#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2015406.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015406_Fobs loop_ _publ_author_name 'Cort\'es, Piedad' 'Atria, Ana Mar\'ia' 'Garland, Mar\'ia Teresa' 'Baggio, Ricardo' _publ_section_title ; Three oxo complexes with a tetranuclear [Cu~4~(\m~2~-Cl)~6~(\m~4~-O)] unit ; _journal_coeditor_code DN3008 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m311 _journal_page_last m314 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 106.249 _cell_angle_beta 102.401 _cell_angle_gamma 94.255 _cell_length_a 11.6380 _cell_length_b 16.2370 _cell_length_c 17.1390 _exptl_crystal_F_000 1704.00 _reflns_d_resolution_high 0.8398 _[local]_cod_data_source_file dn3008IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2 in space group P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 373.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1629.23 1870.78 35.63 o 2 0 0 16352.79 15663.34 105.45 o 3 0 0 221.56 353.94 65.14 o 4 0 0 23178.73 23444.17 123.70 o 5 0 0 15313.80 15690.44 165.95 o 6 0 0 5118.34 5133.00 92.96 o 7 0 0 6115.41 6344.23 217.78 o 8 0 0 1068.50 1168.47 131.67 o 9 0 0 547.26 728.09 159.84 o 10 0 0 920.12 1145.42 166.52 o 11 0 0 827.38 640.70 165.61 o 12 0 0 1060.03 1118.03 218.90 o 13 0 0 3.15 361.76 280.43 o -13 1 0 63.37 -50.47 242.79 o -12 1 0 21.86 142.48 188.28 o -11 1 0 445.95 657.66 163.50 o -10 1 0 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