#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/55/2015582.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015582_Fobs loop_ _publ_author_name 'Goforth, Andrea M.' 'Tershansy, Meredith A.' 'Smith, Mark D.' 'Peterson Jr, LeRoy' 'Loye, Hans-Conrad zur' _publ_section_title ; Tetrakis[2-(2-pyridyl)pyridinium] tetra-\m~3~-iodo-hexa-\m~2~-iodo-dodecaiodohexabismuthate and bis[tris(2,2'-bipyridine)ruthenium(II)] di-\m~4~-iodo-octa-\m~2~-iodo-dodecaiodohexabismuthate ; _journal_coeditor_code SQ3025 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m381 _journal_page_last m385 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 78.778 _cell_angle_beta 79.520 _cell_angle_gamma 66.023 _cell_length_a 11.3334 _cell_length_b 12.9913 _cell_length_c 15.7999 _exptl_crystal_F_000 1996.00 _reflns_d_resolution_high 0.7639 _[local]_cod_data_source_file sq3025Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mat087as in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1426.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1438.33 2046.01 64.86 o 2 0 0 31198.76 35145.02 802.76 o 3 0 0 156.62 198.27 44.77 o 4 0 0 18832.50 20214.08 519.08 o 5 0 0 31612.12 32454.42 812.56 o 6 0 0 805.79 1016.68 101.34 o 7 0 0 11544.86 12040.82 739.81 o 8 0 0 6530.15 6351.41 270.74 o 9 0 0 15302.77 13774.62 577.56 o 10 0 0 127594.63 128731.20 5500.69 o 11 0 0 28787.96 30055.66 1467.40 o 12 0 0 447.52 669.01 303.31 o 13 0 0 14602.60 16446.11 1363.90 o -13 1 0 8846.60 9632.08 2218.17 o -12 1 0 11968.71 13407.33 938.45 o -11 1 0 51983.38 57880.43 2422.55 o -10 1 0 3630.22 4843.38 1243.76 o -9 1 0 99333.09 102078.57 2903.75 o -8 1 0 5310.20 5328.65 315.51 o -7 1 0 90.60 135.68 69.33 o -6 1 0 1004.46 1198.48 113.83 o -5 1 0 16026.81 17033.74 473.90 o -4 1 0 4014.77 3762.85 200.19 o -3 1 0 3672.22 3799.12 201.90 o -2 1 0 1115.62 1127.24 59.74 o -1 1 0 101899.41 111374.65 2880.79 o 0 1 0 266036.44 230182.69 11872.03 o 1 1 0 332324.44 278217.03 6986.67 o 2 1 0 54999.23 60410.66 1349.21 o 3 1 0 4819.21 4629.57 222.50 o 4 1 0 850.76 939.93 73.93 o 5 1 0 4807.05 5168.08 190.80 o 6 1 0 19190.15 18707.07 520.31 o 7 1 0 459.31 532.48 85.78 o 8 1 0 1228.73 1327.57 129.78 o 9 1 0 5601.52 5635.53 322.87 o 10 1 0 35567.07 35699.77 1604.04 o 11 1 0 1949.30 1901.30 380.20 o 12 1 0 20325.39 21009.39 1192.45 o 13 1 0 2295.00 2598.82 474.03 o -12 2 0 6814.74 8154.32 758.45 o -11 2 0 17636.31 17064.48 1921.26 o -10 2 0 27468.82 27862.27 1030.81 o -9 2 0 6245.23 5734.75 447.25 o -8 2 0 45063.79 44154.78 1605.88 o -7 2 0 1375.43 1536.78 191.62 o -6 2 0 3159.67 3301.39 206.90 o -5 2 0 64.53 255.49 75.47 o -4 2 0 309.15 407.63 98.24 o -3 2 0 4616.65 5378.51 241.06 o -2 2 0 50.88 138.69 90.17 o -1 2 0 106020.41 111829.52 2463.17 o 0 2 0 13967.15 15237.84 370.72 o 1 2 0 120461.52 121812.13 2673.65 o 2 2 0 32835.17 36140.36 830.77 o 3 2 0 56655.36 60833.88 1615.34 o 4 2 0 9057.44 8983.67 299.22 o 5 2 0 5360.66 5125.74 185.02 o 6 2 0 