#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/56/2015630.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015630_Fobs loop_ _publ_author_name 'Pritchard, Robin G.' 'Ali, Majid' 'Munim, Abdul' 'Uddin, Asma' _publ_section_title ; Effects of d-orbital occupancy on the geometry of the trigonal--bipyramidal complexes [M^II^Cl~3~(Hdabco)(dabco)]~n~, where M is Mn, Co, Ni or Cu and dabco is 1,4-diazabicyclo[2.2.2]octane ; _journal_coeditor_code BC3016 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m507 _journal_page_last m509 _journal_volume 62 _journal_year 2006 _space_group_IT_number 155 _symmetry_space_group_name_Hall 'R 3 2"' _symmetry_space_group_name_H-M 'R 3 2 :H' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 10.5409 _cell_length_b 10.5409 _cell_length_c 12.3030 _exptl_crystal_F_000 609.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file bc3016IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' rgp38a in R 3 2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 223.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'x-y, -y, -z' '-x, -x+y, -z' 'y, x, -z' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'x-y+2/3, -y+1/3, -z+1/3' '-x+2/3, -x+y+1/3, -z+1/3' 'y+2/3, x+1/3, -z+1/3' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' 'x-y+1/3, -y+2/3, -z+2/3' '-x+1/3, -x+y+2/3, -z+2/3' 'y+1/3, x+2/3, -z+2/3' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 44874.43 44707.48 316.28 o -1 2 0 45066.79 44197.71 182.42 o 2 2 0 1935.36 1913.77 45.56 o 0 3 0 5571.47 5830.75 49.55 o 3 3 0 14519.17 14941.64 282.87 o -2 4 0 2360.42 2494.00 69.60 o 1 4 0 16677.89 17342.54 97.97 o 4 4 0 7666.39 7640.99 170.94 o -1 5 0 17277.13 17935.91 418.75 o 2 5 0 3656.18 3703.84 51.98 o 5 5 0 4817.62 4853.73 115.98 o -3 6 0 15340.28 15852.03 204.49 o 0 6 0 9604.31 9416.94 87.91 o 3 6 0 4520.67 4349.26 75.42 o 6 6 0 991.93 897.95 78.37 o -2 7 0 3621.33 3779.22 74.47 o 1 7 0 6506.72 6583.81 87.13 o 4 7 0 299.52 342.91 40.75 o -4 8 0 7602.86 7510.22 173.12 o -1 8 0 6367.06 6492.55 122.07 o 2 8 0 2241.19 2251.91 62.89 o -3 9 0 4319.02 4281.99 134.47 o 0 9 0 10029.32 9987.07 117.02 o 3 9 0 555.27 528.84 50.55 o -5 10 0 4578.30 4477.08 162.85 o -2 10 0 2294.28 2372.24 94.35 o 1 10 0 563.65 601.05 48.31 o -4 11 0 340.41 308.98 74.54 o -1 11 0 516.89 559.21 103.40 o -6 12 0 836.49 696.19 105.73 o -3 12 0 599.97 628.13 87.99 o -3 2 1 10063.47 10494.23 60.37 o 0 2 1 738.74 774.36 31.02 o -5 3 1 969.13 970.09 29.52 o -2 3 1 9164.95 9702.45 82.94 o 1 3 1 11845.48 12042.96 73.20 o -7 4 1 530.84 486.60 28.42 o -4 4 1 9537.83 9343.72 69.92 o -1 4 1 11535.72 11727.81 102.61 