#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/55/2015594.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015594_Fobs loop_ _publ_author_name 'Busi, Sara' 'Lahtinen, Manu' 'Sillanp\"a\"a, Reijo' 'Rissanen, Kari' _publ_section_title ; A linear Fe--O--Fe unit in bis(dibenzyldimethylammonium) \m-oxo-bis[tribromoferrate(III)] ; _journal_coeditor_code FA3029 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m458 _journal_page_last m460 _journal_volume 62 _journal_year 2006 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.7997 _cell_length_b 14.9838 _cell_length_c 18.2833 _exptl_crystal_F_000 2064.00 _reflns_d_resolution_high 0.7535 _[local]_cod_data_source_file fa3029Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' QAFeCl4Acexprep in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 550.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14786.83 12036.64 256.43 o 4 0 0 24733.16 22431.17 333.72 o 6 0 0 47856.90 50784.55 750.48 o 8 0 0 758.58 989.93 79.48 o 10 0 0 8417.41 8229.73 216.98 o 12 0 0 13230.48 14979.76 342.48 o 14 0 0 25204.92 26593.02 591.47 o 16 0 0 755.46 2.41 205.92 o 18 0 0 1202.14 1687.17 470.87 o 2 1 0 2820.44 3011.61 75.98 o 4 1 0 16.34 49.37 24.08 o 6 1 0 32744.47 32007.56 360.09 o 8 1 0 17753.65 17776.53 245.14 o 10 1 0 20.68 -21.67 50.57 o 12 1 0 2765.89 3169.08 114.43 o 14 1 0 177.01 192.67 66.23 o 16 1 0 277.17 590.05 210.73 o 18 1 0 81.46 -160.15 242.04 o 0 2 0 96957.92 74623.24 1562.31 o 2 2 0 1273.13 1261.49 32.53 o 4 2 0 4740.13 4035.78 74.76 o 6 2 0 16898.60 18448.03 239.24 o 8 2 0 15019.05 16243.60 213.64 o 10 2 0 2713.85 2865.66 93.96 o 12 2 0 7279.17 8304.38 189.20 o 14 2 0 369.31 304.66 79.48 o 16 2 0 3398.68 2995.59 202.36 o 18 2 0 31.47 202.30 295.02 o 2 3 0 202654.23 184311.94 2039.29 o 4 3 0 9945.93 9861.00 135.21 o 6 3 0 5451.26 5300.22 101.26 o 8 3 0 24992.11 26254.83 317.90 o 10 3 0 175.21 248.06 59.00 o 12 3 0 1880.67 2059.51 98.76 o 14 3 0 743.97 833.33 110.79 o 16 3 0 523.43 469.64 133.67 o 18 3 0 100.78 186.64 321.51 o 0 4 0 39759.70 32628.61 634.66 o 2 4 0 141331.83 123560.85 1436.48 o 4 4 0 5.67 189.05 30.10 o 6 4 0 339.98 209.53 54.19 o 8 4 0 29128.53 29856.16 370.04 o 10 4 0 23.31 8.43 50.57 o 12 4 0 2596.33 2290.92 125.27 o 14 4 0 8658.92 9585.56 273.56 o 16 4 0 4471.41 5072.58 220.44 o 2 5 0 3674.88 3345.82 95.22 o 4 5 0 14914.71 