#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/56/2015610.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015610_Fobs loop_ _publ_author_name 'Wardell, Solange M. S. V.' 'Vasconcelos, Thatyana R. A.' 'de Souza, Marcus V. N.' 'Wardell, James L.' 'Low, John N.' 'Glidewell, Christopher' _publ_section_title ; Four substituted benzohydrazides: hydrogen-bonded structures in one, two and three dimensions ; _journal_coeditor_code GG3041 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o618 _journal_page_last o624 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.106 _cell_angle_gamma 90.000 _cell_length_a 15.1188 _cell_length_b 3.8801 _cell_length_c 13.6029 _exptl_crystal_F_000 416.00 _reflns_d_resolution_high 0.7650 _[local]_cod_data_source_file gg3041IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1595 P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 134.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 702.56 709.53 23.74 o 4 0 0 6316.47 5830.82 172.33 o 5 0 0 643.33 706.76 23.33 o 6 0 0 372.54 388.30 19.44 o 7 0 0 9919.54 10528.79 302.01 o 8 0 0 8677.13 9291.96 195.28 o 9 0 0 52.33 43.11 8.34 o 10 0 0 415.58 405.29 17.26 o 11 0 0 2211.51 2371.49 69.07 o 12 0 0 429.17 431.56 19.68 o 13 0 0 303.16 291.72 19.70 o 14 0 0 758.79 818.46 49.49 o 15 0 0 665.70 826.64 59.05 o 16 0 0 10.14 20.67 25.89 o 17 0 0 38.82 64.55 25.80 o 18 0 0 1025.69 983.42 108.48 o 19 0 0 484.08 476.19 72.31 o 1 1 0 333.98 270.41 5.57 o 2 1 0 7854.59 7409.26 135.75 o 3 1 0 413.52 344.06 9.77 o 4 1 0 539.63 517.00 11.49 o 5 1 0 873.61 852.05 21.78 o 6 1 0 489.08 632.31 13.25 o 7 1 0 1086.45 1064.40 21.10 o 8 1 0 2377.70 2326.71 38.51 o 9 1 0 214.75 236.98 7.55 o 10 1 0 469.60 476.70 21.48 o 11 1 0 23.54 26.25 6.07 o 12 1 0 769.44 815.29 27.98 o 13 1 0 121.98 89.88 9.65 o 14 1 0 166.01 131.87 12.21 o 15 1 0 2.11 6.58 21.50 o 16 1 0 717.95 713.29 43.63 o 17 1 0 53.65 69.65 34.82 o 18 1 0 1.31 -1.00 48.10 o 19 1 0 214.56 207.26 54.60 o 0 2 0 1075.68 1088.59 26.09 o 1 2 0 128.91 109.49 4.71 o 2 2 0 516.65 460.77 11.42 o 3 2 0 68.47 60.87 6.26 o 4 2 0 0.82 2.60 6.52 o 5 2 0 713.13 707.08 13.72 o 6 2 0 415.68 398.86 11.13 o 7 2 0 19.76 9.44 6.58 o 8 2 0 327.27 323.07 13.40 o 9 2 0 1173.21 1185.61 33.09 o 10 2 0 0.28 -2.14 7.76 o 11 2 0 71.30 72.23 9.81 o 12 2 0 2.77 -10.67 10.67 o 13 2 0 278.18 265.68 25.54 o 14 2 0 408.19 411.05 66.60 o 15 2 0 160.20 165.10 34.95 o 16 2 0 208.81 225.30 45.28 o 17 2 0 61.19 80.05 66.21 o 18 2 0 10.26 14.96 36.74 o 1 3 0 115.00 102.71 5.95 o 2 3 0 13.84 19.59 5.01 o 3 3 0 417.57 433.17 13.50 o 4 3 0 110.80 100.69 7.26 o 5 3 0 13.37 16.84 6.17 o 6 3 0 136.45 130.91 11.20 o 7 3 0 48.18 43.94 5.35 o 8 3 0 582.09 578.20 22.97 o 9 3 0 0.02 -6.36 7.99 o 10 3 0 203.23 199.13 16.90 o 11 3 0 0.03 -6.05 18.35 o 12 3 0 2.79 16.62 27.44 o 13 3 0 34.02 50.91 26.10 o 14 3 0 295.04 258.00 38.59 o 15 3 0 70.29 140.39 28.48 o 0 4 0 0.31 -16.07 16.07 o 1 4 0 188.69 225.46 12.56 o 2 4 0 719.28 757.33 30.79 o 3 4 0 140.20 140.63 12.09 o 4 4 0 6.41 -5.01 7.99 o 5 4 0 406.20 431.16 22.52 o 6 4 0 723.63 767.40 28.84 o 7 4 0 94.27 90.61 16.61 o 8 4 0 78.16 45.21 19.35 o 9 4 0 146.36 145.00 53.03 o 10 4 0 19.51 15.04 22.65 o 11 4 0 52.96 58.53 20.60 o 1 5 0 0.06 4.00 18.33 o 2 5 0 24.38 7.90 21.40 o -19 1 1 5.05 -31.77 31.77 o -18 1 1 1.61 16.56 38.20 o -17 1 1 82.33 104.12 28.01 o -16 1 1 143.48 138.34 14.47 o -15 1 1 157.81 157.65 33.81 o -14 1 1 90.64 72.69 10.06 o -13 1 1 395.02 426.44 17.55 o -12 1 1 213.11 210.98 13.57 o -11 1 1 77.24 75.04 7.94 o -10 1 1 489.07 549.50 15.31 o -9 1 1 322.34 340.53 16.17 o -8 1 1 3.13 3.63 4.33 o -7 1 1 171.32 192.66 7.09 o -6 1 1 1169.85 1271.10 22.88 o -5 1 1 191.19 182.28 6.36 o -4 1 1 173.05 178.21 6.43 o -3 1 1 1283.38 1298.45 26.59 o -2 1 1 6529.32 6141.32 108.62 o -1 1 1 240.05 204.32 6.36 o 0 1 1 3840.10 3683.24 65.77 o 1 1 1 7225.27 6788.50 100.57 o 2 1 1 533.58 523.39 11.68 o 3 1 1 1506.63 1399.86 27.63 o 4 1 1 64.47 66.15 4.94 o 5 1 1 1414.57 1488.82 39.92 o 6 1 1 2698.43 2788.53 65.48 o 7 1 1 227.31 251.85 9.15 o 8 1 1 285.54 306.59 8.67 o 9 1 1 390.47 411.08 10.60 o 10 1 1 822.23 900.67 27.79 o 11 1 1 183.03 173.40 8.97 o 12 1 1 406.35 392.07 17.51 o 13 1 1 45.26 57.68 8.09 o 14 1 1 74.88 54.33 11.09 o 15 1 1 144.54 100.98 13.10 o 16 1 1 133.89 157.56 37.00 o 17 1 1 256.68 311.93 43.58 o 18 1 1 40.78 44.77 32.48 o 19 1 1 146.51 174.07 39.51 o -18 2 1 317.49 325.67 48.10 o -17 2 1 180.46 199.88 42.29 o -16 2 1 110.38 94.01 32.21 o -15 2 1 142.18 105.29 24.08 o -14 2 1 212.89 209.63 30.02 o -13 2 1 776.77 830.02 35.55 o -12 2 1 38.81 51.35 12.87 o -11 2 1 482.76 