#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/56/2015622.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015622_Fobs loop_ _publ_author_name 'Eisenberg, Richard' 'Brennessel, William W.' _publ_section_title ; Redetermination of the trigonal prismatic complex tris(cis-1,2-diphenylethylene-1,2-dithiolato)rhenium ; _journal_coeditor_code SQ3033 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m464 _journal_page_last m466 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 80.190 _cell_angle_beta 76.770 _cell_angle_gamma 68.758 _cell_length_a 9.7949 _cell_length_b 10.8765 _cell_length_c 19.4517 _exptl_crystal_F_000 906.00 _reflns_d_resolution_high 0.7200 _[local]_cod_data_source_file sq3033Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' eisre01 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 284.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 38.21 45.11 6.09 o 2 0 0 14732.87 13038.39 372.94 o 3 0 0 782.37 737.04 39.21 o 4 0 0 5221.32 5196.41 120.77 o 5 0 0 143.87 157.68 24.99 o 6 0 0 4631.03 4177.18 154.47 o 7 0 0 41.53 43.50 44.42 o 8 0 0 4481.06 4487.09 110.61 o 9 0 0 4823.00 4857.50 123.35 o 10 0 0 2500.47 2533.33 277.08 o 11 0 0 225.55 166.06 97.27 o 12 0 0 901.54 685.72 168.03 o -12 1 0 1035.71 1629.08 202.10 o -11 1 0 76.76 -8.04 106.86 o -10 1 0 2463.80 2568.20 129.45 o -9 1 0 1791.25 1774.34 90.60 o -8 1 0 6954.24 7229.77 185.30 o -7 1 0 508.63 530.41 43.09 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