14467.01 236.75 o 6 5 0 11829.24 11812.27 167.71 o 8 5 0 11222.88 11629.89 192.97 o 10 5 0 3320.94 3397.04 104.80 o 12 5 0 4516.85 4924.86 149.38 o 14 5 0 3864.38 4313.59 183.10 o 16 5 0 48.69 130.05 187.85 o 0 6 0 43501.43 38347.90 750.37 o 2 6 0 52347.48 47210.85 684.37 o 4 6 0 10895.33 9862.80 180.99 o 6 6 0 4964.64 5243.35 94.00 o 8 6 0 35066.82 37949.83 515.37 o 10 6 0 4110.40 4556.24 126.50 o 12 6 0 235.63 726.12 68.64 o 14 6 0 508.41 1036.82 122.83 o 16 6 0 379.60 1044.03 214.34 o 2 7 0 362.68 474.47 39.74 o 4 7 0 56.31 125.23 55.39 o 6 7 0 10832.37 11445.53 180.91 o 8 7 0 20093.20 20179.91 286.11 o 10 7 0 1864.25 2269.08 90.33 o 12 7 0 2302.87 2460.63 112.01 o 14 7 0 2739.99 2505.24 163.80 o 16 7 0 790.84 -97.54 287.81 o 0 8 0 38775.48 34658.37 659.47 o 2 8 0 17004.31 17066.87 262.05 o 4 8 0 11588.87 10600.91 207.48 o 6 8 0 7006.44 6468.85 151.87 o 8 8 0 11680.08 11632.77 204.99 o 10 8 0 1995.60 1999.31 93.94 o 12 8 0 4230.00 4388.49 150.58 o 14 8 0 5767.19 8950.11 597.56 o 16 8 0 24.99 210.73 232.40 o 2 9 0 2882.28 2576.79 104.81 o 4 9 0 12044.52 12473.21 226.76 o 6 9 0 43123.21 46114.20 632.02 o 8 9 0 7149.88 6952.41 163.90 o 10 9 0 5102.70 5403.44 166.26 o 12 9 0 1753.23 2040.16 118.03 o 14 9 0 3.65 131.25 191.46 o 16 9 0 114.28 375.70 219.16 o 0 10 0 57576.63 58955.47 1104.63 o 2 10 0 17986.73 17540.79 305.40 o 4 10 0 1610.06 1427.21 78.29 o 6 10 0 2316.50 2160.84 89.13 o 8 10 0 56.17 134.87 69.84 o 10 10 0 1557.08 1593.33 130.07 o 12 10 0 2889.68 3376.11 157.78 o 14 10 0 2158.13 2906.13 327.59 o 2 11 0 5611.39 5244.17 151.83 o 4 11 0 8828.08 8123.38 201.31 o 6 11 0 76291.36 77673.30 998.26 o 8 11 0 14105.11 15922.76 300.27 o 10 11 0 519.62 348.02 66.23 o 12 11 0 3916.25 3796.78 369.80 o 14 11 0 147.10 -20.47 214.34 o 0 12 0 3216.87 3089.82 145.76 o 2 12 0 365.05 274.56 96.34 o 4 12 0 93.90 144.50 63.82 o 6 12 0 2182.81 2242.64 102.38 o 8 12 0 4981.75 5580.35 162.64 o 10 12 0 1826.19 1833.02 114.41 o 12 12 0 713.70 1329.46 228.80 o 14 12 0 1265.15 1356.01 345.62 o 2 13 0 5246.13 5431.41 185.54 o 4 13 0 1129.09 1147.69 86.71 o 6 13 0 1020.20 800.84 87.91 o 8 13 0 516.55 769.49 78.27 o 10 13 0 2266.68 2348.56 244.49 o 12 13 0 22.96 551.50 249.26 o 0 14 0 5997.57 5948.57 203.63 o 2 14 0 1917.44 1777.67 110.80 o 4 14 0 1190.96 1157.32 98.75 o 6 14 0 34.19 30.10 79.47 o 8 14 0 34.47 -139.68 