#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2015757.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015757_Fobs loop_ _publ_author_name 'Jones, Nigel A.' 'Jenkinson, Sarah F.' 'Soengas, Raquel' 'Izumori, Ken' 'Fleet, George W. J.' 'Watkin, David J.' _publ_section_title ; The concomitant crystallization of two polymorphs of 1-deoxy-\a-D-tagatose ; _journal_coeditor_code SK3070 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o7 _journal_page_last o10 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _audit_creation_date 06-10-06 _audit_creation_method CRYSTALS _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 6.0243(2) _cell_length_b 7.5022(3) _cell_length_c 15.9717(8) _[local]_cod_data_source_file sk3070Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 2 0 0 94.10 89.24 3.00 o 4 0 0 112.00 125.53 3.50 o 6 0 0 807.20 740.05 58.10 o 2 1 0 372.30 359.59 6.70 o 3 1 0 2741.60 2765.43 51.60 o 4 1 0 44.80 41.24 1.20 o 5 1 0 100.90 100.66 3.30 o 6 1 0 209.20 213.22 7.90 o 7 1 0 79.90 71.79 10.20 o 0 2 0 3736.50 3807.82 133.00 o 1 2 0 1570.30 1556.46 36.80 o 2 2 0 1706.40 1613.72 33.10 o 3 2 0 133.80 124.24 2.60 o 4 2 0 67.40 75.88 1.80 o 5 2 0 555.40 551.12 16.10 o 6 2 0 12.10 13.39 1.80 o 7 2 0 48.30 48.40 8.00 o 2 3 0 56.90 47.41 1.30 o 3 3 0 5.50 5.11 0.60 o 4 3 0 73.90 77.11 2.00 o 5 3 0 193.30 212.99 5.40 o 6 3 0 7.10 4.80 1.90 o 7 3 0 30.30 30.06 3.40 o 0 4 0 35.60 40.10 1.90 o 1 4 0 688.90 639.17 15.90 o 2 4 0 1362.70 1283.92 31.60 o 3 4 0 1.40 0.24 0.70 o 4 4 0 0.60 1.16 1.08 o 5 4 0 492.80 492.87 14.10 o 6 4 0 22.40 24.96 3.00 o 7 4 0 32.80 33.99 3.90 o 1 5 0 26.20 26.60 1.40 o 2 5 0 294.30 289.26 7.30 o 3 5 0 71.10 69.70 2.20 o 4 5 0 13.80 18.35 1.20 o 5 5 0 23.20 20.83 2.50 o 6 5 0 148.40 133.89 9.40 o 0 6 0 4254.10 3997.63 190.50 o 1 6 0 60.10 65.02 2.20 o 2 6 0 60.40 78.16 2.10 o 3 6 0 62.90 75.65 2.40 o 4 6 0 19.50 21.55 1.70 o 5 6 0 24.00 21.55 3.80 o 6 6 0 261.90 228.36 17.40 o 1 7 0 16.40 19.49 1.80 o 2 7 0 3.30 6.61 1.10 o 3 7 0 71.20 74.92 3.30 o 4 7 0 -1.50 0.27 1.90 o 5 7 0 -3.60 0.28 3.30 o 0 8 0 16.80 19.82 4.20 o 1 8 0 4.80 0.16 3.00 o 2 8 0 14.50 16.20 2.40 o 3 8 0 2.60 0.02 3.50 o 4 8 0 31.40 26.65 6.30 o 1 9 0 46.40 43.58 5.30 o 2 9 0 7.20 13.65 4.60 o 2 0 1 1.10 0.09 0.10 o 3 0 1 238.70 222.57 4.20 o 4 0 1 512.00 518.87 10.20 o 5 0 1 280.20 262.43 12.60 o 6 0 1 145.80 144.17 5.20 o 7 0 1 41.80 36.11 6.60 o 2 1 1 1467.05 1451.00 28.12 o 3 1 1 213.80 211.44 4.01 o 4 1 1 28.80 31.12 1.02 o 5 1 1 37.50 40.50 1.56 o 6 1 1 92.25 91.99 3.96 o 7 1 1 10.80 19.56 6.25 o 0 2 1 30.40 36.00 1.00 o 1 2 1 394.85 398.87 9.25 o 2 2 1 1673.50 1593.41 34.52 o 3 2 1 203.55 197.59 4.45 o 4 2 1 162.55 161.10 3.87 o 5 2 1 92.85 97.21 2.91 o 6 2 1 79.50 84.92 3.51 o 7 2 1 0.95 1.42 4.35 o 0 3 1 222.20 217.59 5.60 o 1 3 1 1569.95 1565.97 35.55 o 2 3 1 1038.95 935.90 23.45 o 3 3 1 586.80 564.24 14.40 o 4 3 1 479.50 475.78 12.48 o 5 3 1 270.60 290.10 7.41 o 6 3 1 16.65 15.98 2.40 o 7 3 1 18.50 14.66 5.38 o 0 4 1 672.30 652.46 16.50 o 1 4 1 67.20 58.27 1.90 o 2 4 1 354.75 330.48 8.87 o 3 4 1 77.35 80.54 2.20 o 4 4 1 52.50 59.17 1.86 o 5 4 1 64.00 71.01 2.35 o 6 4 1 80.55 81.17 5.90 o 7 4 1 3.60 6.50 2.66 o 0 5 1 137.80 126.82 3.60 o 1 5 1 286.00 273.97 7.26 o 2 5 1 85.20 80.94 2.40 o 3 5 1 