o 2 4 1 2561.59 2476.33 51.78 o -9 5 1 5493.64 5455.74 82.23 o -6 5 1 2319.35 2233.44 58.07 o -3 5 1 1070.62 1125.05 42.26 o 0 5 1 18812.56 18690.49 122.58 o 3 5 1 1164.76 1049.03 38.27 o -11 6 1 555.28 583.36 54.26 o -8 6 1 4302.86 4078.15 69.42 o -5 6 1 2084.89 2198.60 55.90 o -2 6 1 2782.62 2649.23 114.67 o 1 6 1 1107.59 1080.58 35.84 o 4 6 1 1286.84 1282.00 51.14 o -10 7 1 745.57 780.28 46.45 o -7 7 1 101.96 77.93 28.50 o -4 7 1 665.33 653.93 42.11 o -1 7 1 880.04 818.66 46.97 o 2 7 1 235.69 311.07 36.95 o 5 7 1 367.65 405.29 49.03 o -12 8 1 814.26 789.31 65.15 o -9 8 1 2543.28 2523.84 63.89 o -6 8 1 3848.94 3655.00 203.35 o -3 8 1 1205.12 1091.92 53.85 o 0 8 1 1239.45 1336.93 81.01 o 3 8 1 1138.61 1199.44 77.14 o -11 9 1 216.45 185.26 42.02 o -8 9 1 2455.52 2451.73 160.40 o -5 9 1 5446.49 5574.97 116.97 o -2 9 1 367.46 435.01 56.10 o 1 9 1 2346.30 2277.15 67.06 o -10 10 1 1059.06 1218.45 55.82 o -7 10 1 821.81 857.84 70.27 o -4 10 1 1501.37 1581.11 152.28 o -1 10 1 2453.52 2535.68 97.66 o -9 11 1 248.44 217.49 61.86 o -6 11 1 494.50 516.99 63.01 o -3 11 1 1377.70 1371.63 83.04 o -8 12 1 861.80 808.25 74.51 o -5 12 1 253.56 239.24 114.94 o 0 1 2 303.70 393.32 23.48 o -2 2 2 53.87 42.52 24.90 o 1 2 2 14036.34 14527.02 72.23 o -4 3 2 16198.88 16477.11 87.20 o -1 3 2 13030.98 13283.27 180.77 o 2 3 2 2413.02 2511.33 37.99 o -6 4 2 1924.64 1839.74 37.84 o -3 4 2 15635.60 16082.73 361.28 o 0 4 2 15015.96 15101.03 88.25 o 3 4 2 498.51 470.19 29.11 o -8 5 2 1323.95 1349.73 46.91 o -5 5 2 18075.66 18087.44 181.66 o -2 5 2 2173.61 2257.87 52.24 o 1 5 2 2638.23 2612.37 42.65 o 4 5 2 6299.79 6219.55 86.95 o -10 6 2 2232.18 2304.91 61.91 o -7 6 2 1266.77 1248.11 45.00 o -4 6 2 1932.03 2012.88 58.38 o -1 6 2 2376.55 2337.84 59.29 o 2 6 2 2685.16 2670.86 60.07 o 5 6 2 650.15 724.11 48.16 o -12 7 2 242.63 190.62 46.06 o -9 7 2 191.31 216.72 35.66 o -6 7 2 987.10 978.85 50.87 o -3 7 2 548.45 528.65 43.10 o 0 7 2 102.92 55.40 46.90 o 3 7 2 1001.47 954.34 55.64 o -11 8 2 901.74 841.64 50.99 o -8 8 2 268.08 299.32 37.29 o -5 8 2 1344.71 1345.63 65.68 o -2 8 2 2303.83 2230.40 81.79 o 1 8 2 1178.47 1172.18 50.65 o 4 8 2 703.97 741.51 52.44 o -10 9 2 1683.51 1746.63 60.86 o -7 9 2 319.33 294.10 55.74 o -4 9 2 6394.19 6346.21 164.32 o -1 9 2 1141.52 1179.66 72.60 o 2 9 2 233.22 232.96 48.86 o -9 10 2 1750.23 1757.99 116.94 o -6 10 2 2501.78 2530.56 92.71 o -3 10 2 1161.19 1147.89 72.38 o 0 10 2 1222.46 1369.16 57.56 o -8 11 2 1101.87 1161.01 75.86 o -5 11 2 671.73 569.53 89.75 o -2 11 2 228.42 171.49 60.17 o -7 12 2 169.07 126.16 82.28 o -4 12 2 726.82 780.72 77.38 o 0 0 3 49787.95 49125.07 