139.68 o 10 14 0 53.25 -221.56 221.56 o 12 14 0 343.00 1149.99 341.99 o 2 15 0 3302.87 3101.67 142.13 o 4 15 0 9034.71 9220.78 255.50 o 6 15 0 9017.53 9994.16 291.64 o 8 15 0 6988.72 6607.54 344.59 o 10 15 0 493.20 382.93 256.49 o 12 15 0 1334.18 1227.15 323.95 o 0 16 0 1386.01 1378.92 164.99 o 2 16 0 465.20 351.63 108.38 o 4 16 0 9.79 -85.49 85.49 o 6 16 0 334.82 727.33 158.95 o 8 16 0 9.96 127.64 169.78 o 10 16 0 326.13 375.70 246.86 o 2 17 0 1459.94 1689.63 166.19 o 4 17 0 2155.74 2158.23 221.60 o 6 17 0 30.07 92.72 164.97 o 8 17 0 212.83 -290.20 290.20 o 0 18 0 704.05 217.96 262.52 o 2 18 0 21.56 -156.54 229.99 o 4 18 0 612.07 729.75 239.64 o 6 18 0 292.27 131.26 193.87 o 2 19 0 762.79 581.64 234.82 o 4 19 0 648.13 622.58 317.91 o 1 1 1 31143.51 33581.20 904.66 o 2 1 1 96.08 210.36 18.47 o 3 1 1 302709.25 320437.72 2090.88 o 4 1 1 1110.14 1148.65 76.49 o 5 1 1 31917.94 33697.87 1115.32 o 6 1 1 21460.54 20680.48 854.53 o 7 1 1 1036.37 1204.89 40.98 o 8 1 1 970.18 868.17 34.64 o 9 1 1 15349.81 15602.06 151.46 o 10 1 1 2109.37 1938.45 94.55 o 11 1 1 10979.09 12164.83 361.11 o 12 1 1 2607.76 2810.50 210.79 o 13 1 1 6053.19 6128.82 143.98 o 14 1 1 255.53 238.94 83.09 o 15 1 1 6865.35 6784.04 168.69 o 16 1 1 421.04 458.34 122.99 o 17 1 1 202.53 240.36 246.85 o 18 1 1 54.83 9.71 153.94 o 0 2 1 2820.31 3006.10 78.41 o 1 2 1 9200.91 9491.11 912.04 o 2 2 1 238.12 244.70 14.45 o 3 2 1 26540.77 25896.05 223.94 o 4 2 1 36515.33 35511.41 546.24 o 5 2 1 58306.07 58317.28 878.25 o 6 2 1 3266.12 3235.73 130.74 o 7 2 1 8.26 11.66 34.41 o 8 2 1 19556.04 20037.18 297.13 o 9 2 1 14106.15 14170.87 294.39 o 10 2 1 11096.05 11874.33 144.47 o 11 2 1 3584.57 3596.47 130.10 o 12 2 1 1752.82 1838.37 63.34 o 13 2 1 0.03 24.84 166.17 o 14 2 1 1926.34 1680.89 84.84 o 15 2 1 3.91 -68.03 68.03 o 16 2 1 393.04 403.03 89.10 o 17 2 1 625.24 1178.36 344.40 o 18 2 1 365.78 269.07 165.99 o 1 3 1 5906.83 5847.84 167.79 o 2 3 1 15523.32 14786.22 925.13 o 3 3 1 11176.26 11341.61 930.36 o 4 3 1 702.63 521.81 37.34 o 5 3 1 47480.22 47367.65 1147.37 o 6 3 1 236.90 241.11 36.73 o 7 3 1 3132.85 3000.57 60.90 o 8 3 1 2796.09 2884.01 63.03 o 9 3 1 2472.02 2482.42 63.80 o 10 3 1 168.36 96.06 36.43 o 11 3 1 396.81 337.27 52.60 o 12 3 1 658.38 500.59 146.31 o 13 3 1 2218.38 2221.50 163.80 o 14 3 1 322.62 310.94 130.05 o 15 3 1 109.20 58.83 76.46 o 16 3 