#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2015337.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015337_Fobs loop_ _publ_author_name 'Su, Hong' 'Feng, Yun-Long' 'Wen, Yi-Hang' _publ_section_title ; catena-Poly[[tetraaquamanganese(II)]-\m-4-(carboxylatomethylsulfanyl)phenoxyacetato] ; _journal_coeditor_code TY1014 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m208 _journal_page_last m210 _journal_volume 62 _journal_year 2006 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.584 _cell_angle_gamma 90.000 _cell_length_a 5.0977 _cell_length_b 11.4439 _cell_length_c 12.1830 _exptl_crystal_F_000 378.00 _reflns_d_resolution_high 0.7704 _[local]_cod_data_source_file ty1014Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 120.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -14 0 200.91 188.72 14.74 o 1 -14 0 51.36 55.83 5.88 o 2 -14 0 52.13 45.22 5.91 o 1 -13 0 7.22 10.16 3.58 o 2 -13 0 58.40 59.95 5.72 o 3 -13 0 81.36 95.46 9.53 o 0 -12 0 134.95 140.79 9.85 o 1 -12 0 233.40 251.60 8.26 o 2 -12 0 39.17 43.37 4.21 o 3 -12 0 24.35 16.16 4.70 o 1 -11 0 148.54 144.70 10.16 o 2 -11 0 735.63 714.19 17.46 o 3 -11 0 76.98 76.85 5.26 o 4 -11 0 112.75 113.97 6.75 o 0 -10 0 321.51 303.43 19.42 o 1 -10 0 113.58 111.01 5.51 o 2 -10 0 335.48 314.12 10.10 o 3 -10 0 76.32 77.26 4.33 o 4 -10 0 37.74 36.65 4.31 o 1 -9 0 121.53 122.76 8.61 o 2 -9 0 245.80 237.58 6.69 o 3 -9 0 233.66 241.40 6.63 o 4 -9 0 13.67 15.07 3.11 o 5 -9 0 102.67 103.07 5.87 o 0 -8 0 1848.99 1907.89 61.35 o 1 -8 0 1060.63 1051.31 24.72 o 2 -8 0 159.76 159.84 8.09 o 3 -8 0 122.17 119.26 6.87 o 4 -8 0 63.64 64.99 5.06 o 5 -8 0 9.37 8.23 2.91 o 1 -7 0 20.97 25.21 11.74 o 2 -7 0 251.17 238.95 5.87 o 3 -7 0 296.25 295.61 8.07 o 4 -7 0 1226.87 1190.33 23.36 o 5 -7 0 34.53 36.75 3.26 o 0 -6 0 515.10 476.21 13.51 o 1 -6 0 550.50 509.07 10.96 o 2 -6 0 6.09 7.04 2.28 o 3 -6 0 238.19 238.72 5.84 o 4 -6 0 40.12 44.26 3.68 o 5 -6 0 55.59 58.24 4.50 o 6 -6 0 21.32 17.34 8.52 o 1 -5 0 592.30 624.76 12.63 o 2 -5 0 92.43 86.79 2.87 o 3 -5 0 197.49 192.76 5.38 o 4 -5 0 91.92 89.88 3.70 o 5 -5 0 450.56 458.64 14.24 o 6 -5 0 14.65 14.42 3.51 o 0 -4 0 3648.87 3542.12 115.31 o 1 -4 0 3038.22 3132.19 60.47 o 2 -4 0 1198.00 1206.52 19.62 