#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2015722.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015722_Fobs loop_ _publ_author_name 'Werz, Daniel B.' 'Ohlbach, Frank' 'Rominger, Frank' 'Gleiter, Rolf' _publ_section_title ; Bis(tert-butylsulfonyl)ethyne and 1-tert-butylsulfinyl-2-tert-butylsulfonylethyne ; _journal_coeditor_code AV3049 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o1 _journal_page_last o3 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.267 _cell_angle_gamma 90.000 _cell_length_a 5.7037 _cell_length_b 10.7251 _cell_length_c 10.5678 _exptl_crystal_F_000 284.00 _reflns_d_resolution_high 0.7500 _[local]_cod_data_source_file av3049Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' dwe118 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 98.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 146.40 116.22 2.20 o 4 0 0 371.24 368.69 5.20 o 6 0 0 311.29 294.75 5.97 o 1 1 0 208.11 197.65 1.89 o 2 1 0 1813.06 1833.13 14.67 o 3 1 0 201.25 189.05 2.43 o 4 1 0 403.36 387.43 4.09 o 5 1 0 292.17 271.63 3.44 o 6 1 0 289.25 286.60 4.62 o 7 1 0 177.23 176.79 3.65 o 0 2 0 1.77 0.20 0.41 o 1 2 0 6634.68 6508.88 65.07 o 2 2 0 1822.33 1987.27 19.08 o 3 2 0 372.13 355.60 3.93 o 4 2 0 400.11 373.97 4.34 o 5 2 0 317.15 300.28 4.53 o 6 2 0 12.29 12.22 0.98 o 7 2 0 97.27 103.77 2.69 o 1 3 0 119.29 113.42 1.49 o 2 3 0 482.50 535.04 5.87 o 3 3 0 167.65 151.68 2.48 o 4 3 0 77.37 70.11 1.77 o 5 3 0 290.84 269.33 4.25 o 6 3 0 165.99 160.44 3.73 o 7 3 0 20.93 26.13 1.51 o 0 4 0 1125.57 1266.27 16.09 o 1 4 0 25.79 34.85 0.82 o 2 4 0 2128.62 2195.25 21.24 o 3 4 0 22.77 20.36 0.91 o 4 4 0 246.29 235.18 3.67 o 5 4 0 271.33 252.31 4.14 o 6 4 0 103.78 103.61 2.62 o 7 4 0 1.22 2.27 1.29 o 1 5 0 25.14 29.43 0.95 o 2 5 0 554.81 573.78 6.52 o 3 5 0 5.62 5.45 0.70 o 4 5 0 36.55 35.69 1.34 o 5 5 0 56.06 56.78 1.81 o 6 5 0 9.19 11.63 1.23 o 7 5 0 121.51 131.39 5.41 o 0 6 0 92.16 81.37 2.12 o 1 6 0 36.46 35.52 0.96 o 2 6 0 990.55 964.06 9.31 o 3 6 0 479.12 489.77 6.10 o 4 6 0 133.13 128.44 2.65 o 5 6 0 73.56 72.17 2.46 o 6 6 0 18.30 22.28 1.86 o 1 7 0 37.81 34.74 1.02 o 2 7 0 276.84 261.61 4.60 o 3 7 0 292.44 279.28 4.18 o 4 7 0 66.31 63.19 