1 451.74 432.20 81.27 o 17 3 1 3006.41 2657.70 445.64 o 18 3 1 219.98 111.35 410.62 o 0 4 1 16946.02 17991.82 260.36 o 1 4 1 42036.50 38639.84 2779.72 o 2 4 1 23175.65 22126.92 789.90 o 3 4 1 996.40 1016.72 26.62 o 4 4 1 4520.63 4272.65 56.94 o 5 4 1 12134.08 11809.40 123.23 o 6 4 1 3308.94 3737.22 55.93 o 7 4 1 19.72 18.97 33.93 o 8 4 1 5660.74 6522.75 303.70 o 9 4 1 130.88 134.14 99.34 o 10 4 1 2189.94 2245.69 105.39 o 11 4 1 1212.23 1147.69 87.31 o 12 4 1 318.18 352.95 87.91 o 13 4 1 276.32 391.31 103.56 o 14 4 1 15.50 26.34 58.95 o 15 4 1 296.69 342.50 77.47 o 16 4 1 54.11 101.50 318.50 o 17 4 1 410.47 180.89 289.61 o 1 5 1 5685.52 4979.89 572.83 o 2 5 1 7056.04 6353.34 687.58 o 3 5 1 66672.10 62552.90 2222.39 o 4 5 1 6944.18 7603.93 205.60 o 5 5 1 96455.53 98717.32 755.10 o 6 5 1 9928.57 9888.16 113.46 o 7 5 1 17467.94 16670.75 660.43 o 8 5 1 5127.57 5643.84 88.04 o 9 5 1 38.22 10.87 35.27 o 10 5 1 584.33 590.55 52.61 o 11 5 1 57.40 159.70 39.90 o 12 5 1 6333.29 6578.59 190.98 o 13 5 1 457.19 765.26 72.38 o 14 5 1 284.91 652.51 79.92 o 15 5 1 1024.39 959.94 83.33 o 16 5 1 586.51 291.93 103.36 o 17 5 1 4698.64 5506.50 1160.63 o 0 6 1 12478.94 10808.99 208.91 o 1 6 1 12286.87 11678.33 364.66 o 2 6 1 5242.75 5349.81 483.41 o 3 6 1 12198.46 11208.87 438.18 o 4 6 1 10075.76 9432.27 347.45 o 5 6 1 8424.16 8126.94 252.63 o 6 6 1 2190.92 1942.23 43.01 o 7 6 1 803.96 825.96 60.21 o 8 6 1 991.87 979.69 97.55 o 9 6 1 10799.48 11685.48 147.45 o 10 6 1 6845.85 7359.79 255.48 o 11 6 1 18415.70 19853.11 345.07 o 12 6 1 165.00 87.25 44.91 o 13 6 1 1261.36 1232.20 104.17 o 14 6 1 161.32 94.14 64.97 o 15 6 1 1458.82 1318.12 220.39 o 16 6 1 128.39 144.59 177.01 o 17 6 1 18.60 428.17 359.82 o 1 7 1 19152.17 19103.98 798.90 o 2 7 1 8521.54 7880.62 510.17 o 3 7 1 193.30 326.29 42.15 o 4 7 1 18540.35 18093.80 197.98 o 5 7 1 7079.78 6685.89 257.37 o 6 7 1 1705.58 1609.08 51.52 o 7 7 1 11879.90 12113.12 136.86 o 8 7 1 5.76 77.41 30.96 o 9 7 1 4036.21 4335.74 86.69 o 10 7 1 216.89 358.14 54.19 o 11 7 1 4010.92 4143.77 113.84 o 12 7 1 0.35 39.10 48.34 o 13 7 1 762.26 700.98 150.53 o 14 7 1 228.59 258.17 69.39 o 15 7 1 734.82 815.83 177.02 o 16 7 1 318.40 132.40 179.16 o 17 7 1 45.82 425.00 172.00 o 0 8 1 139.34 329.94 52.98 o 1 8 1 288.90 370.33 37.71 o 2 8 1 3452.86 3066.86 98.19 o 3 8 1 3583.71 2952.10 95.78 o 4 8 1 3005.42 