o 3 -4 0 64.51 70.40 3.15 o 4 -4 0 129.83 124.50 5.38 o 5 -4 0 266.58 252.01 11.52 o 6 -4 0 355.96 342.10 13.39 o 1 -3 0 50.98 57.59 1.82 o 2 -3 0 3813.55 3867.00 77.01 o 3 -3 0 465.51 476.71 12.35 o 4 -3 0 623.75 602.59 18.87 o 5 -3 0 233.34 233.81 5.72 o 6 -3 0 76.10 77.16 5.72 o 0 -2 0 2205.73 2395.73 69.99 o 1 -2 0 1178.61 1176.31 16.76 o 2 -2 0 4.27 6.46 0.92 o 3 -2 0 26.58 31.87 2.41 o 4 -2 0 22.33 18.74 2.16 o 5 -2 0 230.19 222.55 5.99 o 6 -2 0 3.53 5.31 3.67 o 1 -1 0 464.45 459.85 8.97 o 2 -1 0 513.35 517.66 9.36 o 3 -1 0 992.03 971.84 18.14 o 4 -1 0 922.27 906.71 15.85 o 5 -1 0 295.97 296.65 6.24 o 6 -1 0 44.12 44.33 4.38 o 1 0 0 3596.89 3882.58 122.63 o 2 0 0 37.04 32.53 1.63 o 3 0 0 15.07 17.13 1.46 o 4 0 0 1100.62 1081.53 19.79 o 5 0 0 64.65 68.75 3.11 o 6 0 0 55.49 56.17 3.39 o 1 1 0 421.46 429.91 9.20 o 2 1 0 454.41 450.31 8.55 o 3 1 0 1034.75 1019.30 19.92 o 4 1 0 908.38 899.40 15.39 o 5 1 0 329.69 339.16 6.92 o 6 1 0 37.71 39.03 3.47 o 0 2 0 2420.85 2593.69 71.24 o 1 2 0 1222.26 1223.88 17.24 o 2 2 0 1.23 2.00 0.89 o 3 2 0 23.79 27.61 4.15 o 4 2 0 26.04 32.09 2.63 o 5 2 0 233.63 229.74 5.45 o 6 2 0 0.78 1.25 1.72 o 1 3 0 40.08 44.56 2.06 o 2 3 0 3925.43 4036.02 80.68 o 3 3 0 439.98 460.54 9.78 o 4 3 0 615.48 596.20 12.11 o 5 3 0 214.71 199.05 8.94 o 6 3 0 75.74 72.03 3.66 o 0 4 0 3623.67 3512.10 114.44 o 1 4 0 3143.60 3193.66 73.96 o 2 4 0 1204.08 1193.31 24.00 o 3 4 0 60.27 66.08 2.80 o 4 4 0 129.18 120.94 7.04 o 5 4 0 265.58 263.96 9.18 o 6 4 0 352.47 336.91 9.30 o 1 5 0 538.30 561.65 17.01 o 2 5 0 71.15 67.66 8.39 o 3 5 0 250.51 246.19 6.71 o 4 5 0 73.31 71.66 7.17 o 5 5 0 466.82 475.55 19.80 o 6 5 0 15.47 13.02 3.48 o 0 6 0 535.49 508.96 13.94 o 1 6 0 486.94 443.51 10.26 o 2 6 0 6.63 13.15 5.89 o 3 6 0 230.27 226.48 11.07 o 4 6 0 46.74 44.24 3.25 o 5 6 0 53.33 55.28 4.82 o 6 6 0 29.12 15.18 3.78 o 1 7 0 17.22 17.52 4.94 o 2 7 0 273.37 261.22 7.72 o 3 7 0 286.91 286.15 7.63 o 4 7 0 1230.98 1196.38 28.05 o 5 7 0 44.25 48.37 4.66 o 0 8 0 1831.76 1935.88 62.50 o 1 8 0 1061.46 1062.90 22.84 o 2 8 0 149.89 154.62 8.40 o 3 8 0 129.55 128.96 5.13 o 4 8 0 60.88 61.64 5.67 o 5 8 0 7.97 7.34 3.41 o 1 9 0 111.54 126.90 6.09 o 2 9 0 210.34 201.36 9.06 o 3 9 0 232.34 237.43 15.17 o 4 9 0 