#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:10:25 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180826 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/57/2015758.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015758_Fobs loop_ _publ_author_name 'Jones, Nigel A.' 'Jenkinson, Sarah F.' 'Soengas, Raquel' 'Izumori, Ken' 'Fleet, George W. J.' 'Watkin, David J.' _publ_section_title ; The concomitant crystallization of two polymorphs of 1-deoxy-\a-D-tagatose ; _journal_coeditor_code SK3070 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o7 _journal_page_last o10 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _audit_creation_date 06-10-06 _audit_creation_method CRYSTALS _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 6.0177(2) _cell_length_b 6.4672(2) _cell_length_c 18.0218(7) _cod_data_source_file sk3070IIsup3.hkl _cod_data_source_block II loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 2 0 0 691.00 719.33 21.00 o 4 0 0 48.90 49.22 2.30 o 6 0 0 1527.40 1485.29 67.40 o 2 1 0 48.10 53.98 1.40 o 3 1 0 14.40 7.64 1.00 o 4 1 0 16.50 19.76 1.30 o 5 1 0 123.80 126.57 4.70 o 6 1 0 2.60 4.49 2.20 o 7 1 0 224.40 227.72 17.00 o 0 2 0 106.80 102.50 5.20 o 1 2 0 3878.90 4160.97 131.60 o 2 2 0 279.90 271.13 7.10 o 3 2 0 182.10 186.59 4.00 o 4 2 0 527.90 525.16 11.30 o 5 2 0 564.50 566.76 15.50 o 6 2 0 33.40 36.01 4.40 o 7 2 0 -2.10 0.09 3.00 o 1 3 0 1368.40 1319.54 31.50 o 2 3 0 734.80 664.20 20.60 o 3 3 0 741.10 715.56 17.00 o 4 3 0 4425.40 4481.12 154.70 o 5 3 0 956.10 1019.72 30.50 o 6 3 0 118.80 112.23 8.60 o 7 3 0 109.10 124.68 12.00 o 0 4 0 210.00 201.15 9.00 o 1 4 0 2.80 5.22 0.60 o 2 4 0 85.50 74.84 2.80 o 3 4 0 576.80 580.99 18.40 o 4 4 0 681.50 657.56 18.70 o 5 4 0 4.10 5.03 2.20 o 6 4 0 369.50 339.91 20.70 o 1 5 0 13.20 11.57 1.30 o 2 5 0 333.50 315.75 9.40 o 3 5 0 293.30 274.67 9.90 o 4 5 0 194.70 195.29 6.90 o 5 5 0 211.80 199.95 15.60 o 6 5 0 74.80 67.84 7.20 o 0 6 0 40.50 52.13 2.70 o 1 6 0 128.60 135.00 4.30 o 2 6 0 138.80 160.15 4.90 o 3 6 0 79.50 97.51 3.40 o 4 6 0 103.60 71.61 5.60 o 5 6 0 169.70 156.16 15.50 o 1 7 0 188.20 190.68 7.90 o 2 7 0 -1.80 0.15 1.30 o 3 7 0 19.20 16.91 2.30 o 4 7 0 1.20 11.72 3.70 o 0 8 0 397.40 405.75 30.00 o 1 8 0 2.70 4.77 2.30 o 2 8 0 -3.80 0.97 3.90 o 2 0 1 1167.50 1234.35 24.50 o 3 0 1 997.50 1036.42 20.30 o 4 0 1 1204.40 1217.81 24.60 o 5 0 1 52.80 42.62 2.30 o 6 0 1 265.90 259.24 10.70 o 7 0 1 143.30 133.60 12.10 o 2 1 1 1132.45 1170.17 23.32 o 3 1 1 1718.00 1706.10 35.50 o 4 1 1 148.90 142.51 3.45 o 5 1 1 322.40 327.46 8.93 o 6 1 1 229.55 244.69 11.08 o 7 1 1 173.55 182.98 12.66 o 0 2 1 212.80 187.15 5.40 o 1 2 1 203.20 212.65 7.32 o 2 2 1 3192.30 3218.24 84.23 o 3 2 1 393.65 383.50 9.46 o 4 2 1 540.15 533.66 13.25 o 5 2 1 455.10 457.61 12.77 o 6 2 1 32.60 30.35 4.37 o 7 2 1 28.00 32.50 5.30 o 0 3 1 710.80 726.82 21.20 o 1 3 1 633.90 603.81 15.80 o 2 3 1 4339.10 4123.21 159.04 o 3 3 1 160.75 193.07 4.45 o 4 3 1 1058.25 1067.52 39.26 o 5 3 1 345.65 354.54 11.96 o 6 3 1 124.70 134.38 8.90 o 7 3 1 28.60 25.82 5.50 o 0 4 1 21.90 14.64 1.50 o 1 4 1 199.65 181.38 5.85 o 2 4 1 230.90 245.33 5.51 o 3 4 1 125.40 137.75 4.00 o 4 4 1 110.15 121.64 3.65 o 5 4 1 409.80 419.88 20.36 o 6 4 1 411.50 368.20 33.50 o 0 5 1 183.90 187.28 5.20 o 1 5 1 626.05 647.29 16.73 o 2 5 1 106.75 103.21 3.90 o 