2950.64 312.02 o 5 8 1 10.87 23.61 93.32 o 6 8 1 69.04 58.84 62.01 o 7 8 1 7267.74 7369.40 197.06 o 8 8 1 1502.37 1524.07 44.74 o 9 8 1 477.14 447.59 51.42 o 10 8 1 4526.67 4229.04 92.56 o 11 8 1 1759.88 1712.96 68.11 o 12 8 1 646.89 651.68 57.20 o 13 8 1 565.05 450.41 110.79 o 14 8 1 695.37 901.58 180.82 o 15 8 1 310.48 121.02 160.08 o 16 8 1 24.94 -177.27 177.27 o 1 9 1 28353.23 27709.81 495.25 o 2 9 1 16277.99 15899.85 481.63 o 3 9 1 36457.07 34201.64 1458.11 o 4 9 1 122.87 152.62 44.55 o 5 9 1 5132.89 4942.85 360.89 o 6 9 1 11.06 164.06 96.33 o 7 9 1 1.85 31.28 34.93 o 8 9 1 1629.02 1678.23 51.48 o 9 9 1 3885.97 4012.48 86.50 o 10 9 1 280.68 407.59 151.73 o 11 9 1 4178.28 4418.94 255.99 o 12 9 1 869.95 1011.36 73.17 o 13 9 1 182.88 294.47 113.79 o 14 9 1 58.81 62.00 186.04 o 15 9 1 2473.43 2443.69 221.74 o 16 9 1 515.75 758.49 308.27 o 0 10 1 9297.22 8940.40 160.36 o 1 10 1 5188.15 5151.31 140.38 o 2 10 1 1731.57 1889.04 228.24 o 3 10 1 37059.64 35873.72 773.26 o 4 10 1 2289.76 2408.76 62.63 o 5 10 1 16646.34 16793.20 560.49 o 6 10 1 3008.26 3063.42 280.06 o 7 10 1 9559.11 10315.71 447.83 o 8 10 1 17.63 21.92 73.45 o 9 10 1 29276.12 32259.96 564.64 o 10 10 1 620.33 711.79 74.52 o 11 10 1 2781.31 2986.77 116.21 o 12 10 1 291.80 316.34 71.92 o 13 10 1 180.64 221.22 174.60 o 14 10 1 217.16 321.48 152.95 o 15 10 1 296.84 916.29 236.71 o 1 11 1 863.70 894.91 64.43 o 2 11 1 616.60 626.71 304.67 o 3 11 1 297.53 356.65 85.50 o 4 11 1 4990.89 4797.41 145.79 o 5 11 1 8718.64 8450.93 132.56 o 6 11 1 140.92 392.64 58.40 o 7 11 1 241.11 276.72 46.33 o 8 11 1 126.29 242.19 68.20 o 9 11 1 979.22 969.32 99.95 o 10 11 1 4.81 219.49 56.86 o 11 11 1 223.24 298.40 227.59 o 12 11 1 26.58 134.26 177.01 o 13 11 1 987.36 1429.74 552.75 o 14 11 1 86.22 -23.40 390.15 o 15 11 1 403.89 941.49 503.95 o 0 12 1 1433.64 1275.41 79.49 o 1 12 1 25.42 55.22 44.55 o 2 12 1 147.58 163.64 167.38 o 3 12 1 9845.90 9951.12 159.01 o 4 12 1 1893.11 1718.45 137.30 o 5 12 1 6711.91 6654.83 192.20 o 6 12 1 8.10 -11.55 42.21 o 7 12 1 2961.28 3172.89 208.98 o 8 12 1 11.65 24.59 48.33 o 9 12 1 9994.82 9934.40 321.21 o 10 12 1 950.31 1057.26 133.67 o 11 12 1 34.22 91.23 127.30 o 12 12 1 2.32 80.55 331.14 o 13 12 1 302.54 1031.73 439.52 o 14 12 1 112.04 187.19 180.40 o 1 13 1 1520.93 1652.08 165.00 o 2 13 1 8591.86 8657.02 316.38 o 3 13 1 6562.62 