329.10 319.94 8.51 o 4 5 1 32.25 29.75 1.65 o 5 5 1 4.00 3.04 2.60 o 6 5 1 11.75 12.57 2.80 o 0 6 1 1609.00 1587.26 38.20 o 1 6 1 22.75 21.78 1.40 o 2 6 1 9.35 8.47 1.10 o 3 6 1 79.80 105.13 2.90 o 4 6 1 34.90 33.69 2.10 o 5 6 1 20.10 18.49 3.21 o 6 6 1 133.95 116.97 9.36 o 0 7 1 176.20 184.33 5.50 o 1 7 1 139.90 152.96 4.65 o 2 7 1 1.30 0.52 1.44 o 3 7 1 107.15 113.08 4.10 o 4 7 1 12.40 15.43 2.25 o 5 7 1 23.10 25.08 5.67 o 0 8 1 12.50 13.42 3.10 o 1 8 1 22.70 24.41 4.28 o 2 8 1 64.95 62.06 4.40 o 3 8 1 9.20 11.91 2.90 o 4 8 1 8.95 8.16 6.25 o 0 9 1 12.30 10.62 3.30 o 1 9 1 79.30 70.79 6.65 o 2 9 1 33.40 25.71 4.25 o 2 0 2 656.60 686.34 14.80 o 3 0 2 2.90 1.93 0.50 o 4 0 2 11.80 11.83 0.90 o 5 0 2 4.10 4.60 0.80 o 6 0 2 23.20 25.40 4.10 o 7 0 2 171.10 170.61 14.90 o 2 1 2 11.70 9.69 0.55 o 3 1 2 473.50 471.62 10.46 o 4 1 2 133.00 132.81 3.72 o 5 1 2 30.70 29.82 1.61 o 6 1 2 48.70 50.67 2.50 o 7 1 2 95.20 90.49 8.67 o 0 2 2 23.20 20.32 0.90 o 1 2 2 1353.60 1433.99 27.35 o 2 2 2 87.25 86.63 1.80 o 3 2 2 461.10 441.34 9.90 o 4 2 2 179.70 180.38 4.26 o 5 2 2 7.05 8.39 1.10 o 6 2 2 31.00 38.13 2.73 o 7 2 2 2.40 5.45 6.60 o 0 3 2 893.50 905.53 20.60 o 1 3 2 156.45 162.22 3.55 o 2 3 2 2756.85 2634.43 54.07 o 3 3 2 258.00 239.07 5.66 o 4 3 2 258.75 256.58 5.96 o 5 3 2 156.60 162.41 4.35 o 6 3 2 32.95 32.02 3.11 o 7 3 2 26.70 29.64 3.70 o 0 4 2 245.30 272.35 6.00 o 1 4 2 1051.90 1005.95 23.20 o 2 4 2 149.50 140.15 3.81 o 3 4 2 532.35 533.55 13.10 o 4 4 2 383.75 384.46 9.11 o 5 4 2 201.95 210.51 6.65 o 6 4 2 10.40 12.47 2.75 o 7 4 2 24.70 27.08 3.50 o 0 5 2 89.30 93.55 2.60 o 1 5 2 159.90 157.03 3.75 o 2 5 2 252.15 251.75 6.61 o 3 5 2 42.80 46.33 1.75 o 4 5 2 75.10 80.59 2.82 o 5 5 2 4.05 5.60 1.56 o 6 5 2 19.50 16.63 3.31 o 0 6 2 96.30 95.71 3.10 o 1 6 2 217.90 217.21 5.95 o 2 6 2 19.00 23.63 1.26 o 3 6 2 68.30 69.65 2.70 o 4 6 2 2.90 1.40 2.25 o 5 6 2 115.55 115.76 7.83 o 6 6 2 52.70 52.70 6.67 o 0 7 2 857.10 814.99 27.70 o 1 7 2 86.80 84.28 3.69 o 2 7 2 209.55 221.36 8.12 o 3 7 2 12.75 14.80 2.00 o 4 7 2 23.60 26.38 3.40 o 5 7 2 19.60 14.97 4.24 o 0 8 2 25.30 25.61 3.40 o 1 8 2 20.80 20.43 3.15 o 2 8 2 38.35 38.60 4.85 o 3 8 2 31.85 32.84 4.10 o 4 8 2 17.50 14.12 5.55 o 0 9 2 4.40 1.13 4.10 o 1 9 2 82.50 77.69 7.25 o 2 9 2 32.60 30.18 4.65 o 2 0 3 1894.00 1916.47 46.80 o 3 0 3 928.60 918.75 19.60 o 4 0 3 42.20 39.16 1.50 o 5 0 3 493.30 512.75 13.80 o 6 0 3 338.50 323.88 11.60 o 7 0 3 13.50 11.64 2.20 o 1 1 3 1083.55 1206.49 24.74 o 2 1 3 861.65 846.18 19.21 o 3 1 3 662.90 625.53 15.40 o 4 1 3 12.10 14.03 0.76 o 5 1 3 51.00 50.69 2.26 o 6 1 3 370.85 365.47 15.05 o 7 1 3 99.65 93.47 8.22 o 0 2 3 129.80 126.79 3.30 o 1 2 3 2946.95 2880.20 67.75 o 2 2 3 1002.20 996.50 22.21 o 3 2 3 65.55 67.14 1.80 o 4 2 3 353.45 347.24 7.57 o 5 2 3 47.40 50.05 1.96 o 6 2 3 140.25 130.25 9.30 o 7 2 3 30.80 28.46 5.19 o 0 3 3 15.90 10.23 0.90 o 1 3 3 698.90 702.86 14.66 o 2 3 3 3087.10 2862.03 64.35 o 3 3 3 90.65 90.01 2.25 o 4 3 3 2005.50 2025.44 47.96 o 5 3 3 1005.85 996.89 28.29 o 6 3 3 48.35 43.69 6.11 o 7 3 3 1.10 3.99 3.10 o 0 4 3 198.60 224.13 4.80 o 1 4 3 548.25 551.22 13.07 o 2 4 3 652.35 642.99 16.77 o 3 4 3 10.60 9.43 0.95 o 4 4 3 121.30 118.41 3.35 o 5 4 3 27.55 34.25 1.76 o 6 4 3 9.45 8.33 2.70 o 7 4 3 11.70 14.37 4.00 o 0 5 3 