#------------------------------------------------------------------------------
#$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $
#$Revision: 26025 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2015636.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2015636_Fobs
loop_
_publ_author_name
'Ebihara, Masahiro'
'Fuma, Yasuhiro'
_publ_section_title
;
 A zigzag chain structure in
 <i>catena</i>-poly[[[tetra-\m-acetamidato-\k^4^<i>N</i>:<i>O</i>;\k^4^<i>O</i>:<i>N</i>-dirhodium(II,III)]-\m-chloro]
 methanol solvate]
;
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m556
_journal_page_last               m558
_journal_volume                  62
_journal_year                    2006
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 98.854
_cell_angle_gamma                90.000
_cell_length_a                   8.6010
_cell_length_b                   14.2540
_cell_length_c                   12.6640
_exptl_crystal_F_000             996.00
_reflns_d_resolution_high        0.7700
_[local]_cod_data_source_file    fa3040Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' _fuma105'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            252.38
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 37802.83 38588.64 690.94 o
3 0 0 3253.06 4510.70 71.03 o
4 0 0 727.96 973.31 65.07 o
5 0 0 7581.71 7732.80 312.59 o
6 0 0 15349.11 16396.25 309.34 o
7 0 0 28502.67 29691.86 574.83 o
8 0 0 29190.77 30147.32 504.71 o
9 0 0 16374.64 17121.34 398.57 o
10 0 0 8709.18 8996.75 325.55 o
11 0 0 1898.28 1594.82 134.73 o
2 1 0 22846.19 22490.28 174.19 o
3 1 0 25004.73 23910.57 224.29 o
4 1 0 57554.36 57928.75 799.65 o
5 1 0 51978.89 53349.77 490.15 o
6 1 0 17495.90 18624.41 345.56 o
7 1 0 7422.13 7479.38 107.92 o
8 1 0 537.74 571.86 35.77 o
9 1 0 189.72 289.74 51.48 o
10 1 0 3497.05 3483.43 197.50 o
11 1 0 4136.70 4053.33 273.51 o
2 2 0 40546.07 41807.02 489.57 o
3 2 0 7788.99 7851.79 122.48 o
4 2 0 927.29 1090.34 32.23 o
5 2 0 2706.18 2600.73 103.67 o
6 2 0 7656.59 7905.81 147.61 o
7 2 0 7079.34 7243.54 281.51 o
8 2 0 9869.79 10064.24 289.99 o
9 2 0 10254.11 10040.13 185.54 o
10 2 0 7253.40 7500.73 162.73 o
1 3 0 4902.63 5034.98 45.91 o
2 3 0 7600.01 6931.63 64.12 o
3 3 0 10758.02 10558.45 94.02 o
4 3 0 27217.24 28397.89 215.42 o
5 3 0 7954.83 7636.90 118.01 o
6 3 0 4982.82 5361.08 151.23 o
7 3 0 974.19 1016.81 39.56 o
8 3 0 905.23 963.01 48.49 o
9 3 0 86.06 47.86 23.68 o
10 3 0 228.80 228.39 45.48 o
0 4 0 778.58 808.68 12.76 o
1 4 0 2463.50 2364.94 31.82 o
2 4 0 707.73 626.53 9.19 o
3 4 0 11167.95 11499.74 107.93 o
4 4 0 1330.25 1418.88 42.23 o
5 4 0 88.58 81.06 14.49 o
6 4 0 29.92 54.60 23.86 o
7 4 0 215.48 190.77 26.25 o
8 4 0 910.04 1054.90 80.17 o
9 4 0 2480.40 2476.27 110.39 o
10 4 0 1686.74 1392.34 84.14 o
1 5 0 0.85 37.21 5.54 o
2 5 0 930.89 1017.63 16.64 o
3 5 0 28.18 40.32 6.03 o
4 5 0 3568.20 3613.07 83.59 o
5 5 0 833.40 904.61 31.39 o
6 5 0 1145.77 1070.78 39.32 o
7 5 0 97.27 99.54 20.70 o
8 5 0 897.34 911.29 47.83 o
9 5 0 100.51 81.72 25.07 o
10 5 0 499.89 483.02 107.59 o
0 6 0 0.21 29.27 7.85 o