3 5 1 740.90 732.53 24.15 o 4 5 1 73.30 79.55 3.45 o 5 5 1 97.55 82.04 8.58 o 6 5 1 105.65 104.43 9.60 o 0 6 1 143.70 153.00 5.00 o 1 6 1 442.05 467.49 13.41 o 2 6 1 1330.55 1311.35 43.82 o 3 6 1 39.35 38.75 2.97 o 4 6 1 72.70 74.64 7.40 o 5 6 1 33.50 33.68 4.60 o 0 7 1 48.90 46.39 3.10 o 1 7 1 140.15 145.54 5.50 o 2 7 1 145.55 139.24 10.31 o 3 7 1 69.55 63.54 6.63 o 4 7 1 4.10 1.61 3.05 o 0 8 1 22.10 21.62 2.90 o 1 8 1 105.65 107.83 8.75 o 2 8 1 170.25 163.05 14.30 o 2 0 2 236.20 203.54 4.90 o 3 0 2 479.80 422.07 10.80 o 4 0 2 50.10 61.03 1.80 o 5 0 2 39.80 39.90 2.10 o 6 0 2 16.10 20.90 4.60 o 7 0 2 41.30 41.16 5.90 o 1 1 2 309.75 354.15 8.47 o 2 1 2 1306.60 1349.09 30.29 o 3 1 2 220.45 201.29 4.77 o 4 1 2 218.50 218.59 5.30 o 5 1 2 243.85 253.99 6.57 o 6 1 2 426.55 446.13 20.22 o 7 1 2 142.20 159.98 13.30 o 0 2 2 4365.60 4570.47 217.80 o 1 2 2 1865.50 1899.28 66.57 o 2 2 2 3212.60 3263.86 72.03 o 3 2 2 112.15 112.56 3.11 o 4 2 2 46.10 46.06 1.96 o 5 2 2 358.50 347.78 10.86 o 6 2 2 113.05 115.47 7.64 o 7 2 2 290.40 277.68 22.40 o 0 3 2 2395.20 2538.83 66.40 o 1 3 2 2591.70 2566.08 78.04 o 2 3 2 816.55 787.07 20.96 o 3 3 2 474.85 466.08 11.11 o 4 3 2 231.15 226.32 6.16 o 5 3 2 414.05 450.14 21.60 o 6 3 2 9.20 11.21 3.01 o 7 3 2 33.90 27.72 6.20 o 0 4 2 88.80 81.49 3.10 o 1 4 2 1268.35 1297.40 34.36 o 2 4 2 615.85 578.17 15.73 o 3 4 2 422.80 417.75 10.94 o 4 4 2 15.90 16.55 1.45 o 5 4 2 67.70 76.96 4.36 o 6 4 2 25.80 31.36 4.50 o 0 5 2 87.90 93.30 3.00 o 1 5 2 55.10 57.85 2.30 o 2 5 2 677.40 724.92 21.44 o 3 5 2 587.30 596.12 22.98 o 4 5 2 87.10 93.00 4.59 o 5 5 2 9.45 6.92 2.67 o 6 5 2 322.60 289.72 25.42 o 0 6 2 2.50 4.22 1.00 o 1 6 2 282.75 294.67 9.00 o 2 6 2 120.35 110.44 4.61 o 3 6 2 104.15 106.52 5.22 o 4 6 2 348.20 331.12 18.75 o 5 6 2 213.50 195.19 17.00 o 0 7 2 17.40 16.83 3.30 o 1 7 2 544.00 528.66 24.85 o 2 7 2 8.50 5.59 2.80 o 3 7 2 25.05 30.39 4.43 o 4 7 2 128.45 117.70 12.17 o 0 8 2 10.80 12.05 2.10 o 1 8 2 7.00 10.13 4.11 o 2 8 2 135.25 138.97 10.98 o 2 0 3 72.50 49.81 2.60 o 3 0 3 1523.80 1595.15 36.00 o 4 0 3 249.50 251.41 6.80 o 5 0 3 158.20 161.36 5.30 o 6 0 3 475.20 473.80 26.60 o 7 0 3 -0.60 0.10 6.04 o 1 1 3 1813.10 1868.97 55.00 o 2 1 3 446.10 427.05 11.58 o 3 1 3 597.80 614.40 14.04 o 4 1 3 40.75 39.61 1.86 o 5 1 3 707.40 740.66 19.77 o 6 1 3 245.45 256.87 13.61 o 7 1 3 490.60 463.16 36.10 o 0 2 3 17.30 8.20 1.20 o 2 2 3 56.30 65.11 1.75 o 3 2 3 1908.45 1895.73 41.24 o 4 2 3 392.00 380.81 10.26 o 5 2 3 360.25 387.07 10.02 o 6 2 3 32.50 38.24 5.25 o 7 2 3 136.85 138.45 12.14 o 0 3 3 4.70 1.84 0.50 o 1 3 3 2898.90 2858.36 105.77 o 2 3 3 563.10 556.46 14.46 o 3 3 3 761.95 734.96 17.43 o 4 3 3 2237.00 2209.93 59.06 o 5 3 3 262.60 267.72 9.14 o 6 3 3 17.05 15.37 3.73 o 7 3 3 39.20 38.04 6.70 o 0 4 3 106.60 93.71 3.00 o 1 4 3 319.70 294.31 8.90 o 2 4 3 174.85 190.85 5.59 o 3 4 3 569.30 536.90 21.26 o 4 4 3 223.80 230.14 7.51 o 5 4 3 357.40 367.57 18.28 o 6 4 3 34.30 34.14 4.80 o 0 5 3 612.20 624.40 15.70 o 1 5 3 195.05 193.74 5.51 o 2 5 3 19.10 21.11 1.76 o 3 5 3 9.10 17.51 1.33 o 4 5 3 136.60 148.31 8.16 o 5 5 3 94.70 74.49 7.30 o 6 5 3 154.50 155.79 13.40 o 0 6 3 1668.70 1755.03 50.70 o 1 6 3 842.20 898.76 28.33 o 2 6 3 36.80 40.47 2.56 o 3 6 3 293.95 306.86 14.21 o 4 6 3 191.15 189.30 14.12 o 5 6 3 95.05 96.11 9.42 o 0 7 3 20.80 20.57 2.30 o 1 7 