#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2015550.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015550_Fobs loop_ _publ_author_name 'Ebihara, Masahiro' 'Yamada, Kaori' 'Kawamura, Takashi' _publ_section_title ; Paddlewheel dirhodium complexes bridged by para-substituted benzoates ; _journal_coeditor_code FG3029 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m451 _journal_page_last m454 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 98.641 _cell_angle_beta 90.781 _cell_angle_gamma 99.424 _cell_length_a 10.0490 _cell_length_b 12.7520 _cell_length_c 13.4790 _exptl_crystal_F_000 718.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file fg3029Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' _yamada02' _shelx_refln_list_code 4 _shelx_f_calc_maximum 177.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12.40 47.68 12.07 o 3 0 0 12.01 21.95 13.25 o 4 0 0 0.22 55.79 23.25 o 5 0 0 137.74 164.78 27.36 o 6 0 0 462.63 448.16 53.09 o 7 0 0 907.29 889.28 73.90 o 8 0 0 966.43 964.93 80.01 o 9 0 0 685.53 629.56 84.62 o 10 0 0 367.71 351.60 67.68 o 11 0 0 458.49 569.02 118.21 o 12 0 0 328.43 277.27 75.10 o -12 1 0 5.31 81.55 74.71 o -11 1 0 347.39 336.60 86.27 o -10 1 0 1093.78 963.69 100.35 o -9 1 0 1.45 47.70 49.82 o -8 1 0 2264.63 2231.69 117.64 o -7 1 0 2466.15 2399.11 98.95 o -6 1 0 2257.69 2036.85 82.13 o -5 1 0 1.04 110.52 38.74 o -4 1 0 0.71 27.00 16.35 o -3 1 0 170.06 152.71 16.93 o -2 1 0 7005.45 6709.21 113.30 o 2 1 0 5935.42 6307.02 106.87 o 3 1 0 415.19 420.75 25.57 o 4 1 0 2662.90 2466.79 50.70 o 5 1 0 880.27 934.47 53.78 o 6 1 0 402.05 515.58 57.93 o 7 1 0 609.41 630.20 67.73 o 8 1 0 395.40 417.05 61.05 o 9 1 0 915.22 802.05 88.56 o 10 1 0 650.19 554.83 73.05 o 11 1 0 702.13 770.27 112.07 o 12 1 0 347.28 358.43 91.81 o -13 2 0 79.97 37.93 63.06 o -12 2 0 21.48 6.23 99.58 o -11 2 0 0.22 5.64 84.80 o -10 2 0 44.40 111.15 53.24 o -9 2 0 234.50 222.42 70.43 o -8 2 0 1376.14 1445.16 109.11 o -7 2 0 2494.29 2741.33 112.18 o -6 2 0 5025.04 4989.50 139.15 o -5 2 0 3817.56 3679.43 90.32 o -4 2 0 1092.97 1013.60 61.52 o -3 2 0 46.52 97.27 17.28 o -2 2 0 156.15 211.44 17.13 o 0 2 0 879.27 887.65 59.36 o 1 2 0 184.88 195.39 6.13 o 2 2 0 54.65 71.40 13.81 o 3 2 0 8226.95 7840.90 90.73 o 4 2 0 7823.15 7991.13 201.28 o 5 2 0 570.95 564.84 48.05 o 6 2 0 255.96 292.19 46.04 o 7 2 0 119.99 117.02 38.90 o 8 2 0 41.98 60.44 