204.64 o 1 1 3 5684.65 5991.63 49.64 o -1 2 3 5206.93 5501.27 72.81 o 2 2 3 1336.73 1321.02 30.60 o -3 3 3 1051.43 1035.88 28.38 o 0 3 3 1537.36 1521.19 39.93 o 3 3 3 4727.33 4748.16 62.90 o -5 4 3 6525.23 6299.69 98.77 o -2 4 3 1026.61 991.34 40.87 o 1 4 3 6524.60 6115.70 65.77 o 4 4 3 3658.23 3540.49 66.09 o -7 5 3 597.45 538.88 31.35 o -4 5 3 6728.11 6738.15 96.03 o -1 5 3 6672.52 6350.09 175.21 o 2 5 3 766.29 793.60 32.28 o 5 5 3 2868.11 2815.73 67.74 o -9 6 3 1196.95 1151.15 47.41 o -6 6 3 1682.32 1724.51 40.28 o -3 6 3 5301.68 5406.69 124.74 o 0 6 3 1440.25 1411.27 37.63 o 3 6 3 1430.10 1396.81 54.54 o 6 6 3 495.23 499.21 50.13 o -11 7 3 237.30 207.29 58.25 o -8 7 3 1225.11 1168.41 49.12 o -5 7 3 471.96 505.67 42.51 o -2 7 3 607.48 527.20 45.29 o 1 7 3 1333.04 1412.62 51.87 o 4 7 3 281.36 274.06 41.55 o -10 8 3 594.06 661.04 47.26 o -7 8 3 1030.44 1055.90 68.38 o -4 8 3 3645.14 3648.75 94.65 o -1 8 3 1120.92 1131.40 68.44 o 2 8 3 570.76 526.10 48.85 o -9 9 3 3757.87 3691.35 77.74 o -6 9 3 1124.13 1242.26 136.01 o -3 9 3 1349.87 1224.07 72.00 o 0 9 3 3455.26 3437.51 76.36 o -11 10 3 382.68 350.83 48.24 o -8 10 3 719.41 766.75 65.26 o -5 10 3 2844.89 2902.43 96.68 o -2 10 3 680.93 651.64 86.44 o 1 10 3 365.33 433.65 44.76 o -10 11 3 291.87 348.05 63.06 o -7 11 3 346.33 364.75 62.02 o -4 11 3 390.65 377.17 60.71 o -1 11 3 263.31 185.74 87.21 o -6 12 3 366.33 481.32 65.09 o -1 1 4 6713.77 6742.57 61.29 o -3 2 4 5069.89 5253.99 70.13 o 0 2 4 170.90 196.14 29.59 o -5 3 4 982.60 964.79 31.17 o -2 3 4 4458.65 4699.29 159.59 o 1 3 4 3308.05 3164.37 57.74 o -7 4 4 575.88 555.25 31.71 o -4 4 4 8197.53 7553.00 90.41 o -1 4 4 3157.53 3057.32 58.67 o 2 4 4 1461.25 1491.69 36.93 o -9 5 4 3390.62 3402.81 69.93 o -6 5 4 1808.42 1687.00 41.16 o -3 5 4 1246.29 1241.44 46.85 o 0 5 4 9989.96 9536.26 86.65 o 3 5 4 739.46 798.35 50.42 o -11 6 4 301.56 365.97 43.55 o -8 6 4 2417.94 2372.09 59.52 o -5 6 4 1690.51 1618.58 98.36 o -2 6 4 1766.65 1809.88 57.10 o 1 6 4 1380.28 1230.87 71.32 o 4 6 4 559.43 523.84 44.41 o -10 7 4 537.78 564.36 45.52 o -7 7 4 130.13 127.86 36.16 o -4 7 4 781.83 772.71 47.68 o -1 7 4 1133.84 1102.82 62.97 o 2 7 4 126.11 121.79 35.43 o 5 7 4 369.70 427.82 97.42 o -9 8 4 2017.11 2062.50 61.16 o -6 8 4 2086.38 2097.03 82.19 o -3 8 4 658.33 665.20 93.90 o 0 8 4 1839.49 1904.60 56.86 o 3 8 4 827.87 988.61 50.77 o -11 9 4 165.48 181.72 42.09 o -8 9 4 2010.35 2321.08 152.29 o -5 9 4 3329.80 3321.47 98.30 o -2 9 4 128.00 68.28 50.51 o 1 9 4 1689.11 1685.30 62.09 o -10 10 4 1173.93 1198.80 57.81 o -7 10 4 688.05 764.83 98.90 o -4 10 4 631.47 667.17 62.69 o -1 10 4 1766.74 