3 218.35 217.20 12.39 o 2 7 3 18.35 18.70 3.96 o 3 7 3 129.40 128.02 11.07 o 4 7 3 216.40 180.73 14.50 o 0 8 3 56.60 60.05 4.50 o 1 8 3 41.20 49.35 5.58 o 2 8 3 79.75 78.91 7.26 o 2 0 4 4978.50 5082.97 146.50 o 3 0 4 4669.80 4527.24 112.10 o 4 0 4 23.20 25.94 1.60 o 5 0 4 0.80 1.69 2.50 o 6 0 4 1342.40 1312.96 69.30 o 7 0 4 122.10 107.00 11.80 o 0 1 4 995.10 1100.40 21.20 o 3 1 4 201.30 177.22 5.00 o 4 1 4 94.30 92.15 3.25 o 5 1 4 167.95 188.33 6.00 o 6 1 4 461.70 457.65 25.26 o 7 1 4 422.70 390.92 31.70 o 0 2 4 413.50 378.32 10.50 o 1 2 4 1948.60 1974.99 52.86 o 2 2 4 2800.75 2680.67 83.95 o 3 2 4 719.95 727.94 16.71 o 4 2 4 474.90 465.03 12.06 o 5 2 4 232.15 251.11 8.30 o 6 2 4 240.00 224.25 16.60 o 7 2 4 93.50 98.40 10.00 o 0 3 4 709.00 716.53 20.70 o 1 3 4 292.55 302.88 8.14 o 2 3 4 1462.05 1448.08 39.18 o 3 3 4 333.50 336.89 8.10 o 4 3 4 832.90 871.92 24.90 o 5 3 4 263.35 266.64 12.16 o 6 3 4 33.55 36.58 5.36 o 7 3 4 139.30 116.43 14.60 o 0 4 4 37.80 37.60 1.80 o 1 4 4 256.00 263.03 8.80 o 2 4 4 675.15 698.37 19.70 o 3 4 4 2729.70 2651.73 104.61 o 4 4 4 77.85 79.57 4.00 o 5 4 4 3.40 6.41 1.60 o 6 4 4 144.90 141.08 14.30 o 0 5 4 249.80 244.04 8.40 o 1 5 4 685.60 639.81 21.80 o 2 5 4 292.25 290.20 10.36 o 3 5 4 16.70 24.10 2.22 o 4 5 4 76.95 78.84 4.23 o 5 5 4 58.30 39.18 6.10 o 6 5 4 9.00 18.68 3.60 o 0 6 4 -0.10 1.32 0.51 o 1 6 4 57.35 52.25 3.90 o 2 6 4 145.65 134.48 6.39 o 3 6 4 29.15 25.83 3.48 o 4 6 4 117.55 102.80 9.80 o 5 6 4 41.60 41.95 6.75 o 0 7 4 160.00 152.76 7.00 o 1 7 4 72.25 61.87 5.58 o 2 7 4 655.50 647.13 40.56 o 3 7 4 6.15 6.54 4.24 o 4 7 4 134.00 119.00 12.00 o 0 8 4 19.60 22.85 5.30 o 1 8 4 21.35 20.50 4.08 o 1 0 5 1364.70 1489.63 32.50 o 2 0 5 3037.80 2942.48 86.00 o 3 0 5 742.30 729.86 17.80 o 4 0 5 211.20 198.85 6.10 o 5 0 5 695.10 718.86 21.10 o 6 0 5 0.10 0.40 1.96 o 7 0 5 34.60 24.94 7.20 o 0 1 5 8.00 4.51 0.50 o 1 1 5 5420.25 5863.54 171.43 o 2 1 5 3293.25 3294.12 83.87 o 3 1 5 136.35 136.15 3.70 o 4 1 5 382.85 366.21 10.30 o 5 1 5 370.60 422.38 12.33 o 6 1 5 417.50 413.57 24.20 o 7 1 5 190.20 183.87 15.10 o 0 2 5 1269.10 1374.22 28.60 o 1 2 5 1422.70 1359.19 34.74 o 2 2 5 3727.90 3685.06 89.18 o 3 2 5 88.10 87.07 2.80 o 4 2 5 499.25 528.61 13.40 o 5 2 5 92.15 106.11 4.73 o 6 2 5 7.45 9.23 3.51 o 7 2 5 113.75 102.47 12.11 o 0 3 5 687.40 708.45 18.70 o 1 3 5 44.00 48.54 1.76 o 2 3 5 1323.75 1294.73 33.69 o 3 3 5 31.75 25.78 1.60 o 4 3 5 219.75 216.65 6.95 o 5 3 5 386.50 386.86 16.77 o 6 3 5 235.55 241.76 17.14 o 7 3 5 8.50 21.14 6.00 o 0 4 5 720.10 672.83 17.20 o 1 4 5 260.90 251.03 8.51 o 2 4 5 725.10 692.43 24.13 o 3 4 5 966.80 978.27 26.70 o 4 4 5 192.75 210.86 6.47 o 5 4 5 260.90 261.87 10.20 o 6 4 5 14.60 15.48 4.00 o 0 5 5 1599.00 1618.73 44.80 o 1 5 5 31.30 33.67 2.57 o 2 5 5 37.60 32.15 2.83 o 3 5 5 44.35 49.68 3.07 o 4 5 5 443.80 418.80 19.81 o 5 5 5 1.70 0.06 3.38 o 6 5 5 474.30 415.39 37.00 o 0 6 5 28.20 28.88 1.60 o 1 6 5 108.20 107.07 6.14 o 2 6 5 383.00 373.90 17.67 o 3 6 5 40.75 49.20 5.01 o 4 6 5 28.05 34.74 5.30 o 5 6 5 131.60 104.88 10.10 o 0 7 5 1.80 1.89 1.50 o 1 7 5 212.30 213.91 11.03 o 2 7 5 15.85 14.49 4.49 o 3 7 5 44.90 42.15 7.12 o 0 8 5 3.40 8.97 4.30 o 1 8 5 40.55 35.08 5.87 o 0 0 6 3349.60 3590.17 105.00 o 1 0 6 51.20 55.00 1.40 o 2 0 6 102.70 93.81 2.80 o 3 0 6 358.40 360.20 8.10 o 4 0 6 405.10 414.27 9.90 o 