#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:06:16 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180823 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/54/2015401.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015401_Fobs loop_ _publ_author_name 'Smith, Graham' 'Wermuth, Urs D.' 'White, Jonathan M.' _publ_section_title ; Mixed dicationic and monocationic benzidine species in the proton-transfer compound of benzidine with 3,5-dinitrosalicylic acid ; _journal_coeditor_code AV3018 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o402 _journal_page_last o404 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.154 _cell_angle_gamma 90.000 _cell_length_a 18.8622 _cell_length_b 10.5138 _cell_length_c 19.0812 _exptl_crystal_F_000 1620.00 _reflns_d_resolution_high 0.7682 _cod_data_source_file av3018Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' JMWGS49 in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 432.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 41466.16 38150.33 1329.43 o 3 0 0 2735.97 2244.52 79.94 o 4 0 0 16414.38 17187.22 347.77 o 5 0 0 2.64 3.32 12.79 o 6 0 0 2059.21 2103.67 71.63 o 7 0 0 5260.01 5472.34 124.63 o 8 0 0 1910.72 1853.59 117.36 o 9 0 0 7612.88 8042.37 202.68 o 10 0 0 1655.36 1852.95 109.55 o 11 0 0 7.71 -11.71 20.82 o 12 0 0 901.59 878.78 70.10 o 13 0 0 466.00 489.98 66.07 o 14 0 0 39.30 55.14 34.42 o 15 0 0 174.03 145.56 47.18 o 16 0 0 141.76 130.82 44.92 o 17 0 0 302.51 228.13 58.82 o 18 0 0 94.64 176.04 79.14 o 19 0 0 259.08 109.82 74.29 o 20 0 0 20.32 1.08 52.22 o 21 0 0 23.40 29.07 66.75 o 22 0 0 24.69 -17.77 63.52 o 1 1 0 137.84 156.08 8.01 o 2 1 0 1811.42 1573.64 28.38 o 3 1 0 271.28 293.81 16.24 o 4 1 0 19959.08 19561.89 380.74 o 5 1 0 2552.29 2502.42 49.10 o 6 1 0 10719.05 10981.58 249.11 o 7 1 0 1566.23 1586.75 47.41 o 8 1 0 566.94 556.60 33.57 o 9 1 0 18.11 39.01 16.74 o 10 1 0 10.47 -5.56 13.20 o 11 1 0 167.20 209.88 30.14 o 12 1 0 489.49 574.31 45.55 o 13 1 0 250.59 268.49 37.02 o 14 1 0 889.68 959.50 60.27 o 15 1 0 198.49 191.98 35.46 o 16 1 0 0.38 -20.68 23.59 o 17 1 0 0.12 23.06 29.20 o 18 1 0 14.15 14.68 30.44 o 19 1 0 38.57 79.96 40.19 o 20 1 0 1.27 -10.41 40.61 o 21 1 0 4.43 -33.92 59.22 o 22 1 0 0.21 19.38 65.14 o 23 1 0 53.67 87.75 69.98 o 0 2 0 3809.22 3876.46 52.56 o 1 2 0 54.98 