#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/55/2015569.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015569_Fobs loop_ _publ_author_name 'Lu, Wen-Jie' 'Zhu, Yi-Min' 'Zhong, Kai-Long' _publ_section_title ; catena-Poly[[[triaquasulfatocobalt(II)]-\m-4,4'-bipyridine] ethane-1,2-diol solvate] ; _journal_coeditor_code HJ3018 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m448 _journal_page_last m450 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.671 _cell_angle_gamma 90.000 _cell_length_a 7.5232 _cell_length_b 11.7458 _cell_length_c 19.4745 _exptl_crystal_F_000 884.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file hj3018Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 250.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 62513.64 70333.70 1896.66 o 4 0 0 3724.63 4386.43 135.26 o 6 0 0 420.35 393.06 31.65 o 8 0 0 54.03 38.62 20.47 o 1 1 0 569.91 514.37 9.44 o 2 1 0 19673.75 21350.53 411.20 o 3 1 0 403.40 421.74 24.90 o 4 1 0 16358.17 17758.24 348.95 o 5 1 0 1968.58 2051.99 87.43 o 6 1 0 1142.39 1028.66 35.73 o 7 1 0 214.95 206.11 19.94 o 8 1 0 1150.16 1134.31 63.52 o 0 2 0 5114.20 5594.04 106.69 o 1 2 0 426.53 382.08 9.55 o 2 2 0 1945.77 2090.90 41.66 o 3 2 0 35.95 21.70 4.34 o 4 2 0 1618.21 1828.90 36.55 o 5 2 0 480.78 451.58 19.28 o 6 2 0 961.44 836.83 25.08 o 7 2 0 108.04 130.08 16.82 o 8 2 0 628.33 548.62 28.80 o 1 3 0 2.27 0.11 2.21 o 2 3 0 2049.30 2186.46 54.94 o 3 3 0 1185.63 1162.17 21.01 o 4 3 0 5501.33 5636.99 94.69 o 5 3 0 1564.15 1595.18 35.23 o 6 3 0 1253.31 1243.87 31.68 o 7 3 0 916.99 929.12 36.01 o 8 3 0 46.68 60.70 14.48 o 0 4 0 130.85 165.45 8.90 o 1 4 0 1628.10 1762.59 27.22 o 2 4 0 6830.60 7046.75 112.39 o 3 4 0 1629.44 1621.73 27.39 o 4 4 0 3677.17 3881.03 72.60 o 5 4 0 4362.87 4344.85 96.94 o 6 4 0 118.44 120.27 14.73 o 7 4 0 829.29 844.84 34.79 o 8 4 0 218.71 264.90 23.78 o 1 5 0 259.45 247.23 9.93 o 2 5 0 165.02 189.02 10.12 o 3 5 0 3556.18 3464.32 62.19 o 4 5 0 964.31 878.05 24.09 o 5 5 0 129.81 160.98 15.43 o 6 5 0 1457.06 1474.69 46.00 o 7 5 0 313.65 334.45 23.05 o 8 5 0 92.82 118.11 17.88 o 0 6 0 70.82 131.85 7.98 o 1 6 0 2.80 -2.81 4.10 o 2 6 0 97.81 143.48 10.46 o 3 6 0 668.23 565.72 18.81 o 4 6 0 1102.29 1057.79 24.73 o 5 6 0 889.31 901.70 26.75 o 6 6 0 8.06 6.53 13.33 o 7 6 0 258.06 287.77 43.29 o 1 7 0 3701.00 3453.17 47.31 o 2 7 0 165.41 155.82 9.19 o 3 7 0 183.93 221.46 13.75 o 4 7 0 10.61 49.78 17.54 o 5 7 0 290.54 301.71 17.31 o 6 7 0 308.11 425.30 26.29 