#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:06:16 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180823 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/54/2015434.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015434_Fobs loop_ _publ_author_name 'Barnett, Sarah A.' 'Hulme, Ashley T.' 'Tocher, Derek A.' _publ_section_title ; 5-Fluorouracil and thymine form a crystalline solid solution ; _journal_coeditor_code GG3013 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o412 _journal_page_last o415 _journal_volume 62 _journal_year 2006 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 117.813 _cell_angle_gamma 90.000 _cell_length_a 19.3785 _cell_length_b 5.9918 _cell_length_c 20.0293 _exptl_crystal_F_000 1056.00 _reflns_d_resolution_high 0.7505 _cod_data_source_file gg3013Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' str0379 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 400.56 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2989.16 2858.93 32.77 o 4 0 0 332.49 322.41 5.13 o 6 0 0 1575.69 1541.58 19.33 o 8 0 0 4370.66 4248.86 50.08 o 10 0 0 3.46 12.56 1.88 o 12 0 0 2353.89 2298.78 88.59 o 14 0 0 18.69 33.83 5.40 o 16 0 0 357.40 351.35 12.11 o 18 0 0 31.17 35.99 10.87 o 20 0 0 30.64 35.83 5.76 o 22 0 0 2.25 15.56 8.89 o 1 1 0 4046.58 3688.99 36.62 o 3 1 0 903.81 967.45 8.69 o 5 1 0 12611.05 12945.51 102.71 o 7 1 0 71.04 60.41 2.37 o 9 1 0 315.71 324.18 4.50 o 11 1 0 3728.57 3880.46 37.30 o 13 1 0 341.11 356.05 8.16 o 15 1 0 69.14 80.25 4.74 o 17 1 0 181.81 171.87 7.00 o 19 1 0 78.62 75.92 8.00 o 21 1 0 0.14 5.99 3.84 o 0 2 0 7643.58 8388.49 94.89 o 2 2 0 813.89 710.19 7.98 o 4 2 0 138.35 159.68 3.20 o 6 2 0 3256.29 3659.91 30.82 o 8 2 0 924.18 832.13 8.83 o 10 2 0 511.39 511.46 7.70 o 12 2 0 0.86 5.86 1.83 o 14 2 0 4.68 4.24 2.02 o 16 2 0 78.89 77.32 5.73 o 18 2 0 7.88 7.06 3.14 o 20 2 0 163.34 164.76 8.75 o 1 3 0 520.72 588.68 6.72 o 3 3 0 1506.10 1484.55 15.66 o 5 3 0 2061.91 2224.88 22.38 o 7 3 0 441.88 475.72 7.16 o 9 3 0 148.93 139.09 6.16 o 11 3 0 53.54 58.93 3.90 o 13 3 0 0.20 3.80 2.26 o 15 3 0 115.14 119.85 5.84 o 17 3 0 12.39 14.64 3.65 o 19 3 0 13.90 27.21 4.84 o 0 4 0 8229.90 8441.05 97.69 o 2 4 0 1101.97 1192.27 14.24 o 4 4 0 534.48 533.68 14.76 o 6 4 0 7.67 12.05 1.80 o 8 4 0 1931.97 1984.26 25.08 o 