#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/51/2015194.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015194_Fobs loop_ _publ_author_name 'Nichol, Gary S.' 'Clegg, William' _publ_section_title ; Polymorphism in an unexpected caesium complex of 5-hydroxyhydurilic acid ; _journal_coeditor_code SK1870 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m459 _journal_page_last m462 _journal_volume 61 _journal_year 2005 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2bc 2n' _symmetry_space_group_name_H-M 'P n a b' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.6671 _cell_length_b 7.0632 _cell_length_c 23.5991 _exptl_crystal_F_000 1576.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file sk1870Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' gsn50 in Pnab' _shelx_refln_list_code 4 _shelx_f_calc_maximum 367.56 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z+1/2' '-x+1/2, y, -z' '-x, -y+1/2, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, z-1/2' 'x-1/2, -y, z' 'x, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 16521.55 16194.46 422.81 o 6 0 0 307.84 339.48 25.91 o 8 0 0 33764.08 34408.56 774.79 o 10 0 0 30366.87 29480.71 578.71 o 12 0 0 25130.64 25264.13 558.86 o 14 0 0 21882.61 22817.66 1391.56 o 16 0 0 7340.55 6851.48 646.19 o 0 2 0 557.89 526.40 66.48 o 1 2 0 31798.16 32012.82 382.11 o 2 2 0 57714.77 58574.32 711.08 o 3 2 0 15980.73 17088.98 212.92 o 4 2 0 8277.16 8380.44 110.07 o 5 2 0 67619.80 68741.15 920.01 o 6 2 0 1217.80 1271.68 36.74 o 7 2 0 62062.30 64115.98 872.22 o 8 2 0 103.38 63.60 29.60 o 9 2 0 32841.98 33054.67 442.61 o 10 2 0 9111.63 8836.23 138.38 o 11 2 0 4671.04 4474.98 84.96 o 12 2 0 14357.46 14427.23 240.17 o 13 2 0 550.45 495.58 67.59 o 14 2 0 4887.94 5091.83 157.90 o 15 2 0 5834.48 5968.22 200.75 o 16 2 0 12.70 156.91 196.23 o 17 2 0 14282.13 14250.93 668.73 o 0 4 0 7656.51 7904.26 146.05 o 1 4 0 1734.51 1717.50 45.44 o 2 4 0 10591.97 10836.42 148.57 o 3 4 0 3054.29 2937.18 56.12 o 4 4 0 3646.83 3620.47 66.07 o 5 4 0 41581.59 41634.49 500.82 o 6 4 0 1190.70 1061.22 42.61 o 7 4 0 41682.65 40165.31 504.30 o 8 4 0 4435.69 4685.83 107.49 o 9 4 0 3787.53 3932.74 99.75 o 10 4 0 1514.03 1366.30 94.89 o 11 4 0 5567.72 5346.89 146.03 o 12 4 0 5026.24 5156.98 160.94 o 13 4 0 138.72 110.11 99.00 o 14 4 0 5447.23 5453.41 208.30 o 15 4 0 1936.26 1748.22 218.39 o 0 6 0 35511.14 34498.06 697.21 o 1 6 0 1301.15 1244.58 66.92 o 2 6 0 20627.07 20370.53 333.05 o 3 6 0 983.54 972.35 69.30 o 4 6 0 7519.19 7297.22 168.87 o 5 6 0 251.91 144.44 84.28 o 6 6 0 211.24 322.80 105.21 o 7 6 0 217.42 219.40 83.52 o 8 6 0 672.73 842.48 90.00 o 9 6 0 138.26 146.50 107.81 o 10 6 0 11158.08 11235.23 294.96 o 11 6 0 109.41 194.38 146.83 o 12 6 0 9995.28 10530.11 398.19 o 13 6 0 328.58 199.84 211.63 o 0 8 0 2844.12 2856.11 228.94 o 1 8 0 2465.40 2423.42 159.90 o 2 8 0 2106.98 2075.80 144.31 o 3 8 0 9844.84 9915.40 253.39 o 4 8 0 519.31 546.94 118.13 o 5 8 0 10061.54 10265.42 248.68 o 6 8 0 53.79 11.32 142.78 o 7 8 0 9829.16 9501.36 319.80 o 8 8 0 359.57 30.36 171.00 o 4 0 1 26707.20 25381.77 406.29 o 6 0 1 29008.45 28490.82 364.81 o 8 0 1 46260.52 47060.59 587.34 o 10 0 1 14070.01 13879.32 198.12 o 12 0 1 2296.76 2275.86 83.33 o 14 0 1 3401.49 3439.36 157.24 o 16 0 1 2850.05 2347.58 174.04 o 3 1 1 59976.97 58543.50 596.36 o 4 1 1 784.34 946.71 20.11 o 5 1 1 23260.93 23296.04 219.45 o 6 1 1 69.24 57.68 16.24 o 7 1 1 16489.90 15869.27 150.86 o 8 1 1 1088.17 1102.09 24.74 o 9 1 1 2641.00 2677.10 39.43 o 10 1 1 1080.27 1051.91 29.59 o 11 1 1 2763.64 2732.96 52.79 o 12 1 1 703.75 733.56 44.42 o 13 1 1 11.87 166.27 48.26 o 14 1 1 2736.15 2714.75 90.89 o 15 1 1 