5 0 6 510.10 542.62 16.30 o 6 0 6 13.50 7.63 4.60 o 7 0 6 149.10 147.79 11.90 o 0 1 6 81.20 90.00 1.80 o 1 1 6 662.00 651.07 12.65 o 2 1 6 493.05 484.44 11.24 o 3 1 6 1041.90 991.96 24.85 o 4 1 6 1075.80 1090.80 26.26 o 5 1 6 376.35 422.05 12.26 o 6 1 6 345.30 337.20 19.85 o 7 1 6 107.90 111.91 9.90 o 0 2 6 845.90 779.64 17.10 o 1 2 6 71.40 84.61 2.21 o 2 2 6 247.20 239.70 5.43 o 3 2 6 394.95 372.35 9.45 o 4 2 6 1007.80 979.90 28.00 o 5 2 6 338.20 338.51 14.55 o 6 2 6 17.60 21.56 3.90 o 7 2 6 58.75 70.13 8.50 o 0 3 6 1148.60 1228.67 27.60 o 1 3 6 663.80 659.11 18.22 o 2 3 6 322.75 295.74 9.40 o 3 3 6 86.95 83.63 2.79 o 4 3 6 356.50 358.44 10.51 o 5 3 6 37.45 41.72 3.76 o 6 3 6 133.50 124.85 10.35 o 7 3 6 75.20 70.97 9.80 o 0 4 6 2095.60 2271.32 53.70 o 1 4 6 1280.60 1267.01 36.55 o 2 4 6 447.60 432.04 14.13 o 3 4 6 390.65 377.32 12.08 o 4 4 6 196.40 188.97 6.90 o 5 4 6 9.80 12.65 3.53 o 6 4 6 82.50 75.74 7.80 o 0 5 6 3888.10 3939.57 136.70 o 1 5 6 87.25 90.84 5.29 o 2 5 6 128.85 124.16 6.06 o 3 5 6 512.95 496.58 20.60 o 4 5 6 130.35 125.80 8.89 o 5 5 6 55.85 59.17 6.96 o 0 6 6 421.10 417.26 14.20 o 1 6 6 28.95 30.85 3.17 o 2 6 6 112.95 108.43 7.30 o 3 6 6 70.15 70.53 5.74 o 4 6 6 7.85 5.83 3.95 o 5 6 6 49.50 50.85 6.60 o 0 7 6 78.20 75.84 4.80 o 1 7 6 93.85 92.96 6.82 o 2 7 6 58.65 60.37 6.04 o 3 7 6 61.40 53.05 8.56 o 0 8 6 185.30 179.79 14.10 o 1 8 6 147.60 161.32 14.21 o 1 0 7 235.30 223.92 4.90 o 2 0 7 20.70 16.00 1.30 o 3 0 7 356.80 351.90 8.60 o 4 0 7 507.00 532.80 13.70 o 5 0 7 1.50 2.66 1.50 o 6 0 7 177.50 176.73 11.80 o 7 0 7 68.40 67.22 9.90 o 0 1 7 5.40 7.35 0.60 o 1 1 7 3748.85 3774.16 82.42 o 2 1 7 2667.50 2547.78 58.11 o 3 1 7 596.95 603.12 16.03 o 4 1 7 120.25 117.45 3.90 o 5 1 7 263.05 285.02 13.73 o 6 1 7 210.10 207.69 13.61 o 7 1 7 15.00 24.09 4.30 o 0 2 7 784.70 867.28 16.10 o 1 2 7 990.80 916.88 20.40 o 2 2 7 3509.50 3375.71 93.35 o 3 2 7 968.80 1016.47 20.67 o 4 2 7 881.80 884.28 23.70 o 5 2 7 1099.50 1129.41 44.75 o 6 2 7 4.20 4.92 4.09 o 7 2 7 72.40 70.49 8.68 o 0 3 7 374.10 318.06 9.70 o 1 3 7 364.60 355.51 9.41 o 2 3 7 462.55 411.57 12.33 o 3 3 7 471.10 460.07 10.97 o 4 3 7 309.70 308.54 9.30 o 5 3 7 132.25 125.89 6.90 o 6 3 7 -1.65 4.02 5.04 o 0 4 7 265.50 271.99 6.60 o 1 4 7 342.10 334.99 10.26 o 2 4 7 558.30 541.88 15.70 o 3 4 7 937.95 934.31 26.95 o 4 4 7 41.20 29.90 2.79 o 5 4 7 80.75 81.63 5.30 o 6 4 7 265.25 245.60 24.14 o 0 5 7 1247.80 1229.67 33.20 o 1 5 7 652.70 673.06 21.56 o 2 5 7 158.75 181.65 7.06 o 3 5 7 727.55 732.18 31.51 o 4 5 7 21.55 25.50 4.71 o 5 5 7 27.45 24.15 5.70 o 0 6 7 6.70 7.37 1.00 o 1 6 7 25.15 25.95 3.96 o 2 6 7 29.50 24.78 4.76 o 3 6 7 127.65 139.80 9.33 o 4 6 7 29.60 39.45 5.45 o 1 7 7 420.80 428.91 27.34 o 2 7 7 631.20 572.83 40.61 o 3 7 7 9.30 14.81 5.35 o 0 8 7 57.90 67.28 7.30 o 0 0 8 1942.00 2012.97 57.30 o 1 0 8 251.80 262.43 5.30 o 2 0 8 555.90 471.72 12.20 o 3 0 8 0.40 0.39 1.01 o 4 0 8 142.40 156.44 4.70 o 5 0 8 1.60 0.27 2.40 o 6 0 8 58.20 56.95 6.50 o 7 0 8 48.60 63.25 8.10 o 0 1 8 1504.60 1429.94 28.30 o 1 1 8 2174.20 2124.59 42.01 o 2 1 8 696.35 679.30 15.25 o 3 1 8 612.00 623.67 12.71 o 4 1 8 1563.10 1528.22 42.71 o 5 1 8 457.05 474.71 21.08 o 6 1 8 21.50 27.17 5.10 o 7 1 8 118.35 122.58 10.86 o 0 2 8 1419.30 1318.18 28.20 o 1 2 8 2326.00 2348.16 51.45 o 2 2 8 812.70 790.91 17.60 o 3 2 8 228.45 