1718.06 133.84 o -9 11 4 243.01 248.24 60.46 o -6 11 4 204.47 272.00 59.20 o -3 11 4 1025.75 933.56 78.13 o 0 1 5 39532.13 40151.31 383.98 o -2 2 5 7803.54 7949.46 91.15 o 1 2 5 3686.79 3725.85 50.72 o -4 3 5 8530.74 8762.33 76.69 o -1 3 5 3426.48 3673.39 69.52 o 2 3 5 4189.15 4265.94 60.27 o -6 4 5 5110.28 5101.63 70.00 o -3 4 5 8614.02 8977.14 109.98 o 0 4 5 12398.43 12108.36 92.11 o 3 4 5 2222.64 2172.47 55.23 o -8 5 5 3207.77 3233.62 65.56 o -5 5 5 18900.72 18613.02 323.11 o -2 5 5 4527.59 4781.55 88.35 o 1 5 5 5671.28 5536.83 75.66 o 4 5 5 6892.57 6784.22 95.70 o -10 6 5 1831.60 1683.88 61.06 o -7 6 5 2613.13 2469.36 60.65 o -4 6 5 5387.54 5498.51 104.10 o -1 6 5 5614.09 5547.53 160.80 o 2 6 5 4091.46 3755.26 74.11 o 5 6 5 959.79 936.99 52.83 o -9 7 5 1263.00 1155.25 52.33 o -6 7 5 2489.36 2346.25 101.54 o -3 7 5 2364.49 2306.98 79.47 o 0 7 5 2127.48 2040.52 57.76 o 3 7 5 1203.10 1232.28 54.08 o -11 8 5 865.83 982.92 54.21 o -8 8 5 4356.94 4264.13 89.61 o -5 8 5 3172.01 3158.63 136.83 o -2 8 5 3827.72 3782.20 100.95 o 1 8 5 4860.23 4977.53 87.17 o -10 9 5 3429.36 3392.07 81.26 o -7 9 5 1283.16 1313.63 75.00 o -4 9 5 6769.12 6760.68 211.38 o -1 9 5 4806.59 4853.95 124.06 o 2 9 5 605.91 623.97 50.94 o -9 10 5 3482.58 3301.64 267.59 o -6 10 5 1867.68 1946.66 103.00 o -3 10 5 1242.12 1292.41 113.13 o 0 10 5 2317.99 2356.80 87.03 o -8 11 5 1009.27 989.22 80.08 o -5 11 5 867.93 876.70 74.79 o -2 11 5 640.20 558.44 70.26 o 0 0 6 24223.53 24399.52 232.38 o 1 1 6 4076.61 4060.10 76.50 o -1 2 6 3751.38 3875.10 102.02 o 2 2 6 2044.83 2048.46 53.18 o -3 3 6 1022.81 997.14 31.78 o 0 3 6 3747.74 3675.05 99.96 o 3 3 6 2754.16 2646.36 48.91 o -5 4 6 4634.49 4466.66 62.56 o -2 4 6 1779.88 1863.00 80.98 o 1 4 6 8815.87 8647.53 118.33 o 4 4 6 3695.43 3724.66 72.33 o -7 5 6 1211.34 1145.83 47.20 o -4 5 6 4683.91 4667.57 94.52 o -1 5 6 8861.06 8601.75 249.34 o 2 5 6 649.24 612.44 41.85 o 5 5 6 2917.20 2760.87 77.28 o -9 6 6 1991.81 1964.32 80.49 o -6 6 6 973.30 1012.33 45.41 o -3 6 6 3086.75 3089.06 73.65 o 0 6 6 1718.42 1754.50 52.39 o 3 6 6 908.51 926.00 49.97 o -11 7 6 414.03 438.55 47.10 o -8 7 6 1760.62 1771.28 56.42 o -5 7 6 1011.78 967.70 63.61 o -2 7 6 581.33 645.21 58.16 o 1 7 6 576.25 609.17 41.43 o 4 7 6 378.32 490.35 44.68 o -10 8 6 656.53 706.91 50.06 o -7 8 6 1527.40 1485.06 78.18 o -4 8 6 3721.80 3774.73 103.22 o -1 8 6 452.45 445.47 60.30 o 2 8 6 762.88 853.74 51.92 o -9 9 6 3213.74 3334.20 88.43 o -6 9 6 1852.60 1858.36 86.15 o -3 9 6 977.23 1057.21 181.20 o 0 9 6 3167.22 3210.52 78.43 o -8 10 6 684.41 773.41 83.77 o -5 10 6 2960.27 3095.65 106.15 o -2 10 6 923.76 893.97 