6440.52 193.40 o 4 13 1 2484.58 2713.87 87.29 o 5 13 1 64.69 222.45 50.53 o 6 13 1 240.23 367.05 65.03 o 7 13 1 15.45 79.76 49.18 o 8 13 1 3.21 -12.54 112.59 o 9 13 1 442.80 504.01 127.64 o 10 13 1 3.92 128.04 138.88 o 11 13 1 2406.38 2605.07 214.33 o 12 13 1 385.21 123.70 185.45 o 13 13 1 376.32 128.57 233.48 o 0 14 1 2322.08 2426.94 114.42 o 1 14 1 11339.49 11662.24 369.50 o 2 14 1 1607.37 1771.19 93.99 o 3 14 1 1009.20 805.17 74.01 o 4 14 1 590.13 582.34 57.05 o 5 14 1 399.28 215.47 55.73 o 6 14 1 2004.99 1965.86 133.08 o 7 14 1 80.61 22.19 116.20 o 8 14 1 0.14 3.36 66.83 o 9 14 1 2723.17 2520.02 251.73 o 10 14 1 115.15 267.70 210.13 o 11 14 1 4596.97 5120.84 578.81 o 12 14 1 2.91 -81.58 175.41 o 1 15 1 52.99 100.89 66.83 o 2 15 1 46.68 79.60 60.77 o 3 15 1 167.10 206.56 57.80 o 4 15 1 340.37 242.47 52.63 o 5 15 1 0.26 2.35 55.38 o 6 15 1 0.85 149.08 111.99 o 7 15 1 26.11 162.67 86.70 o 8 15 1 17.26 -115.00 115.00 o 9 15 1 158.87 -40.98 229.39 o 10 15 1 30.76 332.21 205.37 o 11 15 1 186.92 -173.36 196.42 o 12 15 1 9.54 533.27 384.59 o 0 16 1 1592.80 1222.39 108.39 o 1 16 1 8071.15 7032.82 192.80 o 2 16 1 3.92 94.16 86.10 o 3 16 1 1422.55 1632.63 190.28 o 4 16 1 315.90 234.93 59.31 o 5 16 1 183.94 192.64 70.87 o 6 16 1 422.51 703.02 110.61 o 7 16 1 103.93 0.34 134.86 o 8 16 1 14.56 -127.32 127.32 o 9 16 1 2119.44 2548.98 311.95 o 10 16 1 65.76 164.06 417.24 o 1 17 1 125.16 -26.29 122.82 o 2 17 1 1880.09 1785.82 132.20 o 3 17 1 993.80 944.99 91.10 o 4 17 1 3020.72 3480.78 223.43 o 5 17 1 832.80 929.58 305.87 o 6 17 1 12.78 -81.28 131.13 o 7 17 1 49.66 178.32 134.52 o 8 17 1 0.25 -101.98 319.70 o 9 17 1 19.18 -213.07 213.07 o 0 18 1 19.68 -149.31 198.68 o 1 18 1 145.04 139.86 320.31 o 2 18 1 155.67 138.97 300.44 o 3 18 1 1349.78 1542.71 417.89 o 4 18 1 168.00 439.48 184.14 o 5 18 1 1413.56 1617.64 172.44 o 6 18 1 38.81 51.30 394.36 o 7 18 1 67.88 -82.53 200.58 o 1 19 1 214.73 389.16 179.70 o 2 19 1 103.35 500.22 222.40 o 3 19 1 3.03 -69.95 268.52 o 4 19 1 348.60 1347.60 308.27 o 5 19 1 2.70 -49.33 167.14 o 1 0 2 10823.56 9585.46 360.32 o 2 0 2 50545.67 53272.50 978.92 o 3 0 2 22559.09 23475.57 291.44 o 4 0 2 8000.41 7729.63 118.29 o 5 0 2 28541.80 28951.80 309.18 o 6 0 2 729.33 886.39 48.17 o 7 0 2 3265.05 2800.07 83.13 o 8 0 2 7520.17 7650.61 126.59 o 9 0 2 41554.62 41930.58 463.90 o 10 0 2 19765.96 