1 6 0 365.19 405.35 10.22 o
2 6 0 41.01 50.21 7.21 o
3 6 0 442.32 476.84 12.89 o
4 6 0 659.18 592.26 22.99 o
5 6 0 1861.57 1891.15 56.02 o
6 6 0 261.04 276.25 38.01 o
7 6 0 41.92 67.37 38.80 o
8 6 0 8.76 104.41 30.91 o
9 6 0 5.30 107.76 49.49 o
10 6 0 130.33 179.80 50.74 o
1 7 0 807.30 879.90 15.04 o
2 7 0 709.43 733.01 22.04 o
3 7 0 3371.16 3372.74 64.35 o
4 7 0 3095.60 3071.98 35.91 o
5 7 0 90.99 77.13 18.28 o
6 7 0 188.97 229.35 20.28 o
7 7 0 310.53 346.64 28.82 o
8 7 0 698.47 723.89 56.25 o
9 7 0 604.49 596.30 54.65 o
10 7 0 763.62 683.63 144.29 o
0 8 0 1193.71 1234.00 24.69 o
1 8 0 2815.79 2885.68 33.42 o
2 8 0 79.45 328.32 96.23 o
3 8 0 123.41 227.49 29.31 o
4 8 0 537.86 577.82 23.72 o
5 8 0 14.31 65.27 27.82 o
6 8 0 477.63 512.84 36.64 o
7 8 0 1981.51 2162.78 87.19 o
8 8 0 2122.69 2002.39 100.45 o
9 8 0 650.36 625.37 53.21 o
1 9 0 2164.86 2133.60 33.04 o
2 9 0 11607.25 11499.17 135.09 o
3 9 0 5424.00 5384.00 66.29 o
4 9 0 4976.94 4962.77 152.22 o
5 9 0 2141.03 2225.54 45.28 o
6 9 0 3370.05 3543.49 76.28 o
7 9 0 1.15 40.11 30.48 o
8 9 0 967.32 1190.01 73.27 o
9 9 0 2251.55 2479.57 150.30 o
0 10 0 12866.28 12013.81 113.67 o
1 10 0 11407.17 11422.46 83.85 o
2 10 0 4556.81 4472.63 57.87 o
3 10 0 1915.37 1918.33 85.45 o
4 10 0 619.93 627.30 34.47 o
5 10 0 712.21 708.56 41.12 o
6 10 0 2704.58 2805.22 71.23 o
7 10 0 4704.46 4868.81 123.95 o
8 10 0 4555.99 4691.64 161.43 o
9 10 0 1354.54 1272.52 96.53 o
1 11 0 36.47 61.33 20.38 o
2 11 0 1022.92 1151.53 36.77 o
3 11 0 2420.23 2448.30 44.82 o
4 11 0 4559.58 4524.71 77.32 o
5 11 0 2514.37 2379.57 99.74 o
6 11 0 2579.39 2572.52 74.53 o
7 11 0 764.69 848.64 61.03 o
8 11 0 100.72 162.43 65.01 o
0 12 0 3131.59 3037.49 55.79 o
1 12 0 3359.06 3344.18 45.19 o
2 12 0 5339.76 5338.43 74.11 o
3 12 0 220.25 239.40 31.08 o
4 12 0 174.04 163.93 21.55 o
5 12 0 361.93 329.62 34.79 o
6 12 0 428.05 494.94 42.95 o
7 12 0 454.76 464.60 52.94 o
8 12 0 1105.43 1287.39 258.94 o
1 13 0 3308.23 3331.05 53.85 o
2 13 0 1551.89 1623.32 44.20 o
3 13 0 54.85 92.46 19.51 o
4 13 0 47.04 89.95 23.24 o
5 13 0 8.92 48.07 28.12 o
6 13 0 68.22 129.50 37.68 o
7 13 0 202.13 295.19 106.34 o
0 14 0 220.56 161.78 40.64 o
1 14 0 320.35 303.48 22.84 o
2 14 0 163.97 165.34 21.66 o
3 14 0 202.35 263.97 40.15 o
4 14 0 214.06 253.78 36.98 o
5 14 0 834.95 938.68 63.21 o
6 14 0 952.67 1033.37 57.50 o
7 14 0 417.99 484.23 56.91 o
1 15 0 347.68 433.20 57.51 o
2 15 0 199.90 298.92 26.80 o
3 15 0 513.88 538.05 35.94 o
4 15 0 527.86 549.22 38.82 o
5 15 0 70.35 134.61 40.96 o
6 15 0 5.60 17.58 52.33 o
0 16 0 17.18 55.35 34.62 o
1 16 0 77.14 191.00 41.61 o
2 16 0 7.49 110.45 42.72 o
3 16 0 14.80 43.85 40.14 o
4 16 0 629.61 631.91 50.15 o
5 16 0 1345.17 1402.75 82.31 o
1 17 0 1.87 13.29 32.35 o
2 17 0 434.06 431.14 43.62 o
3 17 0 65.49 161.22 43.76 o
4 17 0 54.17 130.42 73.97 o
0 18 0 496.81 622.39 96.10 o
1 18 0 1343.48 1359.50 65.18 o
2 18 0 688.63 702.83 55.20 o
-11 1 1 248.19 242.81 50.95 o
-10 1 1 20.06 116.18 61.80 o
-9 1 1 195.93 221.11 42.68 o
-8 1 1 635.30 561.22 27.99 o
-7 1 1 1513.49 1775.34 53.46 o