2.39 o 5 7 0 2.25 2.01 0.98 o 6 7 0 104.80 104.76 4.87 o 0 8 0 790.30 748.44 17.72 o 1 8 0 600.37 577.21 6.28 o 2 8 0 88.82 88.94 2.05 o 3 8 0 1195.86 1135.15 14.23 o 4 8 0 69.47 67.85 2.42 o 5 8 0 0.05 0.08 0.85 o 6 8 0 160.26 170.47 5.27 o 1 9 0 267.16 254.54 3.91 o 2 9 0 21.51 20.41 1.36 o 3 9 0 223.99 210.34 4.37 o 4 9 0 61.45 53.43 2.24 o 5 9 0 198.53 190.72 5.47 o 0 10 0 211.21 201.50 11.35 o 1 10 0 461.38 449.89 6.16 o 2 10 0 728.47 705.10 9.93 o 3 10 0 17.31 17.77 1.40 o 4 10 0 234.10 236.47 5.08 o 5 10 0 99.40 102.92 4.01 o 1 11 0 54.11 58.17 2.18 o 2 11 0 101.55 104.89 3.07 o 3 11 0 17.76 22.40 2.85 o 4 11 0 176.36 179.70 5.35 o 0 12 0 131.86 125.76 7.15 o 1 12 0 209.86 212.02 5.40 o 2 12 0 46.80 49.06 2.17 o 3 12 0 72.26 76.72 2.75 o 4 12 0 64.61 71.77 3.40 o 1 13 0 0.46 1.16 1.05 o 2 13 0 1.16 3.24 1.09 o 3 13 0 54.72 62.81 2.97 o 0 14 0 219.08 223.60 10.30 o 1 14 0 7.04 13.87 3.13 o -7 0 1 40.26 39.89 2.18 o -5 0 1 1034.02 1015.89 14.22 o -3 0 1 1047.87 1007.49 13.41 o -1 0 1 8817.93 8897.52 171.66 o 1 0 1 2610.43 2700.07 55.56 o 3 0 1 0.66 8.89 1.42 o 5 0 1 5.01 11.59 2.34 o 7 0 1 10.10 10.07 1.51 o -7 1 1 20.43 22.83 1.35 o -6 1 1 15.37 23.05 1.15 o -5 1 1 308.37 290.31 4.31 o -4 1 1 49.82 48.98 1.13 o -3 1 1 36.41 40.06 1.06 o -2 1 1 0.06 7.51 1.31 o -1 1 1 2777.60 2807.78 23.85 o 0 1 1 3452.75 3587.46 29.85 o 1 1 1 81.54 131.46 3.43 o 2 1 1 644.89 570.77 5.48 o 3 1 1 506.87 491.40 5.11 o 4 1 1 209.36 190.18 2.47 o 5 1 1 413.49 406.52 4.93 o 6 1 1 794.55 779.41 9.28 o 7 1 1 38.12 45.01 1.99 o -7 2 1 8.42 12.87 1.21 o -6 2 1 377.01 353.65 6.97 o -5 2 1 408.93 386.93 4.87 o -4 2 1 778.84 759.07 8.43 o -3 2 1 928.22 978.45 8.46 o -2 2 1 1081.09 1023.82 9.24 o -1 2 1 20.95 14.28 0.43 o 0 2 1 6937.10 6848.38 92.12 o 1 2 1 8.83 8.28 0.44 o 2 2 1 100.55 111.96 2.25 o 3 2 1 5.48 14.16 1.28 o 4 2 1 0.97 7.08 1.95 o 5 2 1 49.76 49.20 1.44 o 6 2 1 2.30 7.87 1.08 o 7 2 1 22.41 24.46 1.79 o -7 3 1 37.57 44.28 2.03 o -6 3 1 96.54 88.94 2.87 o -5 3 1 394.38 371.41 5.29 o -4 3 1 213.99 196.24 3.21 o -3 3 1 117.09 124.74 2.19 o -2 3 1 1113.01 1246.50 12.43 o -1 3 1 565.63 566.13 5.37 o 0 3 1 2.66 1.44 0.37 o 1 3 1 1367.85 1319.77 11.75 o 2 3 1 246.90 246.37 