43.04 6.16 o 2 2 0 2057.34 1975.54 43.00 o 3 2 0 138.14 131.96 13.23 o 4 2 0 6356.48 6064.13 128.68 o 5 2 0 286.84 282.23 22.50 o 6 2 0 7796.35 7814.27 229.46 o 7 2 0 1016.58 1011.76 37.73 o 8 2 0 5996.90 6183.69 150.60 o 9 2 0 67.51 97.51 20.13 o 10 2 0 617.51 739.59 41.16 o 11 2 0 352.94 406.31 37.48 o 12 2 0 71.86 96.45 24.57 o 13 2 0 19.84 16.18 19.77 o 14 2 0 92.61 92.67 33.71 o 15 2 0 124.67 107.18 35.57 o 16 2 0 3.58 27.01 29.54 o 17 2 0 54.09 69.94 33.72 o 18 2 0 0.73 11.82 39.01 o 19 2 0 203.93 185.01 59.12 o 20 2 0 5.23 -32.23 40.70 o 21 2 0 2.70 -5.38 53.83 o 22 2 0 0.82 27.46 60.83 o 1 3 0 63514.23 64236.66 935.49 o 2 3 0 25.47 16.59 10.42 o 3 3 0 25.49 19.23 9.94 o 4 3 0 1079.49 1030.54 32.63 o 5 3 0 377.83 380.07 24.21 o 6 3 0 1053.87 989.23 37.74 o 7 3 0 34.89 28.80 14.24 o 8 3 0 545.51 600.84 30.63 o 9 3 0 23.01 20.95 13.08 o 10 3 0 9.59 5.97 15.38 o 11 3 0 248.00 266.13 32.00 o 12 3 0 33.37 62.77 29.90 o 13 3 0 45.75 62.75 29.41 o 14 3 0 11.83 11.01 25.66 o 15 3 0 1.32 -29.81 29.81 o 16 3 0 31.47 46.85 37.87 o 17 3 0 38.26 35.37 39.06 o 18 3 0 2.28 -5.00 37.10 o 19 3 0 0.21 14.20 44.08 o 20 3 0 65.85 102.78 52.49 o 21 3 0 0.02 -38.20 38.20 o 22 3 0 19.49 7.67 44.63 o 0 4 0 10088.52 9911.18 121.73 o 1 4 0 285.19 275.01 17.97 o 2 4 0 1216.16 1249.70 43.36 o 3 4 0 4963.96 5296.27 91.59 o 4 4 0 197.85 218.20 21.41 o 5 4 0 599.35 637.32 31.83 o 6 4 0 361.50 383.09 24.56 o 7 4 0 7.29 11.33 12.26 o 8 4 0 4820.47 4913.49 92.78 o 9 4 0 225.76 270.46 30.73 o 10 4 0 45.96 41.39 20.41 o 11 4 0 2.10 -7.40 27.66 o 12 4 0 322.39 328.35 64.30 o 13 4 0 266.73 248.54 60.39 o 14 4 0 283.01 295.39 66.29 o 15 4 0 0.91 16.50 36.88 o 16 4 0 16.30 49.18 40.74 o 17 4 0 217.89 207.27 62.31 o 18 4 0 88.12 96.93 51.75 o 19 4 0 5.52 3.49 41.00 o 20 4 0 11.48 9.49 43.12 o 21 4 0 14.89 12.00 43.45 o 22 4 0 40.21 99.05 83.44 o 1 5 0 272.27 233.21 18.22 o 2 5 0 71.69 64.02 11.58 o 3 5 0 199.02 201.84 23.45 o 4 5 0 596.24 639.88 34.51 o 5 5 0 827.99 899.06 39.13 o 6 5 0 284.49 293.34 40.60 o 7 5 0 1315.84 1272.50 69.47 o 8 5 0 9.67 9.81 19.10 o 9 5 0 432.86 414.58 52.14 o 10 5 0 535.24 531.46 60.15 o 11 5 0 125.24 139.11 38.28 o 12 5 0 254.70 228.37 46.37 o 13 5 0 14.91 27.81 39.19 o 14 5 0 126.65 128.00 54.42 o 15 5 0 192.93 335.84 76.77 o 16 5 0 55.36 61.94 49.71 o 17 5 0 0.31 13.56 