762.47 900.88 103.60 o 16 1 1 1355.53 1382.93 126.50 o 17 1 1 996.89 875.05 140.96 o 1 2 1 79746.77 81939.48 685.33 o 2 2 1 26322.89 27509.13 242.99 o 3 2 1 37785.08 37784.58 326.75 o 4 2 1 3088.40 3126.10 35.44 o 5 2 1 1206.48 1354.73 27.63 o 6 2 1 8278.53 8530.00 109.99 o 7 2 1 566.85 660.60 31.15 o 8 2 1 9057.31 8973.17 90.78 o 9 2 1 16962.85 16817.98 156.46 o 10 2 1 186.17 171.36 27.92 o 11 2 1 5243.97 5310.26 67.95 o 12 2 1 6.07 -6.97 34.45 o 13 2 1 14664.10 14700.29 191.98 o 14 2 1 7.86 -14.41 72.01 o 15 2 1 5006.32 5279.92 132.79 o 16 2 1 148.09 427.63 127.88 o 17 2 1 1049.02 1026.56 169.61 o 0 3 1 8925.05 9096.14 115.07 o 1 3 1 10483.01 11019.82 101.27 o 2 3 1 22643.84 23137.04 197.88 o 3 3 1 2154.28 2281.28 31.33 o 4 3 1 13194.88 13484.84 123.64 o 5 3 1 782.37 754.11 20.11 o 6 3 1 2250.49 2347.26 36.92 o 7 3 1 1131.68 1186.82 33.69 o 8 3 1 2670.04 2772.90 51.35 o 9 3 1 1651.11 1757.31 51.61 o 10 3 1 5401.71 5553.29 80.27 o 11 3 1 46.36 28.40 39.69 o 12 3 1 10897.28 10932.74 151.40 o 13 3 1 603.98 463.58 57.00 o 14 3 1 5165.20 4976.15 130.80 o 15 3 1 0.65 -41.54 104.06 o 16 3 1 1336.52 1523.52 153.28 o 1 4 1 29237.66 29149.69 255.89 o 2 4 1 8889.42 8750.45 87.54 o 3 4 1 16945.44 16785.30 148.91 o 4 4 1 15215.19 15459.94 144.22 o 5 4 1 10324.13 10223.34 103.91 o 6 4 1 11988.65 12100.86 118.60 o 7 4 1 1210.69 1279.02 36.75 o 8 4 1 17519.87 17798.71 221.88 o 9 4 1 4006.02 3857.04 75.75 o 10 4 1 1061.85 1005.77 54.97 o 11 4 1 10979.18 10676.71 147.28 o 12 4 1 131.42 178.97 62.49 o 13 4 1 10676.19 10791.47 175.23 o 14 4 1 204.18 193.32 101.47 o 15 4 1 4493.62 4591.92 167.66 o 0 5 1 1486.45 1322.15 48.80 o 1 5 1 833.78 858.51 32.36 o 2 5 1 2901.38 2944.20 46.09 o 3 5 1 7323.59 7595.32 84.67 o 4 5 1 667.18 577.83 33.44 o 5 5 1 10711.94 10732.17 128.00 o 6 5 1 497.86 450.75 36.42 o 7 5 1 6516.71 6478.61 91.20 o 8 5 1 1239.46 1200.68 51.74 o 9 5 1 5978.82 5555.49 102.12 o 10 5 1 457.04 406.32 59.01 o 11 5 1 542.93 515.79 89.43 o 12 5 1 445.53 501.94 88.94 o 13 5 1 96.50 214.37 93.53 o 14 5 1 122.24 45.65 129.33 o 1 6 1 471.51 514.57 44.70 o 2 6 1 7222.19 7138.18 102.17 o 3 6 1 142.85 145.16 46.77 o 4 6 1 18872.73 18408.85 223.76 o 5 6 1 99.74 135.49 50.29 o 6 6 1 26099.46 25682.30 310.97 o 7 6 1 247.38 218.24 65.23 o 8 6 1 13858.46 13446.93 197.37 o 9 6 1 649.62 708.02 80.01 o 10 6 1 5727.91 5405.50 175.82 o 11 6 1 1393.05 1190.08 121.11 o 12 6 1 814.25 871.66 147.10 o 13 6 1 0.88 40.35 149.80 o 0 7 1 8571.00 8147.18 199.91 o 1 7 1 1120.73 983.23 69.95 o 2 7 1 2397.07 2302.82 74.66 o 3 7 1 800.95 825.27 61.92 o 4 7 1 416.15 434.78 60.76 o 5 7 1 2002.57 2117.25 81.21 o 6 7 1 76.03 84.97 73.29 o 7 7 1 1865.94 1912.91 89.89 o 8 7 1 1230.41 1374.67 117.07 o 9 7 1 1625.64 1833.07 131.83 o 10 7 1 504.63 596.83 132.54 o 11 7 1 99.68 145.69 177.34 o 1 8 1 11426.26 11923.36 216.73 o 2 8 1 857.52 833.77 95.82 o 3 8 1 7751.00 7592.93 155.74 o 4 8 1 365.03 314.15 88.41 o 5 8 1 353.97 443.36 88.62 o 6 8 1 1524.76 2024.01 114.87 o 7 8 1 191.78 141.33 116.25 o 8 8 1 1392.42 1399.33 130.06 o 0 9 1 3422.30 3188.32 248.21 o 1 9 1 144.05 285.40 128.61 o 2 9 1 1715.89 2006.14 135.06 o 3 9 1 11.11 80.22 128.12 o 4 0 2 11921.31 11473.65 141.95 o 6 0 2 10065.33 10395.60 148.76 o 8 0 2 1112.23 1180.33 33.23 o 10 0 2 8523.61 8490.10 133.99 o 12 0 2 8860.13 8502.03 148.70 o 14 0 2 1314.38 1256.02 72.59 o 16 0 2 1686.99 1585.75 245.17 o 3 1 2 76549.92 77055.04 766.62 o 4 1 2 94393.55 95153.14 1028.97 o 5 1 2 5318.45 5080.44 64.45 o 6 1 2 7542.16 7780.28 79.33 o 7 1 2 2146.38 2207.67 34.24 o 8 1 2 14986.68 15168.38 138.96 o 9 1 2 6013.48 5983.27 68.86 o 10 1 2 1483.12 1496.53 31.50 o 11 1 2 17933.21 18324.00 188.97 o 12 1 