75.59 o -7 11 6 475.55 484.24 69.42 o -4 11 6 506.87 505.82 73.21 o -1 1 7 197.23 94.59 25.50 o -3 2 7 6250.35 6199.04 105.99 o 0 2 7 36.20 11.11 26.92 o -5 3 7 2603.00 2510.79 58.06 o -2 3 7 5701.49 5691.58 106.49 o 1 3 7 7427.12 7255.51 80.97 o -7 4 7 392.55 435.93 39.16 o -4 4 7 12152.71 11593.18 108.08 o -1 4 7 7053.74 7001.36 113.20 o 2 4 7 909.17 851.08 44.55 o -9 5 7 3966.16 3751.39 109.72 o -6 5 7 2324.60 2260.27 93.72 o -3 5 7 2368.76 2385.20 68.34 o 0 5 7 8461.72 8271.10 93.04 o 3 5 7 866.57 876.51 45.68 o -8 6 7 962.69 983.76 47.28 o -5 6 7 2139.23 2191.89 93.08 o -2 6 7 867.00 874.69 59.57 o 1 6 7 1255.42 1304.83 48.93 o 4 6 7 1769.14 1912.81 64.30 o -10 7 7 1182.24 1168.77 56.16 o -7 7 7 199.63 172.17 37.69 o -4 7 7 422.61 441.82 55.21 o -1 7 7 997.81 1009.83 67.35 o 2 7 7 18.49 3.55 36.90 o -9 8 7 570.39 613.90 48.33 o -6 8 7 746.61 684.29 63.93 o -3 8 7 828.14 817.43 110.45 o 0 8 7 226.49 305.25 38.73 o -8 9 7 620.96 663.45 65.40 o -5 9 7 4125.98 4354.33 118.06 o -2 9 7 53.48 34.59 110.51 o -7 10 7 1396.96 1393.38 86.49 o -4 10 7 1950.94 2099.72 94.79 o 0 1 8 8980.14 8805.85 85.09 o -2 2 8 1013.43 1016.85 35.09 o 1 2 8 1708.09 1733.71 42.09 o -4 3 8 2052.27 2008.83 45.86 o -1 3 8 1401.06 1389.23 64.63 o 2 3 8 949.37 929.36 45.26 o -6 4 8 1963.39 1912.23 55.87 o -3 4 8 2054.60 2036.62 65.97 o 0 4 8 2980.73 2946.90 70.11 o 3 4 8 393.29 438.42 40.81 o -8 5 8 734.69 688.45 47.03 o -5 5 8 8207.35 8221.77 99.79 o -2 5 8 1220.26 1210.65 68.05 o 1 5 8 1056.02 992.35 46.93 o 4 5 8 3509.29 3587.04 79.70 o -10 6 8 347.40 392.70 46.51 o -7 6 8 623.02 619.00 44.22 o -4 6 8 2261.28 2321.38 84.24 o -1 6 8 974.01 1038.43 67.58 o 2 6 8 2856.13 2854.78 70.80 o -9 7 8 130.56 170.98 40.67 o -6 7 8 530.34 586.20 58.43 o -3 7 8 525.66 501.73 67.58 o 0 7 8 366.01 409.61 41.71 o 3 7 8 378.58 292.73 47.27 o -8 8 8 1423.15 1417.12 59.29 o -5 8 8 730.34 698.08 104.67 o -2 8 8 2560.68 2532.54 98.74 o 1 8 8 2044.42 2169.12 68.84 o -7 9 8 192.06 260.78 92.84 o -4 9 8 3358.92 3366.33 112.98 o -1 9 8 1959.10 1939.65 96.58 o -6 10 8 409.80 446.25 68.75 o -3 10 8 384.99 571.11 152.32 o 0 0 9 16204.62 15925.33 172.76 o 1 1 9 1509.06 1531.60 48.58 o -1 2 9 1340.69 1443.74 78.50 o 2 2 9 280.08 264.95 38.96 o -3 3 9 11.20 21.11 34.90 o 0 3 9 372.65 347.26 38.04 o 3 3 9 4235.57 4178.85 77.74 o -5 4 9 861.49 804.05 45.83 o -2 4 9 231.39 166.75 52.85 o 1 4 9 2508.48 2459.66 60.93 o 4 4 9 840.35 903.74 50.78 o -7 5 9 473.42 446.83 42.47 o -4 5 9 1061.59 1003.29 79.62 o -1 5 9 2746.87 2785.73 113.94 o 2 5 9 25.00 63.88 36.47 o -9 6 9 1294.08 1299.61 59.89 o -6 6 9 426.65 520.25 39.86 o -3 6 9 4741.02 