1186.20 1192.50 30.80 o 1 5 3 10.10 12.95 1.15 o 2 5 3 68.40 69.88 2.30 o 3 5 3 112.85 111.52 3.45 o 4 5 3 13.30 12.35 1.25 o 5 5 3 53.15 50.58 4.17 o 6 5 3 41.10 36.64 5.17 o 0 6 3 21.50 20.20 1.70 o 1 6 3 827.40 786.87 25.06 o 2 6 3 265.30 277.73 9.30 o 3 6 3 48.80 53.86 2.65 o 4 6 3 30.45 34.41 2.40 o 5 6 3 76.80 75.76 7.60 o 6 6 3 114.75 112.25 10.75 o 0 7 3 8.80 9.59 1.70 o 1 7 3 133.60 122.17 5.60 o 2 7 3 80.75 79.87 3.91 o 3 7 3 118.40 134.04 5.40 o 4 7 3 44.50 45.65 4.73 o 5 7 3 10.10 10.15 3.96 o 0 8 3 -0.50 1.04 3.54 o 1 8 3 167.95 142.92 9.35 o 2 8 3 12.20 12.93 2.96 o 3 8 3 3.30 3.18 2.95 o 4 8 3 29.35 27.68 6.51 o 0 9 3 0.20 2.45 3.22 o 1 9 3 1.40 0.39 4.57 o 2 9 3 317.35 279.37 17.90 o 0 0 4 5883.00 6293.54 273.30 o 1 0 4 795.30 858.03 23.10 o 2 0 4 3986.80 3981.91 180.10 o 3 0 4 490.50 439.43 11.50 o 4 0 4 0.50 0.05 1.27 o 5 0 4 150.90 159.32 4.50 o 6 0 4 578.40 564.75 19.00 o 7 0 4 239.20 215.21 13.20 o 0 1 4 8.00 9.57 0.60 o 1 1 4 2786.10 2956.82 68.62 o 2 1 4 742.00 802.98 15.66 o 3 1 4 127.15 111.46 3.28 o 4 1 4 46.05 42.93 1.56 o 5 1 4 20.70 24.02 1.82 o 6 1 4 54.45 58.17 3.69 o 7 1 4 126.85 130.73 8.01 o 0 2 4 855.40 905.99 20.40 o 1 2 4 150.90 161.43 3.27 o 2 2 4 616.55 618.98 13.09 o 3 2 4 13.95 14.39 0.76 o 4 2 4 156.10 153.33 3.81 o 5 2 4 108.50 115.68 3.70 o 6 2 4 80.45 76.45 5.85 o 7 2 4 7.00 3.68 3.98 o 0 3 4 17.90 21.11 0.70 o 1 3 4 421.10 433.35 8.96 o 2 3 4 400.90 411.51 9.11 o 3 3 4 16.05 14.40 0.90 o 4 3 4 992.85 975.28 22.91 o 5 3 4 203.70 204.56 8.94 o 6 3 4 152.65 152.15 7.87 o 7 3 4 3.45 1.77 5.60 o 0 4 4 223.90 219.82 5.50 o 1 4 4 257.10 249.34 6.45 o 2 4 4 106.85 103.68 2.85 o 3 4 4 51.70 45.36 1.80 o 4 4 4 129.05 130.74 3.82 o 5 4 4 143.30 153.56 4.86 o 6 4 4 56.30 58.10 5.60 o 0 5 4 212.90 217.29 5.30 o 1 5 4 363.30 344.53 10.35 o 2 5 4 14.55 18.14 1.35 o 3 5 4 58.55 51.07 2.40 o 4 5 4 6.90 6.54 1.25 o 5 5 4 23.00 29.09 2.69 o 6 5 4 106.80 100.70 9.14 o 0 6 4 655.70 639.73 19.00 o 1 6 4 4.50 5.54 1.35 o 2 6 4 118.50 121.74 4.40 o 3 6 4 50.55 57.67 2.92 o 4 6 4 3.45 1.72 1.56 o 5 6 4 66.10 52.89 6.02 o 0 7 4 25.90 30.28 2.40 o 1 7 4 27.90 33.89 2.65 o 2 7 4 52.30 57.52 3.35 o 3 7 4 16.00 17.74 2.71 o 4 7 4 2.55 0.96 4.31 o 5 7 4 1.20 1.09 3.52 o 0 8 4 5.40 0.93 2.90 o 1 8 4 62.60 59.07 4.95 o 2 8 4 7.75 8.40 3.65 o 3 8 4 -2.75 0.14 2.28 o 4 8 4 6.00 3.18 4.40 o 0 9 4 1.90 1.97 3.30 o 1 9 4 29.85 29.47 4.20 o 2 9 4 92.50 87.35 7.80 o 1 0 5 3865.30 4155.69 80.20 o 2 0 5 2963.50 2955.42 68.40 o 3 0 5 746.70 713.48 14.90 o 4 0 5 17.10 20.35 1.30 o 5 0 5 -0.20 0.03 1.07 o 6 0 5 256.50 257.96 9.50 o 7 0 5 470.20 421.76 24.10 o 0 1 5 11.30 8.65 0.60 o 1 1 5 771.50 754.47 17.60 o 2 1 5 345.50 332.66 8.16 o 3 1 5 795.05 794.97 19.95 o 4 1 5 251.55 244.52 5.72 o 5 1 5 681.15 676.21 20.06 o 6 1 5 90.40 77.66 6.68 o 7 1 5 9.70 9.74 2.67 o 0 2 5 112.70 111.90 3.00 o 1 2 5 645.40 644.52 13.45 o 2 2 5 232.75 225.73 4.90 o 3 2 5 227.95 224.96 4.81 o 4 2 5 642.85 658.90 14.82 o 5 2 5 26.15 28.06 1.46 o 6 2 5 67.40 73.82 6.96 o 7 2 5 86.20 83.95 8.25 o 0 3 5 -0.80 0.40 1.43 o 1 3 5 606.70 658.01 13.18 o 2 3 5 -0.90 0.00 0.83 o 3 3 5 124.40 128.53 3.10 o 4 3 5 528.75 524.20 11.61 o 5 3 5 222.50 224.55 7.13 o 6 3 5 164.45 164.04 8.91 o 7 3 5 -0.60 1.71 4.24 o 0 4 5 23.00 24.45 1.60 o 1 4 5 111.45 