2 596.26 631.03 49.27 o 13 1 2 10021.38 9851.12 139.43 o 14 1 2 1298.20 1437.49 87.82 o 15 1 2 4952.88 4821.77 148.16 o 16 1 2 338.20 506.18 124.54 o 17 1 2 2532.04 2403.90 159.21 o 0 2 2 18894.86 19104.56 234.52 o 1 2 2 2375.34 2493.87 30.11 o 2 2 2 4307.37 4577.63 47.55 o 3 2 2 49.51 73.55 15.39 o 4 2 2 4.82 4.39 15.35 o 5 2 2 22294.01 22985.76 247.23 o 6 2 2 4318.22 4391.45 54.22 o 7 2 2 18009.36 17698.16 175.10 o 8 2 2 131.93 119.72 22.39 o 9 2 2 1273.84 1247.34 29.35 o 10 2 2 284.64 255.95 29.85 o 11 2 2 1020.55 993.50 36.09 o 12 2 2 5263.74 5129.96 75.93 o 13 2 2 284.95 284.47 45.03 o 14 2 2 1849.62 1794.49 76.64 o 15 2 2 51.96 112.45 90.36 o 16 2 2 516.21 645.44 147.67 o 17 2 2 641.87 796.89 167.22 o 1 3 2 3463.08 3831.71 42.96 o 2 3 2 14469.10 15238.75 140.41 o 3 3 2 6679.45 7489.75 78.06 o 4 3 2 36866.12 37056.98 334.56 o 5 3 2 59.57 70.05 18.82 o 6 3 2 49985.97 48805.38 475.17 o 7 3 2 240.02 216.69 24.01 o 8 3 2 18359.31 18143.53 188.55 o 9 3 2 56.11 126.26 32.73 o 10 3 2 23962.26 23604.11 252.16 o 11 3 2 3001.41 2797.63 58.83 o 12 3 2 60.63 46.63 44.79 o 13 3 2 1808.44 1900.35 67.99 o 14 3 2 696.25 899.84 80.69 o 15 3 2 73.23 120.31 105.25 o 16 3 2 3171.08 3602.85 169.84 o 0 4 2 4377.23 4501.27 73.06 o 1 4 2 1716.00 2014.84 34.14 o 2 4 2 567.74 589.74 24.97 o 3 4 2 18299.01 18746.97 172.33 o 4 4 2 4594.16 4785.62 55.83 o 5 4 2 12840.62 12825.37 126.00 o 6 4 2 0.07 67.90 24.77 o 7 4 2 9593.86 9643.96 107.15 o 8 4 2 306.23 307.11 38.99 o 9 4 2 222.09 203.05 46.34 o 10 4 2 1528.70 1551.14 57.56 o 11 4 2 406.89 333.27 54.40 o 12 4 2 1276.11 1253.82 71.61 o 13 4 2 158.10 111.87 74.94 o 14 4 2 608.85 732.46 104.98 o 15 4 2 510.57 590.96 132.01 o 1 5 2 31840.97 31777.19 282.87 o 2 5 2 3850.33 3811.62 54.25 o 3 5 2 20858.74 20430.04 192.96 o 4 5 2 2432.72 2413.16 45.03 o 5 5 2 3884.32 3934.71 58.48 o 6 5 2 1071.47 1097.02 39.03 o 7 5 2 481.53 571.52 44.78 o 8 5 2 7021.45 6749.78 106.22 o 9 5 2 5567.63 5677.59 98.59 o 10 5 2 718.06 748.10 73.80 o 11 5 2 13558.10 13591.48 235.77 o 12 5 2 959.01 1017.76 91.90 o 13 5 2 6982.07 7235.94 168.31 o 14 5 2 183.56 219.95 131.25 o 0 6 2 15772.02 15776.10 263.03 o 1 6 2 1261.78 1286.38 47.32 o 2 6 2 4237.38 4070.15 70.36 o 3 6 2 400.52 392.97 48.21 o 4 6 2 1515.75 1503.22 54.37 o 5 6 2 188.80 145.47 46.82 o 6 6 2 74.33 82.30 48.70 o 7 6 2 14.76 -3.97 52.07 o 8 6 2 1192.37 1132.60 67.05 o 9 6 2 440.21 372.67 80.91 o 10 6 2 2054.18 2254.55 120.61 o 11 6 2 397.65 360.63 119.35 o 12 6 2 2477.34 2362.77 147.53 o 13 6 2 0.15 -56.88 147.37 o 1 7 2 17071.59 16746.41 244.84 o 2 7 2 609.63 754.28 69.69 o 3 7 2 8725.25 8635.37 128.85 o 4 7 2 5100.51 5061.96 96.55 o 5 7 2 1651.61 1739.87 79.60 o 6 7 2 6439.20 6214.41 125.30 o 7 7 2 194.41 275.50 78.72 o 8 7 2 4188.47 4116.73 136.54 o 9 7 2 4463.21 4383.47 139.40 o 10 7 2 1131.56 798.68 154.95 o 11 7 2 2468.66 2874.73 179.60 o 0 8 2 141.06 121.94 131.08 o 1 8 2 70.44 257.20 92.74 o 2 8 2 443.45 279.94 96.39 o 3 8 2 58.53 126.39 88.32 o 4 8 2 12.78 31.00 89.97 o 5 8 2 1772.64 1935.84 106.21 o 6 8 2 27.87 158.00 126.22 o 7 8 2 1546.84 1642.18 122.40 o 8 8 2 16.64 123.20 146.96 o 1 9 2 345.97 106.39 122.23 o 2 9 2 2607.63 2671.71 141.41 o 3 9 2 43.49 34.95 125.64 o 4 0 3 65.10 5.30 18.82 o 6 0 3 3141.25 3381.36 51.92 o 8 0 3 7825.30 7866.28 108.47 o 10 0 3 101.64 187.34 36.41 o 12 0 3 3.16 51.51 58.32 o 14 0 3 674.91 745.77 76.68 o 16 0 3 10.33 404.40 156.20 o 3 1 3 24130.59 24072.48 223.87 o 4 1 3 43707.34 46241.46 450.23 o 5 1 3 102781.80 100969.91 944.21 o 6 1 3 864.18 1034.68 21.97 o 7 1 3 58356.73 56479.87 505.71 o 8 1 3 1299.73 1217.50 25.77 o 9 1 3 44838.06 43738.57 395.32 o 10 1 3 11376.97 11535.68 114.15 o 11 1 