2.83 o 3 3 1 348.34 308.99 3.57 o 4 3 1 464.53 440.44 12.24 o 5 3 1 542.51 528.66 6.82 o 6 3 1 3.60 5.22 0.75 o 7 3 1 349.39 336.41 7.28 o -7 4 1 682.42 691.11 10.66 o -6 4 1 56.54 55.52 2.24 o -5 4 1 161.01 153.52 3.20 o -4 4 1 382.03 329.38 4.63 o -3 4 1 248.91 232.90 3.39 o -2 4 1 443.37 510.66 5.77 o -1 4 1 370.14 378.82 3.91 o 0 4 1 104.45 101.64 1.48 o 1 4 1 879.53 897.78 8.35 o 2 4 1 0.55 8.53 0.86 o 3 4 1 16.99 25.83 0.82 o 4 4 1 135.20 129.44 2.55 o 5 4 1 3.53 5.76 0.82 o 6 4 1 59.78 58.94 2.25 o -7 5 1 6.04 8.07 1.24 o -6 5 1 20.15 22.15 1.52 o -5 5 1 8.22 7.50 1.10 o -4 5 1 144.84 148.66 2.80 o -3 5 1 482.68 483.16 5.90 o -2 5 1 1092.59 1129.15 10.52 o -1 5 1 31.10 30.48 0.81 o 0 5 1 17.78 7.61 0.53 o 1 5 1 1.05 4.24 0.45 o 2 5 1 578.73 568.70 5.84 o 3 5 1 69.08 72.50 1.84 o 4 5 1 944.88 934.90 10.48 o 5 5 1 33.25 34.41 1.47 o 6 5 1 146.16 136.94 4.63 o 7 5 1 39.02 42.28 2.93 o -6 6 1 396.18 393.23 7.67 o -5 6 1 43.49 43.04 1.98 o -4 6 1 17.10 16.93 1.29 o -3 6 1 1488.62 1390.60 14.47 o -2 6 1 433.30 425.71 7.56 o -1 6 1 27.59 20.22 0.73 o 0 6 1 30.24 39.75 1.73 o 1 6 1 6.24 4.98 0.50 o 2 6 1 486.03 490.75 12.31 o 3 6 1 351.91 365.23 4.91 o 4 6 1 0.33 0.72 0.62 o 5 6 1 44.83 39.46 1.56 o 6 6 1 0.51 3.22 1.90 o -6 7 1 12.19 11.51 1.28 o -5 7 1 90.38 84.08 2.81 o -4 7 1 164.19 160.63 3.72 o -3 7 1 403.48 409.13 6.40 o -2 7 1 13.72 16.03 1.01 o -1 7 1 289.47 277.44 3.47 o 0 7 1 1.32 2.25 0.50 o 1 7 1 307.42 288.67 5.30 o 2 7 1 173.70 173.36 2.58 o 3 7 1 1064.79 1060.95 11.64 o 4 7 1 4.85 7.36 0.82 o 5 7 1 295.30 287.07 6.58 o 6 7 1 61.36 66.78 3.15 o -6 8 1 62.84 65.25 3.20 o -5 8 1 181.02 185.57 4.60 o -4 8 1 250.14 238.83 4.86 o -3 8 1 210.83 208.01 4.25 o -2 8 1 1822.78 1733.61 20.14 o -1 8 1 139.19 125.13 2.85 o 0 8 1 11.12 11.94 0.73 o 1 8 1 71.51 67.62 1.55 o 2 8 1 253.95 269.96 3.61 o 3 8 1 29.51 32.57 1.32 o 4 8 1 2.10 6.22 1.04 o 5 8 1 0.24 3.30 1.77 o 6 8 1 0.18 2.04 2.45 o -5 9 1 21.98 17.70 1.93 o -4 9 1 2.34 8.16 1.19 o -3 9 1 8.23 9.08 1.15 o -2 9 1 0.03 12.92 1.19 o -1 9 1 61.19 58.75 1.73 o 0 9 1 741.81 744.61 7.91 o 1 9 1 78.29 73.67 1.71 o 2 9 1 781.63 768.50 10.28 o 3 9 1 103.60 99.90 2.84 o 4 9 1 226.96 214.78 5.52 o 5 9 