107.35 3.21 o 2 4 5 567.90 527.65 14.16 o 3 4 5 98.30 95.78 2.95 o 4 4 5 836.85 844.62 23.22 o 5 4 5 9.90 12.80 1.37 o 6 4 5 48.20 49.22 4.56 o 0 5 5 0.40 2.21 1.26 o 1 5 5 33.20 30.67 1.75 o 2 5 5 62.55 59.17 2.50 o 3 5 5 80.35 88.08 3.05 o 4 5 5 81.45 84.86 3.42 o 5 5 5 45.40 48.66 3.45 o 6 5 5 16.40 16.96 3.82 o 0 6 5 235.50 224.69 8.10 o 1 6 5 261.20 261.90 8.26 o 2 6 5 52.85 55.10 2.81 o 3 6 5 117.85 127.77 4.91 o 4 6 5 5.95 3.07 2.20 o 5 6 5 10.30 5.46 2.87 o 0 7 5 12.00 9.61 2.20 o 1 7 5 395.60 378.18 16.80 o 2 7 5 49.15 55.43 3.45 o 3 7 5 23.85 26.22 2.95 o 4 7 5 9.40 8.36 3.39 o 5 7 5 67.10 62.48 8.15 o 0 8 5 -1.40 0.85 3.10 o 1 8 5 7.60 9.39 3.25 o 2 8 5 36.60 38.29 4.67 o 3 8 5 8.00 3.58 4.36 o 0 9 5 16.20 18.87 4.20 o 1 9 5 0.95 2.82 4.64 o 2 9 5 8.45 5.64 4.09 o 0 0 6 2.50 2.08 0.70 o 1 0 6 683.60 693.84 13.40 o 2 0 6 2376.10 2409.67 48.60 o 3 0 6 1019.40 977.64 22.00 o 4 0 6 0.30 0.00 1.20 o 5 0 6 25.80 25.17 1.90 o 6 0 6 17.70 15.59 2.30 o 7 0 6 297.90 288.30 13.70 o 0 1 6 850.50 876.49 18.60 o 1 1 6 632.00 653.07 13.80 o 2 1 6 134.20 133.76 3.59 o 3 1 6 69.95 72.64 1.88 o 4 1 6 251.75 257.13 5.66 o 5 1 6 27.95 32.36 2.22 o 6 1 6 16.25 17.03 3.65 o 7 1 6 143.75 139.09 8.47 o 0 2 6 727.50 740.36 15.60 o 1 2 6 16.85 15.63 0.95 o 2 2 6 367.55 367.40 8.22 o 3 2 6 186.00 196.76 4.10 o 4 2 6 609.20 614.94 12.90 o 5 2 6 16.80 18.20 1.40 o 6 2 6 10.30 8.78 4.65 o 7 2 6 58.30 48.36 7.12 o 0 3 6 153.50 145.07 3.90 o 1 3 6 49.85 48.81 1.60 o 2 3 6 235.20 215.80 5.26 o 3 3 6 2345.30 2293.19 50.58 o 4 3 6 88.50 86.44 2.55 o 5 3 6 251.80 246.51 8.93 o 6 3 6 55.55 57.57 4.16 o 7 3 6 9.95 9.03 4.81 o 0 4 6 390.90 384.81 10.80 o 1 4 6 45.70 47.18 1.70 o 2 4 6 663.60 636.12 15.36 o 3 4 6 61.25 64.70 2.10 o 4 4 6 130.55 130.38 4.26 o 5 4 6 21.90 20.36 1.70 o 6 4 6 49.65 47.63 4.62 o 0 5 6 21.70 20.30 1.70 o 1 5 6 178.55 167.39 5.47 o 2 5 6 96.05 100.80 3.54 o 3 5 6 58.85 68.21 2.55 o 4 5 6 88.85 87.52 4.26 o 5 5 6 126.80 134.56 6.72 o 6 5 6 41.10 44.67 5.20 o 0 6 6 3.30 2.98 1.30 o 1 6 6 441.05 439.30 13.59 o 2 6 6 697.75 686.55 25.72 o 3 6 6 109.10 111.73 5.30 o 4 6 6 20.15 14.38 2.71 o 5 6 6 20.90 20.44 4.85 o 0 7 6 33.80 40.36 3.10 o 1 7 6 41.55 43.61 3.31 o 2 7 6 16.45 16.32 2.55 o 3 7 6 19.90 20.32 3.51 o 4 7 6 176.45 171.66 14.42 o 0 8 6 3.20 2.72 3.10 o 1 8 6 28.65 28.42 3.75 o 2 8 6 -0.40 0.91 3.24 o 3 8 6 63.95 60.64 7.14 o 0 9 6 0.70 2.88 4.85 o 1 9 6 1.20 0.17 3.91 o 1 0 7 2687.20 2819.86 53.10 o 2 0 7 3082.30 3025.10 65.30 o 3 0 7 6.80 10.52 0.60 o 4 0 7 123.50 109.94 3.50 o 5 0 7 4.00 9.49 1.80 o 6 0 7 3.10 4.92 5.40 o 7 0 7 125.40 109.10 7.70 o 0 1 7 291.40 264.40 5.50 o 1 1 7 11.70 11.59 0.80 o 2 1 7 96.65 97.47 2.51 o 3 1 7 209.85 206.74 4.49 o 4 1 7 185.15 186.60 4.60 o 5 1 7 51.10 51.08 2.89 o 6 1 7 18.20 19.46 3.77 o 7 1 7 107.60 91.94 8.75 o 0 2 7 14.90 18.54 0.90 o 1 2 7 328.05 287.75 7.94 o 2 2 7 280.55 287.84 6.93 o 3 2 7 200.70 196.29 4.58 o 4 2 7 247.25 253.44 5.61 o 5 2 7 3.25 4.55 0.90 o 6 2 7 43.80 42.17 5.14 o 7 2 7 14.20 11.74 5.61 o 0 3 7 330.20 299.18 7.50 o 1 3 7 71.65 66.81 2.05 o 2 3 7 882.05 871.01 17.45 o 3 3 7 112.70 112.88 3.26 o 4 3 7 211.25 211.95 5.26 o 5 3 7 18.30 22.24 1.71 o 6 3 7 78.65 71.37 6.25 o 0 4 7 47.00 45.67 1.50 o 1 4 7 206.05 204.14 4.35 o 2 4 7 54.30 57.38 1.80 