43.39 o 18 5 0 37.14 116.60 52.38 o 19 5 0 16.25 5.82 42.72 o 20 5 0 14.79 28.90 43.98 o 21 5 0 26.17 38.91 45.97 o 0 6 0 42537.67 42108.09 940.31 o 1 6 0 458.40 463.07 27.18 o 2 6 0 14818.41 14957.16 205.76 o 3 6 0 11.91 8.32 15.07 o 4 6 0 964.56 964.21 44.64 o 5 6 0 84.39 68.72 19.46 o 6 6 0 126.25 127.68 32.99 o 7 6 0 12.24 5.12 20.37 o 8 6 0 41.66 27.86 21.90 o 9 6 0 1242.49 1295.63 79.96 o 10 6 0 47.28 52.70 28.03 o 11 6 0 0.13 11.93 25.85 o 12 6 0 173.30 212.01 48.89 o 13 6 0 7.49 27.65 31.64 o 14 6 0 1.94 3.31 39.24 o 15 6 0 15.80 59.71 47.56 o 16 6 0 45.06 32.35 52.53 o 17 6 0 64.52 129.40 63.64 o 18 6 0 13.99 29.67 49.33 o 19 6 0 6.68 24.60 49.97 o 20 6 0 19.00 24.11 42.03 o 1 7 0 588.89 596.69 38.10 o 2 7 0 0.11 5.16 13.82 o 3 7 0 151.36 187.08 28.68 o 4 7 0 34.30 45.77 25.07 o 5 7 0 312.05 275.60 43.96 o 6 7 0 42.42 63.10 26.57 o 7 7 0 561.46 508.46 59.62 o 8 7 0 79.07 79.24 31.79 o 9 7 0 418.90 405.17 58.63 o 10 7 0 91.05 92.16 34.60 o 11 7 0 1.55 14.57 29.44 o 12 7 0 67.93 65.82 36.23 o 13 7 0 5.42 4.59 29.98 o 14 7 0 83.82 67.09 40.36 o 15 7 0 0.02 10.47 44.68 o 16 7 0 31.49 -1.00 50.39 o 17 7 0 0.36 2.83 43.29 o 18 7 0 55.35 66.95 59.38 o 19 7 0 2.46 69.86 50.54 o 0 8 0 371.05 445.73 64.05 o 1 8 0 58.74 44.06 22.19 o 2 8 0 100.04 86.81 26.01 o 3 8 0 203.21 154.75 31.94 o 4 8 0 0.54 3.60 20.48 o 5 8 0 5.32 -2.41 21.45 o 6 8 0 454.07 424.39 56.02 o 7 8 0 16.55 30.94 28.14 o 8 8 0 1.93 -16.87 21.62 o 9 8 0 21.40 -0.26 26.56 o 10 8 0 0.33 -1.15 26.09 o 11 8 0 36.72 1.18 27.91 o 12 8 0 3.22 -0.83 29.87 o 13 8 0 11.71 27.54 35.04 o 14 8 0 45.68 63.77 43.28 o 15 8 0 2.86 -27.46 34.35 o 16 8 0 61.74 39.96 52.52 o 17 8 0 3.99 28.30 51.97 o 18 8 0 1.71 2.70 50.24 o 1 9 0 7142.21 6193.11 171.72 o 2 9 0 5.71 0.63 22.17 o 3 9 0 486.28 457.73 60.79 o 4 9 0 9.03 13.13 23.29 o 5 9 0 2.67 6.74 25.19 o 6 9 0 0.00 -7.53 24.44 o 7 9 0 68.06 95.21 36.22 o 8 9 0 84.62 79.16 37.60 o 9 9 0 4.13 17.98 33.41 o 10 9 0 74.62 49.97 34.34 o 11 9 0 14.92 8.31 32.04 o 12 9 0 11.14 49.69 38.33 o 13 9 0 0.50 2.34 31.92 o 14 9 0 19.60 55.11 38.72 o 15 9 0 9.63 -19.94 30.03 o 16 9 0 8.19 25.32 45.17 o 17 9 0 18.56 66.22 81.29 o 0 10 0 389.06 486.12 120.59 o 1 10 0 133.59 117.11 51.70 o 2 10 0 170.62 161.56 42.65 o 3 10 0 281.54 277.05 51.37 o 4 10 0 74.60 127.69 39.06 o 5 10 0 167.67 166.10 