1 30.92 30.98 2.22 o -5 10 1 204.73 217.91 6.10 o -4 10 1 246.28 244.85 5.27 o -3 10 1 307.27 276.60 5.43 o -2 10 1 37.87 38.67 1.85 o -1 10 1 429.01 414.40 5.83 o 0 10 1 447.72 443.40 6.08 o 1 10 1 132.04 138.27 2.56 o 2 10 1 6.07 5.72 0.99 o 3 10 1 12.57 17.12 1.31 o 4 10 1 8.32 11.46 1.53 o 5 10 1 52.20 58.48 3.02 o -4 11 1 40.52 45.73 2.23 o -3 11 1 34.14 31.90 1.85 o -2 11 1 1.99 3.36 0.95 o -1 11 1 36.41 53.39 2.14 o 0 11 1 8.65 8.91 1.10 o 1 11 1 840.78 806.00 12.87 o 2 11 1 26.13 24.85 1.57 o 3 11 1 109.13 109.97 3.85 o 4 11 1 47.53 50.66 3.06 o -4 12 1 304.30 316.10 7.71 o -3 12 1 22.55 31.06 1.86 o -2 12 1 44.26 40.95 2.03 o -1 12 1 79.92 76.01 2.61 o 0 12 1 124.36 126.01 3.35 o 1 12 1 26.26 31.30 2.01 o 2 12 1 42.76 46.57 2.47 o 3 12 1 0.96 3.41 1.15 o 4 12 1 60.71 70.66 3.31 o -3 13 1 14.34 19.87 1.51 o -2 13 1 12.43 19.32 1.80 o -1 13 1 50.44 51.76 2.71 o 0 13 1 84.86 88.69 4.24 o 1 13 1 36.52 41.12 2.35 o 2 13 1 126.94 136.61 5.66 o 3 13 1 9.87 11.58 1.92 o -1 14 1 9.42 9.90 1.40 o 0 14 1 33.45 39.05 2.92 o 1 14 1 34.52 41.19 2.92 o -6 0 2 411.55 403.56 7.55 o -4 0 2 73.14 71.12 2.13 o -2 0 2 48.56 51.65 2.50 o 0 0 2 1369.42 1323.81 23.02 o 2 0 2 2686.81 2727.66 33.45 o 4 0 2 35.41 25.20 1.07 o 6 0 2 98.12 106.49 4.09 o -7 1 2 17.91 25.14 1.86 o -6 1 2 0.43 2.55 0.67 o -5 1 2 622.47 606.88 6.78 o -4 1 2 273.48 259.64 3.10 o -3 1 2 209.45 198.40 2.37 o -2 1 2 503.04 531.79 5.22 o -1 1 2 2069.27 2018.92 17.52 o 0 1 2 1232.22 1236.89 10.86 o 1 1 2 2168.78 2211.37 17.56 o 2 1 2 96.54 78.75 1.16 o 3 1 2 4.76 4.94 0.72 o 4 1 2 1.88 5.57 0.63 o 5 1 2 390.20 370.13 4.59 o 6 1 2 166.93 163.20 3.69 o 7 1 2 74.15 76.89 3.04 o -7 2 2 190.19 200.57 4.61 o -6 2 2 4.58 11.49 1.10 o -5 2 2 241.91 238.66 3.54 o -4 2 2 17.70 12.86 0.78 o -3 2 2 15.16 9.82 0.57 o -2 2 2 31.43 37.62 0.78 o -1 2 2 382.08 397.81 3.92 o 0 2 2 46.50 35.78 0.87 o 1 2 2 349.08 345.26 3.48 o 2 2 2 12.33 16.38 0.63 o 3 2 2 193.24 180.58 3.04 o 4 2 2 30.80 29.88 0.89 o 5 2 2 260.56 249.18 3.55 o 6 2 2 596.42 588.40 7.46 o 7 2 2 40.10 46.49 2.38 o -7 3 2 97.29 94.14 3.07 o -6 3 2 210.33 201.97 5.14 o -5 3 2 179.15 152.93 3.01 o -4 3 2 430.99 412.89 5.40 o -3 3 2 927.36 964.16 10.21 o -2 3 2 1574.19 1633.30 16.02 o -1 3 2 946.85 1029.54 10.36 o 0 3 2 1508.56 1442.61 12.78 o 1 3 2 303.99 392.95 4.36 o 2 3 2 1503.13 1518.06 13.65 o 3 3 2 185.79 184.58 2.50 o 4 3 2 840.45 829.72 9.30 o 5 3 2 42.12 38.93 1.37 o 6 3 2 219.97 217.39 4.56 o 7 3 2 5.88 12.47 1.32 o -7 4 2 18.77 17.12 1.65 o -6 4 2 95.86 96.93 2.98 o -5 4 2 71.80 68.67 2.34 o -4 4 2 133.19 138.04 2.64 o -3 4 2 2.91 2.06 0.49 o -2 4 2 19.16 13.08 0.68 o -1 4 2 173.87 184.27 2.76 o 0 4 2 3.74 0.65 0.39 o 1 4 2 149.06 157.96 2.25 o 2 4 2 116.32 135.74 1.96 o 3 4 2 49.25 57.47 1.45 o 4 4 2 827.06 802.99 9.15 o 5 4 2 327.75 311.32 4.76 o 6 4 2 161.22 157.93 3.84 o 7 4 2 130.68 126.41 4.04 o -7 5 2 270.88 272.95 6.75 o -6 5 2 0.26 0.68 0.88 o -5 5 2 172.45 158.70 3.75 o -4 5 2 5.50 11.93 1.76 o -3 5 2 929.60 930.64 10.09 o -2 5 2 976.60 1046.27 9.84 o -1 5 2 1065.05 1055.81 10.95 o 0 5 2 1.89 4.36 0.45 o 1 5 2 1099.11 1102.07 10.28 o 2 5 2 42.65 71.47 2.09 o 3 5 2 2180.17 2233.62 20.13 o 4 5 2 728.20 698.02 8.28 o 5 5 2 213.10 224.73 4.52 o 6 5 2 3.32 4.77 0.92 o 7 5 2 19.60 25.18 2.17 o -6 6 2 85.32 77.26 2.83 o -5 6 2 28.89 28.02 1.68 o -4 6 2 169.22 149.54 3.50 o -3 6 2 34.97 41.62 2.21 o -2 6 2 5.88 4.64 0.43 o -1 6 2 0.24 11.51 0.73 o 0 6 2 36.13 35.34 0.97 o 1 6 2 477.82 508.25 5.40 o 2 6 2 41.56 39.01 1.07 o 3 6 2 699.93 661.16 7.77 o 4 6 2 107.69 103.41 2.37 o 5 6 2 149.18 145.63 3.58 o 6 6 2 4.86 7.71 1.34 o -6 7 2 138.65 143.32 3.97 o -5 7 2 36.48 40.19 2.02 o -4 7 2 376.70 355.21 6.15 o -3 7 2 1.78 5.15 2.19 o -2 7 2 740.64 752.53 9.84 o -1 7 2 0.62 2.29 0.36 o 0 7 2 750.91 747.59 8.28 o 1 7 2 59.22 52.51 1.28 o 2 7 2 850.15 864.20 8.71 o 3 7 2 10.33 10.63 0.83 o 4 7 2 383.76 380.09 6.28 o 5 7 2 125.24 127.68 4.10 o 6 7 2 8.26 12.04 2.86 o -6 8 2 194.43 200.29 5.85 o -5 8 2 90.47 84.45 2.93 o -4 8 2 1.16 2.09 1.01 o -3 8 2 370.55 340.17 6.99 o -2 8 2 27.99 36.43 1.69 o -1 8 2 160.86 151.66 2.79 o 0 8 2 45.57 47.09 1.29 o 1 8 2 13.15 14.52 0.79 o 2 8 2 183.84 165.87 3.38 o 3 8 2 141.14 137.75 3.30 o 4 8 2 65.11 62.31 2.78 o 5 8 2 3.54 6.91 3.02 o 6 8 2 49.44 56.97 2.97 o -5 9 2 142.16 151.04 4.13 o -4 9 2 26.98 29.81 1.80 o -3 9 2 337.87 333.52 6.57 o -2 9 2 164.83 152.26 