36.50 o 9 2 0 137.11 124.75 62.27 o 10 2 0 111.74 97.56 57.91 o 11 2 0 258.21 421.33 107.91 o 12 2 0 206.79 213.74 73.28 o -13 3 0 298.85 268.28 105.67 o -12 3 0 51.17 62.08 100.85 o -11 3 0 81.81 102.72 55.41 o -10 3 0 122.20 136.54 57.98 o -9 3 0 22.55 44.89 69.63 o -8 3 0 1104.25 1196.03 101.03 o -7 3 0 2493.33 2362.63 113.18 o -6 3 0 2382.44 2316.65 95.27 o -5 3 0 817.22 672.40 47.14 o -4 3 0 2228.02 2140.67 67.84 o -3 3 0 8500.36 8364.21 61.54 o -1 3 0 2415.50 2295.74 33.73 o 0 3 0 57.89 68.22 13.86 o 1 3 0 134.24 126.89 6.90 o 2 3 0 103.57 115.32 13.91 o 3 3 0 409.91 347.45 24.66 o 4 3 0 6653.64 6648.99 107.38 o 5 3 0 2016.99 2003.81 79.90 o 6 3 0 984.97 1071.46 78.18 o 7 3 0 419.10 419.13 64.04 o 8 3 0 72.27 97.99 46.79 o 9 3 0 31.81 26.79 64.80 o 10 3 0 61.83 25.68 75.36 o 11 3 0 93.08 60.00 53.47 o 12 3 0 34.31 42.24 91.37 o -13 4 0 313.67 241.61 91.14 o -12 4 0 359.79 305.17 87.49 o -11 4 0 298.91 266.27 83.60 o -10 4 0 82.02 55.54 54.65 o -9 4 0 18.12 -8.79 75.12 o -8 4 0 14.78 33.95 67.79 o -7 4 0 525.95 531.03 56.01 o -6 4 0 1213.47 1059.90 69.08 o -5 4 0 2244.89 2098.14 88.58 o -4 4 0 4958.31 5038.48 60.26 o -3 4 0 4808.54 4895.17 82.92 o -2 4 0 11348.36 11097.80 201.40 o -1 4 0 4142.69 3978.80 152.52 o 0 4 0 1383.60 1338.94 24.42 o 1 4 0 1092.56 1064.11 15.15 o 2 4 0 42.53 71.70 8.71 o 3 4 0 4374.55 4442.56 40.52 o 4 4 0 1381.64 1329.29 36.67 o 5 4 0 1015.78 1000.16 63.21 o 6 4 0 580.52 501.68 57.59 o 7 4 0 1362.79 1219.10 85.03 o 8 4 0 290.77 398.10 73.88 o 9 4 0 280.64 387.22 90.14 o 10 4 0 43.96 53.74 80.54 o 11 4 0 5.39 88.54 78.34 o -12 5 0 336.16 582.33 116.08 o -11 5 0 122.08 103.43 60.04 o -10 5 0 583.01 549.68 78.76 o -9 5 0 167.14 214.29 60.99 o -8 5 0 465.60 342.23 58.56 o -7 5 0 2.28 24.68 58.80 o -6 5 0 136.99 114.68 39.39 o -5 5 0 1869.45 1898.80 86.81 o -4 5 0 3611.98 3549.23 77.58 o -3 5 0 6925.80 7003.30 119.53 o -2 5 0 11825.69 12184.49 116.94 o -1 5 0 6575.29 6507.36 96.78 o 0 5 0 3489.18 3423.95 50.79 o 1 5 0 195.67 193.15 14.86 o 2 5 0 10.54 45.41 12.70 o 3 5 0 11.29 30.24 12.24 o 4 5 0 84.77 127.60 25.52 o 5 5 0 173.62 137.92 16.57 o 6 5 0 117.30 51.21 31.59 o 7 5 0 1130.27 1250.03 98.02 o 8 5 0 838.27 756.90 84.67 o 9 5 0 1136.62 1102.98 114.15 o 10 5 0 213.98 201.68 75.00 o 11 5 0 86.71 127.82 64.00 o -12 6 0 206.22 338.57 107.55 o -11 6 0 204.80 297.71 93.98 o -10 6 0 614.63 716.29 113.49 o -9 6 0 529.41 