o 7 7 0 169.07 203.07 27.05 o 0 8 0 279.84 321.15 30.40 o 1 8 0 1428.95 1389.17 23.03 o 2 8 0 229.92 244.62 14.70 o 3 8 0 2115.97 2017.95 44.50 o 4 8 0 4.72 1.44 8.27 o 5 8 0 121.67 129.47 17.15 o 6 8 0 12.92 -3.66 15.58 o 7 8 0 239.41 216.69 23.00 o 1 9 0 9362.81 8837.74 282.42 o 2 9 0 75.38 62.88 10.59 o 3 9 0 133.28 118.28 12.67 o 4 9 0 259.17 341.50 18.65 o 5 9 0 85.92 113.61 21.21 o 6 9 0 60.98 54.21 14.58 o 0 10 0 1274.83 1158.82 35.31 o 1 10 0 548.91 526.15 23.92 o 2 10 0 168.93 147.49 14.05 o 3 10 0 3532.39 3459.14 80.97 o 4 10 0 2.14 -3.19 9.37 o 5 10 0 1233.16 1177.75 35.85 o 6 10 0 1.87 -6.51 10.77 o 1 11 0 2431.26 2357.82 50.26 o 2 11 0 152.52 138.29 11.55 o 3 11 0 414.67 395.70 20.49 o 4 11 0 15.01 33.35 12.42 o 5 11 0 6.93 18.24 12.12 o 0 12 0 0.57 -9.28 15.55 o 1 12 0 12.67 1.44 13.03 o 2 12 0 130.42 152.48 14.18 o 3 12 0 513.40 499.05 20.24 o 4 12 0 843.12 800.46 25.43 o 1 13 0 5.19 21.07 14.69 o 2 13 0 116.70 86.24 18.28 o 3 13 0 160.48 181.16 16.88 o -7 0 1 2949.32 2797.79 105.86 o -5 0 1 17111.61 17251.40 485.07 o -3 0 1 107.66 51.70 10.27 o -1 0 1 28.56 57.33 5.49 o 1 0 1 132.47 83.63 7.03 o 3 0 1 1561.15 1586.53 54.65 o 5 0 1 3536.25 3427.76 113.25 o 7 0 1 5541.78 5283.83 173.88 o -8 1 1 29.47 28.69 14.15 o -7 1 1 470.94 448.79 25.14 o -6 1 1 314.03 285.74 20.56 o -5 1 1 1040.17 1097.96 35.24 o -4 1 1 848.54 848.83 44.38 o -3 1 1 13562.98 13982.67 346.88 o -2 1 1 8069.24 8858.44 228.18 o -1 1 1 17904.88 18348.97 241.48 o 0 1 1 43.24 -1.51 1.53 o 1 1 1 3358.50 3648.22 56.76 o 2 1 1 33830.41 37658.21 588.03 o 3 1 1 2289.57 2306.46 43.29 o 4 1 1 2743.24 3019.63 69.13 o 5 1 1 585.01 615.29 27.36 o 6 1 1 74.96 65.76 13.89 o 7 1 1 360.45 360.30 23.80 o 8 1 1 52.57 49.94 24.27 o -8 2 1 29.12 18.21 12.36 o -7 2 1 2560.59 2639.59 72.00 o -6 2 1 3275.39 3101.31 66.23 o -5 2 1 7035.12 7385.74 149.25 o -4 2 1 703.80 772.72 19.99 o -3 2 1 2551.73 2609.92 46.45 o -2 2 1 432.24 513.58 10.73 o -1 2 1 193.60 176.41 9.84 o 0 2 1 6570.22 7029.96 83.43 o 1 2 1 490.41 459.98 24.00 o 2 2 1 18.31 8.38 2.71 o 3 2 1 407.92 359.17 16.84 o 4 2 1 925.77 914.22 22.37 o 5 2 1 2022.91 2060.49 61.06 o 6 2 1 147.77 147.07 12.26 o 7 2 1 1295.38 1276.53 42.96 o 8 2 1 7.45 13.00 12.33 o -8 3 1 454.67 444.14 27.32 o -7 3 1 120.60 131.30 17.59 o -6 3 1 112.43 119.76 12.69 o -5 3 1 86.24 82.88 9.13 o -4 3 1 174.35 261.97 17.71 o -3 3 1 7836.99 7901.41 243.25 o -2 3 1 9563.07 9831.94 132.66 o -1 3 1 4555.25 4862.50 68.67 o 0 3 1 1522.51 1573.56 32.90 