10 4 0 572.89 599.50 11.40 o 12 4 0 94.59 89.52 5.13 o 14 4 0 11.10 13.69 3.18 o 16 4 0 1.04 5.36 2.92 o 18 4 0 12.94 12.15 4.21 o 1 5 0 1188.61 1125.20 16.16 o 3 5 0 796.52 789.06 12.75 o 5 5 0 2437.94 2283.84 24.80 o 7 5 0 744.43 669.63 12.24 o 9 5 0 96.96 81.75 4.97 o 11 5 0 202.05 211.92 7.31 o 13 5 0 703.27 712.64 14.25 o 15 5 0 31.36 44.01 4.73 o 17 5 0 16.94 10.79 4.50 o 0 6 0 3502.61 3493.39 57.55 o 2 6 0 1869.60 1858.06 24.84 o 4 6 0 10.84 13.81 2.72 o 6 6 0 61.31 51.25 5.01 o 8 6 0 323.93 302.78 10.13 o 10 6 0 92.24 94.58 5.97 o 12 6 0 153.33 173.33 7.64 o 14 6 0 4.93 16.41 4.47 o 1 7 0 602.67 613.17 13.20 o 3 7 0 264.01 289.91 10.22 o 5 7 0 308.65 335.79 12.76 o 7 7 0 2.06 3.88 3.42 o 9 7 0 73.56 75.90 9.17 o -23 1 1 72.90 55.57 10.48 o -21 1 1 83.95 91.15 6.96 o -19 1 1 190.70 188.08 8.20 o -17 1 1 0.00 3.89 2.14 o -15 1 1 496.07 468.22 9.47 o -13 1 1 2.41 11.07 1.69 o -11 1 1 1552.37 1519.84 16.73 o -9 1 1 14.41 13.42 1.15 o -7 1 1 996.70 1088.04 10.43 o -5 1 1 62827.30 61322.86 482.73 o -3 1 1 205.89 157.20 3.04 o -1 1 1 16586.55 16107.34 127.49 o 1 1 1 1175.93 1128.91 18.97 o 3 1 1 1532.11 1486.14 12.91 o 5 1 1 4910.74 5238.65 47.11 o 7 1 1 8004.43 8007.58 71.51 o 9 1 1 104.00 86.01 3.23 o 11 1 1 148.45 122.65 4.20 o 13 1 1 892.00 877.39 13.67 o 15 1 1 14.40 17.13 2.57 o 17 1 1 97.50 91.63 5.29 o 19 1 1 49.99 56.62 5.57 o 21 1 1 153.29 184.26 9.72 o -22 2 1 16.43 19.29 5.81 o -20 2 1 36.60 39.43 5.04 o -18 2 1 184.42 171.81 8.06 o -16 2 1 0.48 15.95 3.28 o -14 2 1 19.49 18.23 2.63 o -12 2 1 1780.84 1757.89 25.49 o -10 2 1 6561.00 7079.95 64.70 o -8 2 1 912.32 855.13 9.03 o -6 2 1 244.51 216.34 3.98 o -4 2 1 6283.12 6366.99 56.68 o -2 2 1 1156.93 1301.50 13.08 o 0 2 1 141.89 199.79 2.88 o 2 2 1 234.93 220.98 3.49 o 4 2 1 178.59 197.02 5.93 o 6 2 1 8587.42 9453.97 76.12 o 8 2 1 413.16 420.81 6.47 o 10 2 1 1242.16 1177.59 18.13 o 12 2 1 178.44 171.78 5.41 o 14 2 1 2742.74 2602.79 31.60 o 16 2 1 437.05 410.64 11.66 o 18 2 1 96.07 105.84 6.99 o 20 2 1 371.10 340.68 29.13 o -21 3 1 124.84 110.50 14.13 o -19 3 1 266.76 276.20 10.32 o -17 3 1 106.37 106.30 10.65 o -15 3 1 361.75 351.13 9.02 o -13 3 1 68.83 78.19 4.58 o -11 3 1 218.23 199.36 6.02 o -9 3 1 38.29 57.58 3.41 o -7 3 1 9.72 26.77 2.03 o -5 3 1 1160.90 1204.50 13.47 o -3 3 1 495.04 631.88 8.51 o -1 3 1 2930.31 3016.48 25.93 o 1 3 1 1278.92 1374.50 13.07 o 3 3 1 1162.23 1117.86 13.15 o 5 3 1 13178.29 14321.71 125.64 o 7 3 1 1350.31 1295.50 14.62 o 9 3 1 142.39 146.19 5.05 o 11 3 1 0.37 4.75 2.25 o 13 3 1 249.95 256.03 7.38 o 15 3 1 542.73 471.90 15.19 o 17 3 1 32.31 44.43 5.17 o 19 3 1 20.88 31.52 5.02 o -18 4 1 4.34 9.17 5.62 o -16 4 1 14.46 16.37 3.52 o -14 4 1 0.17 1.08 2.60 o -12 4 1 24.83 16.55 2.98 o -10 4 1 224.19 177.61 6.05 o -8 4 1 50.08 57.67 3.76 o -6 4 1 285.37 236.66 6.50 o -4 4 1 3774.37 3539.27 58.99 o -2 4 1 190.15 194.31 5.03 o 0 4 1 1524.29 1502.56 16.41 o 2 4 1 1518.26 1592.77 17.41 o 4 4 1 37.94 31.69 3.21 o 6 4 1 722.96 685.14 13.86 o 8 4 1 1082.36 1005.55 15.35 o 10 4 1 1049.84 991.47 15.78 o 12 4 1 112.58 124.75 5.85 o 14 4 1 87.99 86.92 5.52 o 16 4 1 23.31 32.89 6.06 o 18 4 1 17.68 13.06 4.76 o -17 5 1 0.80 1.35 3.27 o -15 5 1 233.76 237.85 8.34 o -13 5 1 1.64 7.63 3.09 o -11 5 1 154.00 122.39 7.74 o -9 5 1 189.00 163.30 6.22 o -7 5 1 1159.72 1168.05 17.39 o -5 5 1 293.38 280.12 9.68 o -3 5 1 1597.18 1579.07 20.71 o -1 5 1 1355.51 1352.41 18.38 o 1 5 1 30.78 36.88 3.15 o 3 5 1 19.38 22.44 2.73 o 5 5 1 1371.42 1258.45 18.06 o 7 5 1 25.03 36.52 3.60 o 9 5 1 14.21 11.80 2.92 o 11 5 1 4.19 7.40 3.07 o 13 5 1 3.11 4.94 3.04 o 15 5 1 0.34 4.64 3.10 o 17 5 1 5.38 14.29 7.46 o -14 6 1 0.08 -2.79 4.81 o -12 6 1 6.03 8.40 3.26 o -10 6 1 84.09 93.67 5.84 o -8 6 1 17.75 30.22 4.23 o -6 6 1 0.08 2.67 2.72 o -4 6 1 469.48 439.84 9.85 o -2 6 1 363.16 337.43 8.48 o 0 6 1 236.90 227.31 7.02 o 2 6 1 1.45 9.56 2.56 o 4 6 1 99.55 82.36 5.99 o 6 6 1 89.59 70.66 5.77 o 8 6 1 309.13 330.38 10.81 o 10 6 1 27.33 38.36 4.37 o 12 6 1 3.71 1.98 3.13 o 14 6 1 10.12 7.95 5.06 o -11 7 1 0.42 0.64 6.67 o -9 7 1 34.70 48.67 5.82 o -7 7 1 15.56 20.45 4.20 o -5 7 1 22.90 33.86 5.08 o -3 7 1 1116.67 1139.84 18.79 o -1 7 1 146.64 156.24 7.22 o 1 7 1 39.45 45.07 4.34 o 3 7 1 52.86 78.43 6.35 o 5 7 1 14.19 21.01 4.28 o 7 7 1 211.69 248.64 12.75 o 9 7 1 36.19 32.57 6.24 o -22 0 2 212.96 222.42 16.67 o -20 0 2 138.90 137.21 9.04 o -18 0 2 255.98 249.17 18.97 o -16 0 2 3744.29 3661.69 59.59 o -14 0 2 219.32 244.77 16.35 o -12 0 2 3505.22 3494.12 51.87 o -10 0 2 1666.22 1678.73 22.26 o -8 0 2 334.59 398.15 7.06 o -6 0 2 39444.10 39014.37 433.04 o -4 0 2 1686.90 1637.38 