20086.86 276.45 o 11 0 2 2637.16 2975.17 95.16 o 12 0 2 13525.42 14849.84 236.36 o 13 0 2 3233.58 2877.66 109.61 o 14 0 2 3500.50 3505.25 127.68 o 15 0 2 3884.74 3448.69 144.55 o 16 0 2 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1142.22 1174.66 267.96 o 7 8 10 8.52 4.09 122.82 o 8 8 10 9402.08 8766.85 185.58 o 9 8 10 764.35 770.93 73.03 o 10 8 10 9136.42 8386.94 912.32 o 11 8 10 1081.46 864.01 345.62 o 12 8 10 355.57 247.43 109.66 o 13 8 10 3310.65 3472.60 221.08 o 14 8 10 165.79 -7.07 156.28 o 1 9 10 120.95 170.33 52.97 o 2 9 10 558.48 464.04 104.17 o 3 9 10 23.87 -0.05 67.05 o 4 9 10 3383.01 3754.17 329.46 o 5 9 10 4378.50 4554.57 355.39 o 6 9 10 12986.22 13374.47 477.49 o 7 9 10 4367.60 4406.08 630.05 o 8 9 10 1717.91 1663.56 93.96 o 9 9 10 211.56 219.41 61.26 o 10 9 10 2788.94 2772.62 131.53 o 11 9 10 354.34 473.94 89.92 o 12 9 10 1844.72 1927.51 181.31 o 13 9 10 0.37 -154.70 163.73 o 14 9 10 13.54 -207.03 207.28 o 0 10 10 183.16 219.16 69.84 o 1 10 10 8939.21 9435.16 177.79 o 2 10 10 212.50 252.96 129.45 o 3 10 10 260.81 115.24 67.29 o 4 10 10 2921.93 2970.83 103.81 o 5 10 10 4075.05 4186.85 119.30 o 6 10 10 103.95 130.86 93.32 o 7 10 10 46.70 -103.60 159.55 o 8 10 10 55.95 227.25 66.12 o 9 10 10 35.70 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2 13 10 1735.09 1745.79 121.04 o 3 13 10 1589.75 1719.56 88.60 o 4 13 10 4.85 176.98 76.46 o 5 13 10 458.62 516.18 154.14 o 6 13 10 19.76 241.19 86.43 o 7 13 10 424.27 121.22 164.97 o 8 13 10 780.21 891.17 368.49 o 9 13 10 231.85 148.49 144.50 o 10 13 10 153.09 165.33 118.94 o 11 13 10 137.21 5.16 320.87 o 0 14 10 358.83 422.67 96.33 o 1 14 10 3912.86 4196.03 130.13 o 2 14 10 2305.32 2398.58 123.77 o 3 14 10 21.85 67.19 161.36 o 4 14 10 866.56 890.18 93.25 o 5 14 10 27.42 42.60 153.53 o 6 14 10 147.52 353.62 105.83 o 7 14 10 45.25 84.51 100.46 o 8 14 10 2535.08 2034.03 177.65 o 9 14 10 15.57 -38.11 762.23 o 10 14 10 639.13 -60.18 314.30 o 1 15 10 75.47 156.58 99.40 o 2 15 10 45.96 206.12 106.70 o 3 15 10 1353.63 1294.81 111.33 o 4 15 10 34.85 70.82 95.09 o 5 15 10 891.85 721.70 113.48 o 6 15 10 11.17 140.11 338.37 o 7 15 10 3954.95 3785.27 1415.33 o 8 15 10 89.50 54.91 282.37 o 9 15 10 565.88 1158.81 358.61 o 0 16 10 218.43 378.11 143.30 o 1 16 10 459.10 527.43 169.79 o 2 16 10 253.33 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