.66 o -33 1 1 730.27 765.35 83.40 o -31 1 1 6.82 -50.04 50.04 o -29 1 1 22.04 57.34 54.32 o -27 1 1 1738.22 1705.44 94.64 o -25 1 1 2133.69 2056.53 85.59 o -23 1 1 1200.97 1241.63 62.71 o -21 1 1 3135.19 3063.23 87.37 o -19 1 1 12.02 -7.79 27.88 o -17 1 1 124.42 111.64 25.72 o -15 1 1 998.89 940.39 37.13 o -13 1 1 2442.51 2703.21 44.78 o -11 1 1 757.02 809.54 28.68 o -9 1 1 13160.48 14157.65 299.47 o -7 1 1 639.95 768.23 24.86 o -5 1 1 2929.37 2935.75 73.02 o -3 1 1 166387.92 155092.92 1686.16 o -1 1 1 46.09 66.90 6.39 o 1 1 1 679.57 724.78 20.66 o 3 1 1 7058.93 7849.10 161.22 o 5 1 1 802.85 707.62 21.32 o 7 1 1 105.87 72.20 15.83 o 9 1 1 596.29 698.40 27.88 o 11 1 1 22563.74 27101.62 413.57 o 13 1 1 160.22 123.96 21.91 o 15 1 1 98.02 50.57 23.14 o 17 1 1 1031.18 1121.58 44.50 o 19 1 1 2711.52 2581.49 61.81 o 21 1 1 207.01 145.12 44.81 o 23 1 1 924.08 928.84 58.62 o 25 1 1 6.21 -41.81 41.81 o 27 1 1 17.96 -12.80 50.08 o 29 1 1 17.65 15.13 52.73 o 31 1 1 95.31 96.70 58.00 o 33 1 1 1021.44 1175.62 95.99 o 35 1 1 78.64 88.25 75.40 o -36 2 1 13.22 41.38 94.49 o -34 2 1 60.00 28.72 60.39 o -32 2 1 448.10 411.65 71.18 o -30 2 1 461.67 608.53 75.24 o -28 2 1 8.88 44.05 54.11 o -26 2 1 270.65 234.12 53.07 o -24 2 1 184.67 199.74 46.11 o -22 2 1 138.19 108.54 42.30 o -20 2 1 3456.24 3561.26 84.30 o -18 2 1 1078.83 1130.02 55.60 o -16 2 1 422.38 282.33 25.25 o -14 2 1 692.01 637.99 29.15 o -12 2 1 13712.71 16175.83 312.36 o -10 2 1 589.14 580.82 22.52 o -8 2 1 38013.61 42532.67 704.41 o -6 2 1 13.25 24.76 11.72 o -4 2 1 75.40 129.78 12.81 o -2 2 1 3492.83 4051.42 39.40 o 0 2 1 68430.59 68647.41 651.08 o 2 2 1 7197.98 7224.76 67.02 o 4 2 1 6620.64 6952.37 89.96 o 6 2 1 1926.83 1687.36 44.30 o 8 2 1 7801.98 9069.38 210.15 o 10 2 1 31092.60 32998.65 575.93 o 12 2 1 15.39 101.33 20.01 o 14 2 1 795.53 791.62 33.59 o 16 2 1 1888.41 1939.17 49.25 o 18 2 1 778.59 838.26 45.90 o 20 2 1 861.89 944.27 57.26 o 22 2 1 140.54 118.80 42.19 o 24 2 1 3056.08 3160.69 105.27 o 26 2 1 131.93 155.28 50.33 o 28 2 1 316.94 442.16 66.89 o 30 2 1 273.95 322.33 66.06 o 32 2 1 79.38 53.64 59.98 o 34 2 1 55.84 132.13 74.94 o -35 3 1 0.00 102.84 129.86 o -33 3 1 42.83 37.85 61.62 o -31 3 1 278.50 386.94 70.83 o -29 3 1 806.48 838.55 72.62 o -27 3 1 1031.95 1160.86 68.87 o -25 3 1 100.63 50.08 42.30 o -23 3 1 224.18 159.93 43.65 o -21 3 1 125.97 133.50 