o 1 3 1 1746.01 1612.80 24.58 o 2 3 1 7193.89 6965.49 86.34 o 3 3 1 8910.13 9660.28 119.28 o 4 3 1 3779.56 3688.98 65.16 o 5 3 1 337.94 384.60 15.49 o 6 3 1 197.52 184.51 17.02 o 7 3 1 71.47 81.32 23.92 o 8 3 1 41.31 9.80 12.59 o -8 4 1 11.99 21.26 16.04 o -7 4 1 184.57 223.32 20.27 o -6 4 1 3.47 6.21 9.02 o -5 4 1 4.68 15.70 6.57 o -4 4 1 195.78 211.06 11.27 o -3 4 1 1773.61 1634.03 32.19 o -2 4 1 828.39 815.86 24.33 o -1 4 1 3105.74 3004.89 38.49 o 0 4 1 1170.19 1045.01 15.98 o 1 4 1 3292.74 3200.82 45.81 o 2 4 1 3744.33 3453.86 59.25 o 3 4 1 1267.39 1137.22 21.90 o 4 4 1 385.53 411.08 13.87 o 5 4 1 385.47 400.24 20.64 o 6 4 1 557.47 624.65 56.52 o 7 4 1 185.57 255.84 21.19 o 8 4 1 4.96 12.94 36.61 o -8 5 1 64.07 70.57 15.74 o -7 5 1 95.14 94.32 27.61 o -6 5 1 6.15 -8.90 23.46 o -5 5 1 108.94 127.35 13.74 o -4 5 1 242.28 337.45 23.80 o -3 5 1 115.96 110.61 9.26 o -2 5 1 10.35 -3.00 7.72 o -1 5 1 6.33 10.98 2.62 o 0 5 1 5184.75 5734.93 71.00 o 1 5 1 1135.42 1044.92 16.38 o 2 5 1 5311.11 5466.35 90.65 o 3 5 1 379.70 382.88 14.51 o 4 5 1 1681.61 1769.29 38.41 o 5 5 1 185.75 216.10 17.33 o 6 5 1 593.14 561.88 27.01 o 7 5 1 12.54 -2.57 11.50 o 8 5 1 19.65 12.17 13.07 o -8 6 1 6.86 0.37 14.53 o -7 6 1 48.10 33.48 14.08 o -6 6 1 27.38 21.03 11.25 o -5 6 1 375.85 380.50 17.19 o -4 6 1 104.28 120.90 21.62 o -3 6 1 239.41 224.81 14.89 o -2 6 1 4289.71 4012.87 70.51 o -1 6 1 7093.40 7135.98 87.86 o 0 6 1 576.43 488.07 17.52 o 1 6 1 218.03 226.38 6.91 o 2 6 1 2990.09 2779.99 51.97 o 3 6 1 2646.37 2494.99 49.19 o 4 6 1 288.20 269.84 14.43 o 5 6 1 32.76 34.68 11.14 o 6 6 1 58.50 78.25 13.91 o 7 6 1 6.28 0.43 12.05 o -7 7 1 112.67 113.78 18.75 o -6 7 1 3183.08 3022.45 77.77 o -5 7 1 224.42 293.40 15.02 o -4 7 1 1772.05 1803.46 41.19 o -3 7 1 680.11 736.27 22.78 o -2 7 1 650.74 629.80 20.15 o -1 7 1 9.13 -3.67 3.80 o 0 7 1 1492.59 1615.05 31.97 o 1 7 1 1265.74 1031.80 17.91 o 2 7 1 22.94 4.42 4.63 o 3 7 1 73.91 74.47 9.66 o 4 7 1 160.52 195.85 13.99 o 5 7 1 117.35 131.15 17.43 o 6 7 1 2109.98 2080.66 60.16 o 7 7 1 4.49 -9.49 11.79 o -7 8 1 46.18 56.71 16.07 o -6 8 1 257.30 210.47 38.12 o -5 8 1 1.66 5.44 8.50 o -4 8 1 734.69 741.90 21.72 o -3 8 1 28.33 9.73 7.91 o -2 8 1 1492.98 1470.85 34.96 o -1 8 1 24.59 43.05 6.91 o 0 8 1 491.58 500.77 11.08 o 1 8 1 78.08 56.80 6.80 o 2 8 1 1150.51 1117.62 32.36 o 3 8 1 264.53 254.76 19.58 o 4 8 1 817.66 820.52 26.34 o 5 8 1 156.92 155.27 15.59 o 6 8 1 46.04 35.58 14.55 o 7 8 1 18.11 22.27 23.67 o -6 9 1 