3 6962.97 6792.14 80.95 o 12 1 3 12410.92 12120.34 136.00 o 13 1 3 5.86 55.67 43.77 o 14 1 3 2276.93 2432.98 96.50 o 15 1 3 4665.85 4699.22 146.71 o 16 1 3 832.45 845.50 125.74 o 17 1 3 5083.38 5408.67 202.13 o 1 2 3 452.59 559.51 19.98 o 2 2 3 10951.85 12034.76 112.45 o 3 2 3 124.92 122.19 16.64 o 4 2 3 40.48 54.23 15.06 o 5 2 3 2939.32 3066.47 40.29 o 6 2 3 1145.94 1232.91 28.87 o 7 2 3 205.14 213.26 20.53 o 8 2 3 2207.19 2219.39 36.46 o 9 2 3 801.26 885.33 30.99 o 10 2 3 0.50 39.56 24.14 o 11 2 3 856.19 879.49 35.38 o 12 2 3 11.35 15.89 35.15 o 13 2 3 233.92 265.58 47.37 o 14 2 3 23.01 -48.90 73.63 o 15 2 3 10.58 -35.37 96.68 o 16 2 3 490.97 578.51 132.68 o 17 2 3 53.47 -3.19 162.07 o 0 3 3 135100.70 134697.59 1642.43 o 1 3 3 109.69 135.26 18.85 o 2 3 3 87795.20 87338.41 753.18 o 3 3 3 809.79 821.22 26.88 o 4 3 3 18527.97 18450.88 172.55 o 5 3 3 478.01 598.17 23.67 o 6 3 3 7.31 88.91 29.77 o 7 3 3 623.39 691.51 26.99 o 8 3 3 8703.09 8735.89 96.96 o 9 3 3 630.38 618.73 37.66 o 10 3 3 26954.62 27117.29 286.36 o 11 3 3 204.80 170.21 39.61 o 12 3 3 14053.14 13991.69 169.90 o 13 3 3 535.36 486.78 59.21 o 14 3 3 10909.11 10777.13 204.18 o 15 3 3 54.91 98.62 101.94 o 16 3 3 6303.18 6267.12 187.85 o 1 4 3 7324.95 7676.54 78.79 o 2 4 3 169.71 205.51 23.18 o 3 4 3 747.32 848.74 26.91 o 4 4 3 257.49 232.59 23.15 o 5 4 3 156.84 199.74 25.35 o 6 4 3 503.70 564.69 29.38 o 7 4 3 31.78 103.30 30.41 o 8 4 3 696.56 734.95 57.18 o 9 4 3 94.20 85.33 44.62 o 10 4 3 2135.41 2061.49 61.47 o 11 4 3 1834.65 1779.21 62.45 o 12 4 3 59.46 195.13 61.96 o 13 4 3 21.72 -15.05 78.36 o 14 4 3 235.03 197.53 98.64 o 15 4 3 18.66 51.44 120.62 o 0 5 3 12286.15 12265.34 175.26 o 1 5 3 70.74 215.12 32.23 o 2 5 3 7036.02 6908.87 76.29 o 3 5 3 23279.47 23192.62 213.32 o 4 5 3 4003.42 3795.02 55.62 o 5 5 3 20251.80 20171.57 212.98 o 6 5 3 1.05 47.37 33.31 o 7 5 3 22436.73 21663.48 246.41 o 8 5 3 417.70 346.64 41.89 o 9 5 3 11088.22 10952.94 164.80 o 10 5 3 2393.73 2373.31 95.49 o 11 5 3 1775.72 1819.70 92.43 o 12 5 3 2286.15 2375.67 112.40 o 13 5 3 106.01 192.39 105.24 o 14 5 3 2580.07 2795.62 151.57 o 1 6 3 313.98 352.16 41.83 o 2 6 3 414.63 372.48 47.42 o 3 6 3 54.81 38.27 45.72 o 4 6 3 1414.96 1384.08 51.82 o 5 6 3 1205.30 1143.71 51.08 o 6 6 3 676.40 694.40 48.17 o 7 6 3 1998.40 1856.97 57.95 o 8 6 3 123.30 267.60 64.95 o 9 6 3 69.03 -56.13 80.77 o 10 6 3 12.18 59.13 98.89 o 11 6 3 63.40 140.82 120.97 o 12 6 3 87.07 234.41 129.34 o 13 6 3 245.23 470.23 146.89 o 0 7 3 3999.14 3884.59 131.13 o 1 7 3 1562.29 1521.46 71.13 o 2 7 3 7393.62 7342.61 120.62 o 3 7 3 4654.52 4608.03 94.29 o 4 7 3 1661.06 1593.77 74.00 o 5 7 3 12944.91 12671.83 196.91 o 6 7 3 663.50 593.42 81.41 o 7 7 3 6910.12 6840.78 137.81 o 8 7 3 1581.46 1689.03 109.68 o 9 7 3 6012.60 6180.71 169.03 o 10 7 3 1053.57 845.55 145.57 o 11 7 3 1446.13 1561.95 172.84 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38.25 o 8 4 8 110.89 150.84 30.24 o 9 4 8 429.67 451.46 61.12 o 10 4 8 700.20 615.76 62.52 o 11 4 8 1615.11 1677.01 79.34 o 12 4 8 531.76 546.65 83.25 o 13 4 8 258.77 250.40 90.81 o 14 4 8 4.82 77.90 108.06 o 15 4 8 83.58 91.91 140.14 o 1 5 8 35862.53 35319.48 370.80 o 2 5 8 651.75 741.02 38.20 o 3 5 8 15926.31 15542.05 165.77 o 4 5 8 6811.25 6612.02 87.45 o 5 5 8 11216.04 10954.28 131.23 o 6 5 8 6244.48 6079.22 89.94 o 7 5 8 470.19 652.15 45.51 o 8 5 8 1083.81 1153.25 55.85 o 9 5 8 10208.20 10269.83 151.26 o 10 5 8 764.50 826.28 83.37 o 11 5 8 12843.80 13271.52 235.13 o 12 5 8 411.29 295.89 107.27 o 13 5 8 13203.79 14133.54 262.12 o 14 5 8 0.22 -169.14 189.34 o 0 6 8 1443.56 1516.99 84.90 o 1 6 8 1458.50 1483.59 58.53 o 2 6 8 2661.29 2701.01 63.43 o 3 6 8 