15.76 11.75 5.34 o 5 9 0 90.95 92.94 7.46 o 0 10 0 323.39 315.49 13.47 o 1 10 0 115.93 111.00 5.52 o 2 10 0 359.21 349.82 17.32 o 3 10 0 72.65 74.78 5.68 o 4 10 0 38.80 38.21 5.67 o 1 11 0 142.07 142.31 6.80 o 2 11 0 745.01 760.19 26.55 o 3 11 0 78.89 77.47 5.43 o 4 11 0 107.69 108.16 6.68 o 0 12 0 106.94 107.74 9.67 o 1 12 0 247.91 269.69 10.04 o 2 12 0 33.62 34.34 4.74 o 3 12 0 21.63 21.41 5.25 o 1 13 0 6.22 6.83 4.46 o 2 13 0 68.58 65.66 6.05 o 3 13 0 71.39 77.04 7.77 o 0 14 0 206.57 228.42 23.21 o 1 14 0 51.07 57.61 7.73 o 2 14 0 56.56 54.69 11.29 o -2 -14 1 3.91 4.49 3.69 o -1 -14 1 81.65 84.39 6.10 o 0 -14 1 111.23 127.41 8.11 o 1 -14 1 230.83 247.33 9.87 o 2 -14 1 31.31 32.79 6.01 o -3 -13 1 23.45 20.28 3.91 o -2 -13 1 48.85 68.97 5.12 o -1 -13 1 0.22 0.33 2.31 o 0 -13 1 174.94 186.67 8.84 o 1 -13 1 44.88 43.97 4.47 o 2 -13 1 1.99 2.89 2.73 o 3 -13 1 17.14 16.38 3.83 o -3 -12 1 7.15 7.25 3.24 o -2 -12 1 22.91 23.84 4.08 o -1 -12 1 107.09 102.58 6.57 o 0 -12 1 127.56 127.55 7.22 o 1 -12 1 91.73 99.40 9.53 o 2 -12 1 133.69 138.26 6.09 o 3 -12 1 21.63 23.04 3.89 o -4 -11 1 30.86 28.43 3.95 o -3 -11 1 271.30 267.43 8.37 o -2 -11 1 284.21 273.08 10.51 o -1 -11 1 415.42 416.21 14.50 o 0 -11 1 67.29 68.41 6.71 o 1 -11 1 43.19 43.74 4.25 o 2 -11 1 11.01 9.34 2.70 o 3 -11 1 20.53 24.83 3.77 o 4 -11 1 3.09 3.25 2.77 o -4 -10 1 24.81 30.80 4.65 o -3 -10 1 95.47 97.95 4.82 o -2 -10 1 85.40 84.94 8.98 o -1 -10 1 178.40 177.44 20.80 o 0 -10 1 288.94 272.16 8.54 o 1 -10 1 602.72 580.96 13.28 o 2 -10 1 499.22 499.18 11.03 o 3 -10 1 143.55 145.48 7.30 o 4 -10 1 14.98 15.12 3.43 o -5 -9 1 25.60 23.79 3.90 o -4 -9 1 183.42 173.37 7.08 o -3 -9 1 50.69 48.18 3.65 o -2 -9 1 111.69 118.07 4.37 o -1 -9 1 67.51 69.42 5.91 o 0 -9 1 311.71 290.48 9.35 o 1 -9 1 57.56 54.28 6.63 o 2 -9 1 56.75 55.37 6.52 o 3 -9 1 153.67 159.89 5.87 o 4 -9 1 242.61 236.49 7.86 o 5 -9 1 49.06 48.27 4.33 o -5 -8 1 181.93 177.13 8.89 o -4 -8 1 717.78 691.56 15.85 o -3 -8 1 209.87 207.47 7.17 o -2 -8 1 41.62 40.26 3.55 o -1 -8 1 123.82 126.38 4.74 o 0 -8 1 1433.00 1403.35 30.92 o 1 -8 1 478.64 453.81 9.39 o 2 -8 1 414.22 415.86 9.18 o 3 -8 1 129.71 128.77 4.45 o 4 -8 1 2.00 3.40 2.61 o 5 -8 1 7.22 6.97 2.64 o -5 -7 1 71.98 71.54 5.00 o -4 -7 