481.49 30.39 o -10 2 1 947.98 1013.20 32.21 o -9 2 1 482.43 510.04 17.22 o -8 2 1 67.29 66.84 4.86 o -7 2 1 931.70 921.38 20.85 o -6 2 1 943.06 908.58 21.74 o -5 2 1 438.92 468.38 10.92 o -4 2 1 48.92 58.62 4.82 o -3 2 1 954.45 944.83 18.14 o -2 2 1 4927.34 4944.83 85.58 o -1 2 1 42.94 41.23 3.80 o 0 2 1 1693.80 1669.32 22.49 o 1 2 1 598.29 564.27 10.36 o 2 2 1 779.43 765.19 16.11 o 3 2 1 36.91 34.55 4.14 o 4 2 1 23.50 15.44 4.26 o 5 2 1 2800.67 2978.99 56.72 o 6 2 1 761.86 836.32 20.43 o 7 2 1 0.35 -5.87 5.87 o 8 2 1 787.67 786.68 25.99 o 9 2 1 69.54 63.59 9.72 o 10 2 1 106.98 114.38 10.22 o 11 2 1 60.54 54.27 10.58 o 12 2 1 840.00 766.62 30.47 o 13 2 1 209.92 232.28 18.83 o 14 2 1 47.23 59.23 19.71 o 15 2 1 4.11 72.64 28.34 o 16 2 1 179.18 208.14 34.15 o 17 2 1 2.28 40.49 52.75 o -15 3 1 0.40 37.10 32.94 o -14 3 1 0.05 9.79 24.48 o -13 3 1 82.68 26.87 52.31 o -12 3 1 75.10 110.62 69.07 o -11 3 1 82.73 98.31 15.44 o -10 3 1 3.20 17.18 9.52 o -9 3 1 532.63 553.94 22.88 o -8 3 1 0.68 0.21 4.98 o -7 3 1 28.13 26.10 5.60 o -6 3 1 81.18 75.50 7.26 o -5 3 1 513.41 503.75 16.69 o -4 3 1 19.22 8.77 7.08 o -3 3 1 10.13 13.24 8.69 o -2 3 1 351.31 342.90 11.41 o -1 3 1 408.01 429.32 11.42 o 0 3 1 45.20 44.60 5.68 o 1 3 1 35.63 35.21 5.43 o 2 3 1 38.35 44.68 5.92 o 3 3 1 93.26 104.05 7.57 o 4 3 1 34.74 34.68 5.81 o 5 3 1 346.87 340.62 12.83 o 6 3 1 622.21 655.29 20.48 o 7 3 1 179.66 150.25 8.01 o 8 3 1 45.41 55.35 8.76 o 9 3 1 465.14 475.82 22.50 o 10 3 1 261.39 224.68 19.27 o 11 3 1 46.44 25.05 24.72 o 12 3 1 2.64 7.77 18.47 o 13 3 1 390.94 348.76 43.18 o 14 3 1 62.21 69.72 24.80 o 15 3 1 397.52 472.34 48.31 o -11 4 1 46.14 96.63 42.01 o -10 4 1 139.68 98.59 22.26 o -9 4 1 188.56 168.36 34.83 o -8 4 1 622.24 630.15 42.70 o -7 4 1 49.48 35.37 12.26 o -6 4 1 288.00 302.80 19.56 o -5 4 1 118.29 136.66 12.05 o -4 4 1 716.53 793.58 45.86 o -3 4 1 20.16 3.61 15.98 o -2 4 1 7.46 6.71 7.35 o -1 4 1 382.15 404.33 16.73 o 0 4 1 24.84 25.84 7.59 o 1 4 1 119.64 104.74 14.03 o 2 4 1 22.31 25.01 8.75 o 3 4 1 865.73 968.28 30.70 o 4 4 1 2.47 10.42 8.17 o 5 4 1 15.34 8.61 8.56 o 6 4 1 39.40 45.84 11.16 o 7 4 1 117.94 145.84 20.09 o 8 4 1 95.32 106.34 23.08 o 9 4 1 87.24 73.55 27.05 o 10 4 1 80.22 69.49 20.81 o 11 4 1 79.44 84.79 30.63 o -2 5 1 55.22 63.84 22.83 o -1 5 1 3.09 -4.08 18.54 