3109.65 2970.83 65.17 o 4 6 8 342.99 361.96 47.02 o 5 6 8 452.58 380.48 53.46 o 6 6 8 984.61 1001.44 58.96 o 7 6 8 1.04 -59.67 59.67 o 8 6 8 131.76 200.79 72.57 o 9 6 8 122.85 285.85 96.02 o 10 6 8 1121.15 1481.53 115.69 o 11 6 8 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4.31 23.86 34.21 o 7 3 9 84.31 72.48 29.50 o 8 3 9 5062.95 5001.01 70.74 o 9 3 9 384.91 344.59 43.73 o 10 3 9 13487.68 13450.83 176.06 o 11 3 9 13.80 -12.68 52.76 o 12 3 9 28793.64 28453.63 391.87 o 13 3 9 278.52 58.09 84.23 o 14 3 9 12808.40 13273.38 222.70 o 15 3 9 232.82 336.93 112.03 o 1 4 9 12.34 99.11 26.19 o 2 4 9 419.10 470.44 27.61 o 3 4 9 3744.48 3752.69 50.97 o 4 4 9 1777.85 1898.60 39.12 o 5 4 9 224.06 258.39 32.39 o 6 4 9 3213.14 3415.75 59.73 o 7 4 9 0.59 35.18 26.64 o 8 4 9 1493.74 1393.48 46.99 o 9 4 9 1.63 -15.37 54.80 o 10 4 9 18.63 -3.48 64.37 o 11 4 9 1767.86 1779.77 88.04 o 12 4 9 35.22 54.73 81.38 o 13 4 9 158.09 57.02 96.40 o 14 4 9 143.85 228.48 116.55 o 15 4 9 471.91 252.23 151.94 o 0 5 9 34260.57 34152.34 507.42 o 1 5 9 599.05 706.87 42.50 o 2 5 9 3956.70 3860.38 62.81 o 3 5 9 15666.93 15473.60 164.91 o 4 5 9 614.06 610.39 39.71 o 5 5 9 37687.24 37175.07 391.95 o 6 5 9 5.61 -39.98 40.27 o 7 5 9 16620.48 16596.12 200.81 o 8 5 9 2176.63 2134.95 61.09 o 9 5 9 10394.85 10632.05 172.70 o 10 5 9 1123.45 1202.05 88.49 o 11 5 9 1898.18 1826.89 100.19 o 12 5 9 342.05 436.00 117.65 o 13 5 9 994.17 1370.20 147.03 o 1 6 9 407.47 488.91 55.24 o 2 6 9 1317.40 1370.01 53.83 o 3 6 9 54.36 61.74 50.08 o 4 6 9 264.53 298.50 49.93 o 5 6 9 1034.37 1077.71 57.93 o 6 6 9 1947.60 1832.52 70.19 o 7 6 9 459.49 505.29 63.03 o 8 6 9 1271.60 1125.52 93.92 o 9 6 9 94.58 70.62 87.49 o 10 6 9 747.63 634.13 114.74 o 11 6 9 381.65 145.98 123.86 o 12 6 9 48.30 112.90 136.39 o 0 7 9 9504.70 9119.80 238.63 o 1 7 9 2448.64 2450.88 92.52 o 2 7 9 4812.83 4645.83 112.01 o 3 7 9 3902.24 3812.47 105.29 o 4 7 9 2674.00 2742.50 90.70 o 5 7 9 2457.89 2500.57 90.56 o 6 7 9 62.62 18.49 79.07 o 7 7 9 12444.21 12855.03 245.68 o 8 7 9 1277.03 1635.44 142.69 o 9 7 9 4539.60 4735.69 179.88 o 10 7 9 2964.48 2869.87 178.66 o 1 8 9 1391.33 1614.73 102.35 o 2 8 9 301.91 166.71 105.15 o 3 8 9 716.04 479.32 102.64 o 4 8 9 1687.12 1687.03 110.32 o 5 8 9 75.24 276.02 130.31 o 6 8 9 9.51 38.39 143.58 o 0 0 10 117702.41 121957.70 2188.80 o 2 0 10 47906.11 46999.07 535.44 o 4 0 10 14622.26 15264.13 178.22 o 6 0 10 350.30 341.79 26.57 o 8 0 10 6587.03 6494.56 97.50 o 10 0 10 15363.62 15270.63 205.69 o 12 0 10 11170.48 11104.54 186.21 o 14 0 10 6424.01 6346.83 208.27 o 16 0 10 5863.34 6332.61 476.55 o 1 1 10 65797.30 66367.44 573.83 o 2 1 10 37.02 132.83 16.73 o 3 1 10 9471.28 9237.86 90.26 o 4 1 10 10319.02 10299.62 101.68 o 5 1 10 953.20 938.32 27.51 o 6 1 10 14697.71 15010.04 142.89 o 7 1 10 114.84 108.67 24.37 o 8 1 10 8793.78 8533.23 96.11 o 9 1 10 5312.03 5302.49 73.09 o 10 1 10 4730.07 4657.96 70.99 o 11 1 10 10496.78 10771.49 135.57 o 12 1 10 1.64 -12.02 48.25 o 13 1 10 10698.68 10691.03 178.16 o 14 1 10 148.43 187.17 74.62 o 15 1 10 1148.51 1188.06 121.40 o 16 1 10 2606.60 2984.12 169.75 o 0 2 10 184.45 135.52 23.58 o 1 2 10 1617.54 1573.19 26.77 o 2 2 10 18735.62 19257.17 170.45 o 3 2 10 13289.46 13341.04 122.60 o 4 2 10 2463.74 2443.52 37.05 o 5 2 10 27817.26 28456.37 259.49 o 6 2 10 2932.57 2834.57 40.91 o 7 2 10 20606.71 20429.84 199.08 o 8 2 10 161.17 98.07 30.95 o 9 2 10 14168.30 13971.27 149.67 o 10 2 10 4164.90 4330.10 72.65 o 11 2 10 942.01 1019.32 53.82 o 12 2 10 5089.02 5157.54 119.61 o 13 2 10 297.37 351.51 71.26 o 14 2 10 1440.43 1590.58 90.52 o 15 2 10 498.90 655.93 130.30 o 16 2 10 1438.13 2031.17 194.60 o 1 3 10 6.43 34.06 21.02 o 2 