#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/52/2015275.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015275_Fobs loop_ _publ_author_name 'Kavitha, Savaridasson Jose' 'Panchanatheswaran, Krishnaswamy' 'Low, John N.' 'Ferguson, George' 'Glidewell, Christopher' _publ_section_title ; Simple hydrogen-bonded chains in 2,2'-bipyridinium thiocyanate, hydrogen-bonded chains of rings in 2,2'-bipyridinium picrate and hydrogen-bonded sheets in 2,2'-bipyridinium hydrogensulfate ; _journal_coeditor_code SK1900 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o165 _journal_page_last o169 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.568 _cell_angle_gamma 90.000 _cell_length_a 12.8274 _cell_length_b 4.4774 _cell_length_c 18.2844 _exptl_crystal_F_000 528.00 _reflns_d_resolution_high 0.7686 _[local]_cod_data_source_file sk1900IIIsup4.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1329 P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 148.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 3770.00 3524.81 35.20 o 4 0 0 0.31 44.97 1.97 o 5 0 0 1.15 0.87 1.01 o 6 0 0 1118.76 1106.32 18.04 o 7 0 0 7.19 7.96 1.48 o 8 0 0 2640.21 2817.23 38.36 o 9 0 0 3.44 -0.61 1.92 o 10 0 0 78.04 79.85 3.98 o 11 0 0 123.16 111.15 5.51 o 12 0 0 175.50 190.14 13.51 o 13 0 0 610.89 631.34 20.04 o 14 0 0 553.00 597.70 23.34 o 15 0 0 277.57 269.82 23.32 o 16 0 0 1282.45 1384.78 46.44 o 1 1 0 4689.84 4477.02 47.44 o 2 1 0 120.75 260.25 6.17 o 3 1 0 1204.59 1274.10 13.03 o 4 1 0 1194.27 1131.44 10.58 o 5 1 0 666.58 649.62 6.55 o 6 1 0 3.62 40.12 2.40 o 7 1 0 45.77 53.13 1.78 o 8 1 0 417.78 479.80 6.69 o 9 1 0 48.12 51.95 2.51 o 10 1 0 728.40 709.65 11.86 o 11 1 0 42.55 39.83 3.34 o 12 1 0 308.40 315.55 9.14 o 13 1 0 244.44 244.77 14.85 o 14 1 0 4.70 3.51 4.20 o 15 1 0 385.96 420.58 13.58 o 16 1 0 17.22 15.16 6.95 o 0 2 0 17.68 2.03 0.91 o 1 2 0 102.30 100.17 1.58 o 2 2 0 78.73 153.77 2.54 o 3 2 0 6508.92 6686.76 57.00 o 4 2 0 524.19 513.63 5.70 o 5 2 0 5957.59 6005.88 49.09 o 6 2 0 435.44 438.63 6.09 o 7 2 0 1278.78 1289.79 13.48 o 8 2 0 13.01 47.97 5.31 o 9 2 0 1553.43 1560.86 23.76 o 10 2 0 4.71 8.00 2.30 o 11 2 0 632.68 576.12 12.51 o 12 2 0 15.91 25.58 3.62 o 13 2 0 55.03 47.04 4.70 o 14 2 0 131.35 114.98 7.68 o 15 2 0 19.13 13.57 8.14 o 1 3 0 20.66 