19.64 o -2 0 2 2357.52 2298.85 26.75 o 0 0 2 6383.76 6229.81 86.58 o 2 0 2 29410.82 28380.47 317.83 o 4 0 2 23.01 38.50 2.11 o 6 0 2 3497.20 3579.54 50.76 o 8 0 2 841.44 777.44 11.72 o 10 0 2 48.10 31.78 2.25 o 12 0 2 299.05 251.60 10.95 o 14 0 2 117.19 106.99 6.94 o 16 0 2 4.28 9.35 4.52 o 18 0 2 4.99 13.44 4.23 o 20 0 2 992.82 940.77 24.59 o -23 1 2 53.49 64.49 7.91 o -21 1 2 44.11 40.32 5.08 o -19 1 2 2.15 4.66 2.93 o -17 1 2 443.79 437.51 9.57 o -15 1 2 1349.13 1386.85 19.20 o -13 1 2 184.79 171.66 4.35 o -11 1 2 2024.09 2000.31 18.57 o -9 1 2 182.12 184.67 3.35 o -7 1 2 2064.65 1895.02 16.79 o -5 1 2 160448.69 156650.83 1229.81 o -3 1 2 98.71 112.51 2.69 o -1 1 2 5693.72 5767.95 50.38 o 1 1 2 454.81 375.49 4.59 o 3 1 2 15736.45 15367.32 133.74 o 5 1 2 2354.01 2384.30 36.64 o 7 1 2 1314.85 1328.69 14.30 o 9 1 2 1837.64 1807.24 19.05 o 11 1 2 1476.98 1433.17 16.40 o 13 1 2 1160.58 1069.14 15.92 o 15 1 2 6.22 5.69 2.38 o 17 1 2 109.36 114.65 7.10 o 19 1 2 1294.17 1297.11 24.74 o 21 1 2 24.23 31.75 8.41 o -22 2 2 50.88 47.59 6.90 o -20 2 2 73.51 66.84 5.95 o -18 2 2 13.23 18.54 3.68 o -16 2 2 235.40 254.21 8.23 o -14 2 2 83.81 70.87 4.07 o -12 2 2 135.93 121.85 4.95 o -10 2 2 9907.42 10142.91 82.24 o -8 2 2 25.65 14.41 1.20 o -6 2 2 164.30 155.96 4.64 o -4 2 2 3312.54 3261.17 30.15 o -2 2 2 2520.83 2652.39 22.38 o 0 2 2 39.26 57.12 2.28 o 2 2 2 1837.80 1828.07 16.07 o 4 2 2 2195.06 2128.08 28.16 o 6 2 2 3534.89 3524.19 35.59 o 8 2 2 498.44 538.78 7.75 o 10 2 2 23.42 35.20 2.79 o 12 2 2 154.09 161.36 5.37 o 14 2 2 117.18 119.62 6.57 o 16 2 2 275.54 290.10 9.92 o 18 2 2 7.66 19.12 4.06 o 20 2 2 121.66 125.91 8.52 o -21 3 2 16.17 17.96 5.35 o -19 3 2 0.00 -6.36 5.28 o -17 3 2 165.14 160.16 6.63 o -15 3 2 493.33 496.32 10.56 o -13 3 2 43.22 42.16 3.62 o -11 3 2 44.53 46.24 3.47 o -9 3 2 519.67 461.05 7.27 o -7 3 2 7.11 7.62 1.34 o -5 3 2 1952.21 2092.60 21.20 o -3 3 2 828.39 978.52 11.22 o -1 3 2 35.31 30.83 1.51 o 1 3 2 2280.37 2727.54 23.75 o 3 3 2 5407.00 5325.90 44.21 o 5 3 2 49.50 52.82 1.95 o 7 3 2 93.05 109.31 4.18 o 9 3 2 274.38 257.33 6.65 o 11 3 2 111.51 123.27 5.98 o 13 3 2 6.74 16.08 2.93 o 15 3 2 0.07 7.61 3.51 o 17 3 2 12.08 14.31 3.85 o 19 3 2 21.68 11.75 5.72 o -20 4 2 0.01 18.57 8.41 o -18 4 2 123.99 129.30 6.85 o -16 4 2 36.49 49.09 4.51 o -14 4 2 