o 0 5 1 300.35 319.43 31.74 o 1 5 1 26.10 10.29 21.33 o 2 5 1 7.79 23.75 28.12 o -19 0 2 6.47 3.55 42.00 o -18 0 2 0.27 34.19 75.70 o -17 0 2 192.96 206.50 34.02 o -16 0 2 491.42 518.26 44.14 o -15 0 2 1.24 27.75 18.92 o -14 0 2 1717.90 1719.99 156.34 o -13 0 2 2152.65 2360.93 103.83 o -12 0 2 67.46 71.36 12.09 o -11 0 2 25.81 26.56 11.97 o -10 0 2 142.84 164.66 11.14 o -9 0 2 228.27 187.11 10.78 o -8 0 2 67.13 64.00 6.89 o -7 0 2 39.11 64.53 5.86 o -6 0 2 54.08 61.91 5.97 o -5 0 2 6453.13 6154.66 173.31 o -4 0 2 1480.86 1433.59 34.91 o -3 0 2 808.77 748.48 23.11 o -2 0 2 327.54 277.91 8.28 o 0 0 2 35.91 24.44 4.97 o 2 0 2 2010.38 1844.42 76.57 o 3 0 2 2321.47 2211.52 109.07 o 4 0 2 6029.34 5866.95 243.21 o 5 0 2 525.55 556.45 28.40 o 6 0 2 695.17 604.43 51.80 o 7 0 2 2494.21 2642.68 100.70 o 8 0 2 40.77 97.24 16.89 o 9 0 2 216.39 232.50 15.14 o 10 0 2 1828.15 1901.50 53.44 o 11 0 2 849.95 888.22 32.54 o 12 0 2 16.95 24.04 12.08 o 13 0 2 105.93 110.36 15.64 o 14 0 2 32.86 19.19 10.99 o 15 0 2 470.49 492.53 107.17 o 16 0 2 35.88 24.52 19.45 o 17 0 2 42.28 30.43 47.87 o 18 0 2 24.32 -35.01 42.11 o 19 0 2 66.81 46.69 64.71 o -19 1 2 312.63 275.68 61.47 o -18 1 2 115.48 99.33 36.85 o -17 1 2 3.31 -32.48 54.47 o -16 1 2 19.79 -4.15 12.19 o -15 1 2 539.55 539.34 31.76 o -14 1 2 34.65 39.97 10.46 o -13 1 2 17.96 12.23 7.88 o -12 1 2 1898.87 1953.79 57.10 o -11 1 2 31.74 29.96 6.03 o -10 1 2 0.29 0.19 4.94 o -9 1 2 699.30 776.72 22.59 o -8 1 2 2391.97 2502.93 42.79 o -7 1 2 1729.26 1744.15 31.04 o -6 1 2 1244.47 1173.71 21.87 o -5 1 2 1719.75 1682.62 29.74 o -4 1 2 2275.47 2159.07 35.95 o -3 1 2 1207.09 1279.62 24.08 o -2 1 2 0.12 5.58 1.90 o -1 1 2 17964.07 16854.62 252.87 o 0 1 2 2895.02 2803.04 42.82 o 1 1 2 895.54 903.31 14.81 o 2 1 2 2179.31 2125.30 35.92 o 3 1 2 12266.03 11435.77 166.14 o 4 1 2 11.16 10.00 3.06 o 5 1 2 1164.78 1163.50 37.15 o 6 1 2 1602.56 1640.13 35.28 o 7 1 2 2983.56 3108.52 48.85 o 8 1 2 229.40 242.50 6.18 o 9 1 2 5.34 7.75 4.65 o 10 1 2 914.99 912.83 23.65 o 11 1 2 2248.51 2391.64 59.64 o 12 1 2 109.38 106.51 10.00 o 13 1 2 14.79 -3.14 6.70 o 14 1 2 407.85 482.44 37.77 o 15 1 2 80.96 57.79 12.35 o 16 1 2 1.41 15.28 20.25 o 17 1 2 124.33 99.00 36.41 o 18 1 2 714.35 692.85 88.09 o 19 1 2 6.85 9.38 39.45 o -17 2 2 53.43 78.02 23.49 o -16 2 2 