2622.85 2559.57 58.69 o -5 9 1 146.92 117.54 17.81 o -4 9 1 1141.46 1074.33 31.53 o -3 9 1 76.76 71.44 11.13 o -2 9 1 10.32 3.91 6.26 o -1 9 1 418.38 457.87 29.84 o 0 9 1 251.97 274.70 9.05 o 1 9 1 162.99 219.93 15.18 o 2 9 1 280.35 307.71 16.99 o 3 9 1 27.47 33.89 9.45 o 4 9 1 368.43 413.02 19.62 o 5 9 1 114.36 91.66 13.28 o 6 9 1 1537.92 1458.24 50.73 o -6 10 1 45.05 45.27 13.03 o -5 10 1 104.70 117.26 19.58 o -4 10 1 899.08 904.34 29.74 o -3 10 1 153.67 153.18 28.34 o -2 10 1 1870.63 1878.65 36.90 o -1 10 1 1539.51 1482.29 34.39 o 0 10 1 526.11 486.83 18.53 o 1 10 1 248.26 270.12 13.13 o 2 10 1 460.11 476.40 20.60 o 3 10 1 221.09 211.21 16.16 o 4 10 1 798.60 797.94 28.05 o 5 10 1 7.37 17.12 11.13 o 6 10 1 0.10 3.61 10.90 o -5 11 1 26.40 8.17 11.07 o -4 11 1 908.11 917.19 26.15 o -3 11 1 0.00 -3.30 7.49 o -2 11 1 98.79 82.27 10.23 o -1 11 1 208.68 272.40 22.91 o 0 11 1 214.38 254.10 32.74 o 1 11 1 652.23 681.19 23.49 o 2 11 1 424.37 407.61 20.64 o 3 11 1 34.66 58.38 14.41 o 4 11 1 1113.04 1048.80 34.02 o 5 11 1 125.81 139.04 24.88 o -4 12 1 163.07 169.19 14.32 o -3 12 1 122.45 111.09 12.59 o -2 12 1 715.75 728.88 26.37 o -1 12 1 136.98 129.08 25.11 o 0 12 1 648.32 691.59 33.01 o 1 12 1 154.62 182.96 24.34 o 2 12 1 213.80 234.96 16.78 o 3 12 1 1023.03 978.95 33.01 o 4 12 1 244.00 240.48 22.91 o -3 13 1 13.01 17.72 11.77 o -2 13 1 721.08 744.79 36.86 o -1 13 1 583.14 602.57 32.94 o 0 13 1 66.70 99.67 18.87 o 1 13 1 710.35 748.81 36.33 o 2 13 1 391.09 459.74 30.21 o 3 13 1 39.79 29.69 13.66 o -8 0 2 883.26 845.98 53.60 o -6 0 2 0.92 6.75 13.29 o -4 0 2 8245.36 8226.38 238.59 o -2 0 2 6214.14 5898.18 167.97 o 0 0 2 18312.86 18597.93 346.25 o 2 0 2 20387.97 22491.55 612.38 o 4 0 2 158.39 154.68 17.51 o 6 0 2 38.53 65.56 18.78 o 8 0 2 337.92 403.26 40.59 o -8 1 2 1082.06 1242.61 45.73 o -7 1 2 68.41 60.64 14.24 o -6 1 2 1278.40 1337.66 55.11 o -5 1 2 266.82 268.05 17.91 o -4 1 2 3406.59 3635.44 88.70 o -3 1 2 1576.12 1496.86 67.03 o -2 1 2 3855.88 4004.63 133.58 o -1 1 2 1462.39 1407.68 16.58 o 0 1 2 5457.80 5913.66 70.37 o 1 1 2 6222.39 6039.33 95.38 o 2 1 2 556.07 560.11 17.12 o 3 1 2 1431.83 1838.15 44.08 o 4 1 2 9764.16 10568.35 212.87 o 5 1 2 141.24 142.95 13.95 o 6 1 2 793.13 832.60 32.50 o 7 1 2 15.25 -4.35 21.14 o 8 1 2 262.41 310.13 38.34 o -8 2 2 42.31 104.20 27.71 o -7 2 2 13.13 1.89 8.00 o -6 2 2 9.71 -0.12 13.75 o -5 2 2 862.32 822.18 34.61 o -4 2 2 1485.50 1479.50 31.23 o -3 2 2 329.04 368.27 11.53 o -2 2 2 335.22 335.79 