#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:08:02 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180825 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/56/2015609.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015609_Fobs loop_ _publ_author_name 'Wardell, Solange M. S. V.' 'Vasconcelos, Thatyana R. A.' 'de Souza, Marcus V. N.' 'Wardell, James L.' 'Low, John N.' 'Glidewell, Christopher' _publ_section_title ; Four substituted benzohydrazides: hydrogen-bonded structures in one, two and three dimensions ; _journal_coeditor_code GG3041 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o618 _journal_page_last o624 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.485 _cell_angle_gamma 90.000 _cell_length_a 7.5511 _cell_length_b 14.4834 _cell_length_c 8.3097 _exptl_crystal_F_000 416.00 _reflns_d_resolution_high 0.7699 _cod_data_source_file gg3041Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 0493' _shelx_refln_list_code 4 _shelx_f_calc_maximum 111.09 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2004.29 1974.80 31.85 o 4 0 0 709.45 675.37 12.45 o 6 0 0 6551.94 6553.28 108.78 o 8 0 0 83.33 80.29 5.69 o 1 1 0 1377.93 1328.98 25.37 o 2 1 0 3199.87 3053.40 34.53 o 3 1 0 26.22 24.75 0.88 o 4 1 0 18.97 15.73 1.01 o 5 1 0 844.20 825.47 10.94 o 6 1 0 1607.58 1608.26 21.39 o 7 1 0 55.32 57.23 2.30 o 8 1 0 384.64 395.91 9.06 o 9 1 0 2.90 6.05 4.77 o 1 2 0 608.13 575.44 8.78 o 2 2 0 5464.93 5332.21 64.59 o 3 2 0 491.20 554.56 7.26 o 4 2 0 2647.68 2570.92 28.58 o 5 2 0 54.05 53.52 1.56 o 6 2 0 6.36 4.47 1.29 o 7 2 0 15.67 16.68 1.46 o 8 2 0 98.27 95.92 5.47 o 9 2 0 6.13 6.24 3.04 o 1 3 0 754.89 733.17 8.47 o 2 3 0 32.09 28.08 0.89 o 3 3 0 285.48 303.26 4.98 o 4 3 0 352.47 311.09 4.58 o 5 3 0 403.60 402.12 6.11 o 6 3 0 51.94 50.37 1.81 o 7 3 0 40.37 36.41 1.85 o 8 3 0 0.87 2.32 3.26 o 9 3 0 111.78 119.67 22.23 o 0 4 0 5840.83 5394.16 77.64 o 1 4 0 731.85 764.34 8.97 o 2 4 0 2.44 6.18 0.45 o 3 4 0 1282.13 1131.50 15.11 o 4 4 0 388.36 423.26 5.96 o 5 4 0 12.43 9.81 0.92 o 6 4 0 971.63 999.94 13.04 o 7 4 0 40.18 39.01 2.51 o 8 4 0 21.66 19.18 4.27 o 1 5 0 608.55 594.44 6.81 o 2 5 0 1260.63 1289.74 14.69 o 3 5 0 175.66 180.03 3.33 o 4 5 0 1794.61 1898.43 26.83 o 5 5 0 0.30 0.55 0.55 o 6 5 0 7.08 7.22 0.89 o 7 5 0 429.58 443.85 8.03 o 8 5 0 110.59 124.39 6.91 o 0 6 0 2712.73 2653.88 38.99 o 1 6 0 5759.54 5484.16 55.70 o 2 6 0 392.23 413.31 5.29 o 3 6 0 68.38 56.78 1.32 o 4 6 0 69.50 84.68 2.33 o 5 6 0 995.01 1002.19 18.54 