21.36 1.04 o 2 3 0 102.71 108.12 2.28 o 3 3 0 279.91 271.73 5.78 o 4 3 0 308.90 325.25 4.56 o 5 3 0 1187.61 1190.76 14.07 o 6 3 0 526.81 519.63 7.71 o 7 3 0 244.61 237.96 4.85 o 8 3 0 871.68 964.47 17.20 o 9 3 0 648.80 623.91 11.94 o 10 3 0 187.24 166.24 6.79 o 11 3 0 280.38 282.63 12.05 o 12 3 0 1.31 3.06 4.26 o 13 3 0 187.79 191.50 12.17 o 14 3 0 0.01 6.73 7.08 o 0 4 0 458.43 462.36 8.93 o 1 4 0 247.58 266.85 4.29 o 2 4 0 1739.76 1793.97 26.48 o 3 4 0 17.80 11.62 2.64 o 4 4 0 816.29 816.96 17.12 o 5 4 0 424.16 460.06 10.82 o 6 4 0 133.21 113.22 9.72 o 7 4 0 73.41 74.39 7.59 o 8 4 0 32.31 38.69 5.70 o 9 4 0 161.76 179.35 14.92 o 10 4 0 381.36 360.70 17.46 o 11 4 0 25.57 11.38 8.28 o 1 5 0 15.67 24.11 5.12 o 2 5 0 140.46 156.42 9.20 o 3 5 0 204.89 204.90 9.32 o 4 5 0 0.07 5.39 5.20 o 5 5 0 120.59 119.02 8.06 o 6 5 0 90.06 78.07 7.92 o 7 5 0 158.62 130.38 10.25 o 8 5 0 73.47 81.71 9.52 o -16 1 1 111.13 111.00 8.26 o -15 1 1 5.62 6.01 5.31 o -14 1 1 60.12 88.30 8.76 o -13 1 1 0.48 4.75 3.71 o -12 1 1 6.65 8.86 3.14 o -11 1 1 98.19 101.55 4.24 o -10 1 1 3.15 8.10 2.35 o -9 1 1 162.41 184.89 4.14 o -8 1 1 7.66 9.76 1.44 o -7 1 1 333.13 356.09 4.39 o -6 1 1 515.29 514.68 5.18 o -5 1 1 1475.55 1498.38 11.42 o -4 1 1 735.43 721.34 6.88 o -3 1 1 32.22 24.33 0.93 o -2 1 1 2651.99 2501.34 21.51 o -1 1 1 615.34 535.94 6.83 o 0 1 1 355.43 340.13 3.08 o 1 1 1 3513.36 3247.94 27.44 o 2 1 1 140.06 382.31 68.15 o 3 1 1 4090.25 3879.92 35.10 o 4 1 1 444.84 524.28 6.63 o 5 1 1 1512.20 1522.56 13.72 o 6 1 1 533.83 633.93 6.28 o 7 1 1 4.16 7.36 1.44 o 8 1 1 158.13 151.73 3.20 o 9 1 1 1.48 4.78 1.84 o 10 1 1 754.28 721.78 14.29 o 11 1 1 1.39 3.16 3.10 o 12 1 1 50.63 44.62 4.02 o 13 1 1 106.61 106.80 6.42 o 14 1 1 0.73 2.93 5.21 o 15 1 1 1.34 -1.53 6.85 o 16 1 1 7.73 3.61 18.53 o -15 2 1 46.63 62.63 8.25 o -14 2 1 26.98 21.88 5.13 o -13 2 1 15.07 13.57 5.46 o -12 2 1 1.57 9.30 4.34 o -11 2 1 230.92 196.70 6.73 o -10 2 1 6.05 11.91 2.15 o -9 2 1 208.78 215.70 4.39 o -8 2 1 181.08 188.18 4.15 o -7 2 1 492.40 511.75 6.28 o -6 2 1 201.22 369.15 13.02 o -5 2 1 826.30 815.54 9.57 o -4 2 1 3.66 0.61 0.78 o -3 2 1 13.76 22.06 1.16 o -2 2 1 498.48 513.84 5.67 o -1 2 1 55.34 52.16 1.26 o 0 2 1 26.96 26.66 0.91 o 1 2 1 397.31 429.07 4.47 o 2 2 1 545.19 541.45 6.41 o 3 2 1 107.58 132.61 