10.71 o -1 2 2 21928.65 23325.88 272.00 o 0 2 2 34663.91 35731.16 415.88 o 1 2 2 15927.11 16165.37 213.40 o 3 2 2 3072.56 3858.45 65.95 o 4 2 2 281.62 355.51 15.86 o 5 2 2 83.83 108.05 21.47 o 6 2 2 690.79 726.87 23.49 o 7 2 2 373.03 406.44 23.88 o 8 2 2 297.98 365.73 27.07 o -8 3 2 239.87 273.50 22.98 o -7 3 2 624.20 695.37 44.24 o -6 3 2 202.60 233.00 14.43 o -5 3 2 770.62 797.58 22.37 o -4 3 2 4597.01 4342.03 106.37 o -3 3 2 7258.25 7233.78 100.31 o -2 3 2 3928.82 4185.11 59.29 o -1 3 2 7814.98 8331.46 99.85 o 0 3 2 275.24 222.62 5.87 o 1 3 2 836.39 870.42 13.41 o 2 3 2 66.97 48.87 4.56 o 3 3 2 838.87 944.74 21.28 o 4 3 2 4592.23 4557.36 78.96 o 5 3 2 2325.37 2398.09 48.15 o 6 3 2 1328.06 1301.58 41.89 o 7 3 2 157.80 139.60 17.63 o 8 3 2 138.56 150.59 19.65 o -8 4 2 759.36 737.15 41.47 o -7 4 2 57.40 44.67 12.98 o -6 4 2 1677.13 1554.06 55.43 o -5 4 2 3377.13 3423.25 63.26 o -4 4 2 516.50 451.56 12.81 o -3 4 2 5744.53 5627.64 79.93 o -2 4 2 3424.08 3375.52 52.73 o -1 4 2 3353.71 3083.63 40.24 o 0 4 2 911.87 949.86 15.13 o 1 4 2 54.70 89.84 4.25 o 2 4 2 3593.71 3634.38 62.29 o 3 4 2 159.51 144.07 12.13 o 4 4 2 863.92 818.96 21.14 o 5 4 2 923.83 921.79 32.37 o 6 4 2 4.51 4.55 9.92 o 7 4 2 178.15 251.25 21.56 o 8 4 2 313.10 333.71 27.16 o -8 5 2 0.78 6.83 12.14 o -7 5 2 310.56 370.42 28.98 o -6 5 2 1537.13 1362.46 43.07 o -5 5 2 137.20 141.51 14.14 o -4 5 2 4077.83 4240.02 75.23 o -3 5 2 5217.83 5179.90 87.45 o -2 5 2 7610.16 8085.51 130.66 o -1 5 2 6891.25 6938.10 88.41 o 0 5 2 0.02 3.65 2.82 o 1 5 2 3256.81 3154.29 41.43 o 2 5 2 630.07 603.01 19.17 o 3 5 2 268.45 250.25 14.29 o 4 5 2 70.20 75.19 18.14 o 5 5 2 33.67 42.56 11.15 o 6 5 2 1433.51 1359.12 44.37 o 7 5 2 197.20 247.25 22.07 o 8 5 2 272.89 294.87 26.07 o -8 6 2 543.91 546.30 30.05 o -7 6 2 562.50 534.66 27.55 o -6 6 2 484.70 480.96 48.43 o -5 6 2 324.73 328.84 17.01 o -4 6 2 1044.35 1024.36 52.56 o -3 6 2 1704.37 1611.75 35.52 o -2 6 2 7866.57 8261.20 133.74 o -1 6 2 4.28 5.58 3.67 o 0 6 2 1281.52 1414.00 22.13 o 1 6 2 956.01 916.46 15.96 o 2 6 2 1417.55 1630.52 48.34 o 3 6 2 1107.22 1136.72 28.29 o 4 6 2 1346.34 1345.56 33.13 o 5 6 2 1292.41 1293.11 71.85 o 6 6 2 918.33 872.31 35.09 o 7 6 2 444.96 517.64 28.64 o -7 7 2 131.01 96.76 16.53 o -6 7 2 612.03 609.35 75.51 o -5 7 2 101.45 112.17 15.06 o -4 7 2 2038.02 2007.68 44.25 o -3 7 2 75.70 79.70 10.12 o -2 7 2 4.89 -2.21 6.09 o -1 7 2 1151.18 1011.72 16.23 o 0 7 2 1077.35 1135.71 19.70 o 1 7 2 7705.30 7454.17 139.91 o 2 