-6 1 1 1366.18 1530.79 39.06 o
-5 1 1 1232.97 1107.22 28.30 o
-4 1 1 4859.37 4707.28 51.40 o
-3 1 1 5587.58 5822.96 66.29 o
-2 1 1 762.27 859.16 58.27 o
-1 1 1 732.94 735.73 9.94 o
1 1 1 3661.41 3844.85 102.32 o
2 1 1 1699.15 1653.20 14.67 o
3 1 1 3515.75 3985.19 39.06 o
4 1 1 334.13 338.70 12.42 o
5 1 1 1839.04 1755.61 71.93 o
6 1 1 0.39 87.57 40.20 o
7 1 1 170.66 279.29 30.08 o
8 1 1 735.05 762.43 58.05 o
9 1 1 3.61 122.00 46.92 o
10 1 1 393.52 356.14 53.76 o
-11 2 1 2029.26 2030.06 103.73 o
-10 2 1 5997.71 6026.88 162.50 o
-9 2 1 6435.41 6240.13 141.34 o
-8 2 1 2978.39 3044.60 92.70 o
-7 2 1 467.94 478.15 35.61 o
-6 2 1 29.66 50.88 9.33 o
-5 2 1 1686.79 1552.90 48.14 o
-4 2 1 12827.28 13068.67 159.95 o
-3 2 1 32423.12 33865.50 425.24 o
-1 2 1 3879.32 4115.51 62.34 o
0 2 1 3552.93 3505.10 30.64 o
1 2 1 0.37 54.05 7.57 o
2 2 1 97.26 107.24 6.64 o
3 2 1 2146.27 2080.05 34.14 o
4 2 1 2393.43 2390.51 40.13 o
5 2 1 16979.09 16923.65 193.30 o
6 2 1 9554.12 9696.72 134.06 o
7 2 1 1282.59 1235.63 46.80 o
8 2 1 30.34 73.47 55.10 o
9 2 1 403.75 482.46 61.39 o
10 2 1 211.75 297.02 117.27 o
-10 3 1 0.51 89.07 59.79 o
-9 3 1 940.33 926.49 52.34 o
-8 3 1 3749.09 4006.05 83.03 o
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-6 3 1 6485.78 6331.14 70.70 o
-5 3 1 7483.77 7220.30 98.69 o
-4 3 1 14508.35 14579.90 258.67 o
-3 3 1 6799.79 6776.31 109.85 o
-2 3 1 46.69 79.79 7.73 o
-1 3 1 574.07 662.31 14.24 o
0 3 1 7574.86 7437.53 43.85 o
1 3 1 25719.61 26209.64 217.77 o
2 3 1 4898.75 4845.04 54.57 o
3 3 1 1266.53 1086.11 32.17 o
4 3 1 1923.91 1979.17 42.20 o
7 3 1 297.30 256.09 28.17 o
8 3 1 1752.70 1759.72 58.73 o
9 3 1 375.86 360.88 50.46 o
10 3 1 357.62 380.60 56.03 o
-10 4 1 4182.06 4051.87 309.02 o
-9 4 1 2125.08 2053.37 153.53 o
-8 4 1 2621.88 2657.60 68.47 o
-7 4 1 1883.24 2025.34 83.70 o
-6 4 1 48.90 107.60 47.30 o
-5 4 1 2527.32 2604.92 43.08 o
-4 4 1 18980.93 18345.58 182.34 o
-3 4 1 32609.98 32181.38 283.10 o
-2 4 1 7392.45 6758.22 64.90 o
-1 4 1 262.03 369.78 14.10 o
0 4 1 10342.16 10280.61 57.66 o
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3 4 1 4038.21 4086.30 67.67 o
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6 4 1 1571.73 1625.31 41.23 o
7 4 1 233.90 237.95 46.72 o
8 4 1 4.85 26.82 28.51 o
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10 4 1 497.97 489.36 62.30 o
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-3 5 1 864.77 818.42 21.17 o
-2 5 1 176.36 163.50 10.22 o
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0 5 1 5.67 38.41 3.82 o
1 5 1 4332.18 4276.42 41.97 o
2 5 1 17570.11 17350.04 132.06 o
3 5 1 106.56 155.68 20.72 o
4 5 1 192.01 143.93 13.37 o
5 5 1 2.12 69.89 19.41 o
6 5 1 31.57 37.93 14.05 o
7 5 1 20.69 36.36 19.22 o
8 5 1 89.86 80.58 25.84 o
9 5 1 104.89 272.38 57.01 o
10 5 1 57.09 109.81 95.57 o
-10 6 1 2191.08 2363.19 216.87 o
-9 6 1 1396.63 1586.49 71.53 o
-8 6 1 1648.06 1667.95 64.38 o
-7 6 1 1738.90 1733.83 70.75 o
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-5 6 1 274.28 283.83 13.67 o
-4 6 1 646.95 627.70 18.25 o
-3 6 1 3366.02 3436.69 36.31 o