o 6 6 0 93.72 83.35 3.84 o 7 6 0 262.83 269.13 8.45 o 8 6 0 20.14 15.58 4.98 o 1 7 0 33.05 42.04 1.11 o 2 7 0 1079.26 996.50 11.84 o 3 7 0 686.77 717.23 11.41 o 4 7 0 140.89 135.42 2.44 o 5 7 0 494.07 524.89 10.08 o 6 7 0 234.12 200.62 6.53 o 7 7 0 190.24 214.64 7.72 o 8 7 0 257.61 265.98 11.15 o 0 8 0 293.68 325.62 5.98 o 1 8 0 2412.26 2564.32 26.07 o 2 8 0 194.46 195.04 3.17 o 3 8 0 3715.22 3768.16 44.10 o 4 8 0 9.25 9.98 1.04 o 5 8 0 121.48 103.37 3.40 o 6 8 0 3.92 3.97 2.49 o 7 8 0 182.97 172.71 7.05 o 8 8 0 12.46 13.03 4.30 o 1 9 0 316.97 343.53 4.28 o 2 9 0 528.54 527.79 6.93 o 3 9 0 36.42 38.00 1.51 o 4 9 0 677.48 702.29 10.20 o 5 9 0 440.56 413.88 9.20 o 6 9 0 7.59 4.09 2.56 o 7 9 0 22.00 19.47 3.90 o 8 9 0 58.80 42.93 6.02 o 0 10 0 59.57 56.74 2.28 o 1 10 0 1183.35 1210.78 14.10 o 2 10 0 399.76 381.75 5.56 o 3 10 0 34.34 34.92 1.83 o 4 10 0 677.10 693.24 9.99 o 5 10 0 378.29 382.92 10.04 o 6 10 0 5.93 8.91 3.28 o 7 10 0 332.28 359.81 14.74 o 1 11 0 14.02 12.56 1.04 o 2 11 0 2106.74 2157.57 26.43 o 3 11 0 13.59 14.43 1.25 o 4 11 0 853.44 868.94 13.91 o 5 11 0 24.22 29.00 2.98 o 6 11 0 39.09 43.48 4.39 o 7 11 0 16.83 23.81 4.81 o 0 12 0 1916.41 2027.47 36.85 o 1 12 0 19.89 17.49 1.60 o 2 12 0 99.56 103.91 2.59 o 3 12 0 1115.88 1161.66 16.18 o 4 12 0 0.03 -1.92 2.31 o 5 12 0 24.82 24.02 3.62 o 6 12 0 559.33 559.25 18.68 o 7 12 0 16.23 4.67 4.69 o 1 13 0 35.24 35.21 1.72 o 2 13 0 16.96 16.61 2.01 o 3 13 0 5.19 5.21 1.71 o 4 13 0 33.48 33.36 3.35 o 5 13 0 69.77 74.70 12.68 o 6 13 0 74.48 80.78 7.94 o 0 14 0 222.45 218.09 6.97 o 1 14 0 25.79 25.09 2.18 o 2 14 0 435.60 448.26 8.80 o 3 14 0 145.31 148.64 4.28 o 4 14 0 213.28 200.96 8.25 o 5 14 0 5.12 5.97 5.24 o 6 14 0 0.36 1.56 4.98 o 1 15 0 28.63 35.41 2.87 o 2 15 0 28.74 23.95 2.76 o 3 15 0 22.41 18.06 2.30 o 4 15 0 2.67 1.83 2.33 o 5 15 0 39.43 36.11 6.25 o 0 16 0 1131.84 1254.48 39.77 o 1 16 0 16.52 12.72 2.56 o 2 16 0 6.93 5.10 2.24 o 3 16 0 0.82 3.32 3.02 o 4 16 0 8.03 3.37 4.89 o 1 17 0 232.01 202.32 10.56 o 2 17 0 59.62 34.01 5.27 o 3 17 0 0.05 -4.08 10.65 o 0 18 0 12.42 16.99 10.19 o 1 18 0 158.95 151.31 14.27 o 2 18 0 199.52 214.96 17.67 o -9 0 1 61.47 45.08 9.51 o -7 0 1 105.31 98.77 4.13 o -5 0 1 641.19 666.32 11.67 o -3 0 1 1867.05 1906.66 25.35 o -1 0 1 1293.14 1397.58 31.71 o 1 0 1 288.09 245.62 6.47 o 3 0 1 454.87 409.97 8.80 o 5 0 1 158.30 160.35 4.38 o 7 0 1 90.88 99.79 5.59 o -9 1 1 211.99 202.20 7.28 o -8 1 1 212.47 208.22 5.01 o -7 1 1 341.33 334.86 5.71 o -6 1 1 354.07 