42.04 60.13 26.05 o -15 2 2 0.63 8.26 19.49 o -14 2 2 247.05 261.29 28.59 o -13 2 2 145.82 180.31 20.18 o -12 2 2 133.17 128.58 12.53 o -11 2 2 749.63 763.26 33.23 o -10 2 2 253.96 252.56 11.54 o -9 2 2 503.71 495.79 14.53 o -8 2 2 179.84 193.23 9.53 o -7 2 2 118.96 105.90 6.44 o -6 2 2 216.61 208.64 8.73 o -5 2 2 3605.29 3684.55 61.19 o -4 2 2 913.83 891.66 16.97 o -3 2 2 1640.29 1647.26 37.58 o -2 2 2 209.28 250.86 10.56 o -1 2 2 775.86 816.21 17.65 o 0 2 2 155.91 181.99 7.96 o 1 2 2 850.79 855.77 14.62 o 2 2 2 1420.09 1433.21 25.19 o 3 2 2 8.91 8.45 4.37 o 4 2 2 697.57 706.64 14.14 o 5 2 2 22.03 8.39 3.82 o 6 2 2 123.70 120.26 7.73 o 7 2 2 193.81 181.89 14.48 o 8 2 2 170.24 172.49 10.47 o 9 2 2 38.57 37.87 8.74 o 10 2 2 219.75 222.94 18.94 o 11 2 2 680.07 679.96 27.82 o 12 2 2 23.14 14.87 11.67 o 13 2 2 1006.62 968.33 48.69 o 14 2 2 10.87 -17.68 17.68 o 15 2 2 636.35 728.75 91.99 o 16 2 2 0.48 -23.76 26.66 o 17 2 2 30.07 38.10 36.40 o -15 3 2 221.66 210.69 32.07 o -14 3 2 311.76 345.07 39.97 o -13 3 2 579.30 595.36 46.29 o -12 3 2 73.50 36.80 20.04 o -11 3 2 108.55 93.31 14.95 o -10 3 2 670.57 615.16 27.97 o -9 3 2 0.15 5.88 8.79 o -8 3 2 37.07 37.15 6.84 o -7 3 2 450.67 448.03 15.91 o -6 3 2 2057.79 2235.74 57.78 o -5 3 2 318.73 356.46 12.29 o -4 3 2 300.94 288.79 11.70 o -3 3 2 1167.08 1150.01 40.31 o -2 3 2 163.00 150.38 13.81 o -1 3 2 81.74 88.66 6.94 o 0 3 2 13.95 13.00 4.94 o 1 3 2 1934.88 2114.97 43.66 o 2 3 2 1107.24 1158.90 30.78 o 3 3 2 1.15 6.08 5.83 o 4 3 2 1145.70 1210.18 33.40 o 5 3 2 386.16 372.57 13.52 o 6 3 2 516.63 514.99 17.15 o 7 3 2 150.67 148.72 11.24 o 8 3 2 494.30 504.53 20.68 o 9 3 2 629.33 634.07 31.52 o 10 3 2 48.42 62.42 13.05 o 11 3 2 0.04 6.43 12.95 o 12 3 2 494.44 462.59 29.15 o 13 3 2 256.06 207.91 28.24 o 14 3 2 196.37 137.57 26.87 o 15 3 2 517.59 529.35 58.29 o -11 4 2 114.79 88.60 31.47 o -10 4 2 27.95 41.30 27.69 o -9 4 2 2.18 -7.23 38.59 o -8 4 2 3.63 -14.44 14.44 o -7 4 2 8.13 18.81 11.83 o -6 4 2 29.02 11.67 9.25 o -5 4 2 24.17 21.48 10.72 o -4 4 2 196.28 178.09 14.60 o -3 4 2 9.82 25.16 10.07 o -2 4 2 0.21 2.18 7.69 o -1 4 2 6.51 7.68 9.01 o 0 4 2 10.53 16.98 8.23 o 1 4 2 6.80 14.60 7.98 o 2 4 2 147.16 143.85 12.36 o 3 4 2 40.60 24.57 8.25 o 4 4 2 71.78 70.49 10.11 o 5 4 2 44.09 50.39 10.64 o 6 4 2 2.81 13.84 12.14 o 7 