234.61 5.35 o 4 2 8 210.65 221.28 6.52 o 5 2 8 120.95 113.82 6.60 o 6 2 8 234.40 229.20 16.65 o 7 2 8 209.20 199.87 21.60 o 0 3 8 328.80 287.78 8.10 o 1 3 8 3.25 4.07 1.18 o 2 3 8 222.30 211.86 6.57 o 3 3 8 41.20 46.08 1.90 o 4 3 8 65.55 76.11 2.83 o 5 3 8 393.85 398.64 14.38 o 6 3 8 29.35 23.28 5.05 o 0 4 8 1449.80 1466.60 38.60 o 1 4 8 316.20 321.50 8.71 o 2 4 8 153.05 150.27 5.69 o 3 4 8 985.55 1034.33 33.73 o 4 4 8 8.05 10.65 2.41 o 5 4 8 180.55 177.37 9.20 o 6 4 8 474.95 432.96 36.18 o 0 5 8 99.00 104.80 3.50 o 1 5 8 105.80 112.83 4.95 o 2 5 8 366.60 351.04 16.30 o 3 5 8 347.20 293.38 23.73 o 4 5 8 120.70 120.33 9.01 o 5 5 8 19.05 19.59 5.47 o 0 6 8 211.40 209.53 14.60 o 1 6 8 230.50 240.74 12.24 o 2 6 8 215.85 211.34 11.95 o 3 6 8 6.50 14.07 4.40 o 4 6 8 17.60 21.99 5.80 o 0 7 8 147.50 157.53 12.10 o 1 7 8 1339.70 1259.26 84.27 o 2 7 8 25.50 21.93 5.80 o 3 7 8 5.00 6.74 4.10 o 1 0 9 65.90 50.45 2.00 o 2 0 9 32.20 19.85 1.70 o 3 0 9 229.00 241.57 5.50 o 4 0 9 225.30 223.09 6.00 o 5 0 9 40.80 49.99 4.90 o 6 0 9 172.30 164.80 12.00 o 7 0 9 19.40 10.76 5.90 o 0 1 9 1579.60 1637.22 30.20 o 1 1 9 515.65 480.61 10.35 o 2 1 9 359.95 369.92 8.86 o 3 1 9 3210.40 3232.58 70.30 o 4 1 9 101.25 97.77 3.60 o 5 1 9 243.35 235.78 12.02 o 6 1 9 110.65 119.00 8.66 o 7 1 9 109.40 109.57 10.80 o 0 2 9 -0.10 0.03 0.44 o 1 2 9 1448.85 1381.70 30.47 o 2 2 9 1874.45 1814.24 41.32 o 3 2 9 33.40 25.00 1.69 o 4 2 9 2086.15 2105.24 46.67 o 5 2 9 178.80 173.73 7.26 o 6 2 9 22.15 27.30 4.90 o 0 3 9 298.90 323.72 6.70 o 1 3 9 381.85 400.86 8.73 o 2 3 9 299.60 285.34 8.49 o 3 3 9 290.20 284.90 7.28 o 4 3 9 24.25 24.92 2.15 o 5 3 9 89.80 105.72 5.22 o 6 3 9 23.65 31.80 4.87 o 0 4 9 12.70 13.46 0.80 o 1 4 9 1015.80 1021.56 29.19 o 2 4 9 13.90 14.06 1.86 o 3 4 9 163.40 166.86 6.91 o 4 4 9 22.75 34.37 2.91 o 5 4 9 120.85 116.36 8.25 o 6 4 9 33.25 31.54 5.46 o 0 5 9 961.30 917.11 26.50 o 1 5 9 218.00 215.72 10.41 o 2 5 9 194.70 192.34 10.51 o 3 5 9 28.95 34.53 3.11 o 4 5 9 51.05 49.24 4.82 o 5 5 9 94.20 86.77 10.46 o 0 6 9 -4.00 0.00 3.30 o 1 6 9 142.45 137.28 10.56 o 2 6 9 21.30 16.91 5.29 o 3 6 9 134.95 134.74 12.19 o 4 6 9 216.75 200.62 20.00 o 1 7 9 205.05 187.50 14.95 o 2 7 9 7.55 9.95 4.30 o 3 7 9 49.30 45.23 6.10 o 0 0 10 1395.30 1333.30 41.60 o 1 0 10 1116.00 1070.34 20.80 o 2 0 10 21.50 25.30 1.50 o 3 0 10 670.40 652.20 14.50 o 4 0 10 32.90 31.02 1.90 o 5 0 10 52.00 49.37 3.90 o 6 0 10 298.40 282.38 16.70 o 0 1 10 418.30 426.96 9.10 o 1 1 10 1012.35 980.45 21.71 o 2 1 10 2288.55 2199.92 55.16 o 3 1 10 1433.65 1418.96 30.66 o 4 1 10 373.10 392.02 9.26 o 5 1 10 3.35 2.97 2.01 o 6 1 10 15.15 19.12 4.53 o 7 1 10 245.30 216.70 22.10 o 0 2 10 574.20 514.42 11.20 o 1 2 10 455.05 446.95 9.35 o 2 2 10 75.95 70.21 2.55 o 3 2 10 582.05 572.83 14.05 o 4 2 10 309.55 295.49 9.14 o 5 2 10 232.10 215.45 9.28 o 6 2 10 5.85 2.06 3.38 o 0 3 10 441.70 465.81 10.00 o 1 3 10 255.60 245.45 6.57 o 2 3 10 249.70 236.37 6.21 o 3 3 10 347.45 330.14 9.75 o 4 3 10 160.50 168.92 6.28 o 5 3 10 25.80 37.67 2.92 o 6 3 10 123.25 119.45 9.28 o 0 4 10 0.90 0.22 1.33 o 1 4 10 298.50 285.03 9.28 o 2 4 10 868.05 950.08 28.03 o 3 4 10 94.05 108.63 4.86 o 4 4 10 115.80 118.07 6.26 o 5 4 10 141.40 135.68 11.32 o 6 4 10 535.70 501.08 44.20 o 0 5 10 774.90 824.27 26.90 o 1 5 10 837.80 897.83 30.19 o 2 5 10 39.10 48.07 3.35 o 3 5 10 140.85 