44.48 o 6 10 0 355.33 293.53 56.70 o 7 10 0 266.60 250.47 67.98 o 8 10 0 61.33 85.38 46.90 o 9 10 0 101.49 43.16 38.38 o 10 10 0 1.20 -30.08 30.08 o 11 10 0 2.00 -8.59 36.92 o 12 10 0 57.67 64.22 35.53 o 13 10 0 56.29 58.35 39.48 o 14 10 0 10.29 14.88 32.64 o 15 10 0 0.01 -29.58 29.58 o 1 11 0 3.25 -2.86 38.24 o 2 11 0 1.71 -20.41 35.03 o 3 11 0 13.68 18.86 41.65 o 4 11 0 23.23 20.76 32.44 o 5 11 0 0.10 -1.01 27.94 o 6 11 0 8.50 30.98 30.45 o 7 11 0 49.45 43.09 37.91 o 8 11 0 11.00 10.05 33.40 o 9 11 0 54.35 8.09 39.45 o 10 11 0 12.51 43.10 45.49 o 11 11 0 0.02 -26.78 34.83 o 12 11 0 0.69 -7.25 38.49 o 13 11 0 6.40 -6.31 33.86 o 0 12 0 4.18 62.45 83.44 o 1 12 0 0.02 7.58 50.82 o 2 12 0 0.88 -10.00 43.10 o 3 12 0 28.38 40.54 55.56 o 4 12 0 43.66 78.09 61.41 o 5 12 0 5.10 28.55 43.87 o 6 12 0 0.31 -2.45 42.17 o 7 12 0 1.15 17.41 34.22 o 8 12 0 2.42 14.30 32.92 o 9 12 0 0.63 -18.55 29.07 o 10 12 0 1.27 13.08 32.96 o 11 12 0 1.72 36.61 50.60 o 1 13 0 223.02 241.86 78.78 o 2 13 0 98.18 147.20 67.66 o 3 13 0 4.59 -13.34 43.30 o 4 13 0 29.94 75.70 55.76 o 5 13 0 24.99 43.63 50.31 o 6 13 0 7.75 8.16 47.08 o 7 13 0 25.82 3.23 63.52 o -23 1 1 19.92 59.22 66.75 o -22 1 1 0.90 46.30 66.22 o -21 1 1 4.86 48.45 68.91 o -20 1 1 76.89 124.37 54.02 o -19 1 1 20.55 44.35 34.52 o -18 1 1 355.40 317.96 56.19 o -17 1 1 90.06 72.71 33.20 o -16 1 1 156.08 117.13 32.25 o -15 1 1 48.52 38.51 25.09 o -14 1 1 53.05 73.55 26.09 o -13 1 1 35.16 43.21 21.97 o -12 1 1 17.36 1.88 17.98 o -11 1 1 317.53 324.92 34.95 o -10 1 1 310.45 325.40 32.83 o -9 1 1 1434.09 1378.63 51.69 o -8 1 1 14.94 84.07 18.37 o -7 1 1 7551.03 8270.68 213.92 o -6 1 1 1190.44 1119.95 45.11 o -5 1 1 334.68 346.74 26.54 o -4 1 1 3162.64 3203.61 84.79 o -3 1 1 2186.20 2155.34 44.37 o -2 1 1 5049.20 4791.84 77.14 o -1 1 1 15999.88 15349.55 127.33 o 0 1 1 4274.03 3586.79 46.96 o 1 1 1 713.19 493.55 16.44 o 2 1 1 4537.35 4126.14 90.76 o 3 1 1 21861.85 23404.12 552.78 o 4 1 1 189.58 221.29 15.15 o 5 1 1 5460.83 5561.30 82.83 o 6 1 1 5.05 0.11 10.04 o 7 1 1 10383.47 10650.81 195.04 o 8 1 1 98.01 108.12 20.03 o 9 1 1 4423.67 4683.02 100.00 o 10 1 1 832.21 860.12 44.52 o 11 1 1 161.35 244.42 32.57 o 12 1 1 24.30 31.94 20.84 o 13 1 1 189.70 176.30 32.57 o 14 1 1 111.32 123.21 29.04 o 15 1 1 71.88 54.47 29.80 o 16 1 1 162.95 154.14 41.05 