350.30 5.26 o -5 1 1 763.41 745.90 9.50 o -4 1 1 2732.96 2748.21 28.86 o -3 1 1 1204.68 1099.32 11.97 o -2 1 1 471.51 461.19 5.21 o -1 1 1 23.73 24.19 0.99 o 1 1 1 5606.35 5162.16 72.45 o 2 1 1 2755.96 2483.61 35.61 o 3 1 1 686.96 635.73 9.42 o 4 1 1 520.74 514.26 8.17 o 5 1 1 20.21 20.46 1.40 o 6 1 1 6.31 8.16 1.47 o 7 1 1 948.94 940.83 14.04 o 8 1 1 190.84 200.84 7.69 o -9 2 1 386.15 427.48 12.83 o -8 2 1 8.59 12.46 1.80 o -7 2 1 29.18 26.07 1.80 o -6 2 1 415.44 411.74 6.32 o -5 2 1 126.46 136.41 2.62 o -4 2 1 296.77 341.94 4.86 o -3 2 1 1005.23 933.91 10.88 o -2 2 1 941.50 924.44 9.89 o -1 2 1 138.83 134.80 3.88 o 0 2 1 2511.72 2481.65 39.99 o 1 2 1 2365.24 2335.37 30.43 o 2 2 1 835.63 866.54 12.36 o 3 2 1 298.15 256.28 4.30 o 4 2 1 604.08 623.97 9.01 o 5 2 1 43.80 41.42 1.66 o 6 2 1 597.25 585.66 8.83 o 7 2 1 21.00 15.73 1.89 o 8 2 1 5.35 0.67 3.50 o -9 3 1 410.83 434.90 15.39 o -8 3 1 468.53 475.55 15.10 o -7 3 1 99.31 93.05 2.77 o -6 3 1 183.83 187.19 3.95 o -5 3 1 1.74 3.03 0.48 o -4 3 1 26.66 31.12 1.73 o -3 3 1 5920.59 5899.50 71.64 o -2 3 1 6097.23 5697.04 68.69 o -1 3 1 588.20 562.70 7.09 o 0 3 1 72.35 107.23 1.73 o 1 3 1 173.82 140.37 2.35 o 2 3 1 1174.74 1264.06 17.80 o 3 3 1 1327.61 1339.73 17.27 o 4 3 1 996.72 984.40 12.69 o 5 3 1 233.43 212.63 4.25 o 6 3 1 180.50 182.15 3.91 o 7 3 1 64.74 61.27 3.21 o 8 3 1 166.00 173.59 6.67 o -9 4 1 0.01 2.85 7.18 o -8 4 1 249.04 273.19 9.57 o -7 4 1 66.97 62.27 3.31 o -6 4 1 331.47 324.69 6.60 o -5 4 1 729.43 762.94 12.24 o -4 4 1 182.24 173.16 3.76 o -3 4 1 1617.88 1685.50 22.14 o -2 4 1 602.55 567.62 6.93 o -1 4 1 7.27 7.77 0.52 o 0 4 1 5989.20 5811.51 71.89 o 1 4 1 265.23 270.60 3.97 o 2 4 1 497.20 510.41 7.22 o 3 4 1 4169.23 4358.96 53.09 o 4 4 1 280.58 315.65 5.15 o 5 4 1 17.63 15.65 1.19 o 6 4 1 309.10 324.24 5.49 o 7 4 1 26.74 22.41 2.71 o 8 4 1 116.43 112.58 5.42 o -9 5 1 49.79 47.48 6.53 o -8 5 1 5.36 3.16 4.26 o -7 5 1 112.25 107.95 4.61 o -6 5 1 144.43 146.18 3.96 o -5 5 1 867.23 841.27 14.15 o -4 5 1 527.76 484.22 7.76 o -3 5 1 1768.81 1831.64 26.32 o -2 5 1 133.81 159.58 2.53 o -1 5 1 120.36 135.03 2.09 o 0 5 1 201.79 193.19 2.74 o 1 5 1 3720.23 3525.38 43.05 o 2 5 1 798.77 747.10 10.33 o 3 5 1 504.51 499.75 7.33 o 4 5 1 0.07 0.02 0.99 o 5 5 1 185.75 183.55 3.86 o 6 5 1 78.56 74.95 2.57 o 7 5 1 120.67 121.04 3.50 o 8 5 1 282.62 298.87 9.22 o -8 6 1 13.55 19.19 4.23 o -7 6 1 81.77 64.36 3.97 o -6 6 1 632.68 657.62 12.12 o -5 6 1 113.81 107.66 3.33 o -4 6 1 137.02 133.11 2.95 o -3 6 1 1116.02 1111.83 13.78 o -2 6 1 104.00 108.89 2.53 o -1 6 1 72.53 104.73 1.84 o 0 6 1 1943.93 1922.93 23.01 o 1 6 1 0.07 2.09 0.59 o 2 6 1 2.44 7.56 0.90 o 3 6 1 79.59 83.67 2.03 o 4 6 1 48.22 43.89 1.60 o 5 6 1 2.76 2.53 1.29 o 6 6 1 410.24 399.61 6.50 o 7 6 1 3.63 3.09 1.72 o 8 6 1 14.35 21.11 6.50 o -8 7 1 239.45 237.98 10.45 o -7 7 1 72.92 76.17 4.74 o -6 7 1 405.52 398.18 8.23 o -5 7 1 432.68 424.04 8.28 o -4 7 1 35.41 36.55 1.92 o -3 7 1 4.27 4.30 1.07 o -2 7 1 984.80 966.25 11.53 o -1 7 1 1548.86 1503.35 16.25 o 0 7 1 782.67 839.60 10.65 o 1 7 1 381.01 386.27 5.38 o 2 7 1 16.53 18.04 0.98 o 3 7 1 66.67 73.37 1.86 o 4 7 1 806.97 810.66 12.25 o 5 7 1 474.00 441.32 7.57 o 6 7 1 206.67 180.89 3.59 o 7 7 1 161.21 158.61 8.21 o 8 7 1 81.68 87.82 7.64 o -8 8 1 186.78 182.95 9.82 o -7 8 1 18.06 8.55 3.56 o -6 8 1 361.23 331.24 8.03 o -5 8 1 23.36 14.13 1.98 o -4 8 1 497.77 498.89 8.88 o -3 8 1 0.52 1.02 1.33 o -2 8 1 794.00 748.31 9.29 o -1 8 1 290.63 325.14 4.26 o 0 8 1 2108.69 2198.42 26.46 o 1 8 1 35.23 34.49 1.25 o 2 8 1 1324.99 1352.95 17.11 o 3 8 1 11.11 11.87 1.07 o 4 8 1 87.04 83.50 2.78 o 5 8 1 1.34 0.13 1.18 o 6 8 1 906.32 893.51 12.20 o 7 8 1 25.46 25.11 3.92 o -8 9 1 66.38 61.02 6.00 o -7 9 1 213.62 216.51 10.60 o -6 9 1 318.70 288.54 7.85 o -5 9 1 35.45 26.74 2.28 o -4 9 1 176.50 171.50 4.19 o -3 9 1 556.64 547.44 7.89 o -2 9 1 660.32 644.60 8.92 o -1 9 1 274.45 236.97 3.46 o 0 9 1 1057.15 1063.05 13.56 o 1 9 1 270.23 283.16 4.31 o 2 9 1 1155.15 1155.17 14.79 o 3 9 1 145.64 143.21 2.96 o 4 9 1 817.47 845.23 12.06 o 5 9 1 30.48 36.03 1.63 o 6 9 1 130.98 123.00 4.72 o 7 9 1 85.62 89.45 6.45 o -8 10 1 39.99 32.09 5.00 o -7 10 1 0.11 3.20 3.80 o -6 10 1 1044.86 1064.88 23.62 o -5 10 1 6.16 8.55 2.44 o -4 10 1 153.28 144.04 3.29 o -3 10 1 45.06 42.68 1.67 o -2 10 1 65.58 63.69 1.72 o -1 10 1 139.87 136.41 2.52 o 0 10 1 966.60 962.66 13.11 o 1 10 1 78.07 65.31 1.67 o 2 10 1 19.67 13.94 1.82 o 3 10 1 384.72 378.25 6.14 o 4 10 1 281.95 297.20 5.29 o 5 10 1 19.35 20.72 1.31 o 6 10 1 64.79 62.10 5.08 o 7 10 1 3.28 -3.48 4.24 o -7 11 1 12.18 12.89 5.29 o -6 11 1 132.68 136.67 8.47 o -5 11 1 240.11 264.97 6.85 o -4 11 1 1481.35 1575.41 21.32 o -3 11 1 1030.99 1069.80 18.84 o -2 11 1 631.87 625.34 8.39 o -1 11 1 0.30 0.74 1.06 o 0 11 1 821.71 813.61 11.51 o 1 11 1 339.57 326.80 5.16 o 2 11 1 1582.51 1589.90 19.74 o 3 11 1 27.74 27.85 1.59 o 4 11 1 160.89 160.01 3.68 o 5 11 1 0.97 -0.70 1.55 o 6 11 1 46.83 43.06 5.28 o 7 11 1 80.39 70.33 7.18 