2.27 o 4 2 1 764.05 977.19 19.97 o 5 2 1 307.26 305.78 4.24 o 6 2 1 10.29 22.67 1.37 o 7 2 1 31.12 35.53 2.07 o 8 2 1 137.91 156.14 4.00 o 9 2 1 153.96 143.83 3.81 o 10 2 1 164.91 164.23 4.76 o 11 2 1 143.69 129.83 4.64 o 12 2 1 214.74 157.50 7.40 o 13 2 1 22.41 27.01 4.97 o 14 2 1 102.28 105.38 9.32 o 15 2 1 1.71 -3.40 7.35 o -14 3 1 5.25 3.73 7.28 o -13 3 1 81.10 70.27 7.95 o -12 3 1 58.24 54.73 5.64 o -11 3 1 13.37 20.13 4.17 o -10 3 1 0.14 3.74 3.36 o -9 3 1 125.94 125.75 3.71 o -8 3 1 188.18 164.44 5.20 o -7 3 1 408.24 406.13 8.77 o -6 3 1 242.36 239.45 4.76 o -5 3 1 16.71 18.32 2.71 o -4 3 1 79.41 70.14 2.94 o -3 3 1 736.80 772.40 11.73 o -2 3 1 65.36 70.66 1.75 o -1 3 1 56.92 50.41 1.41 o 0 3 1 149.83 172.87 2.83 o 1 3 1 17.05 11.79 1.17 o 2 3 1 178.44 205.63 3.61 o 3 3 1 130.41 120.49 2.91 o 4 3 1 34.04 36.20 1.65 o 5 3 1 2.91 2.92 1.74 o 6 3 1 21.16 66.01 4.16 o 7 3 1 487.76 489.97 9.17 o 8 3 1 19.62 20.70 2.00 o 9 3 1 55.04 52.13 2.65 o 10 3 1 197.58 194.51 8.19 o 11 3 1 50.08 43.80 12.11 o 12 3 1 25.49 25.97 5.65 o 13 3 1 48.97 34.82 8.47 o -12 4 1 329.74 353.02 25.89 o -11 4 1 0.06 0.79 6.42 o -10 4 1 11.00 21.15 7.02 o -9 4 1 3.15 0.68 4.56 o -8 4 1 98.62 99.76 6.58 o -7 4 1 18.29 7.78 4.02 o -6 4 1 130.33 132.84 9.13 o -5 4 1 5.44 12.84 3.27 o -4 4 1 69.89 68.10 4.25 o -3 4 1 69.21 65.62 3.63 o -2 4 1 103.70 137.80 7.81 o -1 4 1 251.47 252.83 4.03 o 0 4 1 8.30 7.18 1.16 o 1 4 1 257.74 250.06 4.52 o 2 4 1 456.63 449.56 7.57 o 3 4 1 187.64 185.44 4.44 o 4 4 1 683.46 696.66 12.42 o 5 4 1 1.06 3.16 1.26 o 6 4 1 233.65 217.87 7.46 o 7 4 1 1.07 4.92 5.59 o 8 4 1 28.46 23.35 4.99 o 9 4 1 166.40 194.56 11.29 o 10 4 1 57.74 50.57 7.47 o 11 4 1 111.45 114.26 13.70 o -8 5 1 208.53 200.97 15.49 o -7 5 1 0.30 4.64 7.11 o -6 5 1 79.32 88.72 7.53 o -5 5 1 39.60 16.68 5.42 o -4 5 1 106.38 105.71 6.85 o -3 5 1 2.13 1.51 4.18 o -2 5 1 707.85 783.11 22.13 o -1 5 1 139.56 136.93 7.83 o 0 5 1 3.30 0.94 2.53 o 1 5 1 77.08 83.03 5.75 o 2 5 1 18.95 17.84 6.29 o 3 5 1 68.37 77.61 8.29 o 4 5 1 41.59 41.77 5.89 o 5 5 1 403.10 378.89 16.84 o 6 5 1 129.69 120.84 9.33 o 7 5 1 1.37 1.40 6.13 o 8 5 1 145.81 103.62 26.31 o -16 0 2 18.21 34.04 9.75 o -15 0 2 1278.32 1355.78 61.16 o -14 0 2 174.47 193.26 11.39 o -13 0 2 963.39 1013.17 34.78 o -12 0 2 9.74 89.63 11.52 