o 3 4 7 409.00 408.97 10.31 o 4 4 7 102.65 104.09 3.52 o 5 4 7 7.80 8.31 2.02 o 6 4 7 24.95 31.28 3.60 o 0 5 7 366.30 357.24 10.00 o 1 5 7 16.70 19.27 1.60 o 2 5 7 13.70 17.04 1.45 o 3 5 7 32.35 35.04 2.29 o 4 5 7 61.60 61.11 3.16 o 5 5 7 29.20 31.53 3.13 o 6 5 7 30.10 28.89 4.70 o 0 6 7 35.40 39.43 2.20 o 1 6 7 239.15 241.52 9.45 o 2 6 7 162.65 168.55 6.53 o 3 6 7 97.50 101.11 4.90 o 4 6 7 32.05 33.60 4.43 o 5 6 7 50.25 48.88 5.71 o 0 7 7 341.40 333.73 13.30 o 1 7 7 41.10 41.44 3.51 o 2 7 7 15.20 13.00 3.24 o 3 7 7 83.30 80.36 5.86 o 4 7 7 22.40 30.97 4.95 o 0 8 7 0.50 0.10 3.68 o 1 8 7 6.15 10.12 3.01 o 2 8 7 28.85 29.38 4.05 o 3 8 7 2.55 4.38 4.59 o 0 9 7 23.60 24.11 4.90 o 1 9 7 7.25 4.46 5.98 o 0 0 8 1208.60 1237.50 45.70 o 1 0 8 290.00 295.75 5.90 o 2 0 8 254.30 235.94 5.40 o 3 0 8 351.90 351.27 7.80 o 4 0 8 68.70 77.54 1.90 o 5 0 8 293.90 303.33 8.80 o 6 0 8 19.90 21.72 6.60 o 7 0 8 -3.90 0.08 3.30 o 0 1 8 2498.00 2520.31 57.10 o 1 1 8 1048.90 1053.02 22.37 o 2 1 8 330.85 349.05 7.50 o 3 1 8 286.40 303.84 5.78 o 4 1 8 246.80 237.95 6.61 o 5 1 8 7.10 7.83 1.76 o 6 1 8 15.50 15.90 4.28 o 7 1 8 77.30 63.53 8.28 o 0 2 8 1063.70 1014.83 23.00 o 1 2 8 395.45 420.04 8.79 o 2 2 8 418.80 405.15 9.28 o 3 2 8 13.95 16.22 0.92 o 4 2 8 88.40 92.86 2.51 o 5 2 8 6.10 7.59 1.00 o 6 2 8 150.40 139.47 9.95 o 7 2 8 13.75 12.66 4.88 o 0 3 8 5.80 6.94 1.00 o 1 3 8 11.40 7.27 1.15 o 2 3 8 71.50 66.89 2.05 o 3 3 8 918.75 907.45 23.19 o 4 3 8 391.00 400.17 10.07 o 5 3 8 35.65 39.33 2.21 o 6 3 8 26.95 28.99 5.45 o 0 4 8 360.90 344.01 8.20 o 1 4 8 63.20 57.26 1.90 o 2 4 8 304.60 301.61 7.95 o 3 4 8 386.00 373.74 10.71 o 4 4 8 9.60 8.18 1.20 o 5 4 8 44.75 53.97 3.26 o 6 4 8 5.55 5.07 2.94 o 0 5 8 50.30 49.93 2.60 o 1 5 8 52.30 60.33 2.50 o 2 5 8 131.15 137.15 4.20 o 3 5 8 243.65 227.10 8.43 o 4 5 8 15.85 17.44 2.47 o 5 5 8 164.80 149.27 10.14 o 0 6 8 72.60 67.49 4.60 o 1 6 8 140.55 136.66 6.34 o 2 6 8 344.20 339.50 14.90 o 3 6 8 10.85 14.39 2.52 o 4 6 8 13.05 15.65 4.09 o 5 6 8 55.60 61.90 6.92 o 0 7 8 70.40 66.04 4.80 o 1 7 8 82.15 86.49 5.30 o 2 7 8 176.20 183.06 9.87 o 3 7 8 5.60 6.34 4.52 o 4 7 8 72.85 65.64 7.55 o 0 8 8 -4.10 1.08 2.80 o 1 8 8 66.30 64.28 5.95 o 2 8 8 25.60 26.95 4.80 o 3 8 8 31.10 23.95 6.30 o 1 0 9 1757.40 1707.96 37.10 o 2 0 9 1004.60 990.74 23.10 o 3 0 9 7.30 6.80 0.90 o 4 0 9 551.30 536.66 16.00 o 5 0 9 44.30 40.29 2.70 o 6 0 9 61.30 59.44 8.10 o 7 0 9 321.40 292.41 16.90 o 0 1 9 199.80 212.09 4.50 o 1 1 9 220.45 207.74 4.90 o 2 1 9 562.00 552.55 11.95 o 3 1 9 310.75 299.37 7.57 o 4 1 9 20.40 24.01 1.62 o 5 1 9 442.65 403.47 14.45 o 6 1 9 14.35 11.31 4.34 o 7 1 9 8.80 10.32 3.50 o 0 2 9 237.50 265.10 5.10 o 1 2 9 187.50 172.08 4.32 o 2 2 9 150.95 145.08 3.99 o 3 2 9 395.90 409.58 9.20 o 4 2 9 241.15 244.58 6.37 o 5 2 9 84.55 89.48 3.55 o 6 2 9 58.35 59.92 6.26 o 0 3 9 0.50 0.02 1.27 o 1 3 9 37.40 40.22 1.70 o 2 3 9 26.35 27.04 1.40 o 3 3 9 825.55 825.07 18.55 o 4 3 9 7.00 8.50 1.06 o 5 3 9 77.40 74.95 3.54 o 6 3 9 118.90 129.33 11.70 o 0 4 9 145.70 142.96 4.00 o 1 4 9 77.35 72.54 2.51 o 2 4 9 97.40 101.52 2.85 o 3 4 9 396.20 401.88 10.87 o 4 4 9 76.25 82.84 3.10 o 5 4 9 63.70 68.25 4.33 o 6 4 9 157.85 153.56 10.48 o 0 5 9 212.30 218.10 6.50 o 1 5 9 45.80 45.66 2.28 o 2 5 9 102.15 99.60 3.96 o 3 5 9 16.40 