137.34 9.83 o 4 5 10 137.20 121.70 9.39 o 5 5 10 6.55 8.30 4.70 o 0 6 10 -3.20 0.95 3.50 o 1 6 10 60.00 59.51 6.15 o 2 6 10 28.65 28.52 5.71 o 3 6 10 6.25 5.92 4.47 o 4 6 10 117.65 125.86 11.26 o 0 7 10 116.20 114.87 11.30 o 1 7 10 34.65 41.73 6.65 o 2 7 10 205.60 190.30 19.06 o 1 0 11 516.90 500.87 10.40 o 2 0 11 496.50 528.66 10.90 o 3 0 11 481.40 464.44 11.60 o 4 0 11 1303.00 1272.79 28.80 o 5 0 11 20.50 10.53 2.60 o 6 0 11 3.80 10.51 4.30 o 0 1 11 215.90 237.74 5.40 o 1 1 11 230.35 227.98 4.95 o 2 1 11 928.40 902.68 19.65 o 3 1 11 610.55 602.35 14.96 o 4 1 11 47.90 42.34 2.57 o 5 1 11 216.90 200.83 9.39 o 6 1 11 283.95 262.36 21.06 o 0 2 11 201.40 193.12 4.50 o 1 2 11 684.80 675.24 13.51 o 2 2 11 905.25 816.81 20.87 o 3 2 11 272.75 252.93 6.80 o 4 2 11 236.40 275.91 7.43 o 5 2 11 216.25 205.41 13.14 o 6 2 11 53.45 49.58 6.22 o 0 3 11 302.60 292.52 6.80 o 1 3 11 429.35 414.01 10.89 o 2 3 11 25.40 22.89 1.49 o 3 3 11 43.65 53.04 2.56 o 4 3 11 144.35 146.20 5.82 o 5 3 11 108.70 113.68 6.52 o 6 3 11 35.40 42.34 6.33 o 0 4 11 1065.60 1079.19 27.20 o 1 4 11 411.85 423.57 13.10 o 2 4 11 682.65 713.26 23.99 o 3 4 11 280.60 294.31 12.07 o 4 4 11 136.70 127.29 7.05 o 5 4 11 298.15 270.34 19.74 o 0 5 11 49.80 52.97 2.50 o 1 5 11 74.20 84.50 5.39 o 2 5 11 366.25 360.66 14.35 o 3 5 11 518.55 529.31 30.75 o 4 5 11 94.45 102.17 9.67 o 5 5 11 212.15 187.67 16.32 o 0 6 11 164.50 164.16 10.30 o 1 6 11 308.30 285.81 20.95 o 2 6 11 111.55 106.32 10.32 o 3 6 11 35.25 32.22 6.00 o 4 6 11 149.30 152.30 14.30 o 0 7 11 14.50 9.68 4.80 o 1 7 11 95.45 95.74 10.36 o 2 7 11 230.50 198.68 20.80 o 0 0 12 298.30 275.53 8.60 o 1 0 12 1023.60 980.44 18.80 o 2 0 12 130.30 132.47 3.70 o 3 0 12 2884.20 2900.82 67.60 o 4 0 12 242.90 245.11 7.40 o 5 0 12 78.30 77.82 4.30 o 6 0 12 62.10 60.41 7.20 o 0 1 12 197.70 180.14 4.50 o 1 1 12 124.65 112.62 3.25 o 2 1 12 257.30 264.37 6.45 o 3 1 12 344.55 358.58 9.85 o 4 1 12 27.45 30.01 2.43 o 5 1 12 88.40 79.77 5.07 o 6 1 12 116.85 114.42 10.30 o 0 2 12 1282.40 1322.72 23.60 o 1 2 12 811.00 809.35 16.30 o 2 2 12 213.55 218.11 6.21 o 3 2 12 119.70 119.91 3.92 o 4 2 12 144.65 125.53 5.60 o 5 2 12 67.10 74.16 5.52 o 6 2 12 9.40 11.26 4.73 o 0 3 12 348.40 323.48 8.10 o 1 3 12 730.75 686.74 18.50 o 2 3 12 712.10 679.83 18.11 o 3 3 12 255.35 255.89 8.73 o 4 3 12 126.25 116.99 6.90 o 5 3 12 53.80 58.79 5.85 o 6 3 12 2.80 7.08 3.20 o 0 4 12 108.20 114.79 4.00 o 1 4 12 87.95 90.02 4.50 o 2 4 12 32.80 44.87 2.91 o 3 4 12 2.40 3.55 2.99 o 4 4 12 21.70 17.76 4.00 o 5 4 12 204.70 192.45 16.12 o 0 5 12 865.20 883.18 29.00 o 1 5 12 409.60 398.84 18.50 o 2 5 12 179.10 185.15 10.69 o 3 5 12 75.75 69.58 8.49 o 4 5 12 247.55 226.81 21.61 o 0 6 12 55.20 60.94 6.60 o 1 6 12 26.40 25.85 5.30 o 2 6 12 183.10 179.95 15.16 o 3 6 12 45.40 33.00 7.40 o 0 7 12 66.20 67.61 9.20 o 1 7 12 40.00 34.36 6.20 o 1 0 13 383.70 393.72 8.30 o 2 0 13 23.70 29.38 2.10 o 3 0 13 8.70 10.28 1.80 o 4 0 13 1334.10 1231.88 43.40 o 5 0 13 35.80 41.15 3.70 o 6 0 13 0.00 1.33 0.01 o 0 1 13 42.80 42.27 1.90 o 1 1 13 68.90 78.40 2.30 o 2 1 13 267.60 245.34 6.95 o 3 1 13 1049.90 1030.98 28.58 o 4 1 13 174.85 166.68 7.21 o 5 1 13 21.65 15.19 4.71 o 6 1 13 200.50 168.83 15.61 o 0 2 13 10.30 10.75 1.20 o 1 2 13 822.45 815.85 16.85 o 2 2 13 411.90 422.63 10.55 o 3 2 13 318.25 326.89 9.38 o 4 2 13 12.45 15.75 2.09 