o -7 12 1 92.51 105.72 7.54 o -6 12 1 12.42 12.08 4.65 o -5 12 1 154.82 152.98 7.08 o -4 12 1 13.47 11.64 2.47 o -3 12 1 16.52 14.16 1.42 o -2 12 1 554.41 563.19 8.26 o -1 12 1 192.26 199.63 3.94 o 0 12 1 372.74 378.24 6.41 o 1 12 1 138.21 135.03 3.29 o 2 12 1 68.65 64.08 2.05 o 3 12 1 182.07 168.91 4.22 o 4 12 1 69.20 66.06 2.51 o 5 12 1 85.69 71.98 3.08 o 6 12 1 342.69 360.66 19.25 o -6 13 1 52.18 67.14 11.61 o -5 13 1 0.36 0.10 4.84 o -4 13 1 87.69 79.61 2.96 o -3 13 1 125.61 119.63 3.11 o -2 13 1 1882.34 1990.20 25.55 o -1 13 1 158.48 155.22 3.59 o 0 13 1 477.25 499.36 8.52 o 1 13 1 145.01 142.13 3.51 o 2 13 1 141.63 135.87 3.36 o 3 13 1 360.95 346.13 6.73 o 4 13 1 1223.06 1279.77 22.67 o 5 13 1 59.32 50.83 5.05 o 6 13 1 62.90 67.93 7.08 o -6 14 1 111.53 104.91 7.52 o -5 14 1 200.80 204.47 12.63 o -4 14 1 7.72 5.18 2.52 o -3 14 1 279.21 288.21 5.84 o -2 14 1 139.27 137.17 4.03 o -1 14 1 190.17 179.34 4.42 o 0 14 1 69.76 66.73 2.44 o 1 14 1 73.04 69.74 2.82 o 2 14 1 41.83 35.55 2.06 o 3 14 1 98.69 98.20 3.20 o 4 14 1 7.40 -1.89 4.32 o 5 14 1 67.40 68.00 7.33 o -5 15 1 75.76 79.14 8.01 o -4 15 1 194.32 182.20 7.16 o -3 15 1 349.21 342.10 7.87 o -2 15 1 342.48 364.73 7.65 o -1 15 1 6.89 3.96 2.03 o 0 15 1 35.30 34.92 2.81 o 1 15 1 765.66 780.66 14.79 o 2 15 1 328.51 332.93 9.17 o 3 15 1 294.34 277.60 10.59 o 4 15 1 190.06 200.08 8.14 o 5 15 1 3.31 13.59 11.33 o -5 16 1 500.63 526.93 23.83 o -4 16 1 0.95 6.06 5.86 o -3 16 1 23.71 23.52 4.40 o -2 16 1 2.96 3.97 2.91 o -1 16 1 194.23 192.37 5.52 o 0 16 1 1.70 2.89 2.87 o 1 16 1 568.13 591.46 14.05 o 2 16 1 7.65 8.03 3.15 o 3 16 1 172.90 176.31 8.30 o 4 16 1 6.09 7.36 6.08 o -4 17 1 544.93 569.24 25.67 o -3 17 1 178.10 178.50 17.67 o -2 17 1 1.58 -6.12 6.12 o -1 17 1 116.25 89.57 8.15 o 0 17 1 57.27 51.55 5.04 o 1 17 1 308.43 331.41 24.36 o 2 17 1 406.04 416.46 18.90 o 3 17 1 260.09 271.14 22.20 o -2 18 1 14.56 -11.33 11.33 o -1 18 1 12.80 13.82 11.10 o 0 18 1 4.70 10.14 6.20 o 1 18 1 16.13 19.03 12.68 o 2 18 1 117.91 99.67 14.50 o -8 0 2 541.13 555.98 14.76 o -6 0 2 53.55 49.90 2.46 o -4 0 2 966.59 936.47 14.76 o -2 0 2 12340.46 11867.09 184.11 o 0 0 2 345.45 315.61 8.32 o 2 0 2 3703.67 3536.50 82.01 o 4 0 2 3528.81 3548.79 70.40 o 6 0 2 497.81 507.98 11.66 o 8 0 2 196.84 201.31 12.16 o -9 1 2 4.50 6.64 2.45 o -8 1 2 443.88 468.77 12.46 o -7 1 2 1.28 0.27 1.73 o -6 1 2 0.09 0.90 0.96 o -5 1 2 2026.46 2012.30 21.69 o -4 1 2 1754.29 1715.40 18.80 o -3 1 2 39.99 56.81 1.06 o -2 1 2 2101.53 2084.77 