43.40 o -19 3 1 3380.94 3623.79 181.87 o -17 3 1 454.61 357.08 41.80 o -15 3 1 2450.88 2204.31 100.29 o -13 3 1 939.61 1131.13 32.38 o -11 3 1 25865.25 30950.79 557.86 o -9 3 1 594.77 604.44 22.98 o -7 3 1 1199.28 1019.95 27.37 o -5 3 1 1055.12 1246.99 33.78 o -3 3 1 897.38 891.44 27.21 o -1 3 1 21095.22 19616.11 98.03 o 1 3 1 139.81 104.03 15.91 o 3 3 1 1668.97 1606.17 32.13 o 5 3 1 771.95 977.45 30.23 o 7 3 1 2387.32 2379.98 59.53 o 9 3 1 1730.13 1657.25 57.91 o 11 3 1 463.12 324.93 23.00 o 13 3 1 682.64 767.98 32.58 o 15 3 1 8881.40 9241.60 343.26 o 17 3 1 592.90 541.21 63.00 o 19 3 1 7014.76 7210.75 228.58 o 21 3 1 617.19 649.16 54.73 o 23 3 1 114.48 59.73 41.21 o 25 3 1 206.80 117.06 44.83 o 27 3 1 124.92 186.40 49.36 o 29 3 1 158.41 149.22 56.34 o 31 3 1 197.43 177.98 73.62 o 33 3 1 138.32 197.62 96.25 o -32 4 1 20.94 30.11 80.48 o -30 4 1 748.52 854.10 76.22 o -28 4 1 1341.64 1402.33 76.02 o -26 4 1 115.88 86.49 46.57 o -24 4 1 580.61 569.99 55.29 o -22 4 1 848.18 690.80 56.17 o -20 4 1 4.25 -6.40 38.25 o -18 4 1 6374.74 6818.28 286.87 o -16 4 1 2128.35 1726.69 71.31 o -14 4 1 2.91 2.99 31.22 o -12 4 1 48.28 79.00 22.20 o -10 4 1 3682.93 3623.86 58.54 o -8 4 1 419.03 361.75 21.81 o -6 4 1 187.42 266.29 20.50 o -4 4 1 4552.03 3532.43 46.19 o -2 4 1 2639.01 2345.20 39.60 o 0 4 1 7370.44 7971.03 65.33 o 2 4 1 954.71 1181.83 32.13 o 4 4 1 1008.18 761.34 28.96 o 6 4 1 8.12 8.78 17.61 o 8 4 1 42.91 39.91 18.32 o 10 4 1 2418.26 2541.08 74.49 o 12 4 1 199.03 249.60 24.94 o 14 4 1 1649.58 1709.39 84.48 o 16 4 1 2687.75 2600.77 98.56 o 18 4 1 2136.68 2041.31 104.89 o 20 4 1 896.23 950.43 59.37 o 22 4 1 1235.88 1202.55 66.22 o 24 4 1 550.54 559.39 56.03 o 26 4 1 115.13 85.42 49.82 o 28 4 1 2047.75 1902.55 93.65 o 30 4 1 368.89 290.05 82.13 o 32 4 1 60.74 78.39 83.62 o -33 5 1 88.91 4.13 153.13 o -31 5 1 331.80 281.90 85.02 o -29 5 1 24.45 -20.19 48.72 o -27 5 1 570.09 620.30 68.75 o -25 5 1 861.46 844.49 63.45 o -23 5 1 561.05 501.20 54.54 o -21 5 1 466.20 389.40 48.96 o -19 5 1 2795.83 2845.73 96.96 o -17 5 1 583.99 557.39 51.11 o -15 5 1 3213.11 3299.58 115.91 o -13 5 1 1088.14 1104.94 59.39 o -11 5 1 1253.50 1294.30 55.05 o -9 5 1 259.24 254.03 24.39 o -7 5 1 20797.54 21449.42 191.85 o -5 5 1 654.90 685.14 30.27 o -3 5 1 31529.49 35285.33 345.32 o -1 5 1 4951.02 5025.32 60.28 o 1 5 1 1592.42 1576.27 39.64 o 