601.85 94.90 o -8 6 0 764.35 925.64 93.03 o -7 6 0 95.51 79.24 40.10 o -6 6 0 6.49 89.66 55.84 o -5 6 0 43.81 45.37 7.64 o -4 6 0 1415.72 1431.54 50.94 o -3 6 0 3378.98 3328.88 89.45 o -2 6 0 3682.45 3343.01 84.78 o -1 6 0 5640.48 5370.61 99.47 o 0 6 0 131.95 123.44 31.14 o 1 6 0 2854.12 2878.91 66.07 o 2 6 0 1431.59 1455.32 30.51 o 3 6 0 402.00 399.99 18.91 o 4 6 0 4.61 9.77 14.91 o 5 6 0 43.07 34.56 11.52 o 6 6 0 235.36 268.95 31.76 o 7 6 0 239.09 239.41 32.25 o 8 6 0 708.56 559.06 118.68 o 9 6 0 619.15 767.83 97.57 o 10 6 0 421.37 304.75 75.25 o 11 6 0 193.19 105.10 97.98 o -12 7 0 20.30 114.36 101.10 o -11 7 0 115.30 122.14 73.18 o -10 7 0 364.27 457.93 96.79 o -9 7 0 1524.07 1505.34 121.36 o -8 7 0 627.48 757.19 83.44 o -7 7 0 476.25 511.14 66.86 o -6 7 0 802.32 695.84 58.88 o -5 7 0 729.12 758.90 42.50 o -4 7 0 508.37 487.41 26.49 o -3 7 0 413.73 407.26 41.89 o -2 7 0 887.53 890.40 58.11 o -1 7 0 2234.03 2285.41 81.79 o 0 7 0 1222.17 1119.09 37.78 o 1 7 0 3320.36 3417.19 50.28 o 2 7 0 4004.73 3965.69 64.79 o 3 7 0 1185.69 1236.37 54.67 o 4 7 0 1060.24 1091.35 31.35 o 5 7 0 42.55 50.92 16.07 o 6 7 0 101.49 86.72 23.86 o 7 7 0 33.72 54.87 38.25 o 8 7 0 508.98 531.40 77.10 o 9 7 0 176.38 274.66 85.20 o 10 7 0 227.14 185.86 76.58 o -12 8 0 59.36 13.53 67.98 o -11 8 0 20.32 103.17 78.29 o -10 8 0 183.68 132.14 64.95 o -9 8 0 1377.95 1566.45 121.51 o -8 8 0 1302.97 1587.35 134.62 o -7 8 0 312.38 507.24 78.89 o -6 8 0 923.26 904.15 22.86 o -5 8 0 1367.34 1244.26 64.71 o -4 8 0 3238.26 3083.69 62.14 o -3 8 0 89.86 126.99 40.55 o -2 8 0 16.04 68.57 44.65 o -1 8 0 43.92 55.81 24.85 o 0 8 0 952.93 1047.94 31.09 o 1 8 0 2426.39 2392.07 41.94 o 2 8 0 2567.64 2545.29 61.05 o 3 8 0 1264.44 1194.42 72.28 o 4 8 0 415.14 423.67 31.57 o 5 8 0 500.51 536.95 39.46 o 6 8 0 152.55 126.86 26.44 o 7 8 0 39.15 34.95 66.41 o 8 8 0 35.10 78.20 73.48 o 9 8 0 168.15 235.95 86.96 o 10 8 0 198.33 196.84 84.43 o -11 9 0 105.85 57.47 85.74 o -10 9 0 35.00 90.90 87.15 o -9 9 0 79.29 76.71 48.81 o -8 9 0 160.55 263.02 76.82 o -7 9 0 1871.16 1975.05 128.03 o -6 9 0 3952.17 3979.00 121.46 o -5 9 0 4812.10 4589.00 68.92 o -4 9 0 2141.25 2027.50 99.63 o -3 9 0 888.70 740.15 57.97 o -2 9 0 15.31 78.27 46.79 o -1 9 0 80.39 144.47 35.62 o 0 9 0 173.49 183.68 25.44 o 1 9 0 1210.80 1217.03 35.92 o 2 9 0 1973.33 2085.78 83.94 o 3 9 0 2037.73 2058.33 94.90 o 4 9 0 2.55 95.76 69.53 o 5 9 0 