-2 6 1 4710.62 4510.78 44.18 o
-1 6 1 1918.79 1852.81 22.53 o
0 6 1 615.97 488.34 13.09 o
1 6 1 1749.29 1716.14 22.66 o
2 6 1 102.12 93.65 9.64 o
3 6 1 1087.86 1074.10 37.99 o
4 6 1 224.43 230.26 21.27 o
5 6 1 430.38 401.17 21.74 o
6 6 1 444.45 460.49 39.69 o
7 6 1 47.76 59.88 19.06 o
8 6 1 1.90 87.79 35.60 o
9 6 1 48.15 141.11 50.80 o
10 6 1 0.91 86.45 48.21 o
-10 7 1 754.85 685.27 57.32 o
-9 7 1 1.46 102.03 49.67 o
-8 7 1 937.58 847.78 54.74 o
-7 7 1 2850.93 2885.57 60.14 o
-6 7 1 4736.22 4760.89 77.89 o
-5 7 1 3873.61 3764.60 47.99 o
-4 7 1 13903.27 14068.79 181.21 o
-3 7 1 9638.07 9349.31 104.65 o
-2 7 1 8123.91 7905.10 86.17 o
-1 7 1 2801.06 2909.21 37.84 o
0 7 1 35.51 63.46 13.04 o
1 7 1 175.18 213.31 7.99 o
2 7 1 3318.06 3293.14 48.80 o
3 7 1 1348.01 1373.50 28.84 o
4 7 1 4919.72 4714.92 69.27 o
5 7 1 517.12 481.75 26.71 o
6 7 1 2483.91 2438.01 65.57 o
7 7 1 1336.90 1300.76 56.87 o
8 7 1 2249.30 2425.16 107.41 o
9 7 1 324.65 256.14 56.77 o
10 7 1 111.84 182.35 62.94 o
-10 8 1 1291.21 1266.18 106.78 o
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-8 8 1 6679.80 6818.45 168.31 o
-7 8 1 3217.58 3397.75 88.00 o
-6 8 1 2197.31 2112.11 49.94 o
-5 8 1 1496.81 1618.24 43.70 o
-4 8 1 1158.17 1249.61 51.17 o
-3 8 1 72.59 106.65 18.86 o
-2 8 1 5866.89 6073.01 172.31 o
-1 8 1 8339.46 8369.28 76.41 o
0 8 1 8117.71 7722.35 75.30 o
1 8 1 11643.03 11140.42 91.81 o
2 8 1 10309.65 10231.94 107.98 o
3 8 1 12979.00 12396.35 121.79 o
4 8 1 2658.92 2649.99 79.28 o
5 8 1 48.12 79.82 22.24 o
6 8 1 246.08 250.81 26.60 o
7 8 1 138.08 110.72 25.00 o
8 8 1 1328.23 1351.12 68.32 o
9 8 1 1106.94 1080.35 89.15 o
-9 9 1 1302.25 1402.95 167.03 o
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-7 9 1 43.22 68.78 55.82 o
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3 9 1 2192.44 2132.02 38.99 o
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6 9 1 10949.29 10900.06 164.96 o
7 9 1 9342.97 9678.49 160.50 o
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-8 11 1 2778.23 2866.12 127.52 o
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-5 11 1 110.80 93.64 22.87 o
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0 11 1 22113.70 22148.26 162.49 o
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3 11 1 31.07 78.33 21.66 o
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5 11 1 6395.00 6742.85 109.15 o
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3 13 1 325.62 281.13 26.81 o
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7 13 1 6154.29 6147.18 185.33 o
-7 14 1 1045.61 964.61 70.87 o
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-2 14 1 387.45 419.68 27.75 o
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0 14 1 399.75 503.78 33.97 o
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2 14 1 7568.39 7661.43 121.51 o
3 14 1 8034.46 8373.39 146.70 o
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6 14 1 1342.64 1271.84 71.64 o
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-6 15 1 55.69 129.64 65.76 o
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