3 10 6814.43 6643.18 74.14 o 3 3 10 606.41 698.76 25.55 o 4 3 10 26808.87 26401.59 247.70 o 5 3 10 1118.82 1141.28 30.50 o 6 3 10 20720.16 20198.64 197.85 o 7 3 10 504.28 498.29 34.80 o 8 3 10 14687.11 14173.25 165.81 o 9 3 10 186.44 163.56 36.16 o 10 3 10 634.75 719.41 60.67 o 11 3 10 50.70 62.75 59.16 o 12 3 10 3124.71 3089.89 95.04 o 13 3 10 625.78 821.77 92.23 o 14 3 10 428.47 369.09 98.14 o 15 3 10 6.61 -46.61 131.45 o 0 4 10 4431.15 4419.07 87.59 o 1 4 10 4.04 32.75 27.78 o 2 4 10 3219.56 3317.98 49.62 o 3 4 10 13300.68 13438.09 135.11 o 4 4 10 2132.49 2213.08 42.02 o 5 4 10 12959.67 12673.96 134.02 o 6 4 10 123.05 91.44 37.39 o 7 4 10 12921.39 12546.92 150.33 o 8 4 10 1200.55 1205.28 51.53 o 9 4 10 3497.05 3506.14 73.43 o 10 4 10 3606.12 3591.22 95.46 o 11 4 10 1805.86 1795.80 88.33 o 12 4 10 844.30 808.02 84.30 o 13 4 10 0.12 -4.99 101.28 o 14 4 10 494.86 392.40 118.94 o 1 5 10 10296.36 10325.15 126.50 o 2 5 10 611.15 630.27 38.97 o 3 5 10 7940.79 7801.18 101.50 o 4 5 10 97.70 97.08 37.45 o 5 5 10 222.07 275.19 53.02 o 6 5 10 9054.73 8623.23 115.77 o 7 5 10 317.03 305.12 55.84 o 8 5 10 1405.00 1581.27 59.24 o 9 5 10 2630.56 2848.04 90.57 o 10 5 10 2453.16 2526.07 104.53 o 11 5 10 3291.62 3389.72 120.14 o 12 5 10 173.70 214.65 122.01 o 13 5 10 4692.77 4633.42 160.16 o 0 6 10 9054.96 8756.59 196.04 o 1 6 10 35.82 43.67 55.11 o 2 6 10 9563.22 9212.73 124.96 o 3 6 10 401.76 338.39 50.97 o 4 6 10 3570.46 3489.18 73.84 o 5 6 10 30.98 25.63 52.91 o 6 6 10 10.98 116.29 61.02 o 7 6 10 494.09 486.00 80.81 o 8 6 10 313.54 294.40 86.32 o 9 6 10 54.93 -50.08 94.29 o 10 6 10 3068.74 3172.39 172.13 o 11 6 10 13.39 -141.85 141.85 o 12 6 10 4584.12 4935.68 187.00 o 1 7 10 10353.67 10484.87 187.00 o 2 7 10 1909.52 1936.70 88.48 o 3 7 10 2819.73 2861.63 97.69 o 4 7 10 1732.08 1600.39 86.63 o 5 7 10 890.72 873.63 82.38 o 6 7 10 2219.96 2254.34 114.79 o 7 7 10 556.23 546.37 111.74 o 8 7 10 993.94 886.72 129.44 o 9 7 10 1300.89 1393.15 144.89 o 0 8 10 1232.20 1266.22 156.23 o 1 8 10 2010.80 2114.09 114.52 o 2 8 10 379.31 478.08 105.47 o 3 8 10 2162.21 2006.13 120.21 o 4 8 10 8.69 35.90 131.45 o 5 8 10 4043.48 4359.77 166.27 o 6 8 10 166.84 -75.32 142.94 o 2 0 11 22280.09 22279.54 270.16 o 4 0 11 22883.91 21893.33 259.49 o 6 0 11 25364.78 25292.44 285.34 o 8 0 11 45490.57 46330.66 589.03 o 10 0 11 9903.96 9542.98 142.35 o 12 0 11 673.24 571.55 69.41 o 14 0 11 1728.40 1597.94 158.49 o 16 0 11 4438.52 4025.46 244.59 o 0 1 11 297.09 274.49 29.41 o 1 1 11 1978.69 2054.00 33.45 o 2 1 11 2807.46 2740.44 35.70 o 3 1 11 2063.29 1885.88 29.40 o 4 1 11 319.15 390.44 23.47 o 5 1 11 9.38 7.64 19.29 o 6 1 11 342.00 382.49 23.01 o 7 1 11 2125.00 2202.26 35.36 o 8 1 11 654.88 639.81 30.02 o 9 1 11 332.16 371.62 35.26 o 10 1 11 16.27 93.59 37.02 o 11 1 11 592.94 694.51 47.87 o 12 1 11 131.68 198.30 54.65 o 13 1 11 293.61 405.39 71.86 o 14 1 11 178.94 339.46 93.26 o 15 1 11 24.04 214.12 123.29 o 16 1 11 0.57 167.88 150.20 o 1 2 11 48362.99 49957.98 443.26 o 2 2 11 11358.78 11835.34 112.03 o 3 2 11 21746.59 21434.24 194.41 o 4 2 11 21192.24 21053.53 200.96 o 5 2 11 4264.21 4432.32 56.24 o 6 2 11 7337.41 7175.37 79.51 o 7 2 11 105.93 40.23 28.35 o 8 2 11 2752.36 2707.01 48.18 o 9 2 11 13578.61 13468.72 150.28 o 10 2 11 2732.99 2813.26 57.20 o 11 2 11 7065.44 7228.07 115.24 o 12 2 11 20.73 -18.74 62.82 o 13 2 11 9737.46 9848.51 168.86 o 14 2 11 72.87 222.86 89.58 o 15 2 11 9439.11 9654.02 210.53 o 16 2 11 867.67 802.93 199.17 o 0 3 11 7467.09 7620.82 112.10 o 1 3 11 0.16 6.74 19.78 o 2 3 11 280.89 274.57 27.00 o 3 3 11 929.11 967.72 28.05 o 4 3 11 868.60 862.39 28.17 o 5 3 11 128.97 226.78 32.27 o 6 3 11 421.85 507.41 32.16 o 7 3 