168.85 177.32 6.77 o -12 4 2 56.57 50.22 4.45 o -10 4 2 1768.37 1699.79 22.56 o -8 4 2 2830.16 2678.65 27.67 o -6 4 2 64.81 63.76 3.01 o -4 4 2 515.79 428.35 11.63 o -2 4 2 501.90 440.14 11.23 o 0 4 2 2458.11 2517.37 26.31 o 2 4 2 105.92 79.22 4.81 o 4 4 2 68.62 66.14 2.96 o 6 4 2 22.28 30.81 2.94 o 8 4 2 256.01 255.09 7.00 o 10 4 2 776.12 711.42 14.71 o 12 4 2 300.51 316.27 8.64 o 14 4 2 209.12 229.35 8.06 o 16 4 2 33.06 53.98 6.81 o 18 4 2 45.42 53.82 11.27 o -17 5 2 96.10 127.13 7.12 o -15 5 2 61.72 50.73 4.88 o -13 5 2 760.22 731.01 14.26 o -11 5 2 4.70 10.93 2.97 o -9 5 2 44.21 46.57 4.05 o -7 5 2 918.32 841.34 13.90 o -5 5 2 3411.89 3479.44 35.11 o -3 5 2 121.94 96.69 4.44 o -1 5 2 158.93 165.43 6.55 o 1 5 2 58.01 69.17 3.90 o 3 5 2 345.05 362.36 8.02 o 5 5 2 203.94 211.21 6.42 o 7 5 2 48.59 46.20 4.04 o 9 5 2 91.38 88.23 5.27 o 11 5 2 48.93 51.19 4.68 o 13 5 2 16.60 11.54 3.29 o 15 5 2 89.07 99.77 6.55 o -14 6 2 58.73 63.57 5.39 o -12 6 2 198.35 237.85 8.29 o -10 6 2 309.83 319.50 9.11 o -8 6 2 84.71 76.44 8.36 o -6 6 2 435.26 439.27 11.73 o -4 6 2 2169.44 2153.67 27.84 o -2 6 2 1892.30 1898.84 25.18 o 0 6 2 2357.17 2351.38 29.61 o 2 6 2 0.08 -2.79 2.00 o 4 6 2 36.49 45.13 4.76 o 6 6 2 239.31 251.80 9.22 o 8 6 2 240.65 246.89 11.64 o 10 6 2 107.79 120.97 6.64 o 12 6 2 18.76 38.82 4.51 o 14 6 2 1.25 5.40 7.46 o -11 7 2 8.02 23.81 7.78 o -9 7 2 30.57 36.43 5.09 o -7 7 2 140.55 162.74 8.61 o -5 7 2 567.37 571.38 14.60 o -3 7 2 116.28 132.20 6.48 o -1 7 2 17.51 22.60 4.07 o 1 7 2 143.87 152.72 8.15 o 3 7 2 238.65 238.69 9.35 o 5 7 2 135.08 145.92 8.33 o 7 7 2 0.89 9.21 3.72 o 9 7 2 1.93 9.21 5.05 o -23 1 3 1.11 10.86 4.16 o -21 1 3 34.06 43.70 5.23 o -19 1 3 2.10 8.30 6.91 o -17 1 3 9.20 12.75 2.41 o -15 1 3 1099.99 1064.55 19.92 o -13 1 3 20.49 33.66 2.37 o -11 1 3 476.22 510.94 6.59 o -9 1 3 211.85 168.58 3.23 o -7 1 3 1019.91 1121.78 14.10 o -5 1 3 24532.00 24877.26 213.83 o -3 1 3 12911.25 12801.13 101.19 o -1 1 3 51.21 75.87 1.59 o 1 1 3 2783.06 2826.66 23.34 o 3 1 3 564.51 607.22 7.08 o 5 1 3 0.27 9.08 1.23 o 7 1 3 15.02 27.20 1.80 o 9 1 3 2765.26 2704.20 27.10 o 11 1 3 179.03 174.04 4.47 o 13 1 3 2.01 8.90 2.06 o 15 1 3 75.55 73.75 4.58 o 17 1 3 312.15 314.22 10.47 o 19 1 3 941.09 963.46 20.75 o 21 1 3 3.60 5.24 6.19 o -22 2 3 3.39 1.65 3.23 o -20 2 3 26.78 