o 17 1 1 79.71 95.65 38.07 o 18 1 1 32.78 5.96 31.33 o 19 1 1 43.05 31.00 41.85 o 20 1 1 55.92 41.45 65.68 o 21 1 1 10.82 32.84 65.68 o 22 1 1 0.14 -33.38 54.37 o -23 2 1 8.85 57.60 66.22 o -22 2 1 25.77 51.68 64.60 o -21 2 1 28.01 102.48 56.41 o -20 2 1 14.93 52.34 46.27 o -19 2 1 26.49 58.46 43.69 o -18 2 1 8.65 -34.29 36.49 o -17 2 1 202.92 161.18 40.70 o -16 2 1 27.64 23.93 28.09 o -15 2 1 83.02 68.56 31.45 o -14 2 1 1214.21 1179.44 61.97 o -13 2 1 0.10 9.09 19.07 o -12 2 1 333.70 313.27 36.50 o -11 2 1 57.50 47.16 19.40 o -10 2 1 609.39 562.96 38.71 o -9 2 1 2411.89 2670.58 68.57 o -8 2 1 128.34 145.15 25.81 o -7 2 1 123.50 92.13 21.12 o -6 2 1 1.75 4.01 10.76 o -5 2 1 84.28 93.21 15.74 o -4 2 1 1853.17 1723.15 39.72 o -3 2 1 122.14 117.99 11.02 o -2 2 1 291.54 294.09 13.06 o -1 2 1 680.53 640.04 17.60 o 0 2 1 13.53 18.46 5.47 o 1 2 1 11743.72 12000.08 172.00 o 2 2 1 0.02 -0.79 6.14 o 3 2 1 2875.18 2563.31 49.01 o 4 2 1 13.75 13.38 7.00 o 5 2 1 599.76 585.23 22.78 o 6 2 1 1903.25 1932.45 42.74 o 7 2 1 1080.40 1111.45 39.64 o 8 2 1 3048.55 3251.68 76.49 o 9 2 1 1637.84 1677.71 55.86 o 10 2 1 156.54 143.57 24.79 o 11 2 1 536.57 553.86 42.54 o 12 2 1 15.11 23.02 18.40 o 13 2 1 439.23 439.05 54.35 o 14 2 1 85.13 73.82 31.35 o 15 2 1 73.22 90.14 31.22 o 16 2 1 92.00 91.44 36.00 o 17 2 1 3.50 1.37 26.30 o 18 2 1 26.00 25.23 37.98 o 19 2 1 23.19 38.35 44.14 o 20 2 1 1.66 -24.70 41.25 o 21 2 1 0.04 17.23 57.60 o 22 2 1 18.78 90.44 64.60 o -22 3 1 0.08 12.09 43.55 o -21 3 1 1.35 40.37 47.04 o -20 3 1 65.06 71.38 50.18 o -19 3 1 131.29 147.80 56.91 o -18 3 1 239.56 264.67 70.23 o -17 3 1 66.81 97.26 49.36 o -16 3 1 34.67 39.86 39.30 o -15 3 1 311.24 249.85 62.41 o -14 3 1 3.41 10.48 23.74 o -13 3 1 137.51 141.35 35.61 o -12 3 1 1.68 -0.07 15.97 o -11 3 1 64.67 80.77 22.39 o -10 3 1 3171.66 3265.65 99.30 o -9 3 1 176.91 174.09 29.40 o -8 3 1 5280.96 5496.93 103.56 o -7 3 1 249.47 246.98 25.49 o -6 3 1 8217.26 8585.85 121.49 o -5 3 1 489.11 505.78 25.83 o -4 3 1 398.57 395.29 18.63 o -3 3 1 987.23 964.92 23.89 o -2 3 1 10730.42 10753.13 81.17 o -1 3 1 187258.78 187080.38 2284.74 o 0 3 1 40752.85 41799.87 615.60 o 1 3 1 147662.33 153668.09 1619.75 o 2 3 1 8882.10 8924.72 134.11 o 3 3 1 6185.04 6547.27 137.54 o 4 3 1 1980.01 1783.64 39.78 o 5 3 1 2159.71 2281.40 54.57 o 6 3 1 53.82 