o 5 2 13 632.85 613.89 34.75 o 6 2 13 68.95 88.75 9.30 o 0 3 13 1672.50 1672.41 37.60 o 1 3 13 598.25 586.73 14.76 o 2 3 13 271.40 303.08 7.95 o 3 3 13 115.50 110.57 4.40 o 4 3 13 236.70 227.80 11.56 o 5 3 13 295.10 289.02 21.81 o 0 4 13 2.20 1.97 1.00 o 1 4 13 216.30 231.31 8.16 o 2 4 13 142.40 158.04 6.65 o 3 4 13 170.55 183.81 8.45 o 4 4 13 42.35 33.73 5.77 o 5 4 13 15.85 15.58 6.28 o 0 5 13 64.40 62.49 3.20 o 1 5 13 159.35 170.48 10.86 o 2 5 13 173.55 171.86 11.65 o 3 5 13 57.80 59.64 7.40 o 4 5 13 4.00 1.80 5.53 o 0 6 13 138.30 150.27 11.00 o 1 6 13 104.20 100.99 10.75 o 2 6 13 69.25 57.89 7.75 o 3 6 13 62.60 48.37 7.50 o 0 0 14 309.60 313.92 9.50 o 1 0 14 61.90 71.44 2.40 o 2 0 14 524.70 525.68 13.30 o 3 0 14 1159.00 1188.03 33.00 o 4 0 14 16.00 26.50 2.80 o 5 0 14 101.70 86.98 6.10 o 6 0 14 51.70 45.55 7.00 o 0 1 14 43.00 47.09 2.00 o 1 1 14 135.20 127.76 3.65 o 2 1 14 206.65 198.91 5.95 o 3 1 14 1151.15 1191.93 33.90 o 4 1 14 38.00 26.89 2.95 o 5 1 14 199.35 191.14 13.21 o 6 1 14 228.70 223.09 19.51 o 0 2 14 1.70 2.24 1.10 o 1 2 14 1836.40 1871.08 38.27 o 2 2 14 210.30 210.61 6.55 o 3 2 14 4.35 2.25 1.80 o 4 2 14 27.20 24.54 2.86 o 5 2 14 134.60 117.69 11.05 o 0 3 14 769.90 821.56 18.20 o 1 3 14 408.05 398.76 10.81 o 2 3 14 91.85 114.93 3.85 o 3 3 14 33.30 46.69 2.94 o 4 3 14 -0.05 3.57 4.30 o 5 3 14 61.15 59.92 6.97 o 0 4 14 53.40 53.95 2.60 o 1 4 14 275.80 278.88 9.70 o 2 4 14 267.55 260.84 11.81 o 3 4 14 4.15 2.66 2.97 o 4 4 14 117.10 116.66 9.70 o 5 4 14 4.30 0.28 5.40 o 0 5 14 9.00 17.68 4.50 o 1 5 14 172.00 170.64 11.01 o 2 5 14 7.25 16.68 4.66 o 3 5 14 53.50 51.33 7.36 o 4 5 14 31.80 34.88 7.50 o 0 6 14 51.70 45.07 7.60 o 1 6 14 35.65 33.89 7.40 o 2 6 14 26.20 31.11 6.35 o 1 0 15 712.00 744.68 15.60 o 2 0 15 609.90 618.96 17.00 o 3 0 15 24.90 29.51 2.40 o 4 0 15 135.80 124.01 8.80 o 5 0 15 8.30 5.23 4.30 o 0 1 15 943.10 895.41 18.30 o 1 1 15 98.90 103.04 3.20 o 2 1 15 96.95 96.12 3.75 o 3 1 15 45.45 44.87 3.05 o 4 1 15 275.45 276.06 11.96 o 5 1 15 56.15 53.52 5.90 o 0 2 15 2.10 3.33 1.30 o 1 2 15 294.50 304.58 7.30 o 2 2 15 148.90 159.91 5.55 o 3 2 15 20.55 19.35 2.73 o 4 2 15 161.80 141.68 9.75 o 5 2 15 29.70 32.51 5.33 o 0 3 15 94.50 94.96 3.60 o 1 3 15 1032.10 993.82 27.34 o 2 3 15 310.65 306.71 11.48 o 3 3 15 33.10 36.81 3.50 o 4 3 15 48.35 45.46 5.94 o 5 3 15 178.75 169.10 14.69 o 0 4 15 25.90 30.59 2.40 o 1 4 15 195.60 210.37 12.40 o 2 4 15 129.60 137.95 8.19 o 3 4 15 73.30 67.82 8.90 o 4 4 15 212.65 200.46 17.61 o 0 5 15 7.40 0.20 6.10 o 1 5 15 135.00 134.72 11.47 o 2 5 15 27.50 36.12 6.01 o 3 5 15 74.00 61.17 9.06 o 0 6 15 65.30 67.78 7.80 o 1 6 15 23.35 27.46 6.11 o 0 0 16 1079.30 1076.30 33.40 o 1 0 16 1355.00 1426.23 32.00 o 2 0 16 647.10 643.07 19.00 o 3 0 16 284.00 285.54 10.30 o 4 0 16 463.00 460.75 20.50 o 5 0 16 13.90 16.70 5.70 o 0 1 16 132.90 130.87 4.00 o 1 1 16 220.45 235.97 5.70 o 2 1 16 114.55 120.37 4.55 o 3 1 16 123.05 131.94 5.28 o 4 1 16 88.15 85.95 7.09 o 5 1 16 -1.25 3.53 6.15 o 0 2 16 215.40 235.63 6.20 o 1 2 16 15.15 18.79 1.60 o 2 2 16 161.45 167.77 6.88 o 3 2 16 27.65 32.89 3.61 o 4 2 16 38.95 26.69 4.98 o 5 2 16 6.90 11.59 4.40 o 0 3 16 339.30 335.20 10.50 o 1 3 16 80.85 78.67 3.75 o 2 3 16 523.40 505.67 22.77 o 3 3 16 151.85 141.92 9.40 o 4 3 16 90.60 85.71 8.85 o 0 4 16 376.40 370.68 19.50 o 1 4 16 157.40 164.27 12.21 