3 5 1 7.75 -17.75 17.75 o 5 5 1 2282.29 2118.12 44.63 o 7 5 1 7021.16 7099.52 143.61 o 9 5 1 228.91 209.94 24.91 o 11 5 1 489.68 456.67 34.81 o 13 5 1 468.17 504.58 43.45 o 15 5 1 987.71 1055.67 62.11 o 17 5 1 349.54 372.05 45.82 o 19 5 1 2723.92 2771.43 156.55 o 21 5 1 1088.75 930.48 60.27 o 23 5 1 315.23 289.39 54.08 o 25 5 1 144.25 146.12 58.71 o 27 5 1 459.80 418.60 70.50 o 29 5 1 0.59 -5.66 55.54 o 31 5 1 214.77 248.38 82.74 o -32 6 1 331.35 415.49 186.16 o -30 6 1 10.16 8.03 61.78 o -28 6 1 13.32 -52.51 52.51 o -26 6 1 95.90 101.10 59.41 o -24 6 1 61.65 99.97 51.53 o -22 6 1 244.23 253.33 48.19 o -20 6 1 2482.97 2305.58 179.34 o -18 6 1 192.90 206.75 42.52 o -16 6 1 1592.65 1610.44 71.35 o -14 6 1 1343.89 1237.40 84.74 o -12 6 1 799.90 777.02 54.31 o -10 6 1 31.04 64.89 33.22 o -8 6 1 1957.82 1603.78 46.71 o -6 6 1 1113.08 1137.21 41.67 o -4 6 1 770.85 839.77 38.97 o -2 6 1 884.54 829.74 36.05 o 0 6 1 8384.65 7942.66 81.87 o 2 6 1 39.91 45.30 22.49 o 4 6 1 3605.75 3434.25 58.54 o 6 6 1 308.31 358.36 29.56 o 8 6 1 1285.51 1218.39 46.77 o 10 6 1 150.22 160.67 37.49 o 12 6 1 9815.11 9639.64 330.52 o 14 6 1 634.16 587.67 48.38 o 16 6 1 286.22 266.55 44.88 o 18 6 1 167.65 201.68 47.34 o 20 6 1 45.75 101.36 54.64 o 22 6 1 49.04 2.98 50.76 o 24 6 1 199.48 220.75 62.65 o 26 6 1 354.96 353.52 68.95 o 28 6 1 27.34 -32.01 55.89 o 30 6 1 10.04 -61.41 72.74 o -31 7 1 14.91 -90.83 132.87 o -29 7 1 0.82 24.94 63.36 o -27 7 1 28.06 55.81 62.12 o -25 7 1 136.50 170.13 62.13 o -23 7 1 1759.53 1679.18 100.51 o -21 7 1 949.47 815.85 78.77 o -19 7 1 2.26 -16.78 39.34 o -17 7 1 2658.73 2522.09 148.45 o -15 7 1 220.58 205.53 43.10 o -13 7 1 6262.25 6415.38 313.32 o -11 7 1 2478.26 2732.64 87.77 o -9 7 1 7218.31 6908.82 282.88 o -7 7 1 2646.12 3089.55 82.82 o -5 7 1 1777.62 1581.43 50.43 o -3 7 1 11191.36 11121.53 113.98 o -1 7 1 7030.78 7078.25 86.01 o 1 7 1 3861.38 3579.49 65.41 o 3 7 1 8348.42 8171.80 91.93 o 5 7 1 1919.05 1743.86 52.36 o 7 7 1 18.73 30.38 30.58 o 9 7 1 4997.60 4679.85 142.24 o 11 7 1 26.53 18.90 35.17 o 13 7 1 2394.07 2433.38 135.28 o 15 7 1 359.56 365.19 59.85 o 17 7 1 481.47 365.82 60.62 o 19 7 1 132.41 92.94 55.01 o 21 7 1 819.78 814.98 80.83 o 23 7 1 577.84 550.23 76.02 o 25 7 1 26.30 -17.86 58.24 o 27 7 1 212.66 127.96 65.52 o 29 7 1 311.85 472.59 125.02 o -28 8 1 206.12 352.06 164.39 o -26 8 1 50.78 