3.55 o -1 9 2 517.50 526.90 6.76 o 0 9 2 7.19 8.10 0.83 o 1 9 2 666.38 659.03 7.22 o 2 9 2 0.63 4.59 0.73 o 3 9 2 83.68 86.61 2.57 o 4 9 2 93.22 90.50 3.60 o 5 9 2 74.99 73.70 3.31 o -5 10 2 46.66 58.59 3.15 o -4 10 2 134.84 132.93 3.78 o -3 10 2 20.09 19.56 1.55 o -2 10 2 84.75 77.27 2.58 o -1 10 2 3.46 8.15 1.05 o 0 10 2 124.67 112.21 2.58 o 1 10 2 193.91 195.33 3.54 o 2 10 2 6.77 10.89 0.93 o 3 10 2 20.65 21.84 1.75 o 4 10 2 5.55 8.46 1.59 o 5 10 2 28.49 31.48 3.28 o -4 11 2 177.52 183.80 4.65 o -3 11 2 26.53 24.76 1.67 o -2 11 2 99.95 105.82 3.13 o -1 11 2 8.28 11.18 1.17 o 0 11 2 495.22 479.22 6.69 o 1 11 2 163.06 158.52 3.65 o 2 11 2 219.51 221.16 6.98 o 3 11 2 57.54 65.85 2.96 o 4 11 2 26.96 38.48 2.39 o -3 12 2 28.49 28.64 2.05 o -2 12 2 0.22 1.18 0.91 o -1 12 2 15.78 18.28 1.44 o 0 12 2 67.26 66.32 2.40 o 1 12 2 48.58 47.19 2.68 o 2 12 2 2.69 2.74 1.90 o 3 12 2 0.05 0.58 1.41 o -2 13 2 2.36 6.30 1.08 o -1 13 2 73.77 81.02 3.35 o 0 13 2 241.51 241.27 5.91 o 1 13 2 284.11 296.58 9.83 o 2 13 2 162.10 160.76 6.23 o -1 14 2 6.22 8.31 1.28 o 0 14 2 1.65 6.60 2.53 o 1 14 2 2.64 4.48 1.27 o -7 0 3 56.18 62.88 2.81 o -5 0 3 77.73 74.51 2.92 o -3 0 3 1399.78 1431.87 18.62 o -1 0 3 725.25 849.78 11.01 o 1 0 3 9666.00 10054.95 151.91 o 3 0 3 21.06 41.64 4.74 o 5 0 3 557.90 501.05 29.40 o 7 0 3 61.86 76.74 5.74 o -7 1 3 125.78 127.20 3.18 o -6 1 3 239.52 230.21 3.79 o -5 1 3 115.43 108.83 2.66 o -4 1 3 480.30 442.02 8.03 o -3 1 3 1195.18 1173.05 11.00 o -2 1 3 1203.46 1265.73 11.51 o -1 1 3 492.21 538.27 5.18 o 0 1 3 46.88 39.90 0.77 o 1 1 3 2384.43 2542.94 24.32 o 2 1 3 57.52 70.13 1.88 o 3 1 3 53.70 63.56 1.52 o 4 1 3 1.31 5.61 0.59 o 5 1 3 26.11 23.01 1.13 o 6 1 3 3.51 6.50 1.44 o 7 1 3 15.26 20.29 2.24 o -7 2 3 34.21 41.09 2.01 o -6 2 3 10.39 15.02 1.31 o -5 2 3 0.02 2.50 0.77 o -4 2 3 306.11 288.61 3.78 o -3 2 3 13.94 13.97 0.60 o -2 2 3 551.87 586.24 5.31 o -1 2 3 5424.33 5923.00 54.88 o 0 2 3 1342.66 1343.99 11.95 o 1 2 3 2747.89 3016.03 28.75 o 2 2 3 1474.72 1478.48 15.81 o 3 2 3 2.73 3.60 0.38 o 4 2 3 494.45 459.71 5.14 o 5 2 3 231.07 223.10 4.31 o 6 2 3 235.01 229.76 4.67 o 7 2 3 107.23 105.50 4.75 o -7 3 3 63.74 66.00 3.71 o -6 3 3 18.64 24.17 