o 2 4 16 85.35 93.14 7.95 o 3 4 16 20.05 18.16 6.21 o 4 4 16 64.45 55.45 10.26 o 0 5 16 26.90 26.35 6.30 o 1 5 16 72.95 73.59 8.33 o 2 5 16 49.35 52.57 7.56 o 3 5 16 20.90 29.87 8.70 o 1 0 17 167.10 174.88 5.10 o 2 0 17 657.40 703.46 23.00 o 3 0 17 40.50 49.10 3.10 o 4 0 17 61.30 63.02 4.70 o 5 0 17 5.90 3.30 6.80 o 0 1 17 310.50 305.47 7.80 o 1 1 17 130.45 134.43 4.30 o 2 1 17 495.85 486.48 15.36 o 3 1 17 49.65 54.18 3.77 o 4 1 17 239.95 237.55 16.28 o 5 1 17 72.75 74.06 8.91 o 0 2 17 57.00 60.07 3.20 o 1 2 17 427.30 410.32 13.99 o 2 2 17 124.70 121.17 5.43 o 3 2 17 26.10 28.67 3.62 o 4 2 17 54.30 58.10 5.86 o 5 2 17 14.80 22.87 4.20 o 0 3 17 437.20 402.63 17.90 o 1 3 17 10.80 9.69 4.69 o 2 3 17 19.15 22.91 3.81 o 3 3 17 152.10 135.69 10.28 o 4 3 17 108.10 108.88 9.94 o 0 4 17 85.30 86.50 9.60 o 1 4 17 74.00 72.12 7.45 o 2 4 17 519.90 511.50 36.29 o 3 4 17 6.80 13.27 5.89 o 0 5 17 36.90 23.39 6.40 o 1 5 17 17.35 19.38 5.42 o 2 5 17 -2.35 3.67 4.75 o 0 0 18 740.40 760.98 30.10 o 1 0 18 18.60 21.28 2.10 o 2 0 18 147.70 172.10 6.10 o 3 0 18 523.50 506.35 26.70 o 4 0 18 0.20 0.00 3.76 o 0 1 18 288.80 260.60 8.20 o 1 1 18 114.05 120.26 4.25 o 2 1 18 130.70 143.03 6.15 o 3 1 18 158.65 164.72 8.54 o 4 1 18 239.25 216.60 15.45 o 0 2 18 857.80 860.24 22.00 o 1 2 18 81.75 88.74 4.24 o 2 2 18 20.10 26.12 3.40 o 3 2 18 20.20 18.31 4.00 o 4 2 18 83.55 87.47 7.89 o 0 3 18 18.80 20.06 5.00 o 1 3 18 448.40 451.50 25.32 o 2 3 18 27.25 24.49 5.66 o 3 3 18 170.60 177.89 14.55 o 0 4 18 3.10 0.21 4.50 o 1 4 18 161.70 149.65 14.07 o 2 4 18 62.90 70.07 8.51 o 3 4 18 63.45 54.05 8.75 o 0 5 18 80.30 93.36 8.70 o 1 5 18 2.70 9.70 6.00 o 1 0 19 646.80 647.35 17.10 o 2 0 19 81.70 87.54 4.30 o 3 0 19 48.70 47.98 4.50 o 4 0 19 47.50 56.61 6.90 o 0 1 19 323.00 330.46 9.90 o 1 1 19 72.25 80.66 4.07 o 2 1 19 54.60 57.97 3.98 o 3 1 19 117.80 115.38 9.66 o 4 1 19 65.75 72.52 9.63 o 0 2 19 407.70 372.33 15.90 o 1 2 19 200.00 200.51 11.59 o 2 2 19 300.00 276.93 17.51 o 3 2 19 82.35 82.91 8.53 o 4 2 19 174.55 179.54 13.07 o 0 3 19 73.90 71.86 6.90 o 1 3 19 431.30 400.12 29.20 o 2 3 19 72.50 69.65 8.40 o 3 3 19 183.10 177.10 17.56 o 0 4 19 26.00 27.15 7.50 o 1 4 19 12.00 12.98 5.90 o 2 4 19 -4.05 0.91 5.10 o 0 0 20 -2.30 0.86 2.70 o 1 0 20 311.00 324.09 11.30 o 2 0 20 1.90 2.91 2.80 o 3 0 20 56.70 57.73 7.90 o 4 0 20 19.00 22.19 5.30 o 0 1 20 1.40 2.49 2.10 o 1 1 20 75.30 74.35 4.76 o 2 1 20 161.70 151.13 10.95 o 3 1 20 44.50 42.40 5.89 o 0 2 20 185.40 175.08 13.00 o 1 2 20 390.10 353.96 27.20 o 2 2 20 62.55 64.89 8.30 o 3 2 20 -1.35 2.23 6.70 o 0 3 20 113.30 125.17 9.90 o 1 3 20 219.95 207.07 16.80 o 2 3 20 16.35 30.03 5.79 o 0 4 20 509.50 493.70 36.10 o 1 4 20 147.75 137.04 14.25 o 1 0 21 13.60 11.19 3.20 o 2 0 21 1.10 0.66 3.90 o 3 0 21 -0.30 2.86 6.68 o 0 1 21 256.10 258.10 14.60 o 1 1 21 61.05 55.25 6.70 o 2 1 21 24.70 24.70 5.04 o 3 1 21 44.65 41.86 7.36 o 0 2 21 3.50 3.85 6.90 o 1 2 21 76.75 77.99 7.80 o 2 2 21 28.90 31.96 6.50 o 0 3 21 428.20 411.15 28.40 o 1 3 21 101.80 106.68 12.00 o 2 3 21 19.35 27.95 6.71 o 0 0 22 3.10 4.11 4.60 o 1 0 22 255.60 238.60 21.70 o 2 0 22 32.90 35.76 6.10 o 0 1 22 10.90 7.24 5.30 o 1 1 22 58.75 51.80 8.86 o 2 1 22 109.10 121.79 10.60 o 0 2 22 438.30 428.94 34.80 o 1 2 22 72.45 86.28 9.91 o 1 0 23 3.80 5.78 4.20 o 0 1 23 62.90 64.15 8.00 o 1 1 23 170.80 178.31 14.40 o