48.20 63.30 o -24 8 1 217.52 296.58 71.28 o -22 8 1 21.80 -39.82 49.92 o 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85.50 o -13 3 28 446.96 446.87 76.51 o -11 3 28 963.16 1014.79 96.65 o -9 3 28 123.12 199.24 73.08 o -7 3 28 58.60 58.68 64.35 o -5 3 28 1.87 3.25 66.62 o -3 3 28 46.20 -5.25 162.14 o -24 4 28 0.00 -18.54 78.14 o -22 4 28 35.10 3.98 67.63 o -20 4 28 96.86 71.05 76.46 o -18 4 28 63.76 45.75 94.58 o -16 4 28 142.09 148.95 97.07 o -14 4 28 23.52 5.56 80.88 o -12 4 28 261.38 254.53 100.40 o -10 4 28 2.17 17.29 62.28 o -8 4 28 50.42 72.00 100.52 o -6 4 28 167.71 215.18 111.05 o -4 4 28 2.87 -84.45 152.76 o -21 5 28 8.56 4.32 101.09 o -19 5 28 243.65 83.40 106.97 o -17 5 28 723.76 737.85 136.34 o -9 5 28 415.34 430.50 167.02 o -7 5 28 65.84 93.26 102.98 o -21 1 29 16.76 -6.73 76.10 o -19 1 29 30.79 -5.77 83.85 o -17 1 29 510.72 442.49 76.44 o -15 1 29 935.37 975.42 93.80 o -13 1 29 688.93 720.22 88.04 o -11 1 29 79.48 71.34 66.00 o -9 1 29 58.11 37.72 66.41 o -7 1 29 71.26 82.64 70.75 o -5 1 29 26.45 -93.08 145.63 o -24 2 29 46.15 52.92 124.61 o -22 2 29 0.02 -5.04 109.78 o -20 2 29 42.06 81.80 91.32 o -18 2 29 355.16 366.45 107.08 o -16 2 29 97.42 102.74 90.71 o -14 2 29 108.68 182.44 70.45 o -12 2 29 180.59 125.86 66.94 o -10 2 29 0.34 82.61 67.13 o -8 2 29 71.63 98.78 69.27 o -6 2 29 45.87 139.91 104.43 o -23 3 29 59.40 134.89 94.49 o -21 3 29 84.68 161.99 155.57 o -19 3 29 236.51 219.88 100.96 o -17 3 29 0.23 -50.36 83.58 o -15 3 29 4.56 88.31 89.82 o -13 3 29 198.29 207.56 82.79 o -11 3 29 123.96 195.93 70.18 o -9 3 29 100.19 167.28 101.41 o -7 3 29 236.16 273.59 115.58 o -10 4 29 320.56 476.96 179.22 o -8 4 29 406.30 664.13 131.81 o -18 0 30 458.07 421.80 108.48 o -16 0 30 699.99 694.18 124.24 o -14 0 30 105.51 122.57 93.61 o -12 0 30 372.82 359.40 108.38 o -10 0 30 0.06 42.76 87.10 o -21 1 30 39.19 160.26 133.99 o -19 1 30 118.01 118.47 92.34 o -17 1 30 106.24 116.69 66.04 o -15 1 30 938.20 1098.19 98.87 o -13 1 30 40.21 58.43 66.32 o -11 1 30 56.47 78.40 76.92 o -9 1 30 11.93 87.08 151.26 o -22 2 30 556.25 495.80 115.30 o -20 2 30 168.57 167.41 99.55 o -18 2 30 21.94 -61.53 86.46 o -16 2 30 8.04 38.50 107.34 o -14 2 30 1.31 72.32 90.43 o -12 2 30 0.50 14.24 91.21 o -10 2 30 40.46 42.09 118.60 o -13 3 30 232.26 119.35 133.24 o -11 3 30 223.13 266.30 110.19 o -15 1 31 402.83 201.55 155.76 o