11 342.22 467.98 34.46 o 8 3 11 328.98 289.86 41.86 o 9 3 11 96.18 95.76 43.72 o 10 3 11 35.63 31.72 51.28 o 11 3 11 586.34 801.68 66.00 o 12 3 11 1143.52 1270.41 83.16 o 13 3 11 0.34 -43.39 82.64 o 14 3 11 1514.97 1649.25 111.23 o 15 3 11 310.65 308.70 136.89 o 1 4 11 24607.13 24103.67 233.67 o 2 4 11 6288.41 6168.11 76.10 o 3 4 11 25029.12 24595.12 236.85 o 4 4 11 6841.07 6799.09 83.34 o 5 4 11 4888.43 4804.08 69.44 o 6 4 11 16016.72 15459.10 179.97 o 7 4 11 451.20 387.33 44.24 o 8 4 11 9245.91 9057.62 122.70 o 9 4 11 4821.22 4829.44 92.48 o 10 4 11 3128.31 3174.25 96.61 o 11 4 11 13126.93 12724.04 213.94 o 12 4 11 987.13 1110.38 91.77 o 13 4 11 7841.56 7821.59 169.46 o 14 4 11 209.31 306.35 127.99 o 0 5 11 1207.51 1299.20 70.73 o 1 5 11 4805.79 4842.03 84.10 o 2 5 11 920.36 855.77 48.89 o 3 5 11 1390.48 1449.96 48.32 o 4 5 11 801.42 764.26 40.88 o 5 5 11 3080.48 3082.12 56.97 o 6 5 11 3.93 71.99 44.46 o 7 5 11 579.88 638.83 49.29 o 8 5 11 178.25 194.71 58.06 o 9 5 11 814.43 928.60 77.62 o 10 5 11 3.97 79.35 91.81 o 11 5 11 17.78 178.79 111.04 o 12 5 11 311.87 439.61 121.49 o 13 5 11 207.86 199.31 127.69 o 1 6 11 6549.72 6251.50 109.18 o 2 6 11 7731.68 7386.73 112.89 o 3 6 11 250.66 217.26 48.82 o 4 6 11 23390.21 23196.56 286.61 o 5 6 11 6.90 -41.07 57.54 o 6 6 11 19355.17 19748.29 271.80 o 7 6 11 277.04 333.57 79.57 o 8 6 11 19281.99 19425.51 312.82 o 9 6 11 923.72 1017.90 111.69 o 10 6 11 3869.09 3810.51 143.22 o 11 6 11 57.15 84.46 134.82 o 0 7 11 3131.77 3037.75 143.93 o 1 7 11 792.17 850.58 84.11 o 2 7 11 3.58 134.56 80.65 o 3 7 11 319.15 420.44 81.02 o 4 7 11 500.29 502.92 82.20 o 5 7 11 475.83 403.94 96.62 o 6 7 11 143.71 223.36 96.61 o 7 7 11 1465.94 1313.74 123.00 o 8 7 11 0.41 -43.12 125.78 o 9 7 11 794.67 830.60 162.48 o 1 8 11 10398.51 10539.38 212.04 o 2 8 11 14.85 -66.84 110.33 o 3 8 11 6935.06 7099.51 172.19 o 4 8 11 2712.68 2774.65 141.01 o 5 8 11 995.02 894.93 146.80 o 0 0 12 77111.12 73477.83 1483.46 o 2 0 12 72296.91 72756.35 851.96 o 4 0 12 30532.60 29161.06 333.71 o 6 0 12 566.34 615.09 28.01 o 8 0 12 11052.22 10674.81 148.47 o 10 0 12 16925.82 16408.11 239.69 o 12 0 12 21050.36 21273.92 383.65 o 14 0 12 14582.18 14795.26 339.52 o 16 0 12 2820.43 3000.30 274.87 o 1 1 12 2274.93 2374.47 33.18 o 2 1 12 2738.18 2770.33 36.10 o 3 1 12 2976.65 2928.64 37.78 o 4 1 12 8490.80 8473.54 89.09 o 5 1 12 366.25 314.66 25.32 o 6 1 12 3273.64 3340.30 44.19 o 7 1 12 1927.08 1918.08 37.94 o 8 1 12 377.61 471.11 30.79 o 9 1 12 192.12 201.66 34.74 o 10 1 12 11.22 20.32 39.98 o 11 1 12 1012.87 874.44 49.18 o 12 1 12 141.55 135.74 61.76 o 13 1 12 1036.48 1013.48 76.36 o 14 1 12 390.65 210.78 100.33 o 15 1 12 242.49 206.71 129.28 o 16 1 12 18.18 -119.00 169.01 o 0 2 12 30299.62 29390.46 376.04 o 1 2 12 1390.86 1256.03 29.04 o 2 2 12 7113.46 6939.20 72.35 o 3 2 12 25878.09 25959.25 236.52 o 4 2 12 4329.98 4310.32 53.53 o 5 2 12 35929.61 35054.92 322.21 o 6 2 12 282.87 245.92 26.99 o 7 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76.91 o 2 1 25 11942.47 11833.84 195.52 o 3 1 25 6102.89 6433.29 131.68 o 4 1 25 509.16 650.27 74.48 o 5 1 25 8330.62 8166.95 158.24 o 6 1 25 589.22 486.65 88.27 o 7 1 25 7090.12 7310.35 159.88 o 8 1 25 378.09 299.59 115.87 o 9 1 25 5268.52 5454.78 169.18 o 10 1 25 992.39 226.33 149.14 o 1 2 25 1667.85 1883.65 87.79 o 2 2 25 191.76 260.50 78.54 o 3 2 25 1658.91 1800.15 92.70 o 4 2 25 65.19 102.29 91.60 o 5 2 25 1547.11 1740.20 105.88 o 6 2 25 372.47 238.06 97.00 o 7 2 25 126.12 262.60 108.31 o 8 2 25 1423.60 1401.77 130.73 o 9 2 25 308.51 342.92 145.30 o 0 3 25 19473.28 18925.32 419.73 o 1 3 25 28.25 108.61 88.57 o 2 3 25 9979.55 10248.52 207.00 o 3 3 25 135.21 -20.98 95.54 o 4 3 25 5780.39 5540.88 144.87 o 5 3 25 421.31 216.22 113.50 o 6 3 25 47.11 116.37 114.68 o 7 3 25 18.92 -5.87 145.27 o 8 3 25 1889.94 1826.17 168.14 o 1 4 25 3654.19 3736.67 139.77 o 2 4 25 273.45 458.71 121.38 o 3 4 25 15.14 270.56 112.03 o 4 4 25 23.55 256.55 127.48 o 5 4 25 128.87 76.78 148.00 o 6 4 25 316.56 215.31 135.11 o 0 5 25 1313.35 1149.30 197.21 o 1 5 25 313.34 646.24 136.15 o 2 5 25 1930.34 1965.11 162.38 o 3 5 25 3069.03 3289.85 214.68 o 0 0 26 6250.87 6079.93 292.21 o 2 0 26 236.20 391.53 109.62 o 4 0 26 0.68 -137.11 137.11 o 6 0 26 6.31 159.42 200.89 o 8 0 26 11.21 -12.18 189.73 o 1 1 26 13270.67 13745.82 229.42 o 2 1 26 183.83 380.00 83.57 o 3 1 26 9606.74 9740.68 187.93 o 4 1 26 1603.30 1637.34 98.25 o 5 1 26 2368.33 2850.38 119.28 o 6 1 26 2760.33 2870.14 124.14 o 7 1 26 385.57 404.28 127.57 o 8 1 26 4029.73 3935.69 193.05 o 9 1 26 3643.32 3678.97 200.05 o 0 2 26 4.52 24.47 115.66 o 1 2 26 7.93 74.99 88.59 o 2 2 26 14.60 55.23 87.28 o 3 2 26 365.73 228.64 90.88 o 4 2 26 73.97 68.62 100.51 o 5 2 26 1273.73 1018.11 120.98 o 6 2 26 194.76 275.86 121.01 o 7 2 26 50.24 38.97 133.90 o 8 2 26 1234.35 1543.28 158.18 o 1 3 26 0.69 -34.51 102.71 o 2 3 26 3986.03 4381.10 151.22 o 3 3 26 191.81 29.11 112.46 o 4 3 26 10980.15 10649.79 236.59 o 5 3 26 59.50 239.08 132.72 o 6 3 26 13327.74 13499.59 296.29 o 7 3 26 180.50 154.36 171.85 o 0 4 26 326.54 359.42 223.21 o 1 4 26 292.28 266.57 130.22 o 2 4 26 179.34 196.04 119.06 o 3 4 26 42.42 41.16 132.02 o 4 4 26 122.85 192.95 140.62 o 5 4 26 905.52 962.26 170.62 o 2 0 27 1727.10 1408.58 196.96 o 4 0 27 3110.72 2877.18 173.27 o 6 0 27 8905.88 9037.50 294.57 o 8 0 27 6352.30 6766.03 294.70 o 0 1 27 3000.38 2855.00 154.43 o 1 1 27 197.75 258.83 90.56 o 2 1 27 1828.65 2038.66 118.96 o 3 1 27 2930.74 3098.60 113.80 o 4 1 27 1323.30 1232.02 113.75 o 5 1 27 7159.06 7499.15 194.92 o 6 1 27 431.92 284.72 129.94 o 7 1 27 3366.21 3168.45 166.27 o 8 1 27 877.27 371.31 232.77 o 1 2 27 5011.53 4813.98 132.48 o 2 2 27 194.39 325.12 105.86 o 3 2 27 2790.18 2898.38 121.19 o 4 2 27 1360.30 1464.79 143.09 o 5 2 27 887.91 1117.69 123.98 o 6 2 27 194.88 -123.07 129.40 o 7 2 27 0.91 72.99 157.93 o 0 3 27 8817.61 9041.32 298.69 o 1 3 27 109.64 141.79 113.56 o 2 3 27 4912.31 5307.89 165.02 o 3 3 27 82.30 256.00 126.07 o 4 3 27 2293.40 2505.58 162.21 o 5 3 27 15.74 289.64 151.89 o 6 3 27 0.59 118.75 241.90 o 1 4 27 2379.63 2766.72 154.95 o 2 4 27 1124.33 1141.84 165.51 o 3 4 27 1873.60 1729.00 170.54 o 0 0 28 16024.92 17037.72 602.12 o 2 0 28 9422.46 10032.03 296.98 o 4 0 28 2011.86 2404.66 322.04 o 6 0 28 207.06 200.09 210.64 o 1 1 28 2271.50 2558.14 110.55 o 2 1 28 470.52 644.73 107.21 o 3 1 28 916.58 947.78 133.55 o 4 1 28 451.10 336.17 123.72 o 5 1 28 3.05 -48.37 130.79 o 6 1 28 147.48 119.41 144.95 o 0 2 28 3947.57 4557.26 202.41 o 1 2 28 316.71 324.64 116.40 o 2 2 28 3581.15 3510.31 140.23 o 3 2 28 2492.92 2575.73 135.57 o 4 2 28 292.09 273.51 126.39 o 5 2 28 6993.42 7374.26 215.10 o 6 2 28 43.92 -14.99 161.47 o 1 3 28 37.08 189.74 137.23 o 2 3 28 85.69 275.38 130.33 o 3 3 28 80.42 291.87 133.54 o 4 3 28 1912.67 2056.96 241.02 o 2 0 29 3345.54 3590.93 242.62 o 4 0 29 8509.34 9052.34 330.49 o 0 1 29 22.74 78.43 142.30 o 1 1 29 191.95 287.43 118.96 o 2 1 29 1058.38 1431.36 124.80 o 3 1 29 748.79 725.27 149.29 o 4 1 29 9.56 39.93 154.60 o 5 1 29 863.24 960.13 161.87 o 1 2 29 10840.31 10907.33 257.75 o 2 2 29 2171.79 2450.07 149.88 o 3 2 29 5777.25 6666.84 203.16 o 4 2 29 2750.38 2961.53 196.36 o 0 0 30 8745.55 8388.32 532.76 o 2 0 30 4632.85 5180.42 266.56 o 1 1 30 4122.52 4523.09 188.02 o 2 1 30 588.01 542.15 155.98 o 3 1 30 1952.01 2094.44 179.66 o