66.87 11.11 o 7 3 1 4918.53 4768.81 77.76 o 8 3 1 536.26 519.55 28.49 o 9 3 1 372.66 435.96 29.82 o 10 3 1 49.17 40.40 16.92 o 11 3 1 376.46 346.46 44.52 o 12 3 1 124.20 166.09 35.16 o 13 3 1 234.94 325.62 49.09 o 14 3 1 28.98 62.21 39.67 o 15 3 1 1.36 23.07 34.41 o 16 3 1 0.86 42.89 37.84 o 17 3 1 53.76 87.73 47.58 o 18 3 1 8.88 -23.88 40.51 o 19 3 1 0.03 -5.41 38.26 o 20 3 1 145.89 172.72 60.17 o 21 3 1 0.41 -38.99 38.99 o 22 3 1 7.74 3.77 62.99 o -22 4 1 8.89 64.87 49.33 o -21 4 1 2.41 -13.69 43.60 o -20 4 1 4.72 -14.36 40.48 o -19 4 1 33.67 73.65 51.22 o -18 4 1 60.04 56.27 44.38 o -17 4 1 297.68 346.50 76.17 o -16 4 1 77.92 87.68 62.18 o -15 4 1 122.65 95.70 46.75 o -14 4 1 258.15 245.38 61.65 o -13 4 1 55.46 92.16 43.85 o -12 4 1 0.10 2.89 30.65 o -11 4 1 81.74 119.37 43.39 o -10 4 1 187.25 207.22 29.84 o -9 4 1 365.90 318.21 33.06 o -8 4 1 1176.15 1271.38 60.92 o -7 4 1 59.26 80.77 17.27 o -6 4 1 206.94 197.65 20.09 o -5 4 1 6.12 28.28 29.07 o -4 4 1 33.49 70.21 15.70 o -3 4 1 3633.13 3620.43 68.93 o -2 4 1 5299.64 5093.56 61.60 o -1 4 1 5365.40 5355.37 65.42 o 0 4 1 1170.30 1146.07 29.62 o 1 4 1 318.85 303.73 18.11 o 2 4 1 3721.26 3828.41 86.87 o 3 4 1 6.68 16.31 10.99 o 4 4 1 1836.59 1864.17 43.00 o 5 4 1 197.57 193.87 30.88 o 6 4 1 99.80 122.10 17.53 o 7 4 1 1.66 1.51 12.02 o 8 4 1 542.70 556.70 38.00 o 9 4 1 9.14 21.19 16.25 o 10 4 1 498.17 518.77 58.52 o 11 4 1 230.39 219.56 54.87 o 12 4 1 0.26 -2.29 33.36 o 13 4 1 208.22 253.88 58.99 o 14 4 1 54.88 69.50 41.93 o 15 4 1 76.02 115.71 48.83 o 16 4 1 62.16 113.91 51.91 o 17 4 1 21.50 -2.54 37.95 o 18 4 1 76.89 83.60 54.25 o 19 4 1 36.05 60.31 46.05 o 20 4 1 116.67 182.37 74.83 o 21 4 1 49.23 114.59 57.56 o -21 5 1 22.36 73.32 50.82 o -20 5 1 6.20 54.62 47.00 o -19 5 1 27.07 10.14 43.81 o -18 5 1 47.03 32.13 46.60 o -17 5 1 108.63 105.44 54.20 o -16 5 1 3.01 -2.41 36.11 o -15 5 1 170.54 162.36 56.03 o -14 5 1 0.71 -17.08 33.11 o -13 5 1 191.84 224.71 68.10 o -12 5 1 18.71 44.67 28.91 o -11 5 1 409.23 387.17 56.25 o -10 5 1 2.00 7.05 20.51 o -9 5 1 121.11 143.65 35.21 o -8 5 1 8.75 11.26 20.07 o -7 5 1 1060.71 1050.71 62.92 o -6 5 1 116.41 127.24 22.23 o -5 5 1 1729.45 1779.84 55.91 o -4 5 1 249.97 312.34 28.85 o -3 5 1 1321.19 1394.97 48.55 o -2 5 1 1386.73 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