o -11 0 2 5.43 9.70 5.50 o -10 0 2 117.97 126.90 4.75 o -9 0 2 23.83 22.68 2.84 o -8 0 2 501.23 554.66 9.82 o -7 0 2 114.96 117.21 3.31 o -6 0 2 85.27 108.00 2.76 o -5 0 2 16.03 38.25 1.72 o -4 0 2 630.01 588.60 8.43 o -3 0 2 16326.23 14319.97 163.34 o -2 0 2 419.39 412.47 8.81 o 2 0 2 1710.60 1573.22 19.46 o 3 0 2 13283.82 11755.12 135.82 o 4 0 2 124.68 573.67 17.79 o 5 0 2 59.82 75.11 2.50 o 6 0 2 423.34 451.92 6.58 o 7 0 2 1270.88 1321.56 19.90 o 8 0 2 1097.81 1274.38 18.04 o 9 0 2 17.06 23.26 2.38 o 10 0 2 226.86 211.85 6.04 o 11 0 2 1311.19 1324.99 24.02 o 12 0 2 722.71 828.28 26.33 o 13 0 2 1541.53 1584.22 48.55 o 14 0 2 8.44 5.81 7.82 o 15 0 2 351.26 335.51 19.49 o 16 0 2 314.77 263.62 20.17 o -16 1 2 306.22 304.94 13.08 o -15 1 2 235.36 229.93 10.33 o -14 1 2 1449.52 1548.14 34.43 o -13 1 2 602.59 577.73 13.32 o -12 1 2 11.94 28.86 3.02 o -11 1 2 507.02 529.76 9.67 o -10 1 2 0.81 7.80 2.23 o -9 1 2 144.23 131.59 3.34 o -8 1 2 26.58 32.08 1.82 o -7 1 2 627.95 616.50 5.75 o -6 1 2 20.07 55.61 2.66 o -5 1 2 3557.42 3431.90 24.95 o -4 1 2 351.75 351.64 4.74 o -3 1 2 2981.23 2660.49 19.70 o -2 1 2 8600.23 7936.11 75.14 o -1 1 2 2886.95 2559.60 23.50 o 0 1 2 3583.14 3357.15 26.89 o 1 1 2 5883.20 5526.03 41.67 o 2 1 2 22172.68 20489.27 165.29 o 3 1 2 7640.62 7075.10 58.74 o 4 1 2 8.02 22.66 1.35 o 5 1 2 1929.73 1874.92 15.42 o 6 1 2 488.43 526.94 5.15 o 7 1 2 626.09 621.04 7.04 o 8 1 2 3.38 18.37 1.87 o 9 1 2 95.25 82.31 2.90 o 10 1 2 698.80 755.93 15.33 o 11 1 2 218.46 206.21 6.88 o 12 1 2 313.79 311.08 10.17 o 13 1 2 402.14 361.57 12.46 o 14 1 2 223.63 218.73 9.01 o 15 1 2 4.82 9.15 5.85 o -15 2 2 1.79 -1.74 5.56 o -14 2 2 0.06 -5.02 5.16 o -13 2 2 125.45 126.15 7.36 o -12 2 2 79.83 79.20 4.85 o -11 2 2 60.09 43.01 3.06 o -10 2 2 826.48 828.94 13.89 o -9 2 2 48.34 47.95 2.74 o -8 2 2 1854.13 1880.06 18.30 o -7 2 2 132.70 119.07 2.35 o -6 2 2 3658.00 3717.95 34.01 o -5 2 2 269.28 230.61 2.99 o -4 2 2 181.41 157.19 4.82 o -3 2 2 139.73 108.57 2.70 o -2 2 2 0.73 22.10 2.44 o -1 2 2 0.39 4.13 0.55 o 0 2 2 225.38 232.33 2.80 o 1 2 2 4.88 -0.83 0.87 o 2 2 2 1148.86 1116.39 8.87 o 3 2 2 0.36 1.13 0.77 o 4 2 2 28.16 43.32 1.59 o 5 2 2 742.41 810.50 8.43 o 6 2 2 1896.31 1942.61 19.17 o 7 2 2 4.22 2.18 1.25 o 8 2 2 1800.88 1820.85 22.56 o 9 2 2 12.74 9.25 