690.16 675.63 41.40 o 6 9 0 387.16 373.14 76.14 o 7 9 0 97.70 85.96 49.10 o 8 9 0 24.52 0.01 80.33 o 9 9 0 3.15 -1.52 81.93 o -11 10 0 95.22 96.33 92.42 o -10 10 0 16.76 111.93 87.55 o -9 10 0 0.63 26.23 82.86 o -8 10 0 80.75 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93.30 o 8 11 0 126.82 89.89 57.64 o -10 12 0 326.84 280.87 96.47 o -9 12 0 172.68 318.42 96.56 o -8 12 0 174.69 114.74 60.39 o -7 12 0 19.76 -11.09 79.74 o -6 12 0 53.40 102.30 72.01 o -5 12 0 74.85 45.22 26.56 o -4 12 0 17.22 93.33 71.10 o -3 12 0 50.08 152.99 54.19 o -2 12 0 621.31 598.02 74.89 o -1 12 0 1584.33 1537.92 66.42 o 0 12 0 531.49 500.90 45.42 o 1 12 0 292.47 331.03 58.16 o 2 12 0 268.72 236.62 58.83 o 3 12 0 25.26 18.46 65.30 o 4 12 0 0.34 64.62 68.93 o 5 12 0 15.63 60.72 74.33 o 6 12 0 140.29 229.91 80.85 o 7 12 0 218.46 260.08 86.88 o -9 13 0 469.22 535.05 125.73 o -8 13 0 392.70 284.33 80.13 o -7 13 0 133.86 75.08 55.72 o -6 13 0 210.02 267.01 89.54 o -5 13 0 127.57 92.29 35.78 o -4 13 0 7.08 84.81 74.50 o -3 13 0 24.37 6.45 68.36 o -2 13 0 198.04 170.99 35.22 o -1 13 0 804.17 780.20 57.48 o 0 13 0 684.80 701.54 69.35 o 1 13 0 597.04 716.52 87.83 o 2 13 0 286.01 224.99 63.75 o 3 13 0 208.03 217.89 65.15 o 4 13 0 3.01 33.47 49.57 o 5 13 0 2.05 12.99 79.55 o 6 13 0 18.10 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815.17 54.06 o 2 -13 1 170.66 257.78 86.42 o 3 -13 1 103.43 143.15 52.69 o 4 -13 1 0.46 -8.53 46.57 o 5 -13 1 59.71 126.45 77.75 o 6 -13 1 86.00 -16.44 76.13 o 7 -13 1 177.37 115.09 62.47 o 8 -13 1 304.67 288.91 94.09 o 9 -13 1 268.65 251.71 78.08 o -7 -12 1 405.86 422.58 103.68 o -6 -12 1 332.98 460.62 99.31 o -5 -12 1 127.29 141.39 62.16 o -4 -12 1 27.76 66.41 92.41 o -3 -12 1 102.21 86.71 43.74 o -2 -12 1 187.67 172.61 57.67 o -1 -12 1 340.90 379.54 36.82 o 0 -12 1 871.32 773.22 47.66 o 1 -12 1 1170.59 1323.81 63.99 o 2 -12 1 701.39 704.97 87.43 o 3 -12 1 230.54 215.38 54.17 o 4 -12 1 108.94 103.77 51.55 o 5 -12 1 44.93 132.68 50.67 o 6 -12 1 0.24 35.19 47.89 o 7 -12 1 46.63 2.95 77.75 o 8 -12 1 276.53 291.15 77.22 o 9 -12 1 154.72 170.23 69.16 o 10 -12 1 503.85 424.18 112.14 o -8 -11 1 249.05 164.35 68.72 o -7 -11 1 551.41 607.87 110.86 o -6 -11 1 652.87 814.52 105.48 o -5 -11 1 403.06 423.46 93.83 o -4 -11 1 151.78 183.94 68.25 o -3 -11 1 146.25 167.79 50.86 o -2 -11 1 67.56 73.69 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