1 75.42 71.34 5.03 o -3 -7 1 762.50 756.42 16.37 o -2 -7 1 12.88 12.23 3.06 o -1 -7 1 1997.27 1861.70 41.36 o 0 -7 1 729.86 787.54 34.29 o 1 -7 1 240.31 243.74 5.66 o 2 -7 1 347.64 351.94 7.37 o 3 -7 1 619.46 616.08 12.40 o 4 -7 1 258.42 253.72 8.34 o 5 -7 1 348.13 340.11 12.45 o -6 -6 1 57.60 58.79 7.39 o -5 -6 1 22.10 18.95 3.99 o -4 -6 1 439.75 432.76 8.92 o -3 -6 1 292.24 294.22 7.06 o -2 -6 1 171.82 170.64 4.53 o -1 -6 1 360.80 336.98 12.16 o 0 -6 1 1942.09 2008.80 42.46 o 1 -6 1 1134.40 1147.01 21.75 o 2 -6 1 981.25 923.66 15.14 o 3 -6 1 221.93 218.71 5.53 o 4 -6 1 167.82 166.49 5.19 o 5 -6 1 37.13 32.42 3.84 o -6 -5 1 5.86 6.41 3.07 o -5 -5 1 58.05 52.99 5.08 o -4 -5 1 162.97 169.25 5.55 o -3 -5 1 127.34 130.14 3.80 o -2 -5 1 1501.93 1479.90 25.87 o -1 -5 1 87.10 82.89 4.30 o 0 -5 1 358.09 333.01 6.50 o 1 -5 1 101.53 101.47 3.56 o 2 -5 1 45.39 51.19 4.87 o 3 -5 1 38.76 40.78 2.02 o 4 -5 1 364.77 369.39 7.20 o 5 -5 1 122.97 121.32 5.64 o 6 -5 1 127.62 128.23 9.47 o -6 -4 1 120.79 120.45 8.22 o -5 -4 1 619.81 590.48 18.40 o -4 -4 1 39.98 40.46 2.91 o -3 -4 1 525.54 505.28 9.76 o -2 -4 1 49.18 55.75 2.05 o -1 -4 1 256.68 231.23 5.13 o 0 -4 1 181.38 181.70 7.79 o 1 -4 1 10260.20 11125.25 309.04 o 2 -4 1 2280.22 2413.91 42.88 o 3 -4 1 372.24 376.69 6.77 o 4 -4 1 59.98 55.17 4.25 o 5 -4 1 111.95 112.74 9.29 o 6 -4 1 40.53 35.17 4.61 o -6 -3 1 50.12 48.18 7.49 o -5 -3 1 29.02 40.48 3.00 o -4 -3 1 53.08 53.83 2.97 o -3 -3 1 1958.13 1987.96 35.24 o -2 -3 1 2939.81 3154.22 61.20 o -1 -3 1 1249.85 1279.44 23.81 o 0 -3 1 1966.86 1987.41 39.99 o 1 -3 1 89.08 82.09 2.04 o 2 -3 1 501.48 508.46 7.86 o 3 -3 1 45.80 51.34 2.60 o 4 -3 1 149.93 139.63 4.46 o 5 -3 1 908.83 847.19 26.10 o 6 -3 1 87.24 88.19 5.49 o -6 -2 1 172.21 176.55 7.67 o -5 -2 1 17.73 23.80 3.19 o -4 -2 1 487.84 453.24 12.05 o -3 -2 1 148.53 158.85 4.53 o -2 -2 1 122.80 132.62 2.88 o -1 -2 1 507.15 491.36 6.84 o 0 -2 1 3868.34 4086.75 92.10 o 1 -2 1 1944.78 1922.38 30.08 o 2 -2 1 1651.57 1573.61 23.96 o 3 -2 1 7.67 9.58 1.65 o 4 -2 1 192.32 183.48 5.94 o 5 -2 1 51.42 52.56 3.15 o 6 -2 1 107.09 107.28 5.96 o -6 -1 1 38.45 38.01 3.68 o -5 -1 1 65.59 64.64 3.15 o -4 -1 1 826.25 855.97 15.07 o -3 -1 1 926.43 901.56 17.59 o -2 -1 1 330.72 353.69 