9576.18 9963.50 312.82 o 7 2 0 0.53 39.61 52.39 o 8 2 0 1012.55 1406.56 179.33 o 9 2 0 326.18 378.37 216.05 o 10 2 0 14519.98 15877.50 898.80 o 11 2 0 853.99 890.72 276.49 o 12 2 0 7703.48 8785.31 1702.56 o 13 2 0 8674.97 8738.16 737.90 o 14 2 0 4162.48 3815.91 590.95 o -12 3 0 716.37 904.30 350.42 o -11 3 0 17963.65 17144.24 1262.51 o -10 3 0 16759.32 17305.02 757.47 o -9 3 0 41867.94 41009.19 1362.73 o -8 3 0 3843.37 4725.78 359.39 o -7 3 0 5407.70 5094.68 538.08 o -6 3 0 452.44 647.00 132.05 o -5 3 0 6514.38 6329.12 319.66 o -4 3 0 5985.08 5929.11 288.00 o -3 3 0 26104.86 27314.23 841.02 o -2 3 0 9.12 149.42 65.52 o -1 3 0 92927.30 99760.47 2360.25 o 0 3 0 2103.27 2367.31 129.03 o 1 3 0 50083.41 54362.19 1236.96 o 2 3 0 62878.97 67312.06 1517.00 o 3 3 0 2982.81 3102.74 118.16 o 4 3 0 97370.51 103213.49 2705.53 o 5 3 0 5758.31 5988.82 273.81 o 6 3 0 18172.94 19472.85 527.27 o 7 3 0 622.64 535.25 71.06 o 8 3 0 14781.55 14984.15 761.43 o 9 3 0 285.16 586.67 145.78 o 10 3 0 3568.58 4117.72 304.07 o 11 3 0 2686.18 3229.63 475.72 o 12 3 0 19987.43 20341.23 1638.28 o 13 3 0 5129.54 6197.01 609.75 o 14 3 0 24301.65 26182.30 1422.00 o -11 4 0 5060.50 5424.77 609.96 o -10 4 0 27074.00 27092.26 1045.33 o -9 4 0 7843.57 7207.47 437.89 o -8 4 0 42568.77 39640.47 1318.42 o -7 4 0 21297.28 19705.57 1815.17 o -6 4 0 1382.84 955.95 163.37 o -5 4 0 2653.65 2579.06 292.66 o -4 4 0 9623.91 8153.91 406.06 o -3 4 0 130.32 87.40 82.46 o -2 4 0 21646.45 22303.19 567.42 o -1 4 0 2186.48 2462.24 129.19 o 0 4 0 58422.71 61910.38 1417.38 o 1 4 0 27088.15 29492.09 718.09 o 2 4 0 189507.84 198994.94 5170.63 o 3 4 0 13930.62 13312.72 365.43 o 4 4 0 62532.84 62333.35 1439.04 o 5 4 0 10429.81 11828.62 1056.94 o 6 4 0 13762.76 13668.21 505.95 o 7 4 0 1355.14 1450.91 261.38 o 8 4 0 63.59 -43.74 77.89 o 9 4 0 20863.15 21218.98 775.11 o 10 4 0 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7 0 9.29 9.75 82.81 o -2 7 0 13765.64 14095.32 430.93 o -1 7 0 3452.80 3467.08 171.85 o 0 7 0 1005.28 1297.58 199.54 o 1 7 0 5581.76 5830.26 246.80 o 2 7 0 137974.22 147883.45 3333.50 o 3 7 0 154687.61 156515.05 3524.38 o 4 7 0 643643.44 603364.25 13158.00 o 5 7 0 4119.04 3867.61 186.40 o 6 7 0 7528.41 7623.13 420.32 o 7 7 0 7768.22 7669.35 376.74 o 8 7 0 965.88 785.99 153.63 o 9 7 0 7080.51 6489.46 370.12 o 10 7 0 6641.87 6913.38 396.23 o 11 7 0 459.15 560.39 175.64 o 12 7 0 117.28 241.28 147.88 o 13 7 0 25914.34 25311.98 985.68 o 14 7 0 18975.60 18872.92 1131.11 o -9 8 0 10987.71 11877.26 653.48 o -8 8 0 539.10 1286.49 256.69 o -7 8 0 49548.95 46201.64 1545.81 o -6 8 0 23942.95 21774.43 862.44 o -5 8 0 58081.88 54242.28 1704.21 o -4 8 0 2487.16 2494.78 324.35 o -3 8 0 153.63 99.20 97.11 o -2 8 0 1710.27 1369.35 187.56 o -1 8 0 5632.75 5400.45 248.09 o 0 8 0 3070.66 3149.57 186.34 o 1 8 0 624.16 481.49 101.40 o 2 8 0 17198.52 18511.77 542.13 o 3 8 0 34321.56 32259.63 848.89 o 4 8 0 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