21.41 3.94 o -18 2 3 28.26 27.98 4.65 o -16 2 3 88.44 87.23 4.61 o -14 2 3 167.97 159.84 5.30 o -12 2 3 164.26 173.78 7.10 o -10 2 3 35794.57 37269.82 293.39 o -8 2 3 1117.60 1314.45 13.23 o -6 2 3 1654.98 1721.69 17.37 o -4 2 3 56.40 59.55 2.14 o -2 2 3 18296.83 18921.67 162.97 o 0 2 3 9588.03 9958.72 79.48 o 2 2 3 13588.60 14082.57 122.89 o 6 2 3 883.70 864.94 10.47 o 8 2 3 596.85 703.85 10.68 o 10 2 3 469.50 485.66 7.90 o 12 2 3 5.98 6.28 1.98 o 14 2 3 818.45 802.18 16.71 o 16 2 3 468.94 461.14 12.74 o 18 2 3 349.20 348.35 14.14 o -21 3 3 34.34 43.79 5.54 o -19 3 3 28.50 26.65 4.27 o -17 3 3 0.20 -0.89 2.23 o -15 3 3 763.03 780.32 13.72 o -13 3 3 532.20 524.47 10.72 o -11 3 3 223.06 243.14 6.40 o -9 3 3 4028.26 3740.35 67.54 o -7 3 3 1469.44 1615.63 17.40 o -5 3 3 3896.65 4050.06 37.96 o -3 3 3 1985.66 2035.13 18.31 o -1 3 3 455.82 474.53 5.89 o 1 3 3 6702.56 7270.21 59.34 o 3 3 3 10455.71 10783.31 86.84 o 5 3 3 1465.74 1357.38 13.41 o 7 3 3 16.40 10.23 2.00 o 9 3 3 1197.65 1172.43 16.82 o 11 3 3 30.70 41.17 4.74 o 13 3 3 7.84 10.62 2.81 o 15 3 3 959.12 868.24 18.73 o 17 3 3 919.65 901.44 19.98 o -20 4 3 103.31 141.29 14.92 o -18 4 3 337.25 305.49 9.25 o -16 4 3 27.94 21.25 3.60 o -14 4 3 83.51 81.31 7.48 o -12 4 3 409.08 391.58 11.82 o -10 4 3 2045.81 2043.77 25.92 o -8 4 3 683.15 605.30 9.64 o -6 4 3 628.20 633.48 9.24 o -4 4 3 229.34 254.99 5.24 o -2 4 3 0.07 2.79 1.34 o 0 4 3 1234.61 1225.02 21.53 o 2 4 3 1084.71 1070.23 12.95 o 4 4 3 206.54 174.62 4.49 o 6 4 3 39.81 40.71 3.37 o 8 4 3 371.89 380.81 8.76 o 10 4 3 1.35 1.81 2.30 o 12 4 3 317.10 299.63 8.58 o 14 4 3 44.51 50.29 4.70 o 16 4 3 72.25 70.87 6.63 o -17 5 3 8.13 16.89 3.68 o -15 5 3 0.01 5.02 2.92 o -13 5 3 267.92 280.42 8.42 o -11 5 3 48.86 56.14 4.50 o -9 5 3 2454.64 2263.21 28.74 o -7 5 3 1967.15 1826.60 21.01 o -5 5 3 1654.04 1629.52 18.97 o -3 5 3 0.40 6.65 2.18 o -1 5 3 13.59 10.32 2.21 o 1 5 3 703.81 703.49 11.78 o 3 5 3 40.25 35.99 3.13 o 5 5 3 376.48 348.02 8.42 o 7 5 3 429.36 407.22 9.55 o 9 5 3 109.64 117.13 5.95 o 11 5 3 5.90 14.90 3.45 o 13 5 3 4.00 2.21 2.80 o 15 5 3 150.48 175.11 8.13 o -14 6 3 30.11 38.36 4.40 o -12 6 3 165.18 197.04 7.69 o -10 6 3 10.51 12.54 3.04 o -8 6 3 10.91 5.49 2.87 o -6 6 3 374.81 362.10 12.90 o -4 6 3 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