5.74 o -1 -1 1 962.31 938.18 12.94 o 1 -1 1 3648.56 3930.59 72.46 o 2 -1 1 127.92 142.84 4.50 o 3 -1 1 415.36 400.49 7.48 o 4 -1 1 1013.21 1009.70 19.68 o 5 -1 1 186.78 181.39 5.50 o 6 -1 1 176.72 180.03 6.11 o -6 0 1 30.46 32.91 3.49 o -5 0 1 1077.55 1057.57 20.93 o -4 0 1 1310.59 1328.32 23.57 o -3 0 1 1399.30 1430.41 23.69 o -2 0 1 140.39 127.32 3.09 o -1 0 1 3051.46 3423.72 72.82 o 1 0 1 1915.10 1967.91 88.11 o 2 0 1 18.24 19.10 1.29 o 3 0 1 1167.50 1176.75 17.86 o 4 0 1 0.24 1.08 1.13 o 5 0 1 13.97 12.61 1.64 o 6 0 1 6.14 5.53 3.30 o -6 1 1 34.78 30.10 2.51 o -5 1 1 72.88 69.17 2.82 o -4 1 1 850.69 862.42 17.12 o -3 1 1 910.15 887.22 17.39 o -2 1 1 426.39 442.31 7.06 o -1 1 1 880.80 894.33 14.26 o 1 1 1 3603.23 3941.37 73.01 o 2 1 1 119.29 129.48 4.17 o 3 1 1 380.88 379.92 7.04 o 4 1 1 1072.45 1076.57 18.77 o 5 1 1 155.03 150.45 4.05 o 6 1 1 193.99 179.05 6.27 o -6 2 1 183.90 183.05 5.56 o -5 2 1 29.71 31.79 2.42 o -4 2 1 465.00 454.07 10.52 o -3 2 1 166.70 166.29 5.14 o -2 2 1 122.50 141.32 4.88 o -1 2 1 537.48 532.43 8.95 o 0 2 1 3707.00 3830.74 86.48 o 1 2 1 1909.40 1891.18 29.91 o 2 2 1 1560.27 1477.33 23.06 o 3 2 1 5.31 5.68 1.62 o 4 2 1 192.20 186.95 4.63 o 5 2 1 52.46 55.47 3.80 o 6 2 1 105.22 105.15 9.70 o -6 3 1 54.41 47.90 2.97 o -5 3 1 24.97 28.73 3.39 o -4 3 1 46.44 47.61 2.72 o -3 3 1 1967.86 2047.49 45.19 o -2 3 1 2909.84 3111.37 71.57 o -1 3 1 1284.03 1287.75 25.37 o 0 3 1 1890.74 1934.42 37.66 o 1 3 1 95.80 95.29 3.55 o 2 3 1 499.89 509.64 12.49 o 3 3 1 59.33 59.23 3.71 o 4 3 1 110.44 112.26 6.57 o 5 3 1 918.40 896.56 17.36 o 6 3 1 77.87 77.19 3.96 o -6 4 1 135.32 129.04 5.41 o -5 4 1 625.10 595.84 24.64 o -4 4 1 46.90 40.19 13.85 o -3 4 1 504.17 487.74 10.35 o -2 4 1 51.67 55.83 3.28 o -1 4 1 278.69 250.01 5.96 o 0 4 1 133.65 135.05 6.03 o 1 4 1 10208.12 11395.65 381.68 o 2 4 1 2351.43 2446.12 43.04 o 3 4 1 340.71 346.03 6.34 o 4 4 1 68.66 62.17 2.80 o 5 4 1 108.84 107.74 4.23 o 6 4 1 42.66 40.23 4.43 o -6 5 1 5.92 3.51 3.21 o -5 5 1 63.99 65.34 5.05 o -4 5 1 182.44 189.22 7.46 o -3 5 1 97.08 95.87 10.06 o -2 5 1 1568.24 1529.89 33.26 o -1 5 1 55.28 53.86 2.60 o 0 5 1 326.23 307.03 13.87 o 1 5 1 100.52 99.87 3.02 o 2 5 1 53.03 60.66 8.19 o 3 5 1 25.43 24.08 2.69 o 4 5 1 