2.14 o 10 2 2 327.09 357.64 8.06 o 11 2 2 38.79 39.61 3.65 o 12 2 2 117.50 109.86 6.60 o 13 2 2 5.73 4.97 5.26 o 14 2 2 0.28 -2.17 6.16 o 15 2 2 42.36 46.34 8.16 o -14 3 2 45.99 47.20 11.97 o -13 3 2 0.03 -3.59 5.46 o -12 3 2 245.19 226.17 10.25 o -11 3 2 737.94 699.54 22.61 o -10 3 2 0.46 2.35 2.84 o -9 3 2 1118.30 1079.53 18.84 o -8 3 2 247.51 216.01 4.90 o -7 3 2 524.22 490.79 9.00 o -6 3 2 282.66 255.33 6.58 o -5 3 2 158.07 159.56 4.94 o -4 3 2 267.64 243.49 4.88 o -3 3 2 320.96 339.27 5.76 o -2 3 2 589.27 598.80 9.20 o -1 3 2 460.46 482.14 6.04 o 0 3 2 431.19 455.38 5.79 o 1 3 2 26.61 23.38 1.21 o 2 3 2 317.86 314.92 4.09 o 3 3 2 8.13 8.96 1.59 o 4 3 2 1105.61 1075.93 12.24 o 5 3 2 1903.30 1888.62 22.64 o 6 3 2 0.31 3.98 1.69 o 7 3 2 4205.97 4179.92 55.07 o 8 3 2 21.88 32.01 2.43 o 9 3 2 386.49 384.20 10.25 o 10 3 2 66.07 82.47 4.81 o 11 3 2 111.16 113.95 7.25 o 12 3 2 311.00 320.12 15.27 o 13 3 2 22.11 15.43 7.06 o -12 4 2 0.42 5.38 12.01 o -11 4 2 510.75 475.46 19.80 o -10 4 2 204.65 202.78 11.43 o -9 4 2 164.47 154.63 7.74 o -8 4 2 461.51 503.26 14.85 o -7 4 2 0.58 2.29 3.66 o -6 4 2 0.19 2.25 3.98 o -5 4 2 1226.83 1249.98 25.32 o -4 4 2 389.54 396.51 9.74 o -3 4 2 544.01 519.83 11.43 o -2 4 2 34.86 33.73 3.55 o -1 4 2 611.17 595.96 7.94 o 0 4 2 7.53 7.84 1.68 o 1 4 2 42.59 35.61 1.65 o 2 4 2 0.18 0.70 1.69 o 3 4 2 29.53 24.09 2.00 o 4 4 2 200.65 191.78 4.43 o 5 4 2 679.74 665.61 12.82 o 6 4 2 146.70 146.40 5.48 o 7 4 2 20.19 18.41 3.10 o 8 4 2 304.91 275.38 10.72 o 9 4 2 58.75 61.44 6.05 o 10 4 2 2.05 3.38 7.54 o 11 4 2 475.56 398.59 20.31 o -8 5 2 133.01 102.86 11.19 o -7 5 2 222.11 221.77 12.53 o -6 5 2 5.36 11.25 4.90 o -5 5 2 11.61 23.65 6.53 o -4 5 2 267.75 242.80 10.35 o -3 5 2 5.43 5.59 4.40 o -2 5 2 505.93 521.42 15.75 o -1 5 2 1.86 3.60 5.30 o 0 5 2 1249.15 1341.54 33.93 o 1 5 2 68.62 69.34 4.64 o 2 5 2 290.80 290.26 8.74 o 3 5 2 182.34 190.11 8.64 o 4 5 2 255.00 250.56 11.84 o 5 5 2 37.51 47.17 8.28 o 6 5 2 0.40 2.11 6.59 o 7 5 2 268.67 280.93 18.31 o -16 1 3 101.34 121.75 11.47 o -15 1 3 14.77 17.17 6.97 o -14 1 3 144.89 165.81 7.74 o -13 1 3 125.06 126.57 7.21 o -12 1 3 3.26 2.18 2.47 o -11 1 3 194.87 172.88 4.78 o -10 1 3 109.93 103.64 2.88 o -9 1 3 293.37 280.04 5.01 o -8 1 3 33.43 32.15 1.58 o -7 1 3 934.53 1005.46 9.24 o -6 1 3 