1.81 o -5 3 3 535.33 509.47 6.82 o -4 3 3 146.02 157.41 2.57 o -3 3 3 255.25 255.21 2.89 o -2 3 3 914.75 985.80 8.43 o -1 3 3 1185.98 1240.53 12.43 o 0 3 3 3.30 4.05 0.41 o 1 3 3 3082.58 3177.42 27.53 o 2 3 3 401.75 468.17 4.85 o 3 3 3 246.57 247.30 3.13 o 4 3 3 4.38 6.27 0.49 o 5 3 3 0.18 6.75 1.80 o 6 3 3 2.35 3.44 0.95 o 7 3 3 13.04 19.40 1.45 o -7 4 3 16.73 23.63 1.90 o -6 4 3 0.22 5.76 1.35 o -5 4 3 0.53 4.91 0.96 o -4 4 3 0.14 0.95 0.74 o -3 4 3 59.87 100.15 17.18 o -2 4 3 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11.97 o 2 4 11 33.40 34.85 2.31 o 3 4 11 166.63 160.02 4.23 o 4 4 11 16.27 18.03 1.93 o -3 5 11 40.26 45.10 2.55 o -2 5 11 552.25 538.63 10.24 o -1 5 11 89.25 93.31 3.02 o 0 5 11 15.78 17.34 1.78 o 1 5 11 135.71 132.80 5.34 o 2 5 11 5.50 15.45 1.90 o 3 5 11 0.19 -0.23 1.01 o -3 6 11 4.62 8.50 1.52 o -2 6 11 163.81 161.52 4.97 o -1 6 11 101.45 100.55 3.18 o 0 6 11 268.44 265.14 5.52 o 1 6 11 44.59 47.49 2.68 o 2 6 11 233.00 227.54 7.34 o 3 6 11 53.78 50.28 2.75 o -2 7 11 9.33 9.90 2.69 o -1 7 11 165.24 161.87 4.19 o 0 7 11 23.25 24.95 1.65 o 1 7 11 17.47 24.76 1.74 o 2 7 11 14.77 15.45 1.65 o -2 8 11 0.89 5.37 1.26 o -1 8 11 68.03 70.71 3.27 o 0 8 11 67.64 77.36 2.84 o 1 8 11 55.48 55.88 2.41 o 2 8 11 68.20 71.94 4.11 o 0 0 12 322.23 310.85 8.37 o 2 0 12 871.41 863.07 17.72 o -3 1 12 34.57 41.40 2.31 o -2 1 12 12.51 16.12 2.46 o -1 1 12 20.90 24.32 1.82 o 0 1 12 4.53 6.30 1.23 o 1 1 12 34.15 34.52 1.90 o 2 1 12 236.78 230.80 5.21 o 3 1 12 66.61 73.20 3.34 o -3 2 12 250.33 270.94 8.06 o 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193.49 7.01 o 0 1 13 146.46 155.06 4.85 o 1 1 13 435.25 425.10 9.11 o 2 1 13 377.19 370.89 7.20 o -2 2 13 145.62 150.06 6.10 o -1 2 13 52.69 59.45 4.50 o 0 2 13 36.06 37.36 2.39 o 1 2 13 37.41 37.58 2.74 o 2 2 13 101.16 105.06 4.16 o -2 3 13 0.73 4.03 1.32 o -1 3 13 10.68 15.60 1.66 o 0 3 13 222.93 229.16 6.21 o 1 3 13 190.24 186.01 5.59 o 2 3 13 101.45 99.73 4.09 o -2 4 13 12.69 13.17 2.09 o -1 4 13 56.83 58.31 2.97 o 0 4 13 3.22 4.06 1.25 o 1 4 13 21.12 25.61 2.12 o -1 5 13 6.65 9.97 1.42 o 0 5 13 107.36 114.02 4.28 o 1 5 13 1.55 1.62 1.35 o 0 0 14 53.49 67.84 5.89 o 0 1 14 248.91 257.44 8.64 o