4823.33 139.19 o 0 6 9 1034.64 1069.11 50.43 o 3 6 9 155.29 232.10 47.51 o -8 7 9 1617.23 1585.47 71.76 o -5 7 9 333.08 278.37 67.08 o -2 7 9 13.83 -4.04 54.24 o 1 7 9 619.47 621.20 53.62 o -7 8 9 1433.82 1409.52 86.51 o -4 8 9 827.45 997.25 146.98 o -1 8 9 530.16 490.03 69.00 o -6 9 9 1099.29 1025.66 84.74 o -3 9 9 128.04 122.21 63.96 o -1 1 10 3215.63 3244.59 66.56 o -3 2 10 3000.17 2941.48 65.35 o 0 2 10 695.91 727.38 43.18 o -5 3 10 2111.67 2169.70 61.35 o -2 3 10 2737.94 2676.08 90.57 o 1 3 10 4685.17 4595.20 78.38 o -7 4 10 769.63 685.20 50.12 o -4 4 10 8523.99 8432.05 135.65 o -1 4 10 4526.53 4310.67 111.24 o 2 4 10 1511.01 1442.03 68.37 o -9 5 10 3449.34 3501.67 84.40 o -6 5 10 2369.54 2432.56 66.07 o -3 5 10 2043.46 2121.98 84.67 o 0 5 10 7878.54 7766.34 160.08 o 3 5 10 1068.18 1249.40 57.54 o -8 6 10 1083.23 956.35 55.55 o -5 6 10 2261.59 2409.20 148.99 o -2 6 10 1518.46 1577.91 180.09 o 1 6 10 803.64 778.35 73.60 o -7 7 10 54.91 82.87 40.25 o -4 7 10 795.92 766.62 101.16 o -1 7 10 669.21 573.10 77.43 o -6 8 10 928.14 974.33 75.26 o -3 8 10 1060.98 1250.60 121.29 o -5 9 10 3512.17 3698.76 123.28 o 0 1 11 3032.95 3014.02 73.83 o -2 2 11 486.16 444.19 42.76 o 1 2 11 1832.60 1825.89 67.07 o -4 3 11 2542.70 2524.66 68.25 o -1 3 11 1582.99 1603.72 76.04 o 2 3 11 630.33 638.46 46.73 o -6 4 11 1038.19 970.23 63.84 o -3 4 11 2444.48 2564.79 93.28 o 0 4 11 3698.26 3735.76 89.23 o 3 4 11 469.29 469.30 46.93 o -8 5 11 836.72 848.18 56.70 o -5 5 11 5257.48 5292.26 93.06 o -2 5 11 642.51 609.53 69.38 o 1 5 11 1140.84 1157.13 56.12 o -7 6 11 437.46 584.73 79.55 o -4 6 11 1127.79 1278.72 77.09 o -1 6 11 1037.17 1010.55 80.83 o -6 7 11 330.99 362.17 66.54 o -3 7 11 508.76 443.89 72.62 o 0 7 11 19.81 62.08 42.20 o -5 8 11 841.20 855.48 80.32 o 0 0 12 5458.33 4848.05 355.04 o 1 1 12 1040.13 1025.54 50.48 o -1 2 12 894.52 941.02 84.97 o 2 2 12 547.81 624.33 77.00 o -3 3 12 364.04 337.85 43.27 o 0 3 12 938.82 928.37 51.11 o 3 3 12 971.21 975.92 56.56 o -5 4 12 1681.63 1666.30 62.67 o -2 4 12 429.25 546.93 66.45 o 1 4 12 2563.72 2648.81 105.68 o -4 5 12 1704.82 1847.14 87.00 o -1 5 12 2607.95 2712.96 106.02 o -6 6 12 429.69 340.77 49.56 o -3 6 12 1161.77 1105.29 82.56 o 0 6 12 672.16 676.86 71.36 o -1 1 13 2089.39 2151.55 66.84 o -3 2 13 887.19 895.11 67.00 o 0 2 13 166.40 113.72 48.50 o -5 3 13 424.21 332.70 49.59 o -2 3 13 731.23 941.30 139.52 o 1 3 13 715.11 738.99 51.41 o -4 4 13 3110.08 3214.36 85.60 o -1 4 13 663.71 663.38 71.77 o -3 5 13 514.96 564.93 69.41 o 0 1 14 1858.15 1971.71 68.49 o -2 2 14 19.42 52.78 45.67 o 1 2 14 518.14 580.60 52.44 o -1 3 14 379.92 276.79 72.33 o