15.60 2.10 o 4 5 9 9.95 10.18 2.15 o 5 5 9 27.75 34.08 3.71 o 0 6 9 37.90 32.98 3.50 o 1 6 9 351.10 335.29 14.87 o 2 6 9 51.25 59.35 3.41 o 3 6 9 3.70 3.14 2.26 o 4 6 9 31.40 33.75 4.30 o 5 6 9 36.75 35.07 7.26 o 0 7 9 -1.70 0.01 2.60 o 1 7 9 16.25 19.50 3.21 o 2 7 9 98.05 91.66 6.55 o 3 7 9 15.65 13.94 5.10 o 4 7 9 8.40 11.54 5.10 o 0 8 9 28.20 28.64 4.80 o 1 8 9 -1.55 1.45 4.71 o 2 8 9 28.00 34.82 4.55 o 0 0 10 486.50 501.94 14.10 o 1 0 10 352.30 353.65 7.60 o 2 0 10 340.20 327.60 7.50 o 3 0 10 4.80 3.36 0.90 o 4 0 10 22.10 34.29 1.30 o 5 0 10 5.00 7.59 1.90 o 6 0 10 -2.50 9.78 7.20 o 0 1 10 35.70 30.23 1.50 o 1 1 10 54.50 51.10 1.90 o 2 1 10 856.35 844.41 18.74 o 3 1 10 106.90 103.31 3.52 o 4 1 10 119.05 134.94 3.61 o 5 1 10 129.90 117.45 5.10 o 6 1 10 56.40 51.78 7.49 o 0 2 10 55.30 59.46 1.90 o 1 2 10 238.15 240.32 5.55 o 2 2 10 323.15 315.06 7.75 o 3 2 10 326.80 334.37 7.95 o 4 2 10 15.30 16.47 1.25 o 5 2 10 70.70 73.56 3.36 o 6 2 10 122.45 117.37 10.54 o 0 3 10 11.20 14.31 1.20 o 1 3 10 384.45 388.60 9.10 o 2 3 10 124.65 127.66 3.56 o 3 3 10 1527.35 1486.34 36.81 o 4 3 10 79.65 83.62 2.80 o 5 3 10 61.60 62.67 4.16 o 6 3 10 80.70 76.45 7.53 o 0 4 10 258.60 247.48 6.70 o 1 4 10 13.25 14.13 1.40 o 2 4 10 117.15 118.50 3.50 o 3 4 10 156.60 160.95 5.30 o 4 4 10 78.25 82.25 3.50 o 5 4 10 12.80 9.33 3.07 o 6 4 10 28.70 28.59 7.43 o 0 5 10 11.20 13.63 1.00 o 1 5 10 86.45 88.18 3.56 o 2 5 10 112.10 119.14 3.80 o 3 5 10 13.70 14.45 2.32 o 4 5 10 58.70 62.74 4.44 o 5 5 10 19.40 22.70 4.39 o 0 6 10 36.20 35.21 3.60 o 1 6 10 89.50 86.47 5.10 o 2 6 10 99.05 98.04 5.35 o 3 6 10 13.40 13.08 2.81 o 4 6 10 61.10 69.56 5.27 o 0 7 10 35.80 27.57 4.80 o 1 7 10 28.75 33.76 3.80 o 2 7 10 116.20 111.12 8.06 o 3 7 10 36.80 34.04 4.82 o 0 8 10 1.40 1.97 3.90 o 1 8 10 1.55 0.89 4.90 o 2 8 10 5.50 9.50 4.20 o 1 0 11 17.50 15.42 1.50 o 2 0 11 647.80 600.04 14.30 o 3 0 11 2.30 1.18 1.10 o 4 0 11 9.40 10.76 1.00 o 5 0 11 310.90 275.64 12.60 o 6 0 11 22.20 17.83 6.00 o 0 1 11 62.60 65.29 2.30 o 1 1 11 296.40 294.48 7.41 o 2 1 11 4.05 6.15 1.05 o 3 1 11 63.80 64.85 2.45 o 4 1 11 43.40 42.00 1.97 o 5 1 11 82.20 81.28 4.50 o 6 1 11 16.35 14.06 5.89 o 0 2 11 479.70 493.17 11.30 o 1 2 11 37.20 32.09 1.76 o 2 2 11 234.00 224.86 6.38 o 3 2 11 175.50 174.53 5.39 o 4 2 11 0.00 0.30 0.97 o 5 2 11 36.30 38.75 2.96 o 6 2 11 29.95 31.06 6.17 o 0 3 11 63.50 66.24 2.40 o 1 3 11 146.50 155.73 4.35 o 2 3 11 229.90 219.54 6.23 o 3 3 11 248.50 252.53 7.27 o 4 3 11 181.40 183.82 5.96 o 5 3 11 30.55 31.97 3.63 o 6 3 11 207.20 175.47 15.57 o 0 4 11 75.50 83.26 2.90 o 1 4 11 384.85 383.45 10.55 o 2 4 11 170.90 162.51 4.90 o 3 4 11 68.50 69.91 3.01 o 4 4 11 20.80 23.40 2.51 o 5 4 11 15.35 16.76 3.00 o 0 5 11 66.20 68.48 3.00 o 1 5 11 46.60 43.00 2.53 o 2 5 11 266.20 243.88 10.40 o 3 5 11 70.10 77.41 4.18 o 4 5 11 21.35 20.12 3.30 o 5 5 11 80.70 84.33 8.61 o 0 6 11 11.10 9.69 2.60 o 1 6 11 253.30 236.09 11.29 o 2 6 11 195.20 187.96 10.85 o 3 6 11 -0.50 1.53 4.31 o 4 6 11 20.35 16.53 4.45 o 0 7 11 34.80 41.98 4.50 o 1 7 11 162.95 155.11 9.95 o 2 7 11 98.65 90.29 7.65 o 3 7 11 6.85 2.30 3.90 o 0 8 11 78.10 81.36 7.50 o 1 8 11 96.85 98.64 9.97 o 0 0 12 107.70 112.75 4.60 o 1 0 12 1225.10 1143.24 26.70 o 2 0 12 14.90 27.17 1.40 o 3 0 12 53.80 50.84 2.20 o 4 0 12 63.60 