7 2 737.59 678.62 25.98 o 3 7 2 715.47 686.79 22.16 o 4 7 2 87.95 158.55 32.11 o 5 7 2 418.24 377.40 22.61 o 6 7 2 537.01 502.05 34.40 o 7 7 2 37.51 26.05 14.03 o -7 8 2 970.89 949.14 40.01 o -6 8 2 55.94 24.62 17.09 o -5 8 2 531.73 551.82 22.34 o -4 8 2 34.45 24.17 9.42 o -3 8 2 1924.82 1849.22 42.12 o -2 8 2 367.50 364.90 13.86 o -1 8 2 2696.23 2743.98 37.70 o 0 8 2 582.37 632.69 14.48 o 1 8 2 10.00 -2.63 6.51 o 2 8 2 644.45 657.74 33.92 o 3 8 2 2140.52 2114.10 46.49 o 4 8 2 14.59 0.29 7.85 o 5 8 2 1304.53 1306.26 36.19 o 6 8 2 43.07 43.47 15.69 o 7 8 2 210.51 255.80 25.64 o -6 9 2 21.96 26.81 11.03 o -5 9 2 0.27 1.40 9.46 o -4 9 2 10.52 18.72 9.65 o -3 9 2 161.48 159.50 11.53 o -2 9 2 308.20 291.85 19.82 o -1 9 2 2543.16 2555.62 43.97 o 0 9 2 52.96 47.90 5.46 o 1 9 2 10158.81 10034.67 154.70 o 2 9 2 20.51 2.07 8.66 o 3 9 2 1390.24 1326.66 35.18 o 4 9 2 190.31 206.39 15.92 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1618.47 1757.38 90.81 o -1 0 21 1945.08 1973.47 95.66 o 1 0 21 217.30 165.44 34.47 o -4 1 21 45.93 44.78 14.70 o -3 1 21 295.19 344.37 22.75 o -2 1 21 0.11 -10.23 14.96 o -1 1 21 197.68 195.06 38.48 o 0 1 21 2.81 1.33 15.23 o 1 1 21 1041.54 1102.26 48.96 o 2 1 21 145.13 159.35 25.08 o -4 2 21 51.25 51.38 14.51 o -3 2 21 877.35 867.55 56.72 o -2 2 21 15.35 20.18 17.46 o -1 2 21 870.93 860.25 42.83 o 0 2 21 34.24 4.07 17.60 o 1 2 21 189.93 192.76 67.21 o 2 2 21 4.89 7.75 17.20 o -4 3 21 461.36 428.07 30.73 o -3 3 21 7.34 7.95 10.78 o -2 3 21 22.19 24.09 17.25 o -1 3 21 12.24 18.83 16.20 o 0 3 21 70.20 93.85 21.36 o 1 3 21 368.69 369.07 92.29 o -3 4 21 494.87 511.56 25.98 o -2 4 21 66.76 61.56 13.59 o -1 4 21 90.97 40.19 18.15 o 0 4 21 11.82 2.88 27.85 o 1 4 21 125.94 134.98 35.49 o -3 5 21 12.73 2.99 11.73 o -2 5 21 58.40 54.05 13.71 o -1 5 21 0.52 3.31 15.87 o 0 5 21 2.17 8.44 17.57 o -4 0 22 151.24 147.15 34.54 o -2 0 22 184.08 224.95 38.27 o 0 0 22 368.39 408.96 46.35 o -3 1 22 179.30 237.96 28.46 o -2 1 22 318.46 342.45 32.26 o -1 1 22 3.79 -5.94 16.36 o 0 1 22 490.59 482.05 35.50 o 1 1 22 52.05 60.49 19.46 o -3 2 22 18.41 -5.14 11.90 o -2 2 22 153.66 141.62 24.10 o -1 2 22 321.02 363.10 32.17 o 0 2 22 63.22 41.94 20.55 o 1 2 22 58.62 42.97 23.49 o -3 3 22 317.24 316.61 39.53 o -2 3 22 359.06 336.33 31.97 o -1 3 22 10.25 7.10 16.86 o 0 3 22 139.35 140.40 39.81 o -2 4 22 16.43 11.75 10.99 o -1 4 22 279.58 279.79 29.74 o -1 0 23 1847.58 1966.08 100.16 o -2 1 23 9.87 7.37 31.58 o -1 1 23 126.56 122.11 25.24 o