4 2 1.00 29.28 16.02 o 8 4 2 68.42 2.77 62.08 o 9 4 2 11.08 -0.92 19.32 o 10 4 2 63.95 84.50 32.04 o 11 4 2 0.19 -12.46 33.90 o 0 5 2 3.87 2.95 20.39 o 1 5 2 0.02 10.61 20.06 o -19 1 3 144.20 71.37 31.39 o -18 1 3 85.80 117.02 32.93 o -17 1 3 122.03 129.32 53.97 o -16 1 3 13.66 -3.80 13.45 o -15 1 3 468.75 445.67 33.00 o -14 1 3 663.95 650.11 28.00 o -13 1 3 2.83 5.98 7.40 o -12 1 3 454.59 475.12 17.51 o -11 1 3 10.32 8.29 5.40 o -10 1 3 1118.26 1221.03 29.11 o -9 1 3 533.99 534.32 15.43 o -8 1 3 577.42 593.72 13.08 o -7 1 3 994.24 917.70 19.11 o -6 1 3 322.44 320.84 7.73 o -5 1 3 480.04 508.77 10.50 o -4 1 3 36.99 25.03 3.18 o -3 1 3 613.73 512.43 10.49 o -2 1 3 1257.83 1289.29 20.73 o -1 1 3 5479.87 5161.22 73.01 o 0 1 3 534.76 481.23 9.30 o 1 1 3 1055.47 959.78 16.07 o 2 1 3 117.84 121.07 4.56 o 3 1 3 14.36 17.32 2.77 o 4 1 3 2751.04 2618.94 51.88 o 5 1 3 621.74 650.00 16.31 o 6 1 3 758.59 856.74 20.86 o 7 1 3 350.62 363.79 11.20 o 8 1 3 313.76 294.98 9.93 o 9 1 3 597.01 613.43 16.67 o 10 1 3 86.49 103.09 9.77 o 11 1 3 353.27 337.95 12.59 o 12 1 3 608.63 575.60 23.39 o 13 1 3 520.82 481.10 21.39 o 14 1 3 4.91 -9.20 10.80 o 15 1 3 104.57 82.16 16.56 o 16 1 3 80.80 73.39 12.09 o 17 1 3 28.02 42.46 26.35 o 18 1 3 69.90 110.37 36.49 o -17 2 3 377.58 366.30 50.31 o -16 2 3 218.22 207.74 28.49 o -15 2 3 72.33 54.52 22.93 o -14 2 3 211.58 193.81 27.75 o -13 2 3 41.00 88.60 18.22 o -12 2 3 27.73 29.93 10.07 o -11 2 3 45.48 34.19 9.59 o -10 2 3 365.65 368.13 17.52 o -9 2 3 1243.61 1301.38 35.20 o -8 2 3 0.02 -0.91 5.72 o -7 2 3 2.88 1.55 4.48 o -6 2 3 669.44 657.76 17.03 o -5 2 3 12.76 8.48 3.87 o -4 2 3 428.36 434.43 9.70 o -3 2 3 1553.88 1586.79 28.94 o -2 2 3 2088.63 2107.47 35.26 o -1 2 3 1.75 2.43 2.41 o 0 2 3 60.32 58.60 4.14 o 1 2 3 114.79 98.39 5.33 o 2 2 3 1556.40 1563.99 25.71 o 3 2 3 112.65 121.59 6.51 o 4 2 3 1837.29 1967.39 35.33 o 5 2 3 2387.07 2457.26 50.03 o 6 2 3 3.07 5.09 7.05 o 7 2 3 2.20 4.15 6.12 o 8 2 3 123.92 111.88 11.04 o 9 2 3 1422.21 1466.29 46.64 o 10 2 3 93.11 94.03 11.13 o 11 2 3 122.39 135.95 15.83 o 12 2 3 633.39 772.60 41.29 o 13 2 3 334.11 361.61 39.95 o 14 2 3 22.23 -0.07 21.90 o 15 2 3 21.48 -11.45 25.54 o 16 2 3 469.57 431.07 44.87 o 17 2 3 199.08 239.03 162.70 o -15 3 3 86.31 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