56.55 2.80 o 5 0 12 90.80 110.39 4.80 o 6 0 12 0.40 0.57 6.45 o 0 1 12 17.20 16.38 1.30 o 1 1 12 524.50 527.98 13.65 o 2 1 12 214.50 217.55 5.87 o 3 1 12 70.30 80.05 2.65 o 4 1 12 33.20 32.25 1.88 o 5 1 12 18.25 25.65 2.43 o 6 1 12 -2.35 3.36 4.21 o 0 2 12 10.40 10.08 1.20 o 1 2 12 305.85 322.45 8.20 o 2 2 12 0.95 2.95 2.27 o 3 2 12 95.40 86.10 3.61 o 4 2 12 55.40 61.86 2.66 o 5 2 12 2.45 2.00 4.59 o 6 2 12 32.90 30.42 6.63 o 0 3 12 79.80 84.79 2.90 o 1 3 12 222.80 231.68 6.10 o 2 3 12 143.40 156.55 5.06 o 3 3 12 19.85 20.76 1.77 o 4 3 12 190.35 216.63 6.71 o 5 3 12 46.45 44.89 4.00 o 0 4 12 200.30 186.54 8.70 o 1 4 12 38.75 42.59 2.91 o 2 4 12 10.20 10.72 1.76 o 3 4 12 57.60 60.72 3.15 o 4 4 12 56.35 60.33 4.46 o 5 4 12 20.10 20.35 3.91 o 0 5 12 32.20 25.26 2.80 o 1 5 12 40.50 41.26 3.00 o 2 5 12 43.75 40.65 3.83 o 3 5 12 93.75 86.42 5.62 o 4 5 12 48.30 51.36 4.76 o 0 6 12 170.00 151.92 7.90 o 1 6 12 84.50 84.76 5.36 o 2 6 12 56.10 54.66 5.00 o 3 6 12 37.45 32.65 5.26 o 4 6 12 27.40 34.31 5.50 o 0 7 12 3.60 4.25 3.20 o 1 7 12 198.35 183.49 13.40 o 2 7 12 36.00 39.21 5.79 o 3 7 12 1.80 5.34 5.50 o 1 0 13 1090.20 1121.43 28.20 o 2 0 13 27.90 21.64 1.70 o 3 0 13 25.50 24.96 1.90 o 4 0 13 166.30 176.69 6.90 o 5 0 13 264.20 246.96 14.20 o 6 0 13 -0.60 5.21 8.52 o 0 1 13 50.00 49.72 2.10 o 1 1 13 375.35 369.66 9.86 o 2 1 13 227.20 247.17 6.55 o 3 1 13 224.95 241.13 7.00 o 4 1 13 77.90 83.03 3.71 o 5 1 13 8.05 12.07 2.88 o 6 1 13 15.30 6.44 7.07 o 0 2 13 11.90 16.91 1.50 o 1 2 13 4.50 4.92 1.32 o 2 2 13 231.30 239.75 7.34 o 3 2 13 342.40 339.83 11.40 o 4 2 13 101.45 109.22 5.39 o 5 2 13 21.40 19.16 3.07 o 0 3 13 29.80 32.43 2.50 o 1 3 13 40.20 46.89 2.50 o 2 3 13 37.05 33.39 2.77 o 3 3 13 46.50 52.54 2.65 o 4 3 13 33.30 32.93 3.28 o 5 3 13 13.00 12.13 3.22 o 0 4 13 347.60 369.11 12.40 o 1 4 13 75.85 77.61 4.30 o 2 4 13 185.20 168.86 7.89 o 3 4 13 238.15 220.43 11.75 o 4 4 13 18.25 18.41 3.79 o 5 4 13 30.80 27.23 5.63 o 0 5 13 47.60 39.80 3.60 o 1 5 13 94.55 89.90 4.68 o 2 5 13 94.05 92.33 5.45 o 3 5 13 57.90 62.47 5.01 o 4 5 13 70.50 76.83 6.50 o 0 6 13 55.90 48.66 5.10 o 1 6 13 379.65 338.99 21.87 o 2 6 13 13.45 18.22 3.61 o 3 6 13 6.50 8.59 4.00 o 0 7 13 2.50 1.73 3.40 o 1 7 13 32.00 31.35 5.00 o 2 7 13 4.90 5.95 4.10 o 0 0 14 1532.60 1529.30 56.00 o 1 0 14 352.70 349.36 9.70 o 2 0 14 191.50 174.01 5.80 o 3 0 14 3.10 3.79 1.20 o 4 0 14 56.70 53.89 3.40 o 5 0 14 1.30 4.13 3.30 o 0 1 14 50.90 56.89 2.30 o 1 1 14 339.45 372.17 9.62 o 2 1 14 5.05 5.67 1.41 o 3 1 14 63.85 73.78 3.11 o 4 1 14 4.45 2.01 2.47 o 5 1 14 95.65 88.57 8.16 o 0 2 14 939.40 957.25 30.20 o 1 2 14 149.80 161.81 5.76 o 2 2 14 117.80 116.54 6.17 o 3 2 14 35.15 39.24 3.57 o 4 2 14 11.95 20.38 3.29 o 5 2 14 6.05 5.32 3.20 o 0 3 14 335.20 324.22 12.40 o 1 3 14 120.90 118.53 5.72 o 2 3 14 73.20 76.46 4.55 o 3 3 14 282.70 284.26 11.44 o 4 3 14 32.80 30.21 3.82 o 5 3 14 32.95 35.46 3.91 o 0 4 14 312.60 305.13 13.80 o 1 4 14 88.50 91.40 5.14 o 2 4 14 46.15 43.73 3.67 o 3 4 14 2.50 5.76 2.51 o 4 4 14 56.85 57.06 5.49 o 0 5 14 1.60 5.15 3.40 o 1 5 14 114.20 103.74 7.01 o 2 5 14 30.60 31.13 3.67 o 3 5 14 7.80 6.33 3.35 o 4 5 14 51.80 48.62 8.08 o 0 6 14 163.20 153.53 9.60 o 1 6 14 215.85 195.21 13.35 o 2 6 14 10.35 11.95 4.35 o 3 6 14 2.50 1.15 5.81 o 0 7 14 12.00 