352.42 358.38 7.86 o 5 5 1 112.86 111.48 5.90 o 6 5 1 133.51 102.92 9.02 o -6 6 1 49.18 46.65 9.40 o -5 6 1 22.33 19.90 3.85 o -4 6 1 401.02 387.33 10.42 o -3 6 1 305.03 311.66 7.98 o -2 6 1 173.03 165.09 9.37 o -1 6 1 382.97 355.37 10.21 o 0 6 1 1909.34 2003.64 42.37 o 1 6 1 1175.51 1184.54 39.89 o 2 6 1 970.32 933.61 19.83 o 3 6 1 235.13 238.06 5.84 o 4 6 1 157.50 148.42 5.48 o 5 6 1 38.08 34.90 3.67 o -5 7 1 66.85 62.46 5.95 o -4 7 1 64.85 62.16 6.94 o -3 7 1 776.09 762.43 17.31 o -2 7 1 21.75 24.44 3.97 o -1 7 1 2083.52 1954.99 42.78 o 0 7 1 734.81 800.29 31.71 o 1 7 1 239.71 245.03 7.15 o 2 7 1 324.75 335.32 9.09 o 3 7 1 624.65 617.74 16.01 o 4 7 1 262.32 262.11 9.01 o 5 7 1 325.63 315.70 11.77 o -5 8 1 172.53 166.02 14.53 o -4 8 1 719.56 696.54 20.29 o -3 8 1 195.28 193.28 6.69 o -2 8 1 40.36 46.04 11.82 o -1 8 1 108.92 111.95 4.67 o 0 8 1 1451.41 1464.97 32.17 o 1 8 1 420.37 417.59 11.22 o 2 8 1 498.27 506.80 14.02 o 3 8 1 143.66 136.56 5.09 o 4 8 1 0.76 1.40 3.48 o 5 8 1 8.19 10.62 3.32 o -5 9 1 25.75 16.53 8.39 o -4 9 1 180.95 176.35 9.38 o -3 9 1 35.99 28.89 3.84 o -2 9 1 111.46 117.05 5.32 o -1 9 1 79.70 80.67 4.34 o 0 9 1 290.25 275.60 7.98 o 1 9 1 56.04 58.49 9.42 o 2 9 1 66.24 64.99 3.85 o 3 9 1 174.83 166.45 8.98 o 4 9 1 238.70 246.52 10.04 o 5 9 1 52.07 47.15 4.62 o -4 10 1 23.46 25.05 7.06 o -3 10 1 103.13 103.67 5.85 o -2 10 1 84.30 88.75 12.99 o -1 10 1 171.75 176.03 12.49 o 0 10 1 291.33 283.86 8.57 o 1 10 1 615.82 623.30 15.52 o 2 10 1 481.86 475.62 13.13 o 3 10 1 155.30 147.66 6.31 o 4 10 1 12.10 10.18 6.62 o -4 11 1 27.42 18.59 7.58 o -3 11 1 265.95 275.68 10.71 o -2 11 1 308.14 296.38 25.28 o -1 11 1 399.69 406.90 14.06 o 0 11 1 77.24 84.40 6.25 o 1 11 1 47.28 52.72 5.64 o 2 11 1 11.95 12.73 4.37 o 3 11 1 15.23 13.28 4.77 o 4 11 1 2.94 0.78 2.61 o -3 12 1 6.00 7.00 4.19 o -2 12 1 23.33 22.26 5.44 o -1 12 1 114.78 119.30 12.70 o 0 12 1 117.21 130.15 7.00 o 1 12 1 78.29 86.48 7.35 o 2 12 1 147.78 156.55 9.07 o 3 12 1 14.44 13.28 3.93 o -3 13 1 25.28 19.58 6.25 o -2 13 1 48.80 60.45 7.14 o -1 13 1 0.61 -1.59 2.73 o 0 13 1 162.55 166.30 10.59 o 1 13 1 45.00 52.97 13.29 o 2 13 1 2.66 4.52 5.58 o 3 13 1 22.48 23.50 5.95 o -2 14 1 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