23.79 o -1 1 2 437.29 452.89 5.67 o 0 1 2 4480.64 4254.78 66.47 o 1 1 2 6365.73 6184.76 96.73 o 2 1 2 281.46 324.81 5.71 o 3 1 2 189.25 219.37 4.31 o 4 1 2 42.12 44.36 2.20 o 5 1 2 287.38 273.39 5.79 o 6 1 2 527.99 551.57 9.33 o 7 1 2 173.98 166.74 5.30 o 8 1 2 3.95 2.72 3.30 o -9 2 2 36.19 29.90 3.63 o -8 2 2 6.70 5.22 2.47 o -7 2 2 228.29 225.55 4.53 o -6 2 2 3153.78 3233.41 42.04 o -5 2 2 235.07 233.33 3.85 o -4 2 2 39.02 40.80 1.05 o -3 2 2 162.93 152.68 2.29 o -2 2 2 2434.55 2360.46 25.46 o -1 2 2 142.92 150.81 2.31 o 1 2 2 1143.60 1145.98 17.00 o 2 2 2 758.74 758.56 11.83 o 3 2 2 512.28 494.72 8.51 o 4 2 2 828.23 876.99 13.42 o 5 2 2 384.67 377.13 7.33 o 6 2 2 1630.31 1683.08 24.64 o 7 2 2 210.84 209.60 5.69 o 8 2 2 17.77 14.21 3.31 o -9 3 2 8.16 8.19 3.72 o -8 3 2 541.28 581.86 14.01 o -7 3 2 842.11 887.41 13.39 o -6 3 2 633.19 626.55 8.75 o -5 3 2 0.07 0.50 0.63 o -4 3 2 24.49 40.16 1.09 o -3 3 2 821.93 780.07 13.30 o -2 3 2 2542.78 2552.81 31.78 o -1 3 2 11695.57 11032.49 283.72 o 0 3 2 1280.12 1334.36 18.18 o 1 3 2 173.81 195.08 3.65 o 2 3 2 7.79 3.76 1.06 o 3 3 2 151.89 142.34 3.24 o 4 3 2 14.10 11.04 2.18 o 5 3 2 442.72 433.18 7.38 o 6 3 2 56.71 59.13 2.35 o 7 3 2 159.65 163.95 4.77 o 8 3 2 48.20 54.54 10.95 o -9 4 2 206.75 222.91 15.48 o -8 4 2 142.04 149.03 6.74 o -7 4 2 0.09 -0.01 2.38 o -6 4 2 438.18 432.16 7.81 o -5 4 2 149.61 149.95 3.39 o -4 4 2 0.29 2.79 1.46 o -3 4 2 91.72 90.73 1.58 o -2 4 2 2282.22 2296.97 28.58 o -1 4 2 2263.10 2103.24 26.11 o 0 4 2 1110.17 1092.72 15.26 o 1 4 2 2158.42 2055.40 27.60 o 2 4 2 790.43 755.65 12.46 o 3 4 2 257.91 280.65 8.06 o 4 4 2 1012.48 1036.11 15.86 o 5 4 2 1687.88 1669.53 23.64 o 6 4 2 28.06 24.81 2.12 o 7 4 2 67.72 74.78 4.25 o 8 4 2 140.92 134.01 6.24 o -9 5 2 249.52 306.47 14.57 o -8 5 2 14.16 11.54 3.08 o -7 5 2 131.95 108.09 4.03 o -6 5 2 2.27 5.19 1.87 o -5 5 2 1215.53 1224.37 17.47 o -4 5 2 1584.64 1623.73 22.70 o -3 5 2 1995.32 2139.83 22.35 o -2 5 2 0.63 2.72 0.62 o -1 5 2 1777.64 1853.27 21.79 o 0 5 2 566.67 615.80 8.39 o 1 5 2 286.31 281.42 4.70 o 2 5 2 1850.96 1876.49 25.72 o 3 5 2 155.43 170.64 3.56 o 4 5 2 254.46 250.09 5.57 o 5 5 2 26.04 31.53 3.09 o 6 5 2 72.08 56.46 2.54 o 7 5 2 62.84 62.89 3.16 o 8 5 2 105.21 94.48 6.15 o -9 6 2 115.30 92.04 6.82 o -8 6 2 33.09 38.60 3.71 o -7 6 2 21.17 19.19 2.62 o -6 6 2 74.07 90.70 3.13 o -5 6 2 135.78 135.47 3.36 o -4 6 2 10.89 11.75 1.36 o -3 6 2 1800.69 1727.78 18.32 o -2 6 2 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