21.12 7.40 o 1 7 14 17.80 19.05 5.17 o 1 0 15 8.40 7.33 2.30 o 2 0 15 0.60 0.64 2.01 o 3 0 15 0.10 1.09 1.20 o 4 0 15 18.60 19.56 2.30 o 5 0 15 -2.60 0.16 3.30 o 0 1 15 12.80 15.91 2.20 o 1 1 15 33.45 30.74 3.05 o 2 1 15 96.40 104.82 5.00 o 3 1 15 18.15 25.81 2.30 o 4 1 15 66.25 58.70 6.06 o 5 1 15 40.40 45.63 4.82 o 0 2 15 65.10 74.99 4.20 o 1 2 15 47.60 44.11 3.40 o 2 2 15 18.10 21.22 2.79 o 3 2 15 10.50 12.86 3.98 o 4 2 15 16.95 16.27 4.62 o 5 2 15 78.75 67.75 6.96 o 0 3 15 139.30 137.13 5.70 o 1 3 15 297.65 268.28 12.43 o 2 3 15 122.25 123.90 6.55 o 3 3 15 43.85 44.41 4.98 o 4 3 15 140.35 130.62 9.04 o 0 4 15 25.70 30.88 3.40 o 1 4 15 23.05 25.18 3.31 o 2 4 15 19.55 19.23 3.59 o 3 4 15 47.80 48.08 4.67 o 4 4 15 18.55 26.70 4.06 o 0 5 15 60.80 61.24 5.00 o 1 5 15 126.85 118.20 8.45 o 2 5 15 25.25 23.91 5.10 o 3 5 15 5.20 1.09 6.14 o 0 6 15 139.20 131.82 9.40 o 1 6 15 37.50 37.11 4.90 o 2 6 15 19.55 18.27 5.22 o 0 0 16 304.00 276.47 16.60 o 1 0 16 23.20 25.27 3.00 o 2 0 16 4.80 3.93 2.40 o 3 0 16 22.40 18.17 2.50 o 4 0 16 11.70 10.26 3.10 o 0 1 16 103.40 107.52 6.00 o 1 1 16 388.00 381.40 15.60 o 2 1 16 7.95 6.64 2.45 o 3 1 16 21.60 19.88 3.07 o 4 1 16 36.95 34.69 4.98 o 0 2 16 63.90 63.31 4.40 o 1 2 16 126.65 131.15 6.47 o 2 2 16 116.05 108.71 7.97 o 3 2 16 96.90 80.30 7.77 o 4 2 16 40.20 39.69 5.54 o 0 3 16 153.90 151.60 7.90 o 1 3 16 76.25 82.04 5.05 o 2 3 16 81.00 78.27 5.26 o 3 3 16 11.40 11.01 3.55 o 4 3 16 85.10 87.73 6.59 o 0 4 16 21.10 18.69 3.80 o 1 4 16 79.50 74.43 7.33 o 2 4 16 2.95 0.93 4.10 o 3 4 16 82.70 80.27 6.75 o 0 5 16 44.60 42.94 5.30 o 1 5 16 219.20 207.35 14.05 o 2 5 16 20.85 20.77 4.77 o 0 6 16 43.00 36.93 9.30 o 1 6 16 26.55 34.01 7.16 o 1 0 17 179.10 173.39 9.50 o 2 0 17 84.90 81.05 4.90 o 3 0 17 -0.80 0.00 4.29 o 4 0 17 48.40 46.75 4.40 o 0 1 17 84.00 79.09 5.30 o 1 1 17 10.60 12.81 2.59 o 2 1 17 16.30 19.79 2.75 o 3 1 17 93.45 92.28 6.32 o 4 1 17 170.35 131.73 13.14 o 0 2 17 35.50 40.06 3.90 o 1 2 17 33.40 32.88 3.60 o 2 2 17 110.75 105.38 8.67 o 3 2 17 42.10 41.78 5.18 o 4 2 17 94.35 83.22 8.85 o 0 3 17 -0.40 2.12 4.93 o 1 3 17 94.95 89.46 5.70 o 2 3 17 21.10 22.58 4.09 o 3 3 17 30.00 26.90 5.43 o 0 4 17 18.40 19.26 3.40 o 1 4 17 51.50 53.86 5.70 o 2 4 17 41.55 43.08 5.80 o 3 4 17 14.95 21.51 3.85 o 0 5 17 50.50 56.12 5.30 o 1 5 17 17.80 22.82 4.91 o 0 0 18 48.50 49.71 5.90 o 1 0 18 8.00 10.98 3.10 o 2 0 18 185.30 188.75 12.20 o 3 0 18 24.20 19.52 3.60 o 0 1 18 -2.10 1.04 2.30 o 1 1 18 39.00 42.44 3.70 o 2 1 18 9.20 9.81 2.96 o 3 1 18 29.25 26.09 3.75 o 0 2 18 10.00 8.32 3.30 o 1 2 18 100.55 103.83 6.70 o 2 2 18 17.80 14.99 4.83 o 3 2 18 4.75 7.57 4.03 o 0 3 18 17.90 18.66 3.60 o 1 3 18 55.50 57.05 5.22 o 2 3 18 43.80 48.89 6.20 o 3 3 18 3.90 1.11 8.07 o 0 4 18 5.20 3.87 4.40 o 1 4 18 66.65 72.71 6.75 o 2 4 18 15.00 13.80 4.40 o 1 0 19 101.00 99.71 7.40 o 2 0 19 48.40 52.44 5.30 o 3 0 19 84.40 78.96 7.00 o 0 1 19 259.80 203.38 17.40 o 1 1 19 10.45 7.95 3.60 o 2 1 19 -0.10 4.57 2.85 o 3 1 19 14.50 14.01 3.40 o 0 2 19 67.30 58.89 6.20 o 1 2 19 88.50 87.96 6.95 o 2 2 19 5.15 3.55 3.86 o 0 3 19 1.00 0.49 6.20 o 1 3 19 2.70 8.46 1.98 o 2 3 19 6.10 7.83 5.70 o 0 0 20 305.00 273.62 30.90 o 1 0 20 9.70 9.38 4.00 o 2 0 20 -0.50 3.54 5.09 o 0 1 20 14.90 11.88 3.50 o 1 1 20 24.40 27.24 4.20 o