496.27 542.67 5.43 o -5 1 3 1864.91 1835.98 14.35 o -4 1 3 884.00 912.80 6.73 o -3 1 3 3693.22 3657.24 30.82 o -2 1 3 767.45 1332.60 217.52 o -1 1 3 305.53 289.96 3.41 o 0 1 3 63.56 56.18 0.96 o 1 1 3 258.27 273.54 2.80 o 2 1 3 16806.38 16348.76 121.94 o 3 1 3 133.61 129.05 1.70 o 4 1 3 1652.51 1981.01 19.70 o 5 1 3 17.79 18.99 1.37 o 6 1 3 40.32 238.00 9.16 o 7 1 3 0.89 5.46 1.34 o 8 1 3 250.40 245.01 4.21 o 9 1 3 19.49 15.75 2.20 o 10 1 3 244.41 221.83 6.18 o 11 1 3 205.40 185.28 6.08 o 12 1 3 9.30 12.75 3.85 o 13 1 3 430.34 401.18 12.84 o 14 1 3 8.70 13.95 6.55 o 15 1 3 7.15 7.21 5.86 o -15 2 3 10.59 9.18 6.53 o -14 2 3 36.78 46.61 7.96 o -13 2 3 8.52 6.93 5.12 o -12 2 3 23.11 10.56 2.78 o -11 2 3 6.13 7.06 2.54 o -10 2 3 130.22 164.71 5.60 o -9 2 3 4.39 8.65 2.17 o -8 2 3 221.88 232.83 4.02 o -7 2 3 504.55 472.45 6.30 o -6 2 3 796.77 791.20 9.09 o -5 2 3 275.09 294.30 3.78 o -4 2 3 4584.85 4622.36 42.32 o -3 2 3 81.13 75.54 1.74 o -2 2 3 386.45 417.66 8.31 o -1 2 3 1862.47 1839.29 17.87 o 0 2 3 1699.66 1838.33 14.70 o 1 2 3 456.56 507.00 4.49 o 2 2 3 62.29 77.45 2.74 o 3 2 3 1.86 5.07 0.94 o 4 2 3 494.71 543.87 6.65 o 5 2 3 1349.94 1368.61 10.93 o 6 2 3 63.73 80.74 4.05 o 7 2 3 6.48 10.13 1.46 o 8 2 3 64.55 81.76 3.07 o 9 2 3 441.17 442.14 9.70 o 10 2 3 197.87 208.21 5.62 o 11 2 3 159.19 139.70 6.37 o 12 2 3 332.27 324.16 12.09 o 13 2 3 227.43 226.71 10.52 o 14 2 3 0.52 -1.26 6.76 o -14 3 3 0.26 6.11 6.46 o -13 3 3 19.66 24.92 7.57 o -12 3 3 46.90 48.71 5.01 o -11 3 3 161.61 163.17 9.07 o -10 3 3 482.51 469.77 13.22 o -9 3 3 42.30 29.80 2.85 o -8 3 3 383.99 371.61 8.59 o -7 3 3 17.86 18.84 3.58 o -6 3 3 158.52 166.86 5.01 o -5 3 3 488.56 518.38 9.15 o -4 3 3 76.81 78.29 3.03 o -3 3 3 164.66 165.27 4.16 o -2 3 3 85.47 87.08 3.13 o -1 3 3 770.20 787.98 8.08 o 0 3 3 907.79 968.97 10.81 o 1 3 3 294.78 286.22 3.93 o 2 3 3 52.09 55.59 2.50 o 3 3 3 44.40 47.73 2.13 o 4 3 3 1449.76 1378.23 17.08 o 5 3 3 117.73 121.64 3.29 o 6 3 3 307.05 305.75 6.29 o 7 3 3 127.43 125.82 3.52 o 8 3 3 11.17 25.59 5.54 o 9 3 3 56.79 49.98 3.11 o 10 3 3 36.48 26.26 4.56 o 11 3 3 76.95 85.91 8.81 o 12 3 3 95.77 99.09 9.20 o 13